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Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTIFICATE OF ANALYSIS Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 September 29, 1992 Customer: United Technologies 800 E. Plainwell, MI 49080 VEIA Product 5415 Railcar No. PLWX 44281 Attention: Quality Control Manager Order No 0016359-000 Ship Date: September 25, 1992 Customer P.0. No 11214 Property Test Method Specification Analysis Moisture, % ABR-1A 0.3 Max. 0.14 Hard Particles 8 7 Mins. ABR-12 25 Max. 2 Contamination, BLK/BRN ABR-5A 35/100 Max. 4/ 5 Bulk Density, gm/cc ABR-2B 0.460 Min. 0.496 Brabender Dry Time, Mins. ABR-7 4.0 - 5.5 4.6 Particle Size Distribution ABR-3 % On 40 Mesh 0.1 Max. 0.00 % On 200 Mesh *NDS 3.8 % On Pan 2.0 Max. 1.9 Specification is 15.0% Max. for the 200 Mesh plus Pan Residual VCM, ppm ABGC-26 0.2 Max. 0.279 Inherent Viscosity ABR--10 1.00 - 1.04 1.02 METS IR, % of Control ABR--13 95% Min. 131% Laboratory Supervisor (601) 369-3624 VAB.0001202391 Vista Polymers Highway 25 Aberdeen, MS 397^ RAXLCAR ANALYSX 3 Load Date: 2,5-92- Product: Car No. : Time Logged In: Logged In By: SIlo(s): Ship Date -* _ Order No: fl6lk3S*?-QC>D Scr* e' 'en> * 4 A* nalysis Me6h 40 Weigh t Q.<0 X QP 60 80 /-OO A\ 6 JU 100 120 /2- OX- / /,j-*f 140 3-97 200 /f/ M.6 - 23-- j.f Drytime: Static Flow: o / g-3 Avg. Mi crone: Color L: / 0$ '~?tf 0.0^ b Pan .75 * S Technician: METS: VAB.0001202392 WWMtliMIMf Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-81 1 1 CERTIFICATE OR ANALYSIS A Date: August 20, 1992 Customer: United Technologies 800 E. Bridge St. Plainwel1, HI 49080 Attention: Quality Control Manager Ship Date: August 17, 1992 Product: 5415 Railcar No.: UTCX 46504 Order No.: 0013800-000 Customer P.0. No.: 11056 Property Moisture, % Bulk Density, GM/CC Brabender Dry Time, Mins. Particle Size Distribution % On 40 Mesh X On 200 Mesh % On Pan Vinyl Chloride Monomer Inherent Viscosity Hard Particle e 7 Minutes Contamination, BLK/BRN METS IR, % of Control Test Method ABR-1A ABR-2B ABR-7 ABR-3 ABGC-26 ABR-10 ABR-12 ABR-5A ABR-13 Analvsis 0.16 0.512 4.9 0.00 4.8 1 .6 0.033 1 .03 1 7/ 2 125 agwel Laboratory Supervisor/Lead VAB.0001202393 Vista Polymers Highway 25 Aberdeen, MS 39730 RV C RAILOAR ANALYSIS Load Date Time Logged In: _ In 6 d Ship Date Product: Car No Logged In By: Order No !% oo - ecD Silo(s) Customer: A* Compartment A Sample From Bottom Top Moisture % . /3 BL Contarnination BR 7 2- Bulk Density / 5 Hard Particle 7 Z / 00 Viscosity RVCM LOU Bottom Top .tf $ <-i ,C01 C 1 Bottom Top ,/f 3 2 r Bottom Top ./d s 3 . Sot 3 3 - Screen Analysis Mesh Weight % 40 6.00 0.0 60 2JZ* 2- 80 //.AT J7. J 100 -29./ 120 7. > /!./ 140 J. 24" 200 -2.V/ -0. 2 Pan . 79 /. Drytime: .1 Static F low : Color L: a J f.Z~ Ave. Microns: * b /.// METS: Technician: VAB.0001202394 Villa Polymers A Division of Vala Chemical Company Highway 25 Post Office Box 91 CERTIFICATE OF* Aberdeen, Mississippi 39730 Phone (601) 369-8111 ANALYSTS A Date: June 23, 1992 Customer: United Technologies 800 E. Bridge St. Plainwell, MI 49080 Attention: Quality Control Manager Ship Date: June 19, 1992 VISIAProduct: 5415 Railcar No.: UTCX 46521 Order No.: 0012624-000 Customer P.0. No.: 10948 Property Moisture, % Bulk Density, GM/CC Brabender Dry Time, Mins. Particle Size Distribution % On 40 Mesh % On 200 Mesh % On Pan Vinyl Chloride Monomer Inherent Viscosity Hard Particle @ 7 Minutes Contamination, BLK/BRN METS IR. % of Control Test Method ABR-1A ABR-2B ABR-7 ABR-3 ABGC-26 ABR-10 ABR-12 ABR-5A ABR-13 Analysis 0.12 0.508 4.7 0.00 5.8 1.7 0.002 1.01 2 5/ 10 12 (M Amy E. Bagwell Laboratory Supervisor/Lead VAB.0001202395 Vista Polymers Highway 25 fyu&T Pta7 - .t Aberdeen, MS 39730 ^ O irtUeLj^ E=>VC E? A I LCAR ANALYS I S Load Date:_ Time Logged Ship Date:_ Product: Car No . : Logged In By: Order No: & 0 I'24p`2J{'~()Q.D ( Compartment A CA CB B Sample From Bottom Top Bottom Top Bottom Top Bottom Top Moisture % Contamination BL 4k ___ BR If JL Jk L /? Bulk Density - . 1 .12. ^ yT L. A *. /-3 // z-__^ j 1 1 __V ^ . * /^T JO js y 4. '7 LK jj ^ ' 5 Hard Particle 7 Viscosity RVCM ... _ - _____ . ._ 1 Screen Analysis Mesh 40 60 80 100 120 140 200 Pan Weight _________ _________ _________ _________ _________ _________ _________ _______ % Drytime: Static Flow: Color L: Z b Avg. Microns: Technician: METS Z /o VAB.0001202396