Document 99Y84eXae75Ed02zMe8oOaj7p

DownloadRandom document
BIODEGRADATION (BOD/COD) TEST SUBSTANCE Identity:A mixturecontainingperfluorooctanesuftnatew,hich may alsobe referredtoas PFOS, FG-95, oras a component of L-4647. (1Octanesulfoniaccid)(CAS # 2795-39-3). Remarks: The testsample is1.356% solutionofL-4647. Current informationindicatesitisa mixtureof6.6% PFOS, 20% polyethyleneglycol, 20% hexahydricalcohol,39% sodium decylsulfate1,3.2% Hydroxy foamer, 1% sodium ethylhexylsulfate0,.1% niethylhydroquinonea,nd 0.1% biphenylols,odium salt,tetrahydrate. The followingsummary applies toa mixture with incompletely charactedzed concentrations of impudties. Data may not accurately reftct the biodegradabilityof the ffuorochemical component of the test sample. METHOD: Method: BOD protocol3/10/80. Type: Aerobic GLP: No Year completed: 1980 Contacttime:20 days lnoculum: Chemolitesewage. RESULTS Chemical Oxygen Demand (COD): BiochemicalOxygen Demand (BOD): 5-Day: 1O-Day: 20-Day: 17,000 rng/L 16,000mg/L (duplicate) 7,700 nig/L 8,600 mg/L 11,000 mg/L CONCLUSIONS No conclusionsgiven. Submitter. 3M Company, EnvironmentalLaboratory,P.O. Box 33331, St. Paul,Minnesota,55133 DATA QUALITY ReliabilitKyl:imiscrhankin3g. Studylacksdescriptiaonnd recordosfthe method followed.The inoculumwas not properlycharacterized.There isno charactedzabon ofthe testsubstance puritya,nd the studylacksanalytical confirmationoftheamount offluorochemicalproportioninthe solution. REFERENCES This studywas conducted by the 3M Company, EnvironmentalLaboratory, St.Paul,MN, Lab Request number 5623S, 1980. OTHER Lastchanged: 6/26/00 Form 10620-5-PWO cc: LAB RECIUEST BOOK - 42-5W I ENVIR. AS SESS. INQ. PRODUCT: I- - dlllq 7 -Ax (OJLI,39, PRODUCT ECOLOGICAL ASSESSMENT REQUEST FOR LABORATORY WORK DIVISION L- k/. A FF F c. - ,, 3..M7xuoyraooftpi LAB REQUEST NO SIO& 43@ a r@ r REQUESTER LABORATORY Name: t@c,--- Phone No. 5-0 -2-9 RequesDtate:4g2f.,!I2Z./f/t,i-) Project No.: 9fl-7001 zt a Prob. No. Code No.: Sample Date: Date Needed: Description: c,4L- Date Received Spayt, Analyst: Date Completed: Hours Spent: y B- - /-W() AAT-TF "P Please Call Requester If Delays Are Encounter PurposeofTests: PHYSICAL & CHEMICAL PROPERTIES Heatof Combustion Cal/G (BTU/Lb.) Density -A;@@ Other 4 Ale,917 WY'N TAO WATER POLLUTION -V"-cnh COD BOD 5 BOD, Ultimate TOC Gc Oxygen Uptake Dehydrogenase Activity(TTC) Other BIOASSAY Specify Organism and Method: 9e#, Le-:S-a LEACHATE FROM LEACHING pH COD BOD 5 BOD, U!timate TOC GC Sioassau Olh-- TEST THER Bioaccumulation Persistence Degradation Products ot, QO d v 11 0'0a&wjqa. L/ Z In dft4 ;r1550M,51f k4- v v U. Whk*-PleturntoRequutor Conory -EnvironmentalEngrg.OfflesFile' tEnk:-Environmeo lErigrg.Lob -Goidenrod- Flowmto Requester ivironr;mitLia'-Iomtory 3D Work Shoot -SOMPISS @Laabb Roeqq. No. $L .nolvst BOD Run No-O AnslYst f17 Day BOD Readino 3M ,wnpis orwipti6n b"g DNutlbn inhw Dgution Fee.in@' Me. ................... CWKU of ftw4ftl smnpb $INS 270 Ief*7/foo 00 ofsompledilutetdo IC)O ml with D Iwater 4 lq. (C)ilutifoanctor I ifundiluted) DA). (DI) 0-0- ID2@) Told 0.0. D"down ID1 -021 T5 ompbtwn D" TO INV*" ow wo AwmP oev moo 9-0 Note: 1. Corc. Concentrooon of umple (miA O(E@in SOD bottles. 2. sgmpk Six* ml or g of swnple or dilutedsample added to Boo Botdo. fnrrtont$ 0A co A &-AO- L v A. v Fem 197" FM Work ShW SOVON ab Ftiq.140. sivet p ion bftd OWA" FWW ftm comet 17 00 ow Run NO-* ,'p (@77 Day BOO Readings 3m %f AO-Ddr of Sonpis dilutedto C) C) toilutim factor ml with IDIwater ifwwlluted) how S& sh) D.O.1%) Told DA. 71-%-) DwbdmDN6 To Imp's A"NP .0w off 1AYO) 2.qO Conc. ofonww IMIAwon WD bot*L miko added?ABW gotdo. 2. SWnPisSIR* trA,"r.9W4r@4f* ordiiUW nuntwLabgrstwV #VorOkhm swou LobRiq.No. ANWVU 600 RunNO-* 2-0 Ar.~ t rl DayBOD Readinp kAm Ded*w Pow one" CbmiLof bkbl ' lowaft on@ll how D& oil OfSempldeilutetdo mlwithDiwater 101futiofnactor I ifundiluted) rL To%iD.O. Dwbd" ow * .Day 02) D@Pbo" TO ftw4pb ic-0 4DI-D2) Avemp ow DOD No%: 1. Cone.'c.w-wmtroboafnnn%*IMIAoc n 900 bottks. 2. SompieS,ige.i6Mof9ofSolopokrdilutmeqdge addedtoBOD gott-i 0 c@v Fo-m 19766 PWO Oman lok,W4 ewdwo RequestNo. Dom Stw"d SOD Run No. Anal Day SOD Roadlr*s 1-1130 lonowdedDNtA'd*-RWaoww oo"lmoe. cko. iall 0.0. (A2) 0 1).0D.OOGIOM IAI-A2) AVWOP D-0- Depletion X2) o,5 SeededDUution.Wow oknk (oplion 00"10No. lidd0.0. 4cil F.Sm t0.0. (C2) D.O.Depwim ICI - C2) 0,575- c),nq Avwap D.O. D@O&Uon tej 'C2) -Seed ConI trall I So"le No. am*" give INMW 0.0. 1 pr@t D.O. (821 C).O. Depletion 7,6 Glutarn"i,cttKW214 BattleNO. S*nW6 slz* INNW DA. (Dil 3,0 5.0 '95 Pr@nt D1 .O. (02 6 potswum Hydrogen Phthels" Sftndm4 (optional) Battle No. SWN* $in 0.0. (Oil Fmant 0.0. (D2) my Total D.O. Depletion Dwe Depleflon To Standard BOD so (01 -D2) 4?-C' 1(7 , f,C?T 2-13 Tatm D.O. DW"on D@pWion Due to Standard Avwsp Day Day SOD @OOD Fotm 19755 PWO -tal Shlo)t-BL=ks. 3m .Rjequ*sNto. $odd Type 4b oo&Wao Doit*f$to neentrotwn 7/,;7 ISODRunNo. #Maly" 7 DaySOD Readings Date Nonme" Dgutio-nWeew" SoldM@e. bd" D.O. (All ppamt0.0. Mal DA.Dapbdon (Al -A21 AvereDp.O. DepWien gp',t'/o 71 oo q:) (),7,5 .57c) 0 -(OC) S@WW Dlution-Wow Bk" S"d Controll h*M DA). lcl) no 7.-5' Fromm DA). IC2) 1*71 Of I 71 YO 0.0. Dopieden ICI -c2) 0160'. 0, 6E; Averep D.O. Deoction (al -a2) 00"WNo. gsmpban WAM DM. (all PMM DA. L3- td 60 2jO Glucos-eOlutwniArc.idStomlwd BottleNO. Sair@$-iAn DA. IDII z 2() t7 _i/,5,1;7 h@- D.O. 021 Totm D.O. Dapl*tion om TO sumdwd D.O. O"ftdon /.00 1.50 Awwoo SOD -. a" i 25 95- q5 4 - c,;*o le 4:9, so Potosskum Hydropn ftdwk% tandwd topdww) F'B-ottle OW" DA. N-o. swnpk size IDII h@ t D.O. ID2) Tmd D.O. Dspl*Von Due Day A-sp Depledon To @to Wo-d ---law (01 D2) F o-, pWo ohm-BLVJK, o Requat No. 901)Run No.0 2-0 <30 i 7- - Day BOD Readings Date DNvdon-wsw"- bd" DA Pi DAL tA2$ DA. Dqftdoe (Al -Aal .Gem. smw Devi& -wow mw* wpowl swab Nil% WAND& fell P"mM D.O. IC2) se"wa@ el '50 hwm 0.0. fall 905L-1 D.O. D@Pkoon OCI - C21 2,W 2,0.0 2,2-0 hma" 0.0. zo .2.50 Avemp D.O. Copkition (A, - A2) 55 Avwop 0.0. DopkM-. el E2) 2.13 D.& Oop'l' 5.90 GIUWW -OkdW*W OAM bm"W-.. fo 3,0 0 7,0 H"k"oo 1",Iiomo. sampleow qo sio@W (Rpm bMd DAL all /0 > ft@- D.O. (D21 T*W D.O. Dolmi" IDI -D2) 4-go 6,50 To Sbwjftd Totd 0.0. D@Piolim 401 -D2$ ompkrwm ow To 91mulmd A"mp MD -----.ftv MD ow A"-p Day Fort,,197SS FM 10620-0-FWO SAMPLE DESCRIPTION ENVIRONMENTAL File: Page No. ENGR. LAS - WORK SHEET Date: Analyst: Hrs.: F,l 2 C/ Fc- L- q6,q7 cA'@ F,o 297, oloo ff30 0 Z?9. ir 3CO -3oo) 3701-000olk c --7San "Q 4n -0- Y300) @ell00 q,9 c 300 32- /30 Z3 @l-32.<Z 2. Ec? l@ lot 9570 K-65 - o q9 C-7-IL/220 5'/30 0 Reviewed by: ro4m lo,20-,&-Pwo SAMPLE DESCRIPTION ENVIRONMENTAL File: Page No. ENGR. LAB - WORK SHEET Date: Analyst: Hrs.: F L - t-6f4 7 .300 @/:300 @v 3 3 00 7.w 57 z6y3O,,, 32-49 2-0 32-1 300 .0noc) 64KC@ s:2-0 0, 5 7 14 /300)@ en . .17 J92/q ei., 952-0 'go760 Reviewed by: FO@m 1062*7*'Pwo SAMPLE DESCRtF!TION6' ENVIRONMENTAL File-. Page No. ENGR. LAB - WORK SHEET - Date: Analyst: Hrs.: 310 2. 1 510 50 26-11 Fc 71 rs v I '* C7- V q 7.* Al. alo C12 (2 ;o",300 12-3 @acxp 40 rlt 'CD1300 c /Soo /O(iil@az ?/3',Co @ic4n @@z /20000 2. (@lC 29 /3w 7/300- @z 86viewed by-.