Document B5jMM7EmJaxpZ9mm9G93vad0o
Interoffice Communication
To From Dace Subject
J. W. Leigh S. K. Biegler September 24, 1982
AN$ CRUDE TE$T RUN
I have developed a list of test samples to be taken during the Alaskan North Slope Test Run. Tables 1 and 2 present sample data required; Tables 3-7 separate sample requirements into groups; Table 8 is a list of important sample data. The five sample groups include: the FCC, the Regular Coker, the Distillate and Gas Oil HDS Units, Jet-50 Components, and No. 2 Heating Oil Components. A reformer test run is not included in the sample list. However, test run data should be collected if coker gasoline is being de sulfurized and reformed. A test run on.the No. 3 CTU is not planned but will be done if deemed necessary.
A cursory test run on the FCC Unit should provide yield information on the heavier ANS gas oils and will determine product sulfur distribution for the higher sulfur feeds. Sample requirements are presented in Table 3. A mini test run on the Regular Coker will provide product yield and sulfur informa tion on coking ANS resid. Sample data is shown in Table 5.
Desulfurizing ANS gas oils provides a good opportunity to determine Gas Oil HDS Unit capabilities. If manpower is available, a complete test run should be conducted on the Gas Oil HDS Unit. The Distillate HDS Unit should be included in the test run because of the interaction of the two units. Sample requirements are presented in Table 4.
Sample data on the refinery kerosene streams (Table 6) will provide the capability to optimize the amount of off-spec ANS kerosene that can be blended to Jet-50. Cetane information on No. 2 Heating Oil blend components will enable the refinery to produce two heating oil blends, grades 76 and 77. Production of grade 77 fuel oil should be optimized as limited by cetane index specifications. Sample requirements are shown in Table 7.
If additional test runs or data are desired, let me know. Also, I would like to know priorities on the proposed test runs for scheduling purposes.
Sue Biegler Staff Engineer Lake Charles Refinery
dim Encs cc/encs: DFM/PWL RH MSJ TJM RBW RHC WJW ARM JOT SGC PAM File: 03.13
MCD 000021097
TABLE 1 SAMPLE TEST DATA REQUIREMENTS
AMS CRUDE TEST RUN LAKE CHARLES REFINERY
MCD 000021098
Gravity, *APl Total SuIfur, WtX
Mercaptan Sulfur, WtX
Total Nitrogen, WtX
Basie Nitroeen. PPM
Distillation, *F
IBP
10X Recovered
30X Recovered
50X Recovered
70X Recovered
90X Recovered
End Point
PONA
Para ffins , X
Ole fins, X
Naphthenes , X
Aromatics, X N-Paraffina. X
Metals
Vanadium, PPM
Nickel, PPM
Iron, PPM
Sodium, PPM
CoDDer. PPM
Smoke Point
Cetane Index
Carbon Residue
Pour Point, Color
Cloud Point. *F
Freeze P_pintj "C
Rl
R1 Temp
1
Aniline Point, *F
Bromine No.
Benzene. X Octanes
Research Clear
Research + 1.1 Gtn Pb
Kotor Clear Motor 1.1 Cm Pb
Viac (? 100* F, CS
0 122T, CS
0 210*F, Cfl
Silicone, PPM
Aah, WtX
No. 2 CTU
Kerosene Diesel
X X X
ffe
X .x
ft,
TV AGO^/Casoline Kerosene
X X-
X vr X
XX
XX
X
X&
No. 3 CTU Diesel AGO
XX XX
X
LVCO X X
X
HVGO X X
X
Resid
X X
X X
Miic. Streams
Cit-Con Cit-Con
Hole*
Gas Oil Reaid
Raffinate
XX XX
X XX
X X X
a*
X
XX
XX
X
XXXX
X
XX
X c
X
XXXX
X
XX
X
X XXXX
X
XX
X-
X
XXXX
X
XX
XV
X
XXXX
X
XX
XV
X
X X X *X
X
XX
X/
X
XXXX
X XX X
X X XX
X X JC
X X '
X X X X X X X
X
X X
X X X X X X X XX XX X X
X. X X
XXXX
X
X
XXXX
X
X
XXXX
X
X
X X .X X
X
X
XXXX
X
X
X
X
X X XXX
X
X
X X XX
X
X
X ..
X
XXX
X
XXX
X
X X
X X
X XX
X
X X X X
X ,X
X X
X
XXXXX
X
X
X
XXXXX
X
X
MCD 000021099
TABu. 2 SAMPLE TEST DATA - CONTINUED
ANS CRUDE TEST RUM
Chareef1)
Coker Caeoline Distillate
Gas Oil
Coke
Total Chi.
FCC Caaoline LCO
HC0
Slurry
Distillate HDS Ca* Oil HDS
Desulf.
Desulf.
Feed Dist. Feed Gat Oil
Gravity, `API Total Sulfur, WtX Mercaptan Sulfur, WtX Total Nitrogen, WtX Basic Hitropen. PPM Distil lation, F
IBP 10X Recovered 30Z Recovered 502 Recovered 702 Recovered 902 Recovered End Point PONA Paraffins , 2 Olefins , 2 Naphthenes, 2 Aromatics, X N. Paraffins. 2 He ta Is Vanadium, PPH Nickel, PPM Iron, PPM Sodium, PPM
Copper, PPM Smoke Point Cetane Index Carbon Residue Pour Point, F Color Cloud Point. *F
freeifi Point* *C RI RI Temp Aniline Point, *P Bromine No. Benzene, X Oc tanea
Research Clear Research +1.1 Cm Pb Motor Clear Motor 1.1 Cm Pb Vise @ lOO'F, CS
@ 12 2 *F, CS
9 210 *F, CS
Silicone, PPM Aah, WtZ
X X X X
X X X X X X
X X
X X 'X X X X X X X X X X X X X
-X X X X X X X X
X X
X X X X X X X X
X X X X X
X
X X
X 'X X
X XX
X X X X X X X
X X
X
X X X X X X X
XX XX XX XX XX
X X
X X
X
X X X X X
X X
X X X X
XX XX
X XX X X X X XX X X X X XX
XX
-r- X X X X X
X XX X X X X XX X X X X XX X X X X XX X X X X XX X X X X XX X X X X XX X X X
XX XX
XX
XX XX XX XX XX XX XX
XX XX X X XX XX
X X X X X
XX
XX
XX
X
XX X X X
XX
XX
XX
X
XX
X
Xx
XX X X X
X X X X
X XX X X X X XX X X X
XX XX XX XX XX
XX XX
XX XX XX
XX XX
(1) If not 100Z ANS Relid
TABLE 3 SAMPLE GROUP-! FCC TEST RUN
ANS CRUDE TEST RUN LAKE CHARLES REFINERY
UNIT FCC
No. 2 CTU Tank Farm Gas Oil HDS Reformers
SAMPLE
TESTS
Total Charge Gasoline Light Cycle Oil Heavy Cycle Oil Slurry Fuel Gas to PCP Abs. Tail Gas P-P B-B Flue Gas
(2) (2) (2) (2) (2) GLC GLC *GLC ,?&GLC
V GLC
GLC SO,
Atmospheric Gas Oil No. 2 CTU Overhead Gas
GLC
Cit-Con Gas Oil- h
(1)
Desulfurized Gas Oil
No. 1 CRU Stab. Overhead^} No. 2 CRU Stab. Overhead^ *
(2)
GLC GLC
(1) See Table I. (2) See Table 2. (3) If unit is operating and sending gas to FCC.
000021100 MCD
TABLE 4 SAMPLE GROUP 2 - DISTILLATE AND GAS OIL HDS TEST RUN
ANS CRUDE TEST RUN LAKE CHARLES REFINERY
UNIT Distillate HDS
Gas Oil HDS
Reformers No. 3 CTU
Coker FCC
SAMPLE
Total Charge Desulfurized Distillate Distillate Stripper Ovhd Recycle Hydrogen
Total Charge Desulfurized Gas Oil Gas Oil Stripper Ovhd
Make-up Hydrogen
Diesel Atmospheric Gas Oil Light Vacuum Gas Oil Heavy Vacuum Gas Oil
Distillate Gas Oil
Light Cycle Oil
TESTS
(2) (2) GLC, "API, Distillation GLC
(2) (2) GLC, API, Distillation
U)
(1) (1) (1) (1)
(2) (2)
(2)
(1) See Table 1. (2) See Table 2.
MCD'000021101
TABLE 5 SAMPLE GROUP 3 -REGULAR COKER TEST RUN
ANS CRUDE TEST RUN LAKE CHARLES REFINERY
UNIT Coker
No. 3 CTU Misc.
SAMPLE
Gas Gasoline Distillate Gas Oil Coke Total Charge
Resid^
Cit-Con Resid^
TES
GLC GLC,
(2) (2) (2) (2)
(2)
(i)
(1)
(1) See Table 1. (2) See Table 2. (3) May want to conduct test run the same day(s) as
Sample Group 2, since two of the samples are required for that test run. (4) This sample could be taken separate from the scheduled Test Run.
,tfCT> 00002T^2
TABLE 6 SAMPLE GROUP 4 -JET-50 COMPONENT
ANS CRUDE TEST RUN LAKE CHARLES REFINERY
UNIT No. 2 CTU No. 3 CTU
-
SAMPLE Kerosene Kerosene Molex Raffinate
TESTS (i) (i) (i)
(1) See Table 1.
MCD 000021103
TABLE 7 SAMPLE GROUP 5 - NO. 2 HEATING OIL COMPONENTS
ANS CRUDE TEST RUN LAKE CHARLES REFINERY
UNIT No. 2 CTU No. 3 CTU FCC Distillate HDS Tank Farm
SAMPLE Diesel Diesel Light Cycle Oil Desulfurized Distillate No. 2 Heating Oil Blend
TESTS (1) (i) (2) (2)
(1) See Table 1. (2) See Table 2.
00002^4
TABLE 8 IMPORTANT TESTS ANS CRUDE TEST RUN LAKE CHARLES REFINERY
UNIT No. 3 CTU
SAMPLE Kerosene
Gas Oil HDS Distil late HDS
Diesel
Res id
Feed Desulf. Gas Oil Recycle Feed Desulf. Distillate
Coker FCC
Gasoline Coke
Feed LCO
Slurry
TESTS
Sulfur Mercaptan Sulfur Aromatic Content Smoke Point
Carbon Residue(on 10% Btms) Cetane Index
Sulfur Metals
Sulfur Sulfur GLC
Sul fur Sulfur Cetane Index Carbon Residue(on 10% Btms)
Sulfur Sulfur Metals
Sulfur Cetane Index Carbon Residue(on 10% Btms) Sulfur
10s