Document 91RddE8EMaKLkGzmNDL5ny9eV
FILE NAME Brakes BRK
DATE 1997 Jan 29
DOC BRK133
DOCUMENT DESCRIPTION Internal Report Prepared for Law Firm - Friction
Product Fiber Release Studies
Report of Results MVA1810
FRICTION PRODUCT FIBER RELEASE STUDIES
Prepared for Law Offices of Peter G. Angelos 300 East Lombard Street 18th FI
Baltimore MD 21202
Prepared by
James R. Millette Ph.D. MVA Inc.
5500 Oakbrook Parkway Suite 200 Norcross GA 30093
29 January 1997 Preliminary Issued 24 May 1996
D PROJECTS
MVA Inc.
+ Excellence in
Microanalysis
5500 Oakbrook Parkway 200
Norcross GA 30093 770-662-8509 FAX 770-662-8532
www.mvainc.com
Report of Results MVA1810
FRICTION PRODUCT FIBER RELEASE STUDIES
INTRODUCTION
Asbestos fiber was used as a component in some friction products such as brake linings brake disc pads and clutch friction parts Some studies have shown that work performed by mechanics and other individuals have caused asbestos fibers to be released into the air This study was designed to determine if asbestos fibers are released when certain types of activities are performed with friction products
STUDY DESIGN
According to information collected in some instances when a new brake lining was installed it would be ground or sanded with coarse sand paper to scuff down the high spots and bevel the edges With brake discs that had a lot of squealing they might be
treated by chamfering the edges or cutting grooves into the lining with a either file
hacksaw or grinder
This study for possible fiber release involved sanding new brake linings in a controlled area while air samples were collected A second test involved cutting grooves in brake
disc pads with similar controls and air monitoring The grooves were cut with a file and
then in a separate test by a pneumatic hand muffler grinder
Air samples were collected while the cleanup activity of sweeping was performed following the sanding test
STUDY SITE
The study was conducted in a warehouse in Norcross Georgia An asbestos abatement type enclosure was built for the study to isolate the testing from any other source of asbestos and to prevent any fiber release from contaminating the building The containment barriers in the area consisted of two layers of mil polyethylene plastic sheets on a wooden frame and three layers of mil polyethylene plastic on the
floor The containment work area approximately 8 ft high by 8 ft wide by 7 ft high was
completely contained within a larger containment area The study area had a High Efficiency Particulate Absolute HEPA air filtration device AFD which is used to clean the area of particulate including asbestos before and after the activity In the outer area the AFD operated throughout the test to prevent any contamination if there was a fiber
release
PROJECTS
All personnel inside the study area were protected by air purifying respirators and complete head and body coverings The decontamination system consisted of an enclosed changing room outside the testing area and a clean suit room
STUDY PROCEDURES
The study consisted of the collection of air samples before and during the activities with 4 brake shoes and 3 brake disc pads manufactured by Ford
Prior to starting the study three 3 area air samples were collected to determine the background level of asbestos in the air of the study area The sampling cassettes were located on the walls at the breathing zone approximately five feet from the floor During the studies the person doing the activity was fitted with two personal air sampling devices Two area air samples were collected during each activity A sample was also collected outside the containment Samples were collected from the surface of the worker's hand before and after the activities Photographs were taken to document the activity
ANALYTICAL METHODS
Stereomicroscopy was used to examine the friction materials prior to testing Polarized light microscopy PLM was used to determine the type and amount of asbestos in the friction product materials
Personal air samples were analyzed by the standard phase contrast microscopy PCM
Method NIOSH 7400
Although the phase contract microscope enhances the analyst's ability to see fibers over other types of light microscopes the standard procedure does not involve identification steps which specifically determine how many of the fibers counted are actually asbestos PCM also only counts those fibers longer than 5 ...m The samples
were prepared forfurther study by transmission electron microscopy TEM The
samples were prepared and analyzed using a direct preparation and counting procedure This TEM analysis method identifies asbestos fibers on the basis of morphology crystal structure and ray elemental analysis All asbestos fibers longer than 0.5 ...mare counted by TEM so that a total asbestos concentration could be determined Information about those fibers longer than 5 ...mcan also be determined to give an asbestos count equivalent to the PCM data
The hand surface test was examined by scanning electron microscopy with ray analysis
A friability test was performed on the sample of friction material before cutting and on
the residue after the activity The EPA friability test is a field test in which an attempt is made to crumble the containing material ACM by hand If the material produces dust when crumbled by hand it is considered friable
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RESULTS
Stereomicroscopy showed that white fibers were protruding from the surfaces of the friction materials See figures These fibers were tested and found to be chrysotile
asbestos
Polarized light microscopy PLM bulk analysis showed all the friction materials to contain approximately 50 chrysotile asbestos As received the friction materials were not friable However they produced dust when scratched or rubbed The residue materials from sanding filing and grinding were dusty The hand surface sample collected after the worker filed the brake disc pad showed very high levels of asbestos
The PCM results of the air monitoring are summarized in Table 1. The TEM data are presented in Table 2
During sanding which lasted approximately 10 minutes the asbestos fiber level for the person sanding was 2.2 fibers PCM TEM analyses of the airborne fiber
concentration during sanding showed a level of 54 chrysotile asbestos structures per cc
During sweeping of the sanding dust and debris with a broom which lasted approximately 5 minutes the asbestos fiber level for the person sweeping was 2 fibers PCM TEM analyses of the airborne fiber concentration during sweeping showed an average level of 28 chrysotile asbestos structures per cc
During filing grooves with a steel file which lasted approximately 5 minutes the asbestos fiber level for the person filing was 0.3 fibers PCM TEM analyses of the airborne fiber concentration during filing showed a level of about 7 chrysotile asbestos
structures per cc
During the making of grooves in the brake disc pad with a power grinder which lasted approximately 2 minutes the asbestos fiber level for the person grinding was 8 fibers PCM TEM analyses of the airborne fiber concentration during grinding showed a level of 230 chrysotile asbestos structures per cc
CONCLUSIONS
Sanding an containing brake shoe friction product with a coarse sandpaper released high levels of asbestos fibers in the breathing zone of the sander Sweeping the containing dust and debris following sanding can release significant levels of asbestos fibers into the air over 1 cc Filing grooves into a brake disc pad also releases asbestos fibers into the air in the vicinity of the filer but at a lower level than sanding Using a power muffler grinder to cut the grooves in an asbestos containing brake disc pad causes high levels of asbestos to be released High levels of asbestos fibers were found on the hand surface after work with filing the containing brake disc pad
D PROJECTS RP052496
Page 3
TABLE 1
Summary of Average Personal PCM Air Sampling Results for Sanding and Sweeping Filing and Grinding
Activity
PCM
cc
Sanding of the Brake Shoes
2.2
Sweeping of Dust & Debris
1.7
Filing Grooves in Brake Pad
0.3
During Grinding Grooves in Brake Pad
8.5
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TABLE 2
Summary of Personal TEM Air Sampling Results for Sanding and Sweeping Filing and Grinding of
Brake Friction Materials
Activity Background Before Sanding Brake Shoes Sanding of the Brake Shoes Sweeping of Dust & Debris Background Before Filing Brake Pad During Filing Grooves in Brake Pad Background Before Grinding During Grinding Grooves in Brake Pad
TEM
asbestos str BDL 0.003
54 28 0.04 6.7 0.05 230
D PROJECTS RP052496
Page 5
Figure 1. Ford Brake Shoe Used in Study
Figure 2. View of the top of a Ford brake shoe used in the study
PROJECTS
Page 6
Figure 4. Magnified View of Protruding Fibers in Figure 3
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Figure 6. Magnified View of Protruding Fibers in Figure 5
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Page 8
Figure 7. Ford Brake Disc Pad Used in Study
Figure 8. Close View of the side of Ford brake disc pad used in the study
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Page 9
Figure 9. Closer View of the Surface of Brake Pad Protruding Fibers are Visible
Figure 10. Magnified View of Protruding Fibers in Figure 9
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Page 10
Figure 12. Sanding the Edges of a Brake Shoe
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Page 11
Figure 13. Sweeping Brake Shoe Sanding Debris and Dust
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Page 12
Figure 14. Scanning Electron Microscope Image of a Sample taken directly from the Surface of a Hand of the Worker After Filing Fibers are Chrysotile Magnification 350x
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Page 13
MVA1810 Hand sample after filing
600
550
500
450
Si
400
LOUS
LOUS
350
LOUS
0
n
t 300
"
250
200
150 C 100-
50
5
JS
Fe
Anta
Ntesesiecnent
atacs ch
niniatsindanpe
1
2
3
4
5
6
7
8
9
10
Energy keV
Figure 15. ray Spectrum of Chrysotile above and Scanning Electron Microscopy Image of Chrysotile Fibers among other Particles on the Hand Sample shown in Figure 14. Magnification is approximately 1,100 x
D PROJECTS
Page 14
Figure 16. Cutting Grooves in A Brake Pad with a Steel File
D PROJECTS
Page 15
Figure 17. Closer View of Cutting Grooves in A Brake Pad with a Steel File
D PROJECTS
Page 16
Figure 18. Cutting Grooves in A Brake Pad with a Muffler Grinder
D PROJECTS
Page 17
Figure 19. Closer View of Cutting Grooves in A Brake Pad with a Muffler Grinder
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ton Hy
Figure 20. Transmission Electron Microscopy Image of an Airborne Chrysotile Fiber Collected on a Filter During Sanding
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APPENDIX 4.
a PLM Bulk Analysis of Samples
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MVA Inc. 5500 Oakbrook Parkway Suite 200
Norcross Georgia 30093 404 662-8509
PLM ASBESTOS ANALYSIS
MVA 1810 SAMPLE ID # G0922
CLIENT Law Offices of Peter Angelos
CLIENT SAMPLE ID #
Ford SEC GF
Macroscopic Description Tan pads attached to metal plates 2 pieces
ASBESTOS MINERALS
OTHER FIBERS
Chrysotile
Amosite Crocidolite
Anthophyllite Asbestos
Tremolite Asbestos
-50
------~--
Glass Fibers Cellulose
Synthetic Fibers
Other
TOTAL ASBESTOS
-50
PIGMENT %
-50
* PIGMENT IDENTIFIED
Vermiculite
--
Synthetic Foam
---
Gypsum
Other
---
*
Pumice Carbonate
Pigment
----wee ---
---
*
---
COMMENTS
ANALYST Randy Boltin
DATE 05/13/96
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MVA Inc. 5500 Oakbrook Parkway Suite 200
Norcross Georgia 30093 404 662-8509
PLM ASBESTOS ANALYSIS
MVA 1810 SAMPLE ID # G0923
CLIENT Law Offices of Peter Angelos
CLIENT SAMPLE ID #
Ford PRIM RW
Macroscopic Description Tan pads attached to metal plates 2 pieces
ASBESTOS MINERALS
OTHER FIBERS
Chrysotile Amosite
Crocidolite
Anthophyllite Asbestos
Actinolite Asbestos
-50
---------
Glass Fibers Cellulose
Synthetic Fibers
Other
TOTAL ASBESTOS
-50
PIGMENT %
-50
* PIGMENT IDENTIFIED
Vermiculite
--
Synthetic Foam
---
Gypsum
Other
---
*
Pumice Carbonate
Pigment
-------
*
---
COMMENTS
ANALYST Randy Boltin
DATE 05/13/96
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MVA Inc. 5500 Oakbrook Parkway Suite 200
Norcross Georgia 30093 404 662-8509
PLM ASBESTOS ANALYSIS
MVA 1810 SAMPLE ID # G0661
CLIENT Law Offices of Peter Angelos
CLIENT SAMPLE ID #
2001A
Macroscopic Description brown consolidated material adhering to metal plate
ASBESTOS MINERALS
OTHER FIBERS
Chrysotile
Amosite Crocidolite
Anthophyllite Asbestos
Tremolite Asbestos
---------
Glass Fibers
Cellulose
Synthetic Fibers
Other
TOTAL ASBESTOS
-50
PIGMENT %
-50
* PIGMENT IDENTIFIED
Vermiculite
--
Synthetic Foam
+>
Gypsum
Other
---
*
Pumice Carbonate
Pigment
--1 -----
---
*
---
COMMENTS Ford disc brake pads
ANALYST Randy Boltin
DATE 05/13/96
D PROJECTS RP052496
Page 23
MVA Inc. 5500 Oakbrook Parkway Suite 200
Norcross Georgia 30093 404 662-8509
PLM ASBESTOS ANALYSIS
MVA 1810
CLIENT Law Offices of Peter Angelos
SAMPLE ID # G0965
CLIENT SAMPLE ID # Debris & Dust After Sanding
Macroscopic Description Brown powder
ASBESTOS MINERALS
OTHER FIBERS
Chrysotile Amosite
Crocidolite Anthophyllite Asbestos
Actinolite Asbestos
-50
-~------
Glass Fibers Cellulose
Synthetic Fibers
Hair
TOTAL ASBESTOS
-50
PIGMENT %
45
PIGMENT IDENTIFIED *
Vermiculite Synthetic Foam Gypsum
Other
woe -----
*
Pumice Carbonate
Pigment
COMMENTS
-5 % %
ANALYST Randy Boltin
DATE 05/24/96
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APPENDIX B
TEM Analysis Sheets
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Summary of TEM Analysis Results
Sample # | Description
Air Vol
Liters
Asbestos Structures cc
G0943
Background before Sanding
Brake Shoes
1800
BDL
0.003
G0947
Sanding of Brake | 28
Shoes
54.4
G0950 G0952
Nearby Area During Sanding
176 0
13 NSD
G0958 G0960 G0961
During Sweeping | 15.6 During Sweeping | 15.6
0
11.7 44.5 NSD
G0964
Background before Filing
Brake Pad
1230
0.039
G0969
During Filing
13
6.7
Grooves in Brake
Pad
G0971
0
2 str
G0975
During Grinding
7.3
Grooves in Brake
232
Pad
G0976
0
NSD
G0980
Background
1240
0.05
Before Grinding
BDL - Below Detection Limit Analytical Sensitivity Given
NSD - No Structures Detected
D PROJECTS
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MVA Inc.
SAMPLE ANALYSIS INFORMATION
MVA Project # Lab Sample I.D Client Sample I.D
Instrument I.D
Magnification
Acc Voltage
1810 G0943
JEOL1200 21,000 120kV
Amount Collected
1800
Amount Prepped DIRECT
Filter Area mm
Filter Type
385 PC
Openings Analyzed
10
Grid Opening mm2
0.008
Analyst PF
Date
5/22/96
Comments
Grid 1
2
Opening C7 G6 18 F7 D3 D2 F4 H7 F9 C5
Structure
Number
NSD NSD NSD NSD NSD NSD NSD NSD NSD NSD
Structure
Type
Length m
Width
um
SAEDfi
EDS
Comments
*
On Screen Measure
B = Bundle C = Cluster F = Fiber M = Matrix PC = Chrysotile A = Amphibole C = Chrysotile AM = Amosite CR = Crocidolite AC = Actinolite AN = Anthophyllite TR = Tremolite
N = Non Asbestos NFD or NSD = No Fibers Detected or No Structures Detected
D PROJECTS RP052496
Page 27
MVA Inc.
SAMPLE ANALYSIS INFORMATION
MVA Project # Lab Sample I.D Client Sample I.D
Instrument I.D
Magnification
Acc Voltage
1810 G0947
JEOL1200 21,000 120kV
Amount Collected
28
Amount Prepped DIRECT
Filter Area mm
Filter Type
385 PC
Openings Analyzed
3
Grid Opening mm2
0.008
Analyst PF
Date
5/21/96
Comments
Grid 1
Opening
G6
C5
Structure
Number
1 23 23 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35
Structure
Type
BCCMM
BCCMM
-- BCCMM
O O O
MBOLUNUNM0 0 MBOLUNUNM0 0 MBOLUNUNM0 0 MBOLUNUNM00
MBOLUNUNM00
MBOLUNUNM0 0
MBOLUNUNM00
MBOLUNUNM0 0 MBOLUNUNM00
MBOLUNUNM00
MBOLUNUNM0 0 B
C
B B B B B B B B
C C C
B
Cc
Length um
2.9 19.0 5.0 7.6 5.7 7.1 2.4 9.5 4.3 2.9 6.7 1.0 2.4 2.1 13.3 7.6 7.4 1.0 1.1 5.7 10.5 5.7 7.6 8.1 5.0 2.9 0.1 2.9 9.8 0.7 2.6 1.4 1.4 16.2 2.4
Width
um
0.24 14.29 3.81
_ SAEDfi
C Cc
Cc
0.48
Cc
0.48
Cc
5.24
Cc
1.19
C
5.71
Cc
4.29
Cc
0.95
Cc
2.38
Cc
0.10
Cc
1.43
Cc
1.90
Cc
6.19
Cc
5.71
Cc
0.24
Cc
0.48
Cc
1.05
Cc
0.62
c
7.14
Cc
3.33
Cc
0.48
Cc
0.48
Cc
0.19
Cc
0.62
Cc
0.14
Cc
1.05
Cc
0.19
Cc
0.48
Cc
0.24
Cc
0.71
c
0.95
Cc
0.48
c
0.71
EDS C Cc
U
C
Comments
*
On Screen Measure
B = Bundle C = Cluster F = Fiber M = Matrix PC = Chrysotile A = Amphibole C = Chrysotile AM = Amosite CR = Crocidolite AC = Actinolite AN = Anthophyllite TR = Tremolite
N = Non Asbestos NFD or NSD = No Fibers Detected or No Structures Detected
D PROJECTS
Page 28
MVA Inc.
SETTLED DUST ANALYSIS
MVA Project # Lab Sample I.D Client Sample I.D
Instrument I.D
Magnification
Acc Voltage
1810 G0947
JEOL1200 21,000 120kV
Amount Collected
28
Amount Prepped DIRECT
Filter Area mm
385
Filter Type
PC
Openings Analyzed
3
Grid Opening mm2
0.008
Analyst Date
PF 5/21/96
Comments
Grid OpeningOpening
1
C5
D9
Structure
Number
36 37 38 39 40 41 42 43 44 45 46 47 48 49 50 51 52 53 54 55 56 57
58
59 60 61 62 63 64 65 66 67 68 69 70
Structure
Type
MMO MMO
MMO O Oumm
Oumm B M mcmm
mcmm
mcmm mcmm BMCBCLO OBEBCLOM BMCBCLO OBEBCLOM BMCBCLO OBEBCLOM
BMCBLO BE CLOM
BMCBCLO OBEBCLOM BMCBCLO OBEBCLOM
BMCBCLOOBEBCLOM
BMCBCLOOBEBCLOM BMCBCLOOBEBCLOM
BMCBLO BE CLOM
BMCBCLO OBEBCLOM
BMCBLO BE CLOM BMCBLO BE CLOM
BMCBCLO OBEBCLOM BMCBCLO OBEBCLOM BMCBCLO OBEBCLOM BMCBCLO OBEBCLOM
BMCBLO BE CLOM
BMCBCLOOBEBCLOM
BMCBLO BE CLOM BMCBLO BE CLOM
BMCBCLO OBEBCLOM
BMCBLO BE CLOM
Length um
2.9 1.4 6.2 3.8 14.3 1.0 3.1 3.8 6.7 7.1 1.2 1.9 4.8 1.8 1.2 7.6 2.4 0.6 9.5 1.5 0.7 15.2 16.7 1.2 12.9 1.9 5.2 4.5 2.6 1.9 0.6 2.6 11.4 1.4 1.8
Width
um
1.90
_ SAEDB
Cc
0.95
Cc
2.38
C
2.38
C
4.76
Cc
0.24
Cc
0.48
Cc
0.95
Cc
0.95
Cc
3.33
Cc
0.19
c
0.29
Cc
1.43
Cc
0.33
Cc
0.71
Cc
7.14
C
0.14
C
0.10
c
1.43
0.05
Cc
0.05
Cc
1.43
Cc
0.48
C
0.95
C
10.00
Cc
0.57
Cc
0.71
Cc
0.24
Cc
0.19
Cc
0.71
Cc
0.05
Cc
1.90
C
5.71
Cc
0.24
Cc
2.00
Cc
EDSS Cc Cc
Comments
On Screen Measure
B = Bundle C = Cluster F = Fiber M = Matrix PC = Chrysotile A = Amphibole SC = Chrysotile AM = Amosite CR = Crocidolite AC = Actinolite AN = Anthophyllite TR = Tremolite
N = Non Asbestos NFD or NSD = No Fibers Detected or No Structures Detected
D PROJECTS
Page 29
MVA Inc.
SAMPLE ANALYSIS INFORMATION
MVA Project # Lab Sample I.D Client Sample I.D
Instrument I.D
Magnification
Acc Voltage
1810 G0947
JEOL1200
21,000
120kV
Amount Collected
28
Amount Prepped DIRECT
Filter Area mm
385
Filter Type
PC
Openings Analyzed
3
Grid Opening mm2
0.008
Analyst
Date
PF 5/21/96
Comments
Grid Opening
1
D9
Structure
Number
71 72 73 74 75 76 77 78 79 80 81 82 83
84
85
86
87 88 89 90 91 92 93
25
95
Structure
Type Cc Cc Cc
c F
B F B
CBCBc om
CBCBccomm
CBCBc om
CBCBc om
CBCBc om CBCBc om CBCBc om
CBCBc om CBCBc om
C
WO WO B TINTO M F
Length um
11.4 21.4 2.1
1.0 1.9 7.1 4.3 0.5 0.6 0.9 2.6 3.8 2.9 2.4 31.4 3.3 0.5 2.4 16.7 1.9 3.3 11.0 0.5 2.9 0.6
Width
um
9.05 5.71 0.48 1.05 0.00 5.71 0.19 0.05 0.14 0.43 0.14 2.86 1.05 1.81 1.67 2.38 0.14 0.48 8.57 0.48 0.71 3.81 0.05 1.43 0.05
SAEDfi
Cc Cc Cc Cc Cc c Cc LC C C Cc Cc Cc Cc Cc Cc Cc Cc Cc C Cc C Cc Cc Cc
EDS
00
Comments
* On Screen Measure
B = Bundle C = Cluster F = Fiber M = Matrix C= Chrysotile = Amphibole C = Chrysotile AM = Amosite CR = Crocidolite AC = Actinolite AN = Anthophyllite TR = Tremolite
N = Non Asbestos NFD or NSD = No Fibers Detected or No Structures Detected
D PROJECTS
Page 30
MVA Inc. SAMPLE ANALYSIS INFORMATION
MVA Project # Lab Sample I.D Client Sample I.D
Instrument I.D
Magnification
Acc Voltage
1810 G0950
JEOL1200
21,000
120kV
Amount Collected
176
Amount Prepped DIRECT
Filter Area mm
385
Filter Type
PC
Openings Analyzed
2
Grid Opening mm
0.008
Analyst PF
Date
5/23/96
Comments
Grid Opening
1
04
C5
Structure
Number
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21
22
23 24 25 26 27 28 29 30 31 32 33 34 35
Structure
Type
B
C
B
B F M
C
M B B
C C
B M B B F B B F
C
B B B B B
C Cc Cc Cc Cc Cc Cc
c
Length um
1.2 15.2 0.7 11.9 2.1 1.4 0.7 16.7 2.4 7.6 4.3 5.2 7.1 1.4 1.4 1.0
1.9 2.1 18.1 3.3 1.1 4.8 0.8 1.2 1.4 7.1 1.2 11.4 2.9 1.0 8.6 1.4 4.3 6.2 8.1
Width
...m_ SAEDfi
0.29
C
16.19
0.14
C
2.38
C
1.19
Cc
0.05
Cc
0.43
Cc
10.48
Cc
0.95
Cc
0.95
Cc
0.24
Cc
3.81
Cc
8.10
Cc
0.48
Cc
0.71
C
0.95
Cc
0.10
Cc
0.07
Cc
0.95
Cc
0.24
Cc
0.05
Cc
3.33
c
0.29
Cc
0.33
Cc
0.10
Cc
0.71
c
0.14
c
2.86
Cc
2.38
Cc
0.86
Cc
5.71
Cc
1.43
Cc
2.86
c
2.38
Cc
4.76
C
EDS C
C
Comments
* On Screen Measure
B = Bundle C = Cluster F = Fiber M = Matrix PC = Chrysotile A = Amphibole C = Chrysotile AM = Amosite CR = Crocidolite AC = Actinolite AN = Anthophyllite TR = Tremolite
N = Non Asbestos NFD or NSD = No Fibers Detected or No Structures Detected
D PROJECTS
Page 31
MVA Inc.
SETTLED DUST ANALYSIS
MVA Project # Lab Sample I.D Client Sample I.D
Instrument I.D
Magnification
Acc Voltage
1810 G0950
JEOL1200
21,000
120kV
Amount Collected
176
Amount Prepped DIRECT
Filter Area mm
Filter Type
385 PC
Openings Analyzed
2
Grid Opening mm2
0.008
Analyst PF
Date
5/23/96
Comments
Grid __Opening
1
D4
H8
Structure
Number
36 37 38 39 40 41 42 43 44 45
46
47 48 49 50 51 52 53 54 55 56 57 58 59 60 61 62 63 64 65 66 67 68 69 70
Structure
Type CMCMEONCO
CMCMEONCO CMCMEONCO CMCMEONCO CMCMEONCO
CMCMEONCO
CMCMEONCO
CMCMEONCO CMCMEONCO
m m m m MCCMCMC
MC MCMC MCCMCMC
MCCMCMC
MCCMCMC
MCCMCMC
MCCMCMC CM
CM EM B MULB
MULB
MULB MULB
C C
B
C
B
Length m
4.8 7.1 9.5 5.2 0.6 3.3 2.9 11.0 11.9 0.8 0.7 2.4 1.4 2.6 7.1 0.7 1.4 7.1 2.4 15.7 2.1 2.6 0.6 2.1 7.1 0.7 3.3 1.1 3.8 8.1 8.1 11.0 2.4 10.5 8.1
Width
um
2.38 5.71 4.76 1.19 0.05 1.90 2.38 4.76 14.29 0.10 0.10 2.38 0.24 0.71 5.71 0.57 0.24 4.76 0.14 5.71 0.95 0.38 0.05 0.14 0.71 0.24 0.07 0.14 1.43 3.81 1.43 9.52 2.38 7.14 0.48
SAEDfi
0 0 0 0 0 0 0 0
00000
00000 00000 00000 00000 Cc
Cc
Cc Cc Cc Cc c Cc Cc c Cc Cc Cc Cc Cc Cc
Cc
Cc Cc Cc C C
EDS C
C
Comments
* On Screen Measure
B = Bundle C = Cluster F = Fiber M = Matrix PC = Chrysotile A = Amphibole C = Chrysotile AM = Amosite CR = Crocidolite AC = Actinolite AN = Anthophyllite TR = Tremolite
N = Non Asbestos NFD or NSD = No Fibers Detected or No Structures Detected
D PROJECTS
Page 32
MVA Inc.
SAMPLE ANALYSIS INFORMATION
MVA Project # Lab Sample I.D Client Sample I.D
Instrument I.D
Magnification
Acc Voltage
1810 G0950
JEOL1200
21,000 120kV
Amount Collected
176
Amount Prepped DIRECT
Filter Area mm
385
Filter Type
PC
Openings Analyzed
2
Grid Opening mm2
0.008
Analyst PF
Date
5/23/96
Comments
Grid Opening
1
H8
Structure
Number
71 72 73 74 75 76 77 78 79 80 81 82 83
84
85 86 87 88 89 90 91 92 93 94 95
Structure
Type
MCFCM
MCFCM
MCFCM
MCFCM
MCFCM B M B CSUBMBUMBUOMELBOU CSUBMBUMBUOMELBOU
CSUBMUMBUOMELBOU
CSUBMBUMBUOMELBOU CSUBMBUMBUOMELBOU CSUBMBUMBUOMELBOU
CSUBMUMBUOMELBOU
CSUBMBUMBUOMELBOU CSUBMBUMBUOMELBOU
CSUBMUMBUOMELBOU CSUBMUMBUOMELBOU
CSUBMBUMBUOMELBOU CSUBMUMBUOMELBOU CSUBMUMBUOMELBOU CSUBMBUMBUOMELBOU
CSUBMUMBUOMELBOU CSUBMUMBUOMELBOU
Length um
1.9 0.7 1.9 1.0 1.9 2.6 4.8 0.7 2.1 2.4 2.4 6.7 1.0 7.6 4.8 1.4 6.2 2.1 8.6 5.7 0.6 1.2 1.4 5.0 1.0
Width
...m
0.14 0.48 0.05 0.48 0.24 1.90 3.81 0.38 0.14 2.38 1.90 0.48 0.33 0.38 1.43 0.95 3.33 1.43 5.71 0.38 0.05 0.33 0.95 2.86 0.57
SAEDfi
Cc Cc Cc Cc Cc Cc Cc Cc c c Cc Cc Cc
Cc
Cc Cc Cc Cc c Cc Cc Cc Cc
00 00
EDS
Cc 00 00
Comments
* On Screen Measure
B = Bundle C = Cluster F = Fiber M = Matrix PC = Chrysotile A = Amphibole C = Chrysotile AM = Amosite CR = Crocidolite AC = Actinolite AN = Anthophyllite TR = Tremolite
N = Non Asbestos NFD or NSD = No Fibers Detected or No Structures Detected
D PROJECTS
Page 33
MVA Inc.
SAMPLE ANALYSIS INFORMATION
MVA Project # Lab Sample I.D Client Sample I.D
Instrument I.D
Magnification
Acc Voltage
1810 G0952
JEOL1200
21,000 120kV
Amount Collected
O
Amount Prepped DIRECT
Filter Area mm
385
Filter Type
PC
Openings Analyzed
10
Grid Opening mm2
0.008
Analyst PF
Date
5/23/96
Comments
Grid 1
2
Opening
F3 H4 G7 D5 B2 C2 E4 G5 H8 C9
Structure
Number
NSD
NSD NSD NSD NSD NSD NSD NSD NSD NSD
Structure
Type
Length um
Width
m SAED
EDS
Comments
* On Screen Measure
B = Bundle C = Cluster F = Fiber M = Matrix PC = Chrysotile A = Amphibole C = Chrysotile AM = Amosite CR = Crocidolite AC = Actinolite AN = Anthophyllite TR = Tremolite
N = Non Asbestos NFD or NSD = No Fibers Detected or No Structures Detected
D PROJECTS
Page 34
MVA Inc.
SAMPLE ANALYSIS INFORMATION
MVA Project # Lab Sample I.D Client Sample I.D
Instrument 1.D
Magnification
Acc Voltage
1810 G0958
JEOL1200
21,000
120kV
Amount Collected
15.6
Amount Prepped DIRECT
Filter Area mm
385
Filter Type
PC
Openings Analyzed
10
Grid Opening mm2
0.008
Analyst
Date
PF 5/23/96
Comments
Grid 1
Opening
F7
Structure
Number
1 23
Structure
Type
B
B
Length m 7.6
2.9
Width
um 1.90
0.24
SAEDfi
EDS
Comments
23
mmco
25.7
0.71
4
mmco
1.4
0.33
5
mmco
1.9
0.95
D5
6
mmco
5.2
3.33
7
OZUMUUM
1.2
0.95
8
OZUMUUM
5.2
2.38
9
OZUMUUM
3.8
0.71
10
OZUMUUM
1.9
0.24
11
OZUMUUM
9.5
1.43
B6
12
OZUMUUM
9.5
4.76
13
OZUMUUM
5.7
0.62
C3 G7
2
E8
G5
14
OOO
7.1
5.71
15
OOO
1.9
0.71
16
OOO
4.3
2.86
17
O
8.1
2.38
18
O
19.0
4.76
19
O
14.3
7.14
NnAag Y 20
O
1.0
0.71
21
UBBM
1.1
0.76
22
UBBM
3.1
0.19
23
--
3.0
0.19
24
UBBM
1.9
1.52
25
BELCB
0.7
0.29
NaN 26
BELCB
1.1
0.10
27
BELCB
0.6
0.05
28
BELCB
2.4
0.48
29
--
1.9
0.14
30
M
7.1
7.14
31
B
6.7
0.24
F3
32
M
1.2
0.48
333333
333333
333333
B3
333333
333333
D9
38
* On Screen Measure
CUMMMU
22.9
4.76
0 CUMMMU
20.0
3.81
CUMMMU
0.7
0.10
CUMMMU
7.1
3.81
CUMMMU
2.4
0.24
CUMMMU
5.7
4.76
B Bundle C = Cluster F = Fiber M = Matrix
PC = Chrysotile A = Amphibole C = Chrysotile AM = Amosite CR = Crocidolite AC = Actinolite AN = Anthophyllite TR = Tremolite
N = Non Asbestos
NFD or NSD = No Fibers Detected or No Structures Detected
D PROJECTS
Page 35
MVA Inc. SAMPLE ANALYSIS INFORMATION
MVA Project # Lab Sample 1.D Client Sample I.D
Instrument I.D
Magnification
Acc Voltage
1810
G0960
JEOL1200 21,000 120kV
Amount Collected
15.6
Amount Prepped DIRECT
Filter Area mm
385
Filter Type
PC
Openings Analyzed
7
Grid Opening mm
0.008
Analyst PF
Date
5/23/96
Comments
Grid __Opening
1
G6
E7
H6
Structure
Number
1 234 234 234 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35
Structure
Type CBC02U5MB B CBC02U5MB B
CBC02U5UMBMB
CBC02U5MB B CBC02U5MB B
CBC02U5UMBMB C BC0 2U5UMBMB
CBC02U5MB B
C BC0 2U5UMBMB
CBC02U5MB B
C BC0 2U5UMBMB CBC02U5UMBMB C BC0 2U5UMBMB CBC02U5UMBMB CBC02U5UMBMB BUM UM UM BUMMUMMUM BUMMUMMUM BUMMUMMUM BUMMUMMUM BUMMUMMUM BUMMUMMUM
BUM UM UM
BUMMUMMUM MU MB B BC MU MB B BC MU MB B BC MUUMBBBBBC MU MB B BC MU MB B BC MU MB B BC MU MB B BC MU MB B BC MU MB B BC
MU MB B BC
Length
...m
3.8 2.4 1.2 7.1 1.9 3.3 7.1 14.8 3.8 1.2 4.8 1.1 5.0 0.6 6.7 2.1 2.4 1.4 7.1 13.8 2.9 8.1 20.0 13.8 1.9 4.3 2.4 4.8 6.7 2.9 1.0 3.8 2.6 0.9 3.8
Width
...m_ SAEDB
2.38
c
1.43
c
0.19
Cc
4.76
c
0.95
Cc
1.43
Cc
5.24
c
4.76
Cc
2.62
c
0.48
Cc
3.81
Cc
0.14
Cc
4.76
Cc
0.24
Cc
1.90
Cc
1.19
Cc
2.14
Cc
0.48
Cc
4.76
Cc
3.81
Cc
2.38
Cc
3.81
Cc
12.38
Cc
0.43
c
0.95
c
2.38
Cc
1.43
Cc
3.81
Cc
1.43
Cc
0.48
c
0.33
Cc
1.43
Cc
0.05
Cc
0.07
Cc
3.33
Cc
EDS C Cc
C
Comments
*
On Screen Measure B = Bundle C = Cluster F = Fiber M = Matrix
PC = Chrysotile A = Amphibole C = Chrysotile AM = Amosite CR = Crocidolite AC = Actinolite AN = Anthophyllite TR = Tremolite
N = Non Asbestos NFD or NSD = No Fibers Detected or No Structures Detected
D PROJECTS
Page 36
MVA Inc.
SETTLED DUST ANALYSIS
MVA Project # Lab Sample I.D Client Sample I.D
Instrument I.D
Magnification
Acc Voltage
1810
G0960
JEOL1200
21,000 120kV
Amount Collected
15.6
Amount Prepped DIRECT
Filter Area mm
385
Filter Type
PC
Openings Analyzed
7
Grid Opening mm2
0.008
Analyst PF
Date
5/23/96
Comments
Grid Opening
1
H6
14
H9
Structure
Number
36 37 38 39 40 41 42 43 44 45
46
47 48 49 50 51 52 53
54
55 56 57 58 59 60 61 62 63 64 65 66 67 68 69 70
Structure
Type Cc
OMOMMUMMU OMOMMUMMU OMOMMUMMU OMOMMUMMU OMOMMUMMU
OMOM UM U
OMOMMUMMU OMOMMUMMU
OMOM UM U U
m m
U CEMDOM
CEMDOM CEMDOM CEMDOM
CEMDOM
CEMDOM M MBUMOUOMLO0 0 M MBUMOUOMLO0 0 MMBUMOUOMLO00 MMBUMOUOMLO00 MMBUMOUOMLO00 M MBUMOUOMLO0 0
M BUMOUMLO0 M BUMOUMLO0 M BUMOUMLO0
M MBUMOUOMLO0 0 MMBUMOUOMLO00 MMBUMOUOMLO00
M BUMOUMLO0 M BUMOUMLO0 M BUMOUMLO0
Length m
1.9 10.0 5.7 16.7 6.2 4.8 7.1 1.8 2.9 7.1 3.8 3.1
1.4 4.3 2.4 1.1 3.3 8.6 2.4 1.2 21.4 7.6 4.3 1.0 4.8 1.4 2.9 5.2 3.3 4.3 3.3 9.5 1.9 8.1 17.6
Width
um
1.52 2.14 3.33 7.14 3.81 4.29 2.38 0.10 1.90 3.81 0.95 2.14 0.14 2.38 1.43 0.05 2.86 1.90 2.14 0.24 14.29 7.62 0.38 0.14 1.43 0.48 2.38 2.38 3.33 0.95 0.10 5.71 1.43 7.62 7.14
SAEDfi
C Cc
Cc
Cc c Cc c Cc Cc c Cc Cc Cc
Cc
Cc Cc Cc Cc Cc Cc c c Cc c Cc Cc Cc c Cc Cc Cc Cc Cc Cc C
EDS C
Cc
Comments
On Screen Measure
B = Bundle C = Cluster F - Fiber M = Matrix PC = Chrysotile = Amphibole C = Chrysotile AM = Amosite CR = Crocidolite AC = Actinolite AN = Anthophyllite TR = Tremolite
N = Non Asbestos NFD or NSD = No Fibers Detected or No Structures Detected
D PROJECTS
Page 37
MVA Inc.
SAMPLE ANALYSIS INFORMATION
MVA Project # Lab Sample I.D Client Sample I.D
Instrument 1.D
Magnification
Acc Voltage
1810 G0960
JEOL1200
21,000 120kV
Amount Collected
15.6
Amount Prepped DIRECT
Filter Area mm
385
Filter Type
PC
Openings Analyzed
7
Grid Opening mm2
0.008
Analyst PF
Date
5/23/96
Comments
Grid 1
Opening
H9
C6
F8
Structure
Number
71 72 73 74 75 76 77 78 79 80 81 82 83 84 85 86 87 88 89 90
91
92 93 94 95 96 97 98 99 100 101
Structure
Type
B
C
B M
C
F F
B M B F B
C Cc
c
Cc
B F F F F
0 0 MBUM 0 0 MBUM 0 0 MBUM 0 0 MBUM
0000MBUM --
0 0 MBUM
0000MBUM
Length _ um
2.9 2.1 9.5 3.3 3.8 7.1 8.1
1.4
19.0 5.2 2.4 4.3 2.4 3.3 4.8 4.8 3.8 23.8 10.0 1.0 1.0 1.9 5.2 7.1 9.5 2.9 1.4 7.1 38.1 9.5 1.0
Width
...m SAEDB
0.48
Cc
0.95
C
4.76
C
0.24
Cc
3.81
Cc
4.76
Cc
0.10
Cc
0.05
Cc
4.76
c
0.10
c
1.90
Cc
0.24
Cc
0.14
Cc
0.24
Cc
3.81
Cc
3.33
Cc
0.95
Cc
23.81
c
0.48
Cc
0.05
c
0.10
Cc
0.10
Cc
0.14
Cc
4.76
Cc
4.76
c
1.90
Cc
1.43
Cc
2.38
Cc
0.48
c
4.76
Cc
0.48
Cc
EDS C
Comments
*
On Screen Measure
B = Bundle C = Cluster F = Fiber M = Matrix C= Chrysotile A = Amphibole C = Chrysotile AM = Amosite CR = Crocidolite AC = Actinolite AN = Anthophyllite TR = Tremolite
N = Non Asbestos NFD or NSD = No Fibers Detected or No Structures Detected
D PROJECTS
Page 38
MVA Inc.
SAMPLE ANALYSIS INFORMATION
MVA Project # Lab Sample I.D Client Sample I.D
Instrument I.D
Magnification
Acc Voltage
1810 G0961
JEOL1200 21,000 120kV
Amount Collected
0
Amount Prepped DIRECT
Filter Area mm
385
Filter Type
PC
Openings Analyzed
10
Grid Opening mm2
0.008
Analyst JRM
Date
5/23/96
Comments
Grid 1
2
Opening
G4 E7 B3 F1 H5 87 A10 13 F2 E9
Structure
Number
NSD NSD NSD NSD NSD NSD NSD NSD NSD NSD
Structure
Type
Length um
Width
um
SAEDfi
EDS
Comments
*
On Screen Measure
B = Bundle C = Cluster F = Fiber M = Matrix PC = Chrysotile A = Amphibole C = Chrysotile AM = Amosite CR = Crocidolite AC = Actinolite AN = Anthophyllite TR = Tremolite
N = Non Asbestos NFD or NSD = No Fibers Detected or No Structures Detected
D PROJECTS
Page 39
MVA Inc.
SAMPLE ANALYSIS INFORMATION
MVA Project # Lab Sample 1.D Client Sample I.D
Instrument I.D
Magnification
Acc Voltage
1810 G0964
JEOL1200
21,000 120kV
Amount Collected
1230
Amount Prepped DIRECT
Filter Area mm
385
Filter Type
PC
Openings Analyzed
10
Grid Opening mm2
0.008
Analyst JRM
Date
5/23/96
Comments
Grid ___ Opening
1
B3
E8
G1
18
C2
2
D9
C5
A10
H3
J4
Structure
Number
NSD 1234+ 1234+ 1234+ 1234+
NSD 5 6 7 8 9 10
Structure
Type
CFMM
CFMM CFMM M
FBCCFM FBCCFM
FBCCFM FBCCFM
FBCCFM FBCCFM
Length um
Width
...m SAEDfi
EDS
223
0.95
0000
C
223
0.05
0000
223
0.24
0000
4.8
2.38
0000
4.3
0.10
000000
2.4
0.29
000000
7.1
4.76
000000
Cc
1.9
1.90
000000
2.9
0.10
000000
8.6
2.38
000000
Comments
*
On Screen Measure
B = Bundle C = Cluster F = Fiber M = Matrix BC = Chrysotile A = Amphibole
C = Chrysotile AM = Amosite CR = Crocidolite AC = Actinolite AN = Anthophyllite TR = Tremolite
N = Non Asbestos NFD or NSD = No Fibers Detected or No Structures Detected
D PROJECTS
Page 40
MVA Inc.
SAMPLE ANALYSIS INFORMATION
MVA Project # Lab Sample I.D Client Sample I.D
Instrument I.D
Magnification
Acc Voltage
1810
G0969
JEOL1200 21,000 120kV
Amount Collected
13
Amount Prepped DIRECT
Filter Area mm
385
Filter Type
PC
Openings Analyzed
10
Grid Opening mm2
0.008
Analyst PF
Date
5/24/96
Comments
Grid
1
Opening
D5
F4
H6
G9
C6
2
E7
G9
H4
88
C9
Structure
Number
NSD 123 123 123
NSD NSD NSD
450780 450780 450780 450780 450780 450780 10 11 12 13 14 15 16 17 18
Structure
Type
F
C
B
MCmCmm
MCmCmm
MCmCmm
MCmCmm
MCmCmm B
Umm
Umm B
Um
B UMUM UMUM UMUM UMUM
Length m
Width
...m_ SAEDfi
2.4
0.05
C
5.7
4.76
00
1.4
0.14
C
EDS C
2.9
0.71
Cc
9.0
3.81
Cc
1.2
0.14
c
1.4
1.43
Cc
4.3
0.10
Cc
0.7
0.48
Cc
1.7
1.43
Cc
C
1.0
0.24
Cc
0.6
0.10
C
2.4
1.90
C
3.3
0.71
Cc
14.3
3.33
Cc
2.1
0.71
Cc
1.0
0.05
C
0.7
0.14
C
Comments
* On Screen Measure B = Bundle C = Cluster F = Fiber M = Matrix
PC = Chrysotile A = Amphibole "C= Chrysotile AM = Amosite CR = Crocidolite AC = Actinolite AN = Anthophyllite TR = Tremolite
N = Non Asbestos NFD or NSD = No Fibers Detected or No Structures Detected
D PROJECTS
Page 41
MVA Inc.
SAMPLE ANALYSIS INFORMATION
MVA Project # Lab Sample I.D Client Sample I.D
Instrument I.D
Magnification
Acc Voltage
1810 G0971
JEOL1200 21,000 120kV
Amount Collected
0
Amount Prepped DIRECT
Filter Area mm
385
Filter Type
PC
Openings Analyzed
10
Grid Opening mm2
0.008
Analyst PF
Date
5/24/96
Comments
Grid
1
2
Opening
G8 E7 B6 H4 15 C7 E8
D4 B6
H5
Structure Number
NSD NSD NSD 1 N NSD NSD NSD NSD NSD
Structure
Type
F F
Length ...m
Width
m
SAEDfi
EDS
2.1
0.05
1.9
0.05
Comments
* On Screen Measure
B = Bundle C = Cluster F = Fiber M = Matrix PC = Chrysotile A = Amphibole C = Chrysotile AM = Amosite CR = Crocidolite AC = Actinolite AN = Anthophyllite TR = Tremolite
N = Non Asbestos NFD or NSD = No Fibers Detected or No Structures Detected
D PROJECTS
Page 42
MVA Inc.
SAMPLE ANALYSIS INFORMATION
MVA Project # Lab Sample I.D Client Sample 1.D
Instrument I.D
Magnification
Acc Voltage
1810 G0975
JEOL1200 21,000 120kV
Amount Collected
7.3
Amount Prepped DIRECT
Filter Area mm
385
Filter Type
PC
Openings Analyzed
3
Grid Opening mm2
0.008
Analyst PF
Date
5/24/96
Comments
Grid 1
Opening
F9
C7
Structure
Number
1 2 3 4 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21
22
23 24 25 26 27 28 29 30 31 32 33 34 35
Structure
Type
UNMUZO O O M
UNUMUMZOOOOOM
UNMUZO O O M
UNUMUMZOOOOOM
UNMUZO O O M
UNUMUMZOOOOOM
UNUMUMZOOOOOM
UNMUZO O O M UNMUZO O O M UNMUZO O O M UNMUZO O O M UNMUZO O O M UNMUZO O O M UNMUZO O O M
UNUMUMZOOOOOM
UNMUZO O O M
UNMUZO O O M
MO0000
MO0000 MO0000 MO0000 MO0000 MO0000 UE^MOUMOUE0
UE^ MOUMOUE0
UE^MOUMOUE0
UE^ MOUMOUE0
UE^MOUMOUE0 UE^MOUMOUE0
UE^ MOUMOUE0
UE^MOUMOUE0 UE^MOUMOUE0
UE^ MOUMOUE0
UE^MOUMOUE0 UE^MOUMOUE0
Length m
28.6 1.4 4.8 1.0 7.1 3.8 7.1 4.5 12.9 13.3 1.7 11.0 2.4 1.9 2.1 11.0 2.6 0.7 2.6 1.9 5.7 2.4 3.3 7.1 11.9 5.7 4.8 2.9 2.6 4.8 0.7 2.1 2.6 11.9 20.0
Width
um
23.81 0.95 1.43 0.19 3.81 2.86 5.71 2.14 3.81 3.81 0.48 4.76 1.90 1.43 0.95 4.76 0.71 0.10 0.95 0.95 2.86 2.14 2.14 4.29 4.76 3.33 1.43 1.90 1.43 1.90 0.71 1.90 1.90 4.76 10.95
SAED
C Cc Cc Cc Cc Cc Cc
Cc
Cc Cc Cc Cc Cc Cc Cc
Cc
Cc Cc Cc Cc Cc Cc Cc Cc C Cc Cc Cc Cc Cc Cc Cc Cc
Cc
Cc
EDS C C
Cc
Comments
* On Screen Measure B = Bundle C = Cluster F = Fiber M = Matrix
BC = Chrysotile A = Amphibole C = Chrysotile AM = Amosite CR = Crocidolite AC = Actinolite AN = Anthophyllite TR = Tremolite
N = Non Asbestos NFD or NSD = No Fibers Detected or No Structures Detected
D PROJECTS
Page 43
MVA Inc.
SETTLED DUST ANALYSIS
MVA Project # Lab Sample I.D Client Sample I.D Instrument I.D
Magnification
Acc Voltage
1810 G0975
JEOL1200 21,000 120kV
Amount Collected Amount Prepped
Filter Area mm
Filter Type Openings Analyzed Grid Opening mm2
7.3 DIRECT
385 PC
3 0.008
Analyst PF
Date
5/24/96
Comments
Grid __ Opening
1
C7
E4
Structure
Number
36 37 38 39 40 41 42 43
44
45
46
47 48 49 50 51 52 53
54
55
56
57 58 59 60 61 62 63 64 65 66 67 68 69 70
Structure
Type
0000B 0000B 0000B 0000B
0000B EM EM
,, Cc Cc Cc Cc Cc Cc Cc
B
B B
C
c C B B B
Cc Cc Cc Cc
B B B
Cc
Length um
18.1 2.9 9.0 8.1 1.5 0.9 1.5 2.9 1.0 5.2 3.3 2.1 20.5 5.7 2.4 7.6 3.8
1.2 1.7 1.0 6.7 2.9 1.2 2.1 1.7 18.1 4.8 4.8 3.3 3.8 2.1 7.1 5.2 13.8 8.6
Width
um
17.62 1.43 5.71 5.24 0.14 0.07 0.38 1.19 0.71 2.38 0.71 1.90 15.24 3.33 2.14 1.43 2.86 0.14 0.19 0.48 6.19 2.38 0.71
1.43 0.95 5.24 1.43 2.86 2.14 1.43 0.19 1.90 0.95 4.29 3.33
SAED
Cc Cc
Cc
Cc Cc Cc Cc Cc Cc Cc Cc Cc Cc Cc c c Cc Cc c Cc
Cc
Cc Cc Cc Cc c Cc Cc Cc
Cc
Cc Cc Cc Cc
EDS C
Cc
0
Comments
* On Screen Measure
B = Bundle C = Cluster F = Fiber M = Matrix
BC = Chrysotile A = Amphibole
SC = Chrysotile AM = Amosite CR = Crocidolite AC = Actinolite AN = Anthophyllite TR = Tremolite
N = Non Asbestos NFD or NSD = No Fibers Detected or No Structures Detected
D PROJECTS
Page 44
MVA Inc.
SAMPLE ANALYSIS INFORMATION
MVA Project # Lab Sample I.D Client Sample I.D
Instrument I.D
Magnification
Acc Voltage
1810 G0975
JEOL1200 21,000 120kV
Amount Collected
7.3
Amount Prepped DIRECT
Filter Area mm
385
Filter Type
PC
Openings Analyzed
3
Grid Opening mm2
0.008
Analyst PF
Date
5/24/96
Comments
Grid 1
Opening
E4
Structure
Number
71 72 73 74 75 76 77 78 79 80 81 82 83
84
85 86 87 88 89 90 91 92 93 94 95 96 97 98 99 100 101 102 103
104
105 106
Structure
Type Cc Cc Cc Cc Cc Cc Cc Cc
B
B
Cc Cc Cc
F
Cc
c
Cc Cc Cc
c
Cc C
B
Cc Cc Cc
F B B
Cc Cc Cc Cc
Length
um
14.8 1.2 5.7 9.5 12.9 2.1 6.2 4.5 13.8 11.0 2.1 1.9 2.1 2.0 13.3 1.5 1.9 1.4 2.6 4.8 2.6 0.7 5.0 18.1 2.1 8.1
3.3 7.1 20.0 0.6 9.0 4.5 11.0 2.9 1.2 1.9
Width
...m__ SAEDfi
6.67
0000000
0.71
0000000
0.71
0000000
5.71
0000000
6.19
0000000
0.48
0000000
4.76
0000000
4.29
Cc
1.90
Cc
5.24
Cc
0.62
Cc
1.43
Cc
0.95
Cc
1.43
Cc
4.29
Cc
0.05
Cc
1.19
c
0.95
c
1.43
Cc
2.38
c
1.90
Cc
0.48
Cc
. 2.86
Cc
7.14
Cc
0.48
Cc
2.38
Cc
2.38
Cc
5.71
Cc
15.71
Cc
0.05
Cc
0.95
Cc
0.48
Cc
4.76
Cc
1.19
Cc
0.33
Cc
0.71
(9)
EDS
C
Cc C C
Comments
* On Screen Measure
B = Bundle C = Cluster F = Fiber M = Matrix
PC = Chrysotile A = Amphibole SC = Chrysotile AM = Amosite CR = Crocidolite AC = Actinolite AN = Anthophyllite TR = Tremolite
= Non Asbestos
NFD or NSD = No Fibers Detected or No Structures Detected
D PROJECTS
Page 45
MVA Inc.
SAMPLE ANALYSIS INFORMATION
MVA Project # Lab Sample I.D Client Sample I.D
Instrument I.D
Magnification
Acc Voltage
1810 G0976
JEOL1200 21,000 120kV
Amount Collected
0
Amount Prepped DIRECT
Filter Area mm
385
Filter Type
PC
Openings Analyzed
10
Grid Opening mm2
0.008
Analyst PF
Date
5/24/96
Comments
Grid
1
2
Opening
G4 H7 E7 C5 D2 F2 C4 A7 F4 G6
Structure
Number
NSD NSD NSD NSD NSD NSD NSD NSD NSD NSD
Structure
Type
Length m
Width
um _ SAEDfi
EDS
Comments
* On Screen Measure
B = Bundle C = Cluster F = Fiber M = Matrix PC = Chrysotile A = Amphibole SC = Chrysotile AM = Amosite CR = Crocidolite AC = Actinolite AN = Anthophyllite TR = Tremolite
N = Non Asbestos NFD or NSD = No Fibers Detected or No Structures Detected
D PROJECTS
Page 46
MVA Inc.
SAMPLE ANALYSIS INFORMATION
MVA Project # Lab Sample I.D Client Sample I.D
Instrument I.D
Magnification
Acc Voltage
1810 G0980
JEOL1200
21,000 120kV
Amount Collected
1240
Amount Prepped DIRECT
Filter Area mm
385
Filter Type
PC
Openings Analyzed
10
Grid Opening mm2
0.008
Analyst JRM
Date
5/23/96
Comments
Grid Opening
1
F1
G5
H8
B6
67672
2
67672
67672
67672
E3
19
Structure
Number
1 2 3 4 5 6 7 8 9 10 11 12 13
Structure
Type C
F B M B
COFRO ME
COFROOME COFRO ME COFROOME
COFRO ME COFRO ME
COFROOME COFROOME
Length um
2.4 3.3 8.6 4.8 3.8 4.8 4.8 1.0 2.4 3.8 2.4 9.5 1.9
Width
...m_ SAED
2.38
cS
0.10
c
0.24
Cc
0.33
c
0.48
Cc
2.38
c
0.95
0000000
0.05
0000000
0.10
0000000
1.90
0000000
2.38
0000000
9.52
0000000
0.10
0000000
EDS Cc
Comments
* On Screen Measure
B = Bundle C = Cluster F = Fiber M = Matrix PC = Chrysotile A = Amphibole C = Chrysotile AM = Amosite CR = Crocidolite AC = Actinolite AN = Anthophyllite TR = Tremolite
N = Non Asbestos NFD or NSD = No Fibers Detected or No Structures Detected
D PROJECTS
Page 47