Document 99orEL6Kz8abmmEoRgZnYM433
AR23-Ot(&
PFOA and Associated Salts
Synonyms: FC-26, FX-1001, PFO, FC-143, 78.03, FC126, N-2803-3, FX-1003, FC-118, FC-1015, FC-1015-X
Physical/Chemical Properties Title
Laboratory or Author
Date Type Completed
Water, acetone and toluene solubilitiy estimates - FC-143 3M Env. Lab
Robust summary, 11/17/81 copy of data sheet
Environmental Fate and Transport Title
R ead y biodegradation of F C -143 (B O D /C O D /T O C )
Technical Report Sum m ary - Adsorption of FC 95 and F C 143 or Soil, and a critique from Dr. S. Boyd, M ichigan State University
Technical Report Sum m ary - Biodegradation Studies of Fluorocarbons - III (F C -1 4 3 ) Technical Report S u m m ary - F C -1 4 3 Photolysis Study Using Sim ulated Sunlight T e c h n ic a l R e p o rt S u m m a ry - A n alys is fo r F lu o ro c h e m ic a ls in Bluegill Fish, an d a critique by J. W . Gillett o f Cornell University
R e ad y biodegradation of F C -1 4 3 (B O D /C O D )
C alculated octanol w a te r partition coefficient - F C -14 3
Ready biodegradation of FX-1001 (BOD/COD)
Ready biodegradation of FC-126 (BOD/COD)
Laboratory or Author
3M Env. Lab 3M Env. Lab
3M Env. Lab 3M Agrichem ical
Lab 3M Env. Lab
3M Env. Lab 3M Env. Lab
3M Env. Lab
Pace Analytical, Minneapolis, MN
Completion Type
Date
7 /1 4 /7 7 Robust summary,
copy of laboratory
data summary
2 /2 7 /7 8 , Robust summary,
5 /1 9 /9 3 technical report,
critique by S. Boyd
(MSU)
7 /1 9 /7 8 Robust summary,
technical report
2 /2 /7 9 Robust summary,
technical report.
5 /1 /1 9 7 9 , Robust summary,
3 /8 /9 3 technical report, ,
critique by J. Gillett
(Cornell)
6 /5 /8 0 Robust summary, ~
copies of data
sheets.
12/7/81 Robust summary,
copy of
calculations
Robust summary,
computer-
generated final
report, copies of
2/7/85 raw data sheets.
Robust summary,
computer
generated final
report, copy of
5/20/87 final report
tt
003600
PFOA and Associated Salts
Environmental Fate and Transport Title
Technical Report Summary - Assessment of the Bioaccumulative Properties of Ammonium Perfluorooctanate: Static (fish test)
Ecotoxicity Elements Title 96-hour acute static toxicity to fathead minnow - FC-143
Laboratory or Author
3M Env. Lab
Completion Type
Date
Robust summary,
technical report,
critique by J. Giesy
5/31/95 (MSU)
T.IT{
Laboratory or Author
3M Env. Lab
Completion Type Date
6/29/74 Robust summary, copy of data sheet
96-hour acute static toxicity to fathead minnow - FC-26
3M Env. Lab
Robust summary, 11/10/74 copy of data sheet.
96-hour acute static toxicity to bluegill sunfish - FC-143
3M Env. Lab
Robust summary, 4/8/78 copy of data sheet (
96-hour acute static toxicity to bluegill sunfish - FC-143
3M Env. Lab
Two reports : 'The Effects of Continuous Aqueous
Exposure to 78.03 on Hatchability of Eggs and Growth
and survival of Frv of Fathead Minnow (PimeDhales
Dromelas)" and "Summary of Histopathological
Examinations of Fathead Minnow (PimeDhales Dromelas! EG&G Bionomics,
Exposed to 78.03 for 30 Days".
Wareham, MA
Technical Report Summary - Aquatic Toxicity Testing: FC-
143 (Lot-37) L.R. 5625 S
3M Env. Lab
Toxicity to activated sludge - FC-143 Technical Report Summary - Multi-Phase Exposure/Recovery Algal Assay Test method (FC-143)
48-hour acute static toxicity to Daphnia magna - FC-143 (3 studies on diet) Chronic Toxicitv of Fluorochemicals to Daohnia maana (Water Flea) - FC-143, and statistical analysis of data provided byAScI Corp., Duluth, MN
3M Env. Lab 3M Env. Lab 3M Env. Lab 3M Env. Lab
5/27/78
June 1978 and Sept.
1978
5/8/80
6/4/80
11/16/81 5/5/82, 5/6/82, 6/2/82
8/31/1984, 8/10/98
Robust summary, copy of data sheet
Robust summary, copies of two final reports. Robust summary, technical report Robust summary, copies of data sheets Robust summary, technical report Robust summary, copies of data sheets Robust summary,. summary report, ~ letter report
96-hour acute static toxicity to fathead minnow - FX-1001 3M Env. Lab
2/2/85
Robust summary, copy of data sheet.
003601
PFOA and Associated Salts
Ecotoxicity Elements Title
Activated sludge respiration inhibition (OECD 209) - FC126
Microtox test - FC-126
48-hour acute static toxicity to Daphnia magna - FC-126
96-hour acute static toxicity to fathead minnow - FC-126 Activated sludge respiration inhibition (OECD 209) - FX1003
Microtox test - FX-1003 Static Acute Toxicity of FX-1003 to the Fathead Minnow, Pimephales promelas Static Acute Toxicity of FX-1003 to the Daphnid, Daphnia magna Growth and Reproduction Toxicity Test with N2803-3 and the Freshwater Alga, Selenastrum capricomutum Acute Toxicity of N2803-3 to the Fathead Minnow, Pimephales promelas Acute Toxicity of N2803-3 to the Daphnid, Daphnia magna
Microtox test - FC-143
Microtox test - FC-118
Microtox test - FC-1015-X
Laboratory or Author
3M Env. Lab
3M Env. Lab
3M Env. Lab
3M Env. Lab
3M Env. Lab
3M Env. Lab EnviroSystems, Hampton, New
Hampshire EnviroSystems, Hampton, New
Hampshire T.R. Wilbury Laboratories, Inc, Marblehead, MA T.R. Wilbury Laboratories, Inc, Marblehead, MA T.R. Wilbury Laboratories, Inc, Marblehead, MA
3M Env. Lab
3M Env. Lab
3M Env. Lab
Completion Date
4/20/87 4/29/87 4/30/87 5/1/87 2/16/90 3/7/90 3/15/90 4/9/90 1/24/96 1/24/96 3/7/96 4/24/96 4/24/96 4/24/96
Type
Robust summary, /
copy of data
j
sheets.
^
Robust summary, i
copy of data
sheets.
Robust summary,
copy of data
sheets.
Robust summary,
copy of data
sheets.
Robust summary,
copies of data
sheets
Robust summary,
copies of data
sheets
Robust summary,
final report,
protocol
Robust summary,
final report,
protocol
Robust summary, final report
Robust summary, final report
Robust summary, final report Robust summary, copies of data sheets Robust summary, copies of data sheets Robust summary, copies of data sheets
00360?
i
PFOA and Associated Salts
Ecotoxicity Elements Title
Activated Sludge Respiration Inhibition Test - FC-1015-X Acute Toxicity of FC-1015 to the Fathead Minnow, Pimephales promelas Growth and Reproduction Toxicity Test with FC-1015 and the Freshwater Alga, Selenastrum capricornutum
Acute Toxicity of FC-1015 to the Daphnd, Daphnia magna
Laboratory or Author
3M Env. Lab T.R. Wilbury Laboratories, Inc, Marblehead, MA T.R. Wilbury Laboratories, Inc, Marblehead, MA T.R. Wilbury Laboratories, Inc, Marblehead, MA
Completion Type
!
Date
Robust summary,
copies of data
4/25/96 sheets
Robust summary, 5/15/96 final report
Robust summary, 5/15/96 final report
Robust summary, 5/15/96 final report
Sum m ary Reports
Title
Technical Report Summary - Final Comprehensive Report: FC143
Laboratory or Author
3M Env. Lab
Com pletion Date
3/23/79
Type
Robust summary, technical report
i
I -1 t
t
i
\
003603 l
WATER SOLUBILITY
TEST SUBSTANCE
Identity: Perfluorooctanoic acid, ammonium salt; may also be referred to as PFOA ammonium salt, Ammonium perfluorooctanoate, FC116, FC-126, FC-169, orFC-143. (Octanoic acid, pentadecafluoro-, ammonium salt, CAS # 3825-26-1 )
Remarks: The 3M production lot number was 37. The test sample is FC-143. It's purity was not sufficiently characterized, though current information indicates it is a mixture of 96.5 -100% test substance and 0 - 3.5% C6, C7, and C 9perfluoro analogue compounds.
METHOD
Method: Not noted GLP (Y/N): No Year (study performed): 1981 Remarks field: Test was done in deionized water, toluene, and acetone.
RESULTS
Solvent
Toluene Acetone Dl Water
Concentration
1 gram / 100 mL 1 gram /100 mL 1 gram /100 mL
Description of Solubility Nil Complete Complete
Acetone Dl Water
10 gram /100 mL 10 gram / 100 mL
Complete Complete
Acetone Dl Water
10 gram /10 mL 10 gram / 10 mL
Complete Complete
Remarks: No information is available on the test conditions.
DATA QUALITY
Reliability: Klimisch ranking =4. The method followed is not available. This study lacks sufficient documentation, characterization of the test substance purity and analytical measurement of test concentrations.
REFERENCES
003604
This study was conducted by the 3M Company, Environmental Laboratory, St Paul, MN, 1981. OTHER Submitter: 3M Company, Environmental Laboratory, P.O. Box 33331, St. Paul, Minnesota, 55133 Last changed: 5/24/00
C03G0
' TD P
ENVIRONMENTAL ENGR. LAB
SAMPLE DESCRIPTION
VC \43 ucrr 31 ^ o u u a \b rry
-tih > :
Fiie: Page No.
: i l / l Y / 8 1WORKSHEET Date
Analyusett*
Hrs.:
_______________________ ____________________SobU FdblTY_____
Ikl *Tol1ufkJP.
\ arawi^ /1 oD ml
K1d
1 G C ?!
A tftkiF.
CZJMPbETF,
Y L l WffTER._1a rayv* / 1OQ ndj __ ________ C qKPUETE
Ikl AcFTOKlF
10rttU/lOhHii (l(^/|Ofyv (CMPbCTF
_Iu_lb X
___l.graW\QOvnf U/lQQQ/___QoMPLjETE^_____
Xu AtftowF
lOopwvi^/lO wti Y iono/jnoo') (JorHPLFTF
X u TfvT . \AfmFR lO rtra m s/l wii /lOOft/lOOO^ 0 CiMPl FTF.
>
Reviewed by:
PFOA and Associated Salts
Synonyms: FC-26, FX-1001, PFO, FC-143, 78.03, FC126, N-2803-3, FX-1003, FC-118, FC-1015, FC-1015-X
Physical/Chemical Properties Title
Laboratory or Author
Date Type Completed
Water, acetone and toluene solubilitiy estimates - FC-143 3M Env. Lab
Robust summary, 11/17/81 copy of data sheet
Environmental Fate and Transport Title
R e ad y biodegradation of F C -1 4 3 (B O D /C O D /T O C )
Technical Report S u m m ary - Adsorption o f F C 9 5 and F C 143 or Soil, and a critique fro m Dr. S. Boyd, M ichigan S tate University
Technical Report S u m m ary - Biodegradation Studies of F lu o ro carbo n s - III (F C -1 4 3 ) Technical R eport S u m m a ry - F C -1 4 3 Photolysis S tu dy Using Sim ulated Sunlight T e c h n ic a l R e p o rt S u m m a ry - A n a ly s is fo r F lu o ro c h e m ic a ls in Bluegill Fish, and a critique by J. W . G illett o f Cornell University
R ead y biodegradation of F C -14 3 (B O D /C O D )
Calculated octanol w ater partition coefficient - F C -1 4 3
Ready biodegradation of FX-1001 (BOD/COD)
Ready biodegradation of FC-126 (BOD/COD)
Laboratory or Author
3M Env. Lab 3M Env. Lab
3M Env. Lab 3M Agrichem ical
Lab 3M Env. Lab
3M Env. Lab
3M Env. Lab
3M Env. Lab
Pace Analytical, Minneapolis, MN
Completion Type Date
7 /1 4 /7 7 Robust summary,
copy of laboratory
data summary
2 /2 7 /7 8 , Robust summary,
5 /1 9 /9 3 technical report,
critique by S. Boyd
(MSU)
7 /1 9 /7 8 Robust summary,
technical report
2 /2 /7 9 Robust summary,
technical report.
5 /1 /1 9 7 9 , Robust summary,
3 /8 /9 3 technical report, ,
critique by J. Gillett
(Cornell)
6 /5 /8 0 Robust summary, ~
copies of data
sheets.
12/7/81 Robust summary,
copy of
calculations
Robust summary,
computer-
generated final
report, copies of
2/7/85 raw data sheets.
Robust summary,
computer
generated final
report, copy of
5/20/87 final report
t
i
!
003607
PFOA and Associated Salts
Environmental Fate and Transport Title
Technical Report Summary - Assessment of the Bioaccumulative Properties of Ammonium Perfluorooctanate: Static (fish test)
Laboratory or Author
3M Env. Lab
Completion Type Date
Robust summary, technical report, critique by J. Giesy 5/31/95 (MSU)
Ecotoxicity Elements Title
96-hour acute static toxicity to fathead minnow ^.FC-143
Laboratory or Author
3M Env. Lab
Completion Type Date
6/29/74 Robust summary, copy of data sheet
96-hour acute static toxicity to fathead minnow - FC-26
3M Env. Lab
Robust summary, 11/10/74 copy of data sheet.
96-hour acute static toxicity to bluegill sunfish - FC-143
3M Env. Lab
Robust summary, 4/8/78 copy of data sheet
96-hour acute static toxicity to bluegill sunfish - FC-143
3M Env. Lab
Two reports : 'The Effects of Continuous Aqueous
Exposure to 78.03 on Hatchability of Eggs and Growth
and survival of Frv of Fathead Minnow (PimeDhales
DromelasV and "Summary of HistoDatholoaical
Examinations of Fathead Minnow (PimeDhales Dromelasl EG&G Bionomics,
Exposed to 78.03 for 30 Days".
Wareham, MA
Technical Report Summary - Aquatic Toxicity Testing: FC-
143 (Lot-37) L.R. 5625 S
3M Env. Lab
Toxicity to activated sludge - FC-143 Technical Report Summary - Multi-Phase Exposure/Recovery Algal Assay Test method (FC-143)
48-hour acute static toxicity to Daphnia magna - FC-143 (3 studies on diet) Chronic Toxicitv of Fluorochemicals to DaDhnia maana (Water Flea) - FC-143, and statistical analysis of data provided by AScI Corp., Duluth, MN
3M Env. Lab 3M Env. Lab 3M Env. Lab 3M Env. Lab
5/27/78
June 1978 and Sept.
1978
5/8/80
6/4/80
11/16/81 5/5/82, 5/6/82, 6/2/82
8/31/1984, 8/10/98
Robust summary, copy of data sheet
Robust summary, copies of two final reports. Robust summary, technical report Robust summary, copies of data sheets Robust summary, technical report Robust summary, copies of data sheets Robust summary,, summary report, letter report
96-hour acute static toxicity to fathead minnow - FX-1001 3M Env. Lab
Robust summary, 2/2/85 copy of data sheet.
603608]
Ecotoxicity Elements
PFOA and Associated Salts
kt %
Title
Laboratory or Author
Completion Type Date
Robust summary, :'
Activated sludge respiration inhibition (OECD 209) - FC126
3M Env. Lab
copy of data 4/20/87 sheets.
, "?
Robust summary, l
copy of data
Microtox test - FC-126
3M Env. Lab
4/29/87 sheets.
Robust summary,
copy of data
48-hour acute static toxicity to Daphnia magna - FC-126 3M Env. Lab
4/30/87 sheets.
Robust summary,
copy of data
96-hour acute static toxicity to fathead minnow - FC-126
3M Env. Lab
5/1/87 sheets.
Robust summary,
Activated sludge respiration inhibition (OECD 209) - FX-
copies of data
1003
3M Env. Lab
2/16/90 sheets
Robust summary,
copies of data
Microtox test - FX-1003
3M Env. Lab
3/7/90 sheets
EnviroSystems,
Robust summary,
Static Acute Toxicity of FX-1003 to the Fathead Minnow, Hampton, New
final report,
Pimephales promelas
Hampshire
3/15/90 protocol
~i
EnviroSystems,
Robust summary,
Static Acute Toxicity of FX-1003 to the Daphnid, Daphnia Hampton, New
final report,
magna
Hampshire
4/9/90 protocol
T.R. Wilbury
Growth and Reproduction Toxicity Test with N2803-3 and Laboratories, Inc,
Robust summary,
the Freshwater Alga, Selenastrum capncornutum
Marblehead, MA 1/24/96 final report
T.R. Wilbury
Acute Toxicity of N2803-3 to the Fathead Minnow,
Laboratories, Inc,
Robust summary,
Pimephales promelas
Marblehead, MA 1/24/96 final report
T.R. Wilbury
Acute Toxicity of N2803-3 to the Daphnid, Daphnia
Laboratories, Inc,
Robust summary,
magna
Marblehead, MA 3/7/96 final report
Robust summary,
copies of data
Microtox test - FC-143
3M Env. Lab
4/24/96 sheets
Robust summary,
copies of data
Microtox test - FC-118
3M Env. Lab
4/24/96 sheets
Robust summary,
copies of data
Microtox test - FC-1015-X
3M Env. Lab
4/24/96 sheets
-- k
03608
ii(
PFOA and Associated Salts
Ecotoxicity Elements Title
Activated Sludge Respiration Inhibition Test - FC-1015-X Acute Toxicity of FC-1015 to the Fathead Minnow, Pimephales promelas Growth and Reproduction Toxicity Test with FC-1015 and the Freshwater Alga, Selenastrum capricornutum
Acute Toxicity of FC-1015 to the Daphnd, Daphnia magna
Laboratory or Author
3M Env. Lab T.R. Wilbury Laboratories, Inc, Marblehead, MA T.R. Wilbury Laboratories, Inc, Marblehead, MA T.R. Wilbury Laboratories, Inc, Marblehead, MA
Completion Type Date
!
Robust summary,
copies of data
4/25/96 sheets
Robust summary, 5/15/96 final report
Robust summary, 5/15/96 final report
Robust summary, 5/15/96 final report
Sum m ary Reports
Title
Technical Report Summary - Final Comprehensive Report: FC 143
Laboratory or Author
3M Env. Lab
Com pletion Date
3/23/79
Type
Robust summary, technical report
\
|
il l
i.
-i
1 'I
I
(
S iO
15 i
