Document 99YZpqQ4b8O23gwwE6rnKmw1e

esnencd L N) we'd #0 \ # Anca. meron PFOAPFOSAnalysis Lot#: D8A170279 ' NWTe iololmiamtnhGn reennbniiellrne Tomer Den oia led etn 208 Neuen rst AnhCONOR TOS BAI rms oee2sows.oomna Table Of Contents Standard Deliverables Report Contents (TShtoaRnedpaorrtdCoDveelrpiavgeoraibclonessidaredannogral artofthis `lStlapnadgaersdiDnedlivceartaedbilnophacskTaagbel. oTfhCs roeponrtastroceonmcnupceettd)niss + Table of Contefts Case Narrative Executive Summary - Detection Highlights + Methods Summary * Method/Analyst Summary LotSample Summary Analytical Results QC Data Association Summary + aC Results + Chain-of-Custody Sample Receiving Checklist Total Number of Pages Testamerica 1 DEP2.SDWB-000075 CasDeeANIa7r0r2a1t9ive "QTunealriesMualnsuianlc.luAdeldeisnutlhtiss hreapvoertbheaevefboeunedn1roevmieeewtedalforrecqoumirpelmieanntcseowfilNh EthLeALaabonrdaatonryy `exceptions are noted below. o"Trhisspornespoorrt.shDalilonont bfaeciroerpsroadnudceodineoxtceepsthianvuel,bewietnhopurtovtihdeewd ioneneaacphpdroavtaalshoefetth folaasbsoirsattoinry he merpretaion ofth resuls. `Sample Arrival snd Receipt "ITahbeoroantoerwyaattear tseammppelreatpurreeseonft5ed3inCtohins Jraepnouratrwya1s7,r2e0c0e8i.vedatthe TestAmerica Denver S`Atnaanlydiacradlsstandards were prepared using the acd form of the compound perfuorooctanci acid (PFOR). PFOS is a commercal prepared and certified solution. Perfluoro-n-1,2,3,4-"C Joctancc acd was troduced at the extracion step and was used as aiPnnRtOirSno.tdeumcaeld istatnhdeaerxdtrfaocrtqiuoannstietpatiaonndofwaPsFOuAs.edPaesrfalnuonrfoe-m1-a{l1,s2a,n3d4-a"r"dCafjoorcqtuaannattietsautlifoonnaofte was `ETShaemxpslaetmplres aprescenattneddiAinntaohlsysnriepsort were analyzed for the target analytes by TestAmerica Denver's SOP DEN-LC-0012. aFnordwtasteerxstaramcptleedsuasi2n5g0smoLdaplhiqausoet eoxfteraaccthiosnatmcphlreiiqsuaeciwdiitfhiemdewtihtahn1olmLcoonfd6oNnHeCdICs1ol8ution fcsiaanramtlrpivldoegleisus.mpeaEsiascbehrdosruagomhuptlg1eh5isthmseip.icakurestdirniwdgigtemh,ettthhheaeniaonntlelamyanildesshtaearnedeaxetrlrdua,tceptdriiswoiratnthao4leyxmztLreaodcftbiyomneL.tOhMaAnfStoIelr.MtSh.Tehe MetQChSaompldes "mbTaihttechMfoeortfth2ho0edtsaBarlmgapentlkeasinsaopifrootshc.eesssaemdermeaaglein.t wTatheermseptihkoedd wbiathnksuwrarosgnatoena-nddeptreeacptahreed rweipthoreiancgh lEeavcelhsbwaetrceh wisiprnepeasrteadblwiisthhedLacboonrtartoolrmyiCtosn.trol Samples (LCS). The LCS recoveries for both APnFalOyStiwcaalsCroecmomveernetdsoutside the QG contol lis, biased high, in the MS for batch 8017446. This is an indicator hal dala may be biased high. All oerGC was i contol 8T0h1e7P4F48OSexstaimbpielde RduPplDicdaattea(oDu8tAsi1d7e02th7e9-Q0C01c)onatnraollysmiis sdata associated with QC batch No other anomalies were noted Testhnerica 2 DEP2.SDWB-000076 EXECUTIVE SUMMARY - Detection Highlights Dentzer free sus suemveorsTIvG mate WG DETRCEARLE PETS waesninc, Testanerica a DEP2.SDWB-000077 METHODS SUMMARY aar7oz7s ARETE moEwmriTnICAL e/ms/ws, Bron om -1c-0012 References: oan Severn Trent Laboratores, Denver, Facility Standard Operating Procedure aPmRiEoPDA.RATION TestAmerica a DEP2.SDWB-000078 ME/T ANALH YSTSO UMMD ARY pen70279 AMnEATLHYODT.IAL yer oan -ic-0012 aqueline Bonnett Referencen: on Severn Trent Laboratores, Denver, Facility Standard Operating Procedure. vst 003601 Testanerica s DEP2.SDWB-000079 SAMPLE SUMMARY Danr70279 WO swipLEs cier ape 1 KENT 001 pROR/BFOS mTooress)i: 3rie tr prtEr Ancts ramettening infars co sovenuisve , 01/16/08 07:05 Bons einpieeee red 1i. cry, Tp.3a, rc ihr. prey resis, op,pee 4, Ae,NS,rg, Testamerica 6 DEP2-SDWB-000080 Cash in Avance / prepaid sales Client Sample 1: Broa/eros wc DLoatt-eSSamapmlpele4.d...:.: D0E1A/L1760/20789-0070:105 DWoartke ROercdeeirve4d.....:: K0F1P/1N7T/I0A8A PPrreepp DBaattec.h..4.......: 08011/71474/608 `AAnnaallyyssiiss DTaitmee..:: 2001:/1281/08 Dilution Factor: 1 Method. .......: DEN -1C-0012 Matrix.........: WATER ornoasnugreR Pron REsuur RieaporRTING rms wmw 0l.0o10s gug//tL s13u0m4mouparToEx. 1304 ROS eREECROcVaENRTY. 5103 RLEaCrOVsERY ((5500 -- 220000)1 Testanerica 7 DEP2-SDWB-000081 Cash in Advance / Prepaid sales Client Sample I: PFOA/Pros DUP sme TDoatt-eBSamapmlpele4d....:.. D0E1A/I1760/20789-0070:105 WDaotrek ORercdeeirve4d.....:: K0F1P/N1T7L/A0D8 PPrroeppBDatacthe.i......:: 80011/71474/600 `nhooaallyyssiiss TDaitne.e.:.: 2001:/5201/08 Dilution Pactor: 1 Method. .......: DEN -1C-0012 Matrix.........: WATER PrhoasngTER ron, Rasuur RpEaROrRTING ors w 00.00100% wuga/iLt `TsaucmsmoupTrso.n 1304 PROS pReecrocveery. a100 LReacrovssRy ((5500 -- 7200007) Testhnerica 8 DEP2.SDWB-000082 sneer 01 QC DATA ASSOCIATION SUMMARY Dem70275 Sample Preparation and Analysis Control Musbers wrx awmeumiroTnICAL WER pn -ic-00z Lamacrcus mPraetpcid soars us Row s012ss Testamerica 5 DEP2-SDWB-000083 METHOD BLANK REPORT mic CHB lLotiL-Soeatrpnl.e.t.:: RDEGRALL7700020709-446 Work Order #...: KEPSQIA Analysis pate..: 01/21/06 pPrreepp DBaattec.h........:: 80011/71474/608 Dilution Pactor: 1 Matrix. .......o WATER AnalystsTime..: 19:30 FeraosnnmTER ves Resuur RiEaPOrRTING ours weaoo ww 00..000009 uugg//LL DDEENN --110G--00001127 s1u3R04RoaParToE" 134 prOS RemscRcoevnETRy 5a pREaCrOVsERY ((5x00 -- 220000)) CoruRe(ss)ve reti oe el 7 Aon -- Testhmerica 10 DEP2-SDWB-000084 LABORNTORY CONTROL, SAMPLE EVALUATION REPORT re CCl3ienLtotL-Soatmpl.e.d.:: DREAALLI700207090-446 Work Order #...: KFPSQIAC PPrreepp DBaattec.h..#......:: 08011/71474/608 AAnnaallyyssiios TDaitme.e..:: 0119/:2461/08 Dilution Factor: 1 Matrix.........: WATER aemvyETER ors mPBEcRoCuEsNRTy RaEmCiOVsERY emo _ E0y (009--1213000) DDmExN 1-1cC--o0001122 `3su0m4RoaparTos" 1304 2ROS eReeRccoavNeTry 57 `LRpeacorvsERY ((5500 -- 220000)) CBroerEs(se) edlr rin 70 of 0 ne tp drsetan Testamerica n DEP2-SDWB-000085 LABORATORY CONTROL. SAMPLE DATA REPORT wc 1C0l8ieLntotL-SoatmpNl..e.d:: RDEGAALL7700020709-446 Work Order 4...: KEPSQIAC PPrreepp DBaattec.h..f.l.....:: 0810/11774/4063 RAnoaallyyssiios DTaitmee....:: 0119/:2416/08 Dilution actor: 1 Matrix.........c OTE e= neneTsR ros soeuxset waansvooRED ours 00..220000 o0l.1s82 wwaafrtn eREeRcCoEvNeTry wsmion 52 DDtx 1160--00001172 `1s3mm4oaPaRTOsN. 134 PROS eReercocvaeRTy 5n RLamcrotvsERY ((5500 -- 220000)) CHhomiess)t:err toeia g tf1 i [rr -------- Testamerica 12 DEP2-SDWB-000086 LABORATORY CONTROL SANPLE EVALUATION REPORT mene C1l0i5enLtot%-oStamp4i.e.d.:: DRGEAALL7T00207090-446 Work Order 4...: KFPSQUAD PPrreopp DBaattec.h........:: 0810/11774/4063 BAonaallyyssiiso DTaitme.e..:: 0201:/0221/08 Dilution Pactor: 1 Matrix........: WATER seProtn a pros. PERCENT R7ECOVERY asa RECOVERY LGIoM- I1T0S) (39 - 1200 MDewE-1W co0Oz D pmW -1c-0012 `1su3m4mouPaRTOEN. 134 PROS EscrocVERY 1072 RLeacmoivtesry ((5500 -- 220000)) weoreE(ns)se rti ie 1os ro co EE Spe vytedoe Testanerica 13 DEP2-SDWB-000087 LABORATORY CONTROL, SAMPLE DATA. REPORT me CLlCiSenLtot-TSoatmpfl.e.d.:: DRSEAAIL7700207090-446 Work Order #...: KFPSQIAD PPrreepp DBaattec.h........:: 80011/71474/608 hAnnaallyyesiiss DTiamtee...:: 2001:/0221/08 Dilution Factor: 1 Matrix. os WATER rooAaETER vrs . smoorwer wawrosuwRED parte mpeecrocvEeNrTy msmion 00.2020000 0o.o022374 a wga/lt b12g8 ERww 1-16c--00001127 `1su3R4moapnOTs" n 1304 BROS sr eca y REcovERY 1702 ((5S0o -- 220000)7 porr(es)ve:eer ereode rc hia +Srpnddmeecmoeipinsd i. Testimerica 1 DEP2-SDWB-000088 MATRIX SPIKE SAMPLE EVALUATION REPORT 5Tot-LSoatm-Spalmepl.e..:: DDIAALII00227739-001 Work Order ...: KPENTIAC DParteep SDaamptleed......:: 0011//1167//0088 07:05 aDnaatleysReicseiDvaetde....:: 0011//2117//0088 DPirleuptBiaotnchPact.o.r.:: 81017446 Matrix.........: WATER P= rRETER. Pros `1su3m4moPonRTOs _ 1304 P05 worE(s:) [v---- 1R0e5covmy Py L0ut-s1301 9 - 120 `BPcEoRCvEENRTY 103 eDmRo1,0-0013 Den -1c-0012 RLoEvCeOrVsERY (50 - 200) (50 - 200) Testanerica 15 DEP2-SDWB-000089 MATRIX SPIXE SANPLE DATA RRFORT : mie 5Lot-LSoatm-Spalmepl#.e..:: DDIAALLIT00227799-001 Work Ocder #...: KFPNTIAC PDraetpeDSaatmep.l.e.d......:: 0011//1176//0088 07:05 ADnaatleyRsiesceDiavteed...:: 0011//2117//0088 DPirleuptiBaotncPhac#t.o.r.:: 81017446 Matrix... WATER en=RANETER eros s1u3m4mooparTosn _ 1304 BOS lomoRi(ss)v:epred io ig SAMeOUsNT AsMeTIKE AvMEOAUSNRTD UNITS WmwW 00.220000 00..211858 uvaa//iu RvEERCCOEVNETRY B1E03 Tr rsA pReERCcOaVNEtRY METHOD 1005 DDEiNn -_11.c6--00001122 pRreicmoevyaRY ((s5o0 -- 2200000 Testanerica 16 DEP2-SDWB-000030 SAMPLE DUPLICATS EVALUATION REPORT me CSlDiLeontt-SLoatspl#.e..:: DpaNnL17700227759-001 Work Order 4... KKFPPoNNTTIIAAAD -DSUHPE Matxix.......: WATER DParteep DSaamtplee.d......: 0011//1176//0088 07:05 aDnaatleysReicseivvaetd.e..:: 0011//2117//0088 "Rn gs DPirleuptiBoantcFhac#t.o.r.:: 2201746 Analysia Time.: 20:50 eProEsTER Pron _ smewsoeur _ bmueesLwircaTs outs mp RLepoar wemon ww ww waugr/tL 12600 ((00--2200)) DDEENN 1-16c--60001122 s13u0RsRoopArTosn RECOVERY 2301 pros SBEmCeOLVEERY3 _ RpEuCPOLVIECRMYTE_+ RECOVERY LIMITS 6103 1E0y1 ((ssoo -- 220000)) Testamerica, 17 DEP2-SDWB-000091 3] ol Hi] VE 1 Ciel I ELT i Tip 1] E j oli |e AA aid . Ll. j 8 8 TLR 3 SHEN zr| & "H z i Eft {| ELLIE |8[ i ree | LLLHE i LLE ee {a sir e rr A 0 TT TT en ni EER | eclhcle i ol 3 | iE Ey fr TU BEE FRE qa NF EEE SEQ 1 om Hy | EEE -- 1113 \ + ME | [] Sn enmn BC] [0 i Sr m rr e r 2 10 2 ila 1| i2