Document 93eL28opQgzV87wr84BpmXdrV
CG 36
CODE- RT-444-D
'-27-1982 F2H10
( DATE )
( LOT )
PKG
ESTIMATED WGT
LBS <
PREPARATION NOTES i _______
D. V. 902, 904
PROCESSES ( >RT-444-D(A) COMTYP JOB NAME: TYPED BY: KLW
APPROVED BY EWK 02/05/82 36RT444DMA
STAND ARD HRS *
TIME
EQUIP MENT
MISC i
umE: DUQL CARMINE
FIRJT BATCH FOLLOWING WATCHUNGS, CLEAN SS SPARKLER 6 PRECOAT SPARKLER WITH
"1 5$ FILTER AID. RUN 15" WATER IN V-904 & PUMP INTO V-901 THRU DISTRIBUTOR. IF WATER DOES NOT COME OUT OF ALL DISTRIBUTOR HOLES WITH FULL FORCE, NOTIFY SUPERVISOR.
RECORD: _.<5__BATCHES SINCE SPARKLER LAST ! CLEANED. AFTER 4 BATCHES, CLEAN, DRESS l^SPARKLER & PRECOAT WITH 154= FILTER AID. 4T| OBTAIN 4-AMINOT0LUENE-3-SULF0NIC ACID J^TC/R S I 8 . Z \ OBTAIN 3-HYDRQXY-2-NAPHTH0IC ACID FOR S35
NON-BLEEDING
1 USE I LBS
N-CODE ACCT L3S
| | I 15 |
| i I
1
77'?--A I
I
i |. 777-A | 549-C 1
I
RUN 29* (59? G) WATER INTO V-932
H SODIUM HYDROXIDE IN V-?26 & RUN IN
M '"f
t~f V V
IJ
RN ON AGITATOR & STEAM
E .HEATING, ADD DRESINATE X IN S-9 MIN
460
EAT TO 180-185*F RCD: TEMF\
*F
R 30 MIN. OR LONGER TO DISSOLVE
RECORD: PH_^U3__<11 .8-12.0)
IF PH BELOW 11.3, ADJ. TO PH 11.8 OR
ABOVE FOR S6Q RCD: pH_______
ASSUME 502
7-D 530--A
7-D
1 58
I I 460 I' I I I I______
IFY PROCESSING BEFORE ROPING OFF AREA
BENEATH V-922. THEN ROPE IT OFF.
fN 64* (1318 G) WATER INTO V-922
WEjGH SODIUM HYDROXIDE,. IN V-926 6 RUN IN
iy
,
%
RN ON AGITATOR 6 sfEAM~'r"HiAT"*TO~35-90F
DUMP IN.4--AMINOTOLUENE-3-SULFONIC ACID
FROM S4
, LOT " /:/,
4=1002 f:
^,2
MAY 281982
7-D
133
' #
COHTYP JOB NAME- * 36RT444PMA
PAGE 2
EQUIP MENT
GE 02 OF 04 CG 36 CODE RT-444-D < A)
922 4
CON'T
STIR* 15 MIN & RECORD: BY. rz:.\msr b e +) PAPER TURNS RED.
IF NECESSARY, ADD SODIUM HYDROXIDE TO + BY
RD: BY____ ___ _
ASSUME 50%
CHECK FOR COMPLETE SOLUTION RECORD:
J^ffESULTS___ __________
IN ACTIVATED CARBON
IN FILTER AID
34-*p5TIR 15 MIN.
2%r RECORD: SPARKLER PRESSURE_.C2____ PSI
I W,. NOT ZERO, NOTIFY SUPERVISOR
S^r^IRCULATE IS MIN OR LONGER AT 85-90*F THRU
I SPARKLER UNTIL SOL'N IS CLEAR. MAINTAIN
I AT 85-90*F FOR^S-28. RECORD: START_5|j?_
I TOTALS I N^/<___ CLARITY__J~_
DATE PRINTED: 2/05/82
USE N-CODE I ACCT LBS I LBS
7-0
22 1 1 3-B 2 777-A
\
27 20
901 V (95 G) WATER INTO V-901 5 WHEN S26 COMPLETE, PUMP IN V-922 THRU SPARKLER. MAINttIN>~922.. AT 85~9*F RECORD: START_7$4__ TOTAL MIN,,YiO__,,
MISC 6
902 7
SODIUM NITRITE.IN PT FOR 57 .
MEASURE teSSL UNITS IN V-928 FOR S59
'* -M4fDR0CHL0RIC ACID M,,X-.____
5n I MEASURE / ,_ UNITS IN.V-927 ACETIC ACID
I FOR.S80
M__/______
.422! 92. i
1I
JVlTXpm 20* <503 G> WATER INTO V-902. 33^fjlEreH SODIUM HYDROXIDE IN V-926, i RUN IN
m_x ___ *4 J>?ORN ON AGITATOR & STEAM 6 HEAT TO 95-100*F *35Pn DUMP IN 3-HYDR0XY-2"NAPHTH0IC ACID FROM S3
I ^^fcQT S.t2^.
725-A 28-D 30~D
I
( !
1 |
I
216 268 200
7-D 82-C
378
SS2~
STIR 30 MIN- OR LONGER TO DISSOLVE FOR S67.
922 N S28 COMFLETE, SHUT OFF SPARKLER PUMP 8 INSERT FOOT PLUG. N IN I' (206 G) WATER RN ON AGITATOR 6 HEAT TO 85=f0*F.
4^1 mCORD: SPARKLER PRESSURE ,,_i___PSI. IF T ZERO NOTIFY SUPERVISOR.
IRCULATE 15 MIN OR LONGER AT 85-90*F THRU
SPARKLER UNTIL SOL'N IS CLEAR. RECORD: CLAR ITY_.fi>... THEN SHUT OFF STEAM.
.I
if
DUP050047791
JOB NAME 36RT444DMA
PAGE 3
DATE PRINTED: 2/05/82
ffi fp"
me n t
E 03 OF 04 CG 36 CODE RT-444-D
~ USE (A) LBS
H~coii>g
ac c t
LBS
90.1 WHEN S41 COMPLETE, PUMP V-922 THRU SPARKLER 9 i INTO V-901.
222 WHEN S43 COMPLETE, SHUT OFF SPARKLER PUMP
10 i^r'lNSERT FOOT PLUG *
451 RU^ IN 5'" (103 G) WATER & HEAT TO 85-90F
EN SHUT OFF STEAM.
^
RECORD: SPARKLER PRESSURE
PSI. IF
' \jm ZERO NOTIFY SUPERVISOR
CIRCULATE 15 MIN OR LONGER THRU SPARKLER
I UNTIL SOL1N IS CLE&R,
43 I RECORD: CLARITY,
901 I4^T WHEN^S47 COMPLETE, PUMP V-922 THRU SPARKLER 11 i L^WTO V-901 . \5tr \ WHEN V-922 EMPTY, BLOW OUT SPARKLER INTO I 1 V-901.
904 12* (322 G) WATER INTO V-904
12
ON AGITATOR & ADD CALCIUM CHLORIDE
> 20-A x
TO 70-80*F.
7*d |
] Too
STIR 15-20 MIN TO DISSOLVE FOR S77.
901 13
16*
UST TO~iiWfc*F WITH ICE. RN ON STACK EJECTOR. RJJ*KlN SODIUM NITRITE (N-725-A) FROM S29 N 5-10 MIN & RINSE IN PT. ADJUST TO 74* (6480 G) AT 42"44*F WITH ATER & ICE. RUW-TN V-928 HYDROCHLORIC ACID FROM S30
IMMEDIATELY A^J/TO BjjljgssaX*? RECf^D:
TCCURACY HT.3.__k F ' r e c _3JL..k f
RECORD: CR_Tr^>) CONGO RED PAPER TURNS
BLUE
KLjfetT(+) KI PAPER TURNS BLUE
NOTE 'flF~R+, KI- ADD 20$ * AS IS*.
INC^gftENTS SODIUM'NITRITE ASSUME 33%
(20 IF CR-, KI- ADD 20$ *AS IS".
INCREMENT HYDROCHLORIC ACID
- ASSUME 32%
iUfT REPEAT ABOVE AS NECESSARY TO
CR, +KI RECORD: CR____.,,( + >;
KI.:ri;r'-.(+) H SULFAMIC ACID IN PLASTIC BUCKET &
'<INSE IN
STIR 10 MIN & RECORD KI_*5T,, (MUST BE -)
PAPER STAYS WHITE.
IFNECESSARY ADJ TO -KI WITH SULFAMIC ACID
CORD: KI________ (-)
OFF STACK EJECTOR.
ADJ TO 85* (7560 G) AT il)arH*F WITH WATER
& ic e.
#0X3301 TP 1
1
^X3301 t I
_____ I i
1
_____ I
!
i
l l
25 |
1 I 1
_____ I
1 I
____ _ I
57-A 57-A
725-A 28-0 395-D
395-D 57-A
DUP050047792
COM-TYP JOB NAME * 36RT444DMA
PAGE 4
DATE PRINTED; 2/05/82
EQUIP MENT
USE I PAGE 04 OP 04 CG 36 CODE RT-444-D (A) LBS
H-CUpE
ACCT LBS
901 ItS? | COUPLE V-902 THRU UNDERSURFACE DISTRIBUTOR
13 I I INTO V-901 IN 30-35 MIN. MAINTAIN 42-50*F
COM 1T I I OPEN-VALVE.*.______TURNS RECORD :
_
I TOTAL MINjsClCt, TEMPjfc.CLF
I8"T WHEN S67 COUPLING COMPLETE, IMMEDIATELY
I STEAM EJECT IN V-932 SODIUM DRESINATE OL1N FROM SI 3 IN 12-17 MIN. -
STIR 10 MIN & RECORD:' PHjfifeJKt12.0-12.4-}
DIAZO_s S__(.->
BASE_4frrr_<+> r IF NECESSARY ADJ TO PH 12.0-12.4
RECORDj*-PH_____
ASSUME 50%
IAZO ____ <-)
ASSUME 32%
BASE_____<+>
IF DIAZO TEST +, STIR ADDITIONAL 15 MIN
RECORD: DIAZO<-) BASE _____ < + >
IF DIAZO TEST STILL +, TREAT AS FOLLOWS:
CD ADD +/- 20 GAL WATER TO METAL DRUM <2) ADD 144: "AS IS" SODIUM HYDROXIDE
ASSUME 50%
<3) ADD 104 "AS IS* 3-HYDR0XY-2-NAPHTH0IC
ACID
<4> STIR 10 MIN TO DISSOLVE
C5>P'0UR INTO V-901 & STIR 5 MIN
I
> RECORD: DIAZO___ BASE____________ __<+>
I REPEAT S72 AS NECESSARY TO - DIAZO; + BASE
I RECORD: DIAZO____ SODIUM HYDROXIDE
1 ASSUME 50%
I BASE__ _< + > 3-HYDR0XY-2-NAPHTH0IC'ACID
STIR 60 MIN
RECORD:
MT\ AFTER S74 STIR RCD: TEMP_4R_*F <60-65*F)
^T^KHEAT TO 90~94*F " PUMP IN V-904 CALCIUM CHLORIDE SOL'N FROM
TEP 54 THRU UNDERSURFACE DISTRIBUTOR AFAP
L?^WTIR 10 MIN.
J^Cl RECORD: PH/&13L<1 1.5-12.2)
j RUN IN V-927 ACETIC ACID FROM S3T & STIR
* ' "O^MIN CORD : PH_&if_ C 9.3-9.7)
I IF NECESSARY, ADJ TO PH 9.3-9.7 RECORD:
I PH_^UL NOTE: CD IF PH ABOVE 9.7 ADD
I ACETIC ACID IN SMALL AMOUNTS ASSUME 70% I I (5 TO 24 "AS IS* INCREMENTS) BECAUSE THERE
I j. IS A SUDDEN DROP IN PH BELOW 10.5. C2> IF
I I PH BELOW 9.3, ADD 64 "AS IS" INCREMENTS I | StJJDIUM HYDROXIDETO A PLASTIC ASSUME 50%
JJk
I J^gUCKET * DILUTE WITH WATER.
L8ST| HEAT TO 183~187*F AFAP
RECORD: ACCURACY
1
F, RECjSjffc._*F
, .,
7I&M& MIN AT 183-1 S7*FT RCD; START^*MAj7?JI
HEN *S84 STIR COMPLETE, FLOOD TO 140*F
LOWER.
[ I SHUT OFF AGITATOR RT FIN
OR
* I
___
7-D 28--D
7-D | I
82-C 1,
7~D |, 82-C |,
30-D I____ I
7-D | _j__
DUP050047793