Document 9Zbm4GXOvwrLkbnLKrzdRymp
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In Distribution
C. V* Turner July 9* 1983
REACTOR SLURRY SAMTLES
Tirrlmfnf 1 regulations Unit thi VCM amissions fr
ruetor batch. In ordar to coaply with thoon regulations*
reactor botch la ateen icrlfH* sampled during
and
tly aaalyaed for VCK realduela. The
of
obtaining a alurry realdual aanpla for every batch van recently
healsed in noetlaga with all Vinyl Operatlone personnel. The
purpose of thin latter in to document the proaodoran which hare
established for obtaining and handllag reactor slurry
roeideal a--plea*
1. The slurry
le la to be taken at the
la point op
of the
at flwo to t
iate the
After the A-operater has obtained the aanpla* ha
should radio the Load Operator to ceeflm ha haa the
If the A-oporater haa net coaflmed obtaining the saaple
within ton minutes into the dean* than the
should contact the A-operator and* if necessary* atop
lag the reactor until the aanpla can be collected. Collect'
lag the slurry residual aanpla la the shared responsibility
of both the Load and A-opermtors* and both indiwldnala oust
dananatrata the Initiative to ensure the samples ere
collected.
2 The A-operator in to bring the aanpla to the control i
soon aa practical after it is caught and the Lead Operator la
to verify the
on the aanpla correct. The labeling
should ba checked against the reactor status report and the
blend
Ha will than verify chat ho haa
on the aanpla bottle by underlining the
reactor status report (bar chart). The
battle
be wrapped with adhesive tape to pro-
of the cap
3 After the labeling (reactor wanker* bland nuhber* batch > shift latter designation* data and product) has by the Land Operator* than the A-operator shoe
place the sa^le bottle in the aanpla bottle basks It into the residual aanpla log book (blend nunber* reactor
* and A-operator initials).
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VAB.0001136487
Distribution 7/9/89
P 2
4. fill Lab Tadmieiaa picks up cba alurry raaldnal
ha will varify that ha plekad up Mch
with .hia Initials la tha residual
la log book
5. If a soapla la brokaa or dlscofcnC to ha aiaalag, thaa It vat ha raportad f--ill Italy to tha Vinyl Shift Supervisor. Tha Shift Supervisor will Investigate cod doeuvaat tha raaaoaa for tha brokan/alssl&f soapla. Failure to eollaet and aaalyaa a slurry raaldnal aaapla for ovary raactor batch la a aarloua problav that requires thorough firllow up. If a aaapla la aiaaad dva to oparacor nag11panea, disciplinary action any ha takan.
Our objective t ha to never niaa a raactor alurry raaldnal
c&.'i
C. V* Turnar Vinyl Oparatloua Supervisor
rah p
ccs 411 Vinyl Oparatlona Faraoonal / JF, JWf9 DMU UHt J8V VD(. 14ft DSC,-M
VAB.0001136488
Wastewater Stripp,
6j.65 (t)(9)(t)
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VAB.0001136489