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BIODEGRADATION TEST SUBSTANCE Identity: [2-(N-Ethylperfluorooctanesulfonamido) ethyl acrylate; may also be referred to as B1228, D-1, EtFOSEA, or FX-13. (2-Propenoic acid, 2[ethyl[heptadecafluorooctyl)sulfonyl]amino]ethyl ester, CAS # 423-825) Remarks: Material is an amber solid. Sample purity not recorded. 3M lot number 13. METHOD Method: Not noted. Type: Aerobic GLP: No Year completed: 1984 Test solution preparation: Sample weighed onto a cover glass, dissolved in acetone and washed into a bottle with acetone. Bottle coated with acetone solution. Acetone was then purged from the bottle with nitrogen. Contact time: 20 days Inoculum: Not noted RESULTS Test substance: 5-day BOD: 10-day BOD: 20-day BOD: COD: Not measurable 18,990 mg/kg 23,000mg/kg 240,000 mg/kg Reference substance: The glucose-glutamic acid standard achieved a BOD of 201 mg/L in 5-days, which is within the recommended range for the Standard Methods BOD test method. CONCLUSIONS This testing indicated that the test substance is not capable of readily biodegrading in aerobic environments. DATA QUALITY 0 0 0 4 9A: Reliability: Klimisch ranking 3. This study, while well conducted using the methodology acceptable at the time, lacks analytical data for determination of the sample purity. Testing was also done well above the solubility limit of the test substance with the use of acetone as a solubilizing agent. REFERENCES This study was conducted by the 3M Company, Environmental Laboratory, Lab Request number B1228, 4/26/84 OTHER Submitter: 3M Company, Environmental Laboratory, P.O. Box 33331, St. Paul, Minnesota, 55133 Last changed: 5/22/00 000495 Epvironmantal Laboratory "B O D Work Shet - Blanks, Controls, and Standards L - o D Lab Request No. | Analyst y' Saad T yp s ft Source sA /* Vo, 21?, 3 l? P Date Started BOD Run No. I ----- :=. V -6 - / ______ Seed Concentration Analytt ___________________________ % Y' l*/ C. D a y B O D R e ad in g s Date Bottle No. ---------------------------------- 0------------- Initial D.O. (At) Present D.O. (Aa ) 7f ?o xyo ? .io S .io Z .lO ..... l Q ________ t'V* Seeded Dilution.-W ater Blank (optional) i . a: 111 Botti No. * Initial D.O. (Ct) Present D A (Ca> * f g rV g ... J-SS S-VO , % .0 0 _______ 3Jf. ________ %10 Seed Controls -- r ------------------------- 1Bottle No. Semple Size Initial D.O. IB ,) ' 93 */ ) So \ Vo * /* ' y.po <? / ^ D.O. Depletion (At A j) 6- SO s r>-10 I ________ Q . J L ____________ Average D.O. Depletion (t - 2 I D.O. Depletion ICt -C 2 ) 0 fi 0 HO o - 3o Average D.O. Depletion v (St ' Sg) 0-V2 ---- - -- Present D.O. (B) 7^ ' 5.^ o D.O. Depletion (Bt B j) O. fo / VO 3. Glucose Glutam ic A d d Standard Bottle No. 6"0 5-3 &2 8ample S ix . 3 7- initial D.O. (D tl t io ? Y* t V o _____ Prarnnt D.O. (O2I H bo 3.3 0 Total D.O. Depletion (Dt -D 2 ) a -V o 3 %0 Depletion Due To Standard /<?<? 3 - 3? f - j o _____ JJ y' C - BOD D*v Average ____ 1 -P v C - BOD m _ 2o 3 2o 1 7. ---------^ -- , _... . Bottle No. Semple Size Initial D.O. (D tl 7V - - Form 19760 PWO ?-yp ____g v g 'to Present D.O. (Oa l % .Jo % to Total D.O. Depletion (D, - O j l 0. 30 30 0 - 2^ O**nlWs iiUe nlimBrOile ""V > /* P O / / i'l/. r- ^ -- - .B O D - JA -1.J 000496 Day -a e e -- ^ L a b o ra to ry *Shaat Blanks, i, and Standard A ----------------------- T m w n m r ? Lab Requett No. | t / 2 3ot # 2 3 ? , t f P Anelyet OeteBtertad Seed /ype i f Source " Seed Concentration BOD Run No. f j0 $ Y'"A d "V C- * Day BOD Reading 7 -/* - o ' Bottle No. ---------------------------------- -- ------------ Initial 0 .0. <At l 79 1T-o 1. 10________, g. i d 9 -Ho MO Seeded Dilution Water Blank (optional) PSVW- *N_i l InW(aClD,lA. 7-2 vi If V .io `i - i o 1.H Seed Contrla ! BettleNe. lnnpli <? 2 Hi 2o Vo Prtant 0 .0 . (Aa ) 7 ?o 7-fo 9o PretentOX). (Cjl ? . 2T 7-Y r ?. T 0 Initial DA. 1 y.po 9 /S' 0 .0 . Depletion (Af - A j ) Average D.O. Depletion o. f O l* 1 * * 2> kf!O f ______ (2 . ^ -- __________ ______________ DjO(C.D,e-pClej)tion o-fo o s S' 0 >C>O ADveerapgleetioDnA. (Ct-Cal E"7 Nennt DA. (Sa> 7 30 L j . a 3- DA. Depletion (Bt Bj) / r 2. c o 3.9 a Glucoae Glutam lo AoM Standard Boni*No. InitiaIDlD!)A. PrieIDnt,)DA. So y - y ? S ?-i* & 2 _ J : ____ i i o H 3 (? 2 ?D Potauium Hydrogen Phthalat* Standard (optional) BottleNo. StMptoSiM Initiatl)DA. Note(Dnt,)D.O. TD(oDet-ap,lleDDtio.a0nl. 7.1 H lo 1-1o TD(oDetpa,lel.0Dtio.3Onl. Form 19756 FWO 000497 DTeoplSettaionndaDrude -..*3 2..3 0 1B0OO * A/vtfNQB-Dev O BOD 2 111 T i l 2 |z tir-/ s>ao DTeopSlettaionndaDrdu* BOODay y AvBeOraOge-Day Asntal Laboratory York Shaat Blanks, >ols, and Standards -------------------------- u w y r v m Lab Request No. | f t j Q l d t Analyst -- v ---------------------------- 10&P |Data Started v-6 -vy BOD Run No. | XO Saad Type a Source Seed Coneantratlon Analyst l ,, ay. -- C Day BOD Readings OBtB y -z c -w -- ---------v---- BottleNe. InitiIaAlt0l.0. Prew(Aiatt>OX). 0.0(A.DteAplaet)ion ADveerpalgeetioDn.O. . 71 T-o ___ _ Sid 77-- Si of 7- ro 7 o. %0 j 0*7 __ Q.-10______ Seeded Dilution ` Water Blank (optional) 1 Bottle No. _____ ^ ...... - Saad Contrail Initial D A (Ctl S', 1/ * tf-y o 1 - 1 ______: Ptewnt 0 A . (C jl 0.0. Depletion (C, -Ca> 1-1 0%*> o -M Average D A . Depletion (C fC a) [>?3 I Bottle No. inhiai D A . It ,) Prew ntDA. a D A . Depletion IB , Ba) <? ? Qo f./e . V<? * 0 _______ ? ___ ___________ G Iucom Glutam ic Acid Standard 1 Bottle No. |mip|g SfaM Initial DA. <0i) Pre(wDnat)DA. T 'o *3 02 3 1 HP. 5 -1 i . ? . ? ..... t t -H o ' l>Ve Potassium Hydrogen Phthalata Standard (optional) ( ' / o < o SO TDoetaplleDtio.On. (D<| 0^) 3. Jo H *to C .fo Depletion Due To Standard 2>ld 3-a 8 y. 2- 3 Too 3 ?cf - - .... - i %O >Dav 'BOD A vw i|i O'B2O<yD -Dev 33?i 23-2. 7 237- f 237^/ J Bottle No. Sample Site Initial D A . (D ,) Prevent D A . (03) Total D A . Depletion (D, -D a) Depletion Due - r = r To Standard BOD Average Dev BOD Form 1 9 7 M PWO . / /ronmental Laboratory JD Work Sheet - Samples Lab Req. No. | Analyst /5 ) 3 3 8 Sampla Oaacriptlon /3 ; a a t-i Initial Dilution Initial Dilution Factor Data Startad BO D Run N o .^ $ / ~/-y / ^ Analyst - D ay B O D Readings Data -- _____________________________________ f * - n ( L - 3 i- r f) F/*> - y - j / f of Sample diluted to A / /3 ml with Dl water / (Dilution factor - 1 if undiluted) Bottle No. Cone, of Semple1 Semple Site* -In itial 0 .0 . <D,I Praeent 0 .0 . (D2 ) 7 '7 a3 ?3 ll.o l 7 _7 V < 1 33 .2 7 5 5 A O .ooff^ e .o io , Mf % YO 0 . 3 c V0 . 3 7 f g O < o % i 7j t yt ~ i xi ,d % .0o .s f t / ?o Total D.O. Depletion (O , D2 ) O -H i .% i 0 - 1 3 ?>Q o ,*0 <>f Depletion Due To 8ample 7 " . D. v BOO o 3> j-n o.H K 1. %% 0-38 23 Cm *) ( y y 35"0 ) C (p 1 3 j C i Vi io ) C iv e t) ai* ^earaga Day BOO _- Note: 1. Cone. Concentration of sample (ml/l oi<$ng/J^?i BOD bottles. 2. Sample Size ml o/g of sample or diluted sample added to BOD Bottle. Com m anta CoQ: a v W y M j J ^" -j^L__h i___ M t z U ... F o r m 1 9 7 5 6 PWO f/J - d -rfC y i ? 000499 ~ 7? $ tai Laboratory brk Sheet * Sampits _____ 3M LabReq.N o. Analyit ft J %Q & Sam ple O aacrlptlpn H i 5 3 '/ Initial Dilution Initial Dilution Faetor Date 8trt<l BOO Run No. /o Anelyat Day BOD Readings |OMa ;_________________ 9 - / * ~ t y / V - / 3 C L -a s -ii) f/* > - V 3 /9 of Sample diluted to M / 3 __________________ ml with Dl water (Dilution factor 1 if undiluted) Bottle No. Cone, of empie1 O-o if ' i ,7 ?3 taomop*le Initial 0 .0 . (O il Praaent 0 .0 . (0 3) O.OOffj T v T O.ctoVl y/< ? 0 . oa;u. O.P3,,?fo r - y <2.^.1t?VM r o 'ro jdT y r * 7 - J>` 0 S'* 7 * (p-l&o 5-5o 7<' <0'fO Total 0 .0 . Depletion (0 1 D j) 0 HS' 1J0 1. C 0 i*! j .00 .i-i Depletion Due To Sample ' 0 .O n -B O O 0 32T J,T 3 1 b3 2 /3 D' V 3 > 6r fa G ift") ( 1}&>') n><no C!7O r g ? y 3?oo 1Aworape 0 -Oaw _B O D 1 ; Note: 1. Cong, Concentration of sample im l/l or mg/l) in 80D bottles. 2. Sample Size ml or g of sample or diluted sample added to BOD Bottle. IComments CoP- f r j ! t * * oV^>__- c / > s i L . J / a j. -f~?Jf~<?<// . atc*7ps* -- -- . /7e.t/pr^t ih l(*-vj L0/t 7.1} * 7i Form 19786 PWO 000500 X ta l Laboratory . JfV . Shaat Samplas 3I\ ^b R e q .N o -l Analyst Data Started BOD Run N o .| $ ^ %O Analyst * Day BOO Readings Data JtW - r f Sample Oaaerlptidn !3 ) 3 3 * - / Initial Dilution f * - n ( b n - / * ) f /*> - s o y 9 of Sample diluted to y j /3 ml with 01 water Initial Dilution Factor (Dilution factor * t if undiluted) Botila No. O.oost. -?.(o \-ir?-0 (iJ7 \` Q0.OIoj/. $%HV.1*io300 FH'<{.0.7HH-o5oo.. 2-? 3 Cone, of empie1 * ampia ln2 Initial 0 .0 . ID ,) Present D .0 .103 ~ uT L / ' 0.0 }?f. a. <7 Total 0 .0 . Depletion (0 , a) 2 '5 Ho Oaplation Oua *2 -Day 0H2 (WOo)To Sample C' BOO c " B90 ?I3160,.*0.3-?*?f2t?) ((2231312)00o0)) _ >1C ?3 0 Cj0)p' 2 3 ovo^dAc ,. Not: ' 1. 2. Con. Concentration of sample (m l/l or mg/l) in BOO bottles. Sfm plt Size - ml or g of sample or diluted sample added to BOO Bottle. 000501
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CUNY - The Graduate CenterColumbia University Mailman School of Public Health - Sociomedical Sciences