Document B8Lw8EaZNa1pNd2oOb8jdGymo

02/28/2001 ENVIRONMENTAL LABORATORY ARCHIVED FINAL REPORT B A C K T O M AIN LAB REQUEST NO. 8442 REQUESTOR NAME: EAR DEPARTMENT: 0535 PROJECT NO: 9970012600 DATE RECEIVED: 09/07/1982 DESC: ENVIRONMENTAL SCREEN ON L-6778 CONTRACT LAB(S): EXP COMP DATE: 11/12/1982 DATE COMPLETED: 11/09/1982 PROJECT LEAD: PHONE NO: 3M FAX NO: 651-778-6176 EVAPORATE TO DRYNESS UNDER AIR OR N2. PRODUCT CONTAINS 40% WATER SO HEAT TO ABOUT 40 DEGREES C IN WATER BATH OR BY OTHER METHOD TO INCREASE EVAPORATION RATE- MO HAS SAMPLES SAMPLE DATE CODE DESCRIPTION RESULT MDL or (95% C.I .) TOTAL PROD. 96-HR-LC50 BOD-05 BOD-10 BOD-20 COD SLUDGE-TOX FISH ACUTE TEST - 96 HOUR BOD-05 BOD-10 BOD-20 COD SLUDGE TOXICITY SOLIDS 96-HR-LC50 BOD-05 BOD-15 BOD-28 COD SLUDGE-TOX FISH ACUTE TEST - 96 HOUR BOD-05 BOD-15 BOD-28 COD SLUDGE TOXICITY >1000 MG/L 220000 MG/KG 270000 MG/KG 330000 MG/KG 530000 MG/KG SEE ATTACHED REPORT >1000 MG/L <8800 MG/KG <8800 MG/KG SEE ATTACHED REPORT 280000 MG/KG NOT ANALYZED B A C K T O M AIN ./ Environmental Laboratory B O D Work Sheet - Samples (i/o.-w) ULT. K o O Lab Req. No. | A n a ly it <7P T Sample Description Initial Dilution Oat Started 9-/6> BOD Run No. t 3 ^Z Analyst - Day BOD Readings at# _______ ;_____ P j P G a s x * - . _____________ ------- m 2 - 1___________ V :r?cL-(U QIC L - 77% 3 ,0 0 Q of Sample diluted to /q q q ml with D 1water ' Initial Dilution Factor (Dilution factor = 1 if undiluted) Bottle No. t' ,5 7 J i 3 _2 _ Cone, of Sample1 Sample Size2 Initial O.O, <D1) Present D.O, (D2) Total 0.0. Depletion <0, D2) 0 -S & . 2 . 9 0 _ _ 7 y ^ " . . /. y .s ' t-0 'fr) p ,o p J L P _______ t - 9 0 HO 1 ^ 0 -2,/S' H> o K W . < 0 ,fc --I t _________ M S - < p . TO v so b-f.P '-- ' -' Depletion Due To Sample - 7 -Day ^__ Average BOO O Dev BOO o -r 1 .M S P <9q pot ~. 21% 2 1 ^ ,0 0 0 -p> v. o -ru~\ niV ^ k 2 2 1 , on' 3 ; .-- -- - f '- Note: 1. Cone. = Concentration of sample (ml/l or mg/l) in BOD bottles. 2. Sample Size = ml or g of sample or diluted sample added to BOD Bottle. la! Laboratory Shaft aPw'^ ..........--.. ; -ib B#q. No. | Q a t s l Jtoetyst ..;7. B A C K T O M AIN -, . . ^ I , I. y , ' ; ? .-- ;;' ^ r ^ m v . ' B Q ^ R u n N o . v''1 v-- V'?vu i-V . j. Dane Started if) Analyst \ .- Data am p ia Description a Initial Dilution Initial Qhitiot Factor * *11 1" . * 1r..... ..... "" -r----l -------- ------- ------ -------------------- - V*-**-- ----- ------ ------ \ \). S r n e e t j w l ~677% . . . a , o o Ft of Sample diluted to /fQ Q ml with D l water \< & (Dilution factor f . f ifundiluted) .'v Bottta Cone, of 6?/No. tempt*1 V o ', ; ^ 5* 0.5 10 i0 ?3 /6U O MW IMX (Of) fraw t D^MOai Tota D.O. : CNpfc|l|PII ? -fo " 6 '/ o < o*o< r ,c S M if km *. ,rJO - Depletion Doe Dev To Somalo '. ~ " b p ' IH f.$ + 3W ax> 2 7 j o o $ sH C,cOQ > ' U i/ ;;'; A n n |i m OiV BOD ' - S .T Note: 1. Cone. = Concentration of sample(ml/l or mg/l) in BOD bottles. 2. Sample Size = ml or g of sample or diluted sample added to BOD Bottle. Comment CoO - S'iO .flG O b a c k t o m a in itti Lsborttory Sht SampfM M iftl Baq. MO` l C ____ __________2 . S.!t..e/iivM r i 'l f ' tempi* Dstcription Initial Dilution tnitiet Dilution Factor Dt* St*rt*d 9 'o ~ q n . 1" ....'1 BO D fu n N o .> $ $ ! *&* 't'***1!""""*. IIInnpp 1 rir - ; It. v V / V .. j 2q Analyst -- r- --.-- - D jy tO D R e a d ir ;'. ......................... Data : JQL .Soa.eJs.u.,<3.!i. L-$17$, of Sample diluted to ml with D l water ! if undiluted) Pettis Me. Cone, of Semple1 6-2 (0 si $5 3 7 O -K i0 7 -0 HO i0 /6 le ill# 0 .0 . (0,1 PlBt ' 0 .0 . <0a> Teta 0Jt>. 20^lq (Or - O ) S -p X 7T < X3Q J./ C -.V t-. X 30 ' /' " ` s` ' - .' Oapiatien Dus To Semple . j.vr. . .-0 -Dm OO /X3 P i s t e s 33-0300 V , > f - -'V 3 3 7 , add ' / V^\0n:'v3 j- -' = .'> . 1*:~'v . ` V,,. ; . 'M eta: t. Cone. = Concentration of sample {mt/l or mg/1) in BOD bottles. 2. Sample Size ml or g of sample or diluted sample added to BOD Bottle. Wim*nu C o O .:.s3Q,a&>_ :***rr`m ' ' .' ***** fartu lataPWO 1 r labomorv B A C K T O M AIN S p ,.N o . g vva ' . / - t , '.,1 femtjMmamai Pt tetnrta d : -.S '-' y V.r:.v`i ' < % : -: A rw ivw ' ' ' - V>-'> v ' ^* tv Pete Sample Description Initial Dilution Initial Dilution Factor i--ei'. ... ~ ------- V.- ~,-r------ ' ^.Tv'V' a . o o . ^ rjffg g iu o a j l - ^ 7 7 8 of Sample diluted to __________ _ ml with Dt water (Dilution fpetor - 1 if undiluted) Bottle No. Cone, of Sampta1 #4$750 7 '.''a':' '. Semole \ MM Preeent : sS T o .p .# ,i //D^O.lPal Total D.O. Depletion 10, O jl 7-0 rsr 6C>0-52* iO M & o . .. w . / o P*ZQ wo /6$ 0 ? ?? v;;-' - ? - ' v* Depletion Due a om--lm IO ... '7.^' Dev v, Amr^ BOO 3<k 900 p 2 .(= n T *y i 'f t g c Q.OCO SCi,0<X> V i i .of0. \' ; ' ' ' - : . ' ;"V -;' '*_, ; : V.; '. : N o te: 1. Cone. = C o ncentration o f sam ple (m l/l or m g/l) in BO D b o ttles. 2. Sample Size = ml or g of sample or diluted sample added to BOD Bottle. dammentt CbO - 5*^077 *, --, ...........r.'..............:.-...y.:y*.e..' tak hrrle .^11 TcSol-t-S . tv;;: ...... '- r'k. .-r .'. ", ! : ' '7vv;>t'' / .- . .*;-s-.rv. Jt.- **. ' 7i C". .-f''v.''*,r*'vrv' f ' Y *-.' *-- V;'c..' c . :r . '` t>' .`ii -, . ; . O.-.V'.^'VA-r'*'-, *. v;.-.VVy^-V ;-h ''1y / ... ';v- tt^.-V.'V...' ; ' ';V . .. .'-7'Vr^S^'r'^- 'W~----*-------------- Mli. . l*.'.'v''fc-.V<,?;^t'AV:iV*'i.,^h ']";,'.'v. "V iv-s '>v ;-. ' V/;,Vi7;V.^:^V`'4' -7 ;c: i- Environmental Laboratory OD Work Sheet - Blanks, Controls, and Standards S JO ' ~* o lT .O o B A C K T O M AIN Bottle No. Initial O.O. (A-)) Present D.O. <A2 ) 0 .0 . Depletion <A, A 2) HO . Y> .7 0 5 > v 5*7. % c> S'. 6 5 " ^ Sr Seeded Dilution - Water Blank (optional) so r S '/ s ' C -tb . C '.frO O 60 Bottle No. ; a n Seed Controls Initial D.O. (C ,) ^ 9o 6 g --T Prtant D.O. (C2 ) S ro S 'S o S - 7 r ." D.O. Depletion (C , -C2) 6 O 66 O -* Bottle No. Sample Size Initial D.O. (B ,) Present D.O. (E^ l 76' a 65" 6 a--. vd _____Zck2__________ 56 7`6 7 ' c{o 7.7 0 S VG V-C.C' 7*60 6 -o r Glucose - Glutamic Acid Standard Bottle No. Sample Size 79 ^7 Oj i^H 7U 7 .0 10 Initial D.O. ID ,) 2 -ZO 5-80 Present D.O. <D2) b. f S.O H.co Total D.O. Depletion (D , -D 2) 2 '3b tio H . 60 Depletion Due To Standard 7. 7 / 751 H7 | Potassium Hydrogen Pfithalata Standard (optional) Bottle No. Sample Size Initial D.O. (D ,) Prtant D.O. (D2) Total D.O. Depletion (D , - D2) Depletion Diia To Standard Average 0 .0 . Depletion ( , A2) 0 60 Average D.O. Depletion (5-j * 2) O -6 0 D.O. Depletion (B1 -B 2) 0-70 0-7.5' 0 60 i.O 7 " -Day BOD /7 / 0 /b 7 ? / t J Average 0 -Day BOD z". . //- - Dey BOD 7-. Average - Day BOD Form 1 9 7 5 6 PWO B A C K T O M AIN Aiutai Laboratory Jork Shoot *Blanks, >trols, and Standards ? t"'r utfr. r* % %: ' Ofiy teQ. Lab Raquatt No. f Analyst '' S**d TypAft Source , . ' - - . -'V. - - : DataStartad 9 /o *i IS**d fameuitntlw -- :------------ : -- '-- e p D R u n N o .|^ 2 S . i-.u a ti.,a <0** n r # s : fp) O sv BOD Raadinjj* Analytt .o A . Oat* ^ ___1 fa-Qr / -- _ _ -- _ Nonsatdnd Dilution Watnr Wank 8ot0* No. Initial D.O. ' - " (A il no 9 : .- 5 ?.S O . x .r 775" Itadad Dilution -Watar Blank (optional) Botti* No- ' '7 ' '' . Initial D.O. (C ,l 6S &9o 5. 1(1* ..... * ^ 77 Saad Controls 5 ?- 5 ' .. . V -. Botti* No. . SamptaS*# ' ' Praaant O.OtAg, . ; - 0 .0 .Oapiation (At A jl 7-3< " 7 -9 0 *7*SO _______.0 - ? - T ' 7 o ,7 r : : o . ? < Pr***nt D.O. (Cal ~7'90 *7.?0 9,00 . Initial 0.0. ' 0.0. D*pl*tlon (Ct da t.oo 0.90 r>:.t S ' . Pr***ntD.O. (Bai ; Avarag* D.O. Papietton (Si Aal C.// 'O? c " ' . .'. W ' . ' a Avarag* 0-0. P*pi*tkn. fit 0-91 .. .. D.O. Oaplatfon (B, Ba> ' ' ,,*." ' '- 7 .5 Xt>" y7 . ........... i*1--------- ------- 9b m . ______ !M ____________ %-<O 9 '7<r 9-90 7 .7 0 ' 7 7 (3 . . . . 7*90 -7 5 T : 5770 '- A /0 / 3T 5 : ?-o Botti* No. 7? yy 7X Sample Siza 75 0 .5 0 70 w tiaio .o . " 1 5 -o Praaant OX). * <*> Total 0.0. Oaplotlon (P iO g l 'S '* 7 0 7 -3 0 ; 3 /0 7 .5 0 .0 0 : Daplatlon Dua To Standard . / O -Dav : boo /(5W . d BOO zU 5 7 / : -V ^ ; y ----- ---rr-----"77T" 19 J . BMtiaNo. Sampl* Sis* M ial 0 .0 . : rnaantQ.Q. ' (Dt> (Oal Total OA . Daplation 10g r Ogl Captation Dua To Standard -Day BOO .. ; .. Avarag* ; v..- ' .Oav ' BOO ^ ' ' form t76#PWO tjlt?. B A C K T O M AIN tl Laboratory [o rk Sheet - Blanks, is, and Standards S,iO j ulT, IP. CHV.foP Lab Request No. ) BOD Run N o .# < ?. - Q vV jMWJ :<*** 1 "r A n a ly it ________ j { U . > Saad Typa &Sourca ^ D ata Startad Seed Concentration ? `!0 < 1 b lU /uA --ACi--- A n a ly it - Day BOD Readings Data Q a $ '- Y L Nonaaadad Dilution Watar Blank Bottta No. Initial D.O. (A ,) 1C . : : 7 . . . ` r K :. C -T> Saadad Dilution - Water Blank (optional) Praaant D .O . (a 2) D.O . Dapiation (A | - A2> 7 -h O . 7-7 7 . sT ' 2 0 ' S ' b' /7 ________ / Q -P 7 Avaraga D.O . Dapiation ( , S 2) hU e Bottla No. 6X I 1 BotiNo.Sead Controll 66yVy Initial 047. IC ,I X -y I _____________ SantpiaSua Praaant D.O. <C2 ) "7- 7 0 7- SO 7 ,? 0 Initi(a8l,D1.O. 3 %C 80 M 7.70 D.O. Dapiation 1C, -C 2i A70 hQ 1 o is 7VPSra"aInBt,)0.0. 7* tO 6 .so S'.to >: . Avaraga D O . Dapiation. (C , -C2) A O - iT ;a7y-D'.,O3b<.98ojD,r0aT-piBaat)i/onloA'i Giucosa * Glutamic Acid Standard Bottta No. Sam plaSiza Initial 047. (0 ,) - Praaant 0 .0 . 10,1 79 7>o H S0 X 7 o5 tf-io S-\<T 27gP 3>IT s p *o :x 2 HO 7 Total D .O . ID ,- D a ) rrsf v.9r V Dapiation Dua To Standard 431; 4/ Xfz s ix M - i< r .a* BOO Avanga -Day BOO *23i -p 7?3P -- ~^ 2 3 P!1y/f-(/ Potaasium Hydrogan Phthalate Standard (optional) otttoNo. -'A. Initial 0 .0 . t -7 ' A' > 7 7 7 V X - "7 -7 Praaant D.O. (Dal. v:; '7*: 7> . v --:-- - r Fonii tersa nwo Z ------ - --------- Total 047. Dapiation (P rO j> 7.. m - i 1: Qerdptian Hes# T ttfirtriwrt ; 900- Day ~ . Avaraga . .'Oar -- i& r fl. v;4y.A 7. 77 "7 ':v '. Xr . , 1 //;///- . . v "' 7.-'' V .. `--r-1- - ...... 7-- B A C K T O M AIN Ml Laboratory jk Sheet * Blank*, li, and Standard* UfaT, 2<? MV.fcO.,, 3M W ^ n - YT ' " Lab Request No. t " , . , . . / - BOD Run N o .| f ? 'V9' ' ' m lyit 4 _. v Saad T yo* & Saures ^ - Oat# Started " 9 /0 Saad Concentration Analyst C j - D ay B O D Readings ': Oats ci- '2 o __________________________________________ Nonseeded Dilution - Water Blank ' Bottla No. //-. ... f ' ' Initial D.O. (Ail - , / PraaantD.O. (a 2> . b &->. ' b .b b " - ' v-7.> " b r b -7.SO 0 .0 . Oaplation (At A2) / .3 0 /; 3 0 : Avaraga D.O. Captation (, 2) . i- z f Seeded Dilution - Water Blank (optional ) Bottla No. . Initia D.O. IC ,I /V // :i >y. 7 0 : bo : b b b " _______ __ Seed Controls Praaant D.O. (C2> 7 60 n >7 s ' D.O. Oaplation (Ct c 2i /X 5 ` /.20 /'/ Avaraga O.O. Oaplation. /.aa Bottla No. Sampia Siza Initial D.O. <B,I 82Praaant D.O. < D.O. Oaplation IBl-Ba) y7 ;^ . . .9 0 io ' vie' : :. _____ ___________________ b'-bu b . 70 7. 7 0 ; 7^20 ' C-8 ' ' 67 O s' : Glucose - Glutamic Acid Standard r * -- ---------- Bottla No. Sampia Siza Initiai 0.0. (Dt) Praaant D.D. ' (D2) ; /y ^ '7 V.. / C/ . . b xo . : b T ,/ > o ,s o 6i ? Total D.O. Daplation <i - Da) 3 -7 iT 7 Daplation Dtia To Standard 2m . Hd ' '6 1 3f) -Day BOD 73.H H vo T ^20Avaraga -Day BOD Potassium 1Hydrogen Ptidiaiata Standard (optional) 00Initial . . (Di) Praaant D.O. . . : (D2| V ;b Total D.O. (bt-Da) ' Daplation Dua To SyyHtdyd .. , -Day BOO 7'.vv-bb;-.'-':- . J _V. - Avaraga -Day ' -b o d v Form 18755 PV 0 ;-bi, .V O O 'H s ' =' 0{ -O. * '`s:7-`x 1.; "B A C K T O M A IN tal Laboratory haot Blanks, /and Standards sfp / / y ^ -U L T .lO n4V ^ O ; Lab Request No. f Analyit .7 / / . . su o TVQ* a sourt* . a fe k BOD Run No l f y . ' Q : joate Started S*d Concentration ?/< Analyst ^75? * _6. <Q1~J. f J ____________ - <Ot(ga*~ Noneeeded Dilution W aterBlank . ; ^ (7D Readings ' ; Date ;/ ` Bottle No. Initial D.O. (All Prtent D.O. (Aal iiu " /> / . s ', i f . . .' '!.> 7/ Seeded Dilution-W ater Blank (optional) ': " 7 2e. * 7 '3 5 ' ff, '0 7 r to /--:0 Bottle No. - 6 ;< il /?- Seed Controls Initial D.O. <C* 2Prtant D.O. IC ) Vf 9 0 7.30 S *o ; -i-io f if S ' : ' -y-sS ' 0 .0 . Depletion (A, - A2I !,Q 0 . Airerage D.O. . i wpletion f j 1Ai *2> : /.s t o f 'HS O r K - 0.0. Depletion 1'OaV / 60 ' _a ' ' ' Averepe D.O. : (1 2Depletion -C I ; : h io /<3o / : / M '3 Bottle No. Sample Size , - ?v'*" ' - 3- i i io --- v______________ --mo0 _______ / t 1Initial 0.0. (B I Prtant 0.0. <Ba> . ; 3^575 - vsf fi- Vf 7 . 7c; V-Ts' ' ^>-90 - z .js D.O. Depletion ( B f Bai ' (4.s o S . 70 r ' H-s :f .' Qlucote Glutamic Acid Standard 7*7Bottle No. /W Semple Site ./ArC-'-.:.__ f7,37../?0C Initial 0 .0 . <0,1 $.-t PrtMntD.O. (D2) Potassium HydrogenPhthalataStandard (optional) Total 0.0. -2Sr.Day :Depletion ' bod(Dt *Dp) 9. ^ 'SOO 9.2*=?S 2 0 Depletion Due To Sondarti : 7,/ -10 . 'S 7 '-ff.-/: . . BOO 'Average 2% -PSY ..... v r " ; Bottle No. Semple Size Initial D.O. Prtant D.O. (D,) ; ; (0?) Total D O. Depletion (D, - 0 2) 7-ff;f.'.;' DepletionOua ToStandWd 7."' -De BOO Average Day -:'BOO ::'0 ' ":;V,> 77.;;-';v.J-;-.;*/7".