Document 9LeO67E8w05R7748JN0JwRoLq
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DIRECTIONS FOR TEST MO, 14-63-il
SUBJECT: Evaporation Test of Liquid Aroclors
MSTHOfe; / 6 Hours Heating at 100*C*
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Weigh on a' rough balance about 25 grama -'of'. the veil mixed ! >" '*
Aroclor Into an accurately tared tin box, 55 sat* 41a* x 35 mm*
deep (3 z*Gill-style ointment Vox, deep pattern)* Fisher #1--520.
Let stand until box and sample are at room temperature, then weigh
accurately*
.
Place the box In a ventilated oven maintained at 100*C* i 1*
for 6 hours* Remove, cool in desiccator to room temperature and
accurately reweigh* From the loss in weight calculate the evapor
ation in percent* Report't,o second decimal place only*
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:-V ....... *1 ' '[ .V . Noted
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1* Be sure box is at room temperature whenever exact weight
is taken*
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2* The oven should not contain other samples which might in terfere with evaporation*
'' v 3* The method differs from <J*Z* test H-8955622 in that the
oven is of the gravity-connection type Instead of forced eireula--
tion with fan*
*
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4* Because the evaporation loss is sensitive to temperature*
the air bath must be closely maintained at 100*C*
5* Evaporation loss of Aroolor 1254 is normally between 0*05 and 0.1056* Results outside of this range should be promptly checked*
.ABQTP
DSW 330714 STLCOPCB4077358