Document 93eDYQYnqL0YxKD2o2675VL66

. AR R26 _ 0690 ACUTE TOXICITY TO FISH TEST SUBSTANCE Identity: A mixture containing perfluorooctanesulfonate, which may also be referred to as PFOS, FC-95, or as a component of FC-201. (1Octanesulfonic acid, perfluoroalky! sulfonate salts (5) + (5140P)) (CAS # 2795-39-3) Remarks: The 3M production lot numberwas Lot 1. The test sample is. FC-201. Its purity was not sufficiently characterized, though current information indicates it is a mixtureof 6% PFOS, 36% diethylene glycol butyl ether, 36.44% water, 12% Sultone foamer, 9% sodium octyl sulfate, 0.5% sodium lauryl sulfate, and 0.06% benzotriazole. The following summary applies to a mixture with incompletely characterized concentrations ofimpurities. Data may not accurately reflect the toxicityof the fluorochemical componentof the test`. sample. ME0 THOD: 00000 Method: Not given. Type: Static acute GLP: No Year completed: 1975 Species: Pimephales promelas Supplier: Not given. Analytical monitoring: Temperature, pH, and DO Exposure period: 96-hours `Statistical methods: LCs values calculated using graphic interpolation, recalculated using probit analysis. Test fish age: Juveniles Length and weight: Average length = 2in. Loading: Not given. Average weight = 1.5 g (wet) Pretreatment: None. Test conditions: Dilution water: Carbon filtered St. Paul citywater, St. Paul, MN Dilution water chemistry: Not given. Lighting: Not given. Stock and test solution preparation: Not given. Concentrations dosing rate: Once Stability of the test chemical solutions: Not noted Exposure vessels: Not given. Number of replicates: 1 Numberoffish per replicate: Not given. Numberof concentrations: five plus a blank control Water chemistry during the study: 000167 pH range (0-96 hours): 7.0~7.0 (control exposure) 6.86.9 (750 mg/L exposure)* Temperature range (0-86 hours): Dissol6v9ed-7o0xygFen range (0-96 hours): 4.7 - 5.6 mg/L (control exposure) 4.0~ 5.0 mg/L (750 mg/L exposure)* +be7c5a0usmeg/tLh.e(hsiegchoensdt hciognhceesnttrcaotnicoenntursaetdiorne)suelxtpeodsiunrteotvaallmuoerstaulsiteydby 72 hours. RESULTS Nominal Element concentrations: values: 96-hour BK control, LC50 = 526 1(0309,7 2--506,315)00m,gi75L0, and 1,000 mg/L Element values based on nominal concentrations. Remarks: Testing was conducted on a mixture as described inthe Test tShuebsfltuaonrcoechReemmicaarlkpsrfoipeolrd.tiTonhealvoanle.ues reported apply to that mixture and not CONCLUSIONS `5T2h6e mtegs/tLswuibtshtaan9ce5%96c-ohnofuirdLeCnscoe fionrtefravtalhoefad3m97intnoo6w31wamsg/dL.etermined to be SPuaublm,itMtienrn:esot3aM, C5o5m1p3a3ny, Environmental Laboratory, P.O. Box 33331, St. DATA QUALITY `ReTlhieabsialimtpy:leKpiumriitsycwharsannkoitngpr3o.peTrelsytcihnagrlaacctkesrirzeecdoradndoftmheetshtouddoylloagcyksused. analytical confirmation of the amountoffluorochemical proportion in the solution. REFERENCES TPahuel,teMsNt ,waLsabcoRnedquucetsetd nbuymtbheer32M56C3o,m1p9a7n5.y, Environmental Laboratory, St. e TEEe R eecim-------------------- Last changed: 6/26/00 000168 a. ---- "roRM 10620-PWO : te ng Wasps eV-- VInSy=> ] . TO: ENVIRONMENRTEAQLUEENSGTIFNOERERLIANBGOLRAATBOORRYAWTOORRKY-- LabRequest No.J563 BUILDING 5361 rear Coron ST -- CHSaeomrrlleeoS2R aDnm0nep0erl0eipFioEa orO nOEp OIwO RNpeEgauSeeTiotmmee:e FTA=u6J S2g WnLS,r "ie|he le-eom-- HmoeoencSN xi o- uooAmemaA]gBofi 2 sT ie-5 zo0 dI -- \-- S ----Fe-z25Te Calcium Hardness, mg/lasCaCO3 |I I | 1 1 TP"Alkalinity, mg/l as CaCO3 "M" Alkalinity, mg/l as CaCO3 r TTT TT 17 oH TT TT Rulfate, mgfT las$0s T I Tr] Chloride, mg/l as CI ica, mg/l as 5102 TTT rr TT 117 TT Tuoride, mg/l as OrthoPhosphate, mg/1 asP_ TTT rrrrr `Total Phosphate, mg/l asP_ o Total Chromium, mg/l as Cr_ I TTT rT TT 7 Fiex_ Chromium, mg/l as r Total Cyanide, mg/l as CN. MTTTT T T 17 TTT 71117 Ferrocyanide, mg/l as CN Tron, mg/l as Fe I TT TTT Wanganese, mg/l as Min Surfactant, mg/l as LAS T I r T r r T r r 11 Phenolmgh BOD, mg/l 11 11 TT TTT COD, mg/l (Short, Long, Dilute] TotalSuspendedSolids, mg rrr 11 TTT rT Volatile Suspended Solids, mg/l Turbidity, mg/l Silica. I TTT 17 TTTTT Total Solids, mg Total Volatile Solids, mg/l TTT T r rrr Conductivity, mhos Total Bacteria, No./100 mi TTT Tr TTT T r Total Coliform, No./100 mI Fecal Coliform, No./100 ml rT TTT TTT T T Fecal Streptococcus, No./100 ml Ammonia Nitrogen, mg/l as N rrTTT TTr T r Kiedidahi Nitrogen, mg/l as N TTTTTT --1 Oil and Grease, mg A TT TT ----1] ESE To, ZY Le [S000 [000 | OOCPY[R50PaN is o= TT TT rT tenemos ron oh iT eIT on Gia eTrTeTTTTTeTsTTr0rr0m0a1n6e9 " : . ws i . Vg "ioior ENVIRONMENTAL ENGINEERINGLABORATORYee cr AQUATIC TOXICITY WORK Srer } . 0 3 ; Faerie ty: & Type Test___96 Hours - Sintec Material Tested F(-2of re " Test Organisa_Fathead Minnow Avs. Veta 50 Si%e_2 Tuches 8 =sw] Toler] a ledas] 20"legad wees _100 7052f]oo lojas] fed encror| joo 7] 54Ho edsalin Lele] bo [ula i Date Started -2-75 Date Completed. L={-75. Tine Started Room Ploteed 10s GATOOM Dilution MWaaterrCCaarrbbonFFiillteresd - St. Paauull CityCity MatMater Ol AnSoe.oe 555 2576 i 5I1R; 20+hes 0.0 4a+hs Tans 0.0 ` sens 397 D.0 v7 D0 Go__nSureviv.al pH ppm Survival pH ppm Survival pH pm': SurvivalpH sppa 2% Jn Jzelsa] 100 [zelsol lo |zolodo[z7la]s. solr o [70]50] (00 arial70jo 4[5 20 elseA am | 50 6050] ? 20 leslas| 0 leslao] 0 ||1 ~ CAovmemmesnptes:Temperare Of] 70 70 0 Leg, Calculation @ g = comb nEe 3 100C % RLTG Ta L q T HAE noFTi ESm CIe TE a = RE = - (rp hh ed 8 5 ! Lod > 5 : oye ee ge Conair c = . = fu jimplitnyll Bb - . || P Yhi ubn s $ : | Coy RRR 5 ys 10 2 30 40 see 70 80 Teo ioe i -- pms a 0001705" oy So ET ens See CE HE E LT e PEPE EE FRE SEE @o Sie re Re A EE CG Hest Hi Sly E E m EE Ee a ee e tH = E ii id E e a HE e H EiraHe EEE DHE IEE EE FALL La z EEL ERE Ee NG IT TE 8 LB EEE REET EITA aTT Tp aEgle] Ba nie ng Sil Hhesasiest i H ORIa EN HES E EH e aH He EEE Ea Shinn fH PRE ET Re pened piri ea riipi: On Li ierHiHlbie rnoadiyynbn i p FEEERERih En FRE|R:aREiLHRdEELT]Y S BH EsR A H FE e BE e Ep E :Do H HEHE EE HHH he eeeER ie HOHE REI ETT HE HH SH Eig dH fH Hh gEE REi EHH H HE TTC Hires EERE B TI O BEEER RSI mL n FiE piTn Yea 3 pi Thi ih SabT i n iH se Phin e2 mpbie e deePle UTdLER | E SHEEEEREnd SHEER aE . (Lib lindSl Ei [14] Zoufoiom Be `er 000171 ER E es Sa REE TI } RC LE TP EESEEAE a FREY ee Hi Sie we aed aad oe Fok ee FEL FEAUNT FE oh 1a 0a 0 es SRE 1PUR a VRE Tf PBRAERSEBEIEN 3) Ae eskbrhn 1 1 Ea Tenn gy lees eas a Sih ACHEE R A E i5ggeEe a a iG2ini S Es - LETT R hiEThN in EBEers led EEY Fi c ee n aee ir Fe Ge e BP R RC 10 L RE E RE sB dk E MhEeE et a HE Ph CRATERS Cate ee SE Ce 4 PO 4 2 TREE hy CH BESTCOPY AVAILABL . 000172 Te Sate stated; 27.73 fone ' Sa ovoual Hl DBiohssy - wl SoEraN n . - 2. Lek _\ (14 (onCehtute) esl woe. il H * aPe] Soruvat Tod PP Sorviemy Sow aJo | LPer|Hpa [ToEr nl Alc ToL mE oZos om | e o/ ! i 2d / ero of rl ith IL it ) Lt 250 3 tL / 3I Ny 1"] ) 04 _ nl : BE J 8 1 tel | 8 i | SCPeening ess pest Yom a Dead Tue peal al nad ' TIGVIVAY AdOD 1939 SL x+