Document 8kgb7kG7Zwveord2Np7dnEna

RarEermencaioay SSUFung M27i03n5e05s, s25M 1Catmeoorn R: 6 036] THO SYTEUADRYOORFALFL(UDOIRETO)CHETMOIXCIACLITYFM-/39C2A4RCIINNORGAETNSICITY (RIKER Experiment No. 0281CRO012) Conducted During April, 1981 - - May, 1983 Volume 5 of 5 RIKER Laboratories, St. Paul, Minnesota Inc. / 3M Company 55144-1000 U.S.A. -- 002312 Js Er GRAAGTIEeT)omTOaR-ONIC NSTTUDIYSOF 14F-33E24e8 Toby's Dares 2aisez FCS-e1s4i3croInNizRATS . : LS5e0abNtuneEnEnRa"Funr0e-"F3no4nu6ie.e0S-e3e3s8 ezsomans veer. 40 sFpoeuse 015 sreasrceo1n5 A 2 eve + FTRneoaosrns 115 ws fitz al sE ess Y c &4 Seer i F4o3ownoeane 115 ess o WES meses ome se h81n 1 [psrreecesigoes Flin 113 E SaIfaolconad Eon Dd Fuathoan e1l15 erBremsEL11 Hp iosstiteeg115 ibis ei MEHeteEL1 Ey rHLuaoisetaheter ntiisf pret mEBEeEldoOfn i leHaeasealwn wfsf Futian 115 mMeesss n41 HeEon irMweasEtoLrEe Pious 115 Wi esda5 sess i ikoviie 61 Mae d stpkogsraisoiserkv11]152 Moma mMHoiEee 4on mE a Fiifriaesdinneen eaoai1sez od 1 mHmeiEoLQon Mek nm wMiiSEaazsaoNsz eoTias LR fal MEHPeRaaC ooin Had pFfueemslem1hi1i8e RET aE EmSEaNngion Sed Nhoorv. o&n STUY ss aSWses0E1592 32B450e.53n 0WaEi 3Mm67ee51 HEHeLas HEFiEEe F3355i071.5008 d336E65 EEEE aEzzaee 3636016.6as3 ES3325s:te&a2BEST COPY AVAIl fBWeeanat peEieS Sh 5 m8 E .oy327 002313 rmrpooaassmemiwasi mama HrRERsEECLBomh ma i ppLpdeoeaesssmeeepersra REBHmEiEEReCCAC bOiL EE 4 pemiToamsmmeiaorie pemens . EBLO msc oh:3db BEG mpesepepnereasa:r Gamer BeBMEExETcC o4h oh mE 4 pppppeeooensewnmnmennnsrtr mmEEhEEC Ee 4i bh Gmmpeeaamrmemlasa smear EMmRREECC i1O4L EEC ESTmimmoan . BamEeSS:1 omppnmaezemrenaewsls mpm mRmBBeyEEAsoL LLO344L Fa pmS ega2 Tusa . eBeEs mez iiO:b mpmpmoaemsmemeadesss pesrar WEWSEEE0EE.C0Gb41ohh pEHpmememmmomranesrsr EBmEERaECCdL4 pena u smFEeSrEee m WEmisaa. EB5BEus3tH smwmsEga mmBmEyEz EEEohHx FnmErauEE ne sEeR swsssii08 2oEGaigs s=Weea5 EEEodi8] mtmEsE 002514 . 1328 in ERE GRALIET TONG STULY OF FH-33EEse8eFCe-z3s4i3creToH1zRATS ; ToEiCHeUICISEDeNAsTEI6NIeTI2nAvaLicSzt/e5cLIS - TFlaEn arBeE sFUL2LpPouscih JR 5 SZGORANS wei a0 Fe1oroopabarriasrne 1eB4aa%ss iirRoRuarreSes 084s3 FLopaarasraere ipoara 1o4i5s eas Fopfseratuooreesz ev1s4iss pSfRaeaari rcesd ebeiitf pFioRroanderaever i1e4an5 FrLoeoondoiririeeses oo1ii4ss2 FFoeotaimre 1EEATTL e14a2x wad SFrOnOicRrEs w1i4t5 FRooodtTeTr iF6sTTa C1a1s5 nak FSFopoaniatrreTses e1a4t5 bis FReodontre? m3i4ss p FLroaoiur rIrke ef1i4t5 FrfFooaoaitrzieeedn oc1ia4ss2 pfRoouirrse:z Foobar eoiiss 145 SreMaarreess Footank Goaaz 145 FrPeooansrtiseee eis 14 SFpoFooravareees 1h4a2t sFBeieE es 44 as Giesse oe4 Z5i7s.i3e4s Seda 0ca14 ca EHmaEirEreIa Sererrs Jeiz2 14 4 JiSegsesoi a4e a TGfoieuereero 41aa TEece ive 4aoae ZTiieerh 4ae EpoERa HE 4 ZSNeHeaErEss4ae EF Sers r2r o]4 eSesitez ez a4e 4 Sfeanns ozo cdae a S ZavEze Leo 1ads D Sfeei e0 csaae eSez wri a1a oa Hjeirte a1a 332343.8425 f3eirc Zoi s5s8 21355073.316458 2F7e5 57 eSee.e aves 3SS0o62a8 2o52ra SpFreiiree Spreeog 7s Z3S5hi6enee2se8 saes eSeerm 3S3h45e.8753381 S5acr 6es 23604257 S3ee5zi6z2e8 vsea ZSeiae 357 z24e =< BEST COPY AVAILABLE 2Saoa7 33364551352880 - Ez67E13 .1329 356211 002315 pFraoroolaTisare 0a: 145 WJseeaEer oA4ow 338430..2274 F36rs 16 FSieoRooaiaerraeensse eeda:: 14% Reiss eis loEezaE0]41a 302650 4 337961256 302.63 . FuGaCmIaREs fpouree 3v4a7i 042 SIlEeEe oa 4ae 4 . 3a2m8ie 2s6e5 1223 - Freoaorn o1a4%t iSrraouairza:s oedis ZSeimaarz co 4as Seexnosn: 44 Spornop3ee 254.05 FioroaraIsAoer roacer 18445% eas Siemrs: Isis cae4 a SESE as 239715.8517 25757s18 FiOrOoCsIzRaEz 1e4a5s Firoooavzaen:e 1e4d5s SSsicearcoc ies 44 as 335466126 371 6% FiRoRoaGrasBToRsE e61s44s55 rSoazesso0 SEE 44ae 235072.386 Ses riRopuacsea:s Fools 03423 145 sZSmi1as 0 Tees 44ow 225591.1351 3r2e6 6e1x FiioRRoooeaiIceReeess 0ea4s5 14 Spoutic eas SF Seiarr es cae4 ido 4 326634 6715 266 FioRogractialk 1e1a%s SFoug: eas SMeedza csa fiers 334706 2146 ESnzees RITE Gus dee 4 Fipoaioztna o1u4s5 IRpezas 042 Hssseoas 0 Bile o1s9 4 Gres ae i65s.2E8e 3fo168 FRopuirziies a04s3 FRoecazIRiE 1e4d5 HSooi Sie a44e izoz z16e Sie sn Fpforeoosteishmirecge1e4an:s GPfeEanEiiRsi csae 2314721354 pSreezg Fiopopniazaor ms pgaszy ons Haw o1d Zeeads SSs$, w36s1.02s2 Zs 11 Frooaavcceze e15z5 1s 339.42 rapaaaacczad: Foo0IRE oessss 155 0 GBioess7 eccS1s 53650..5757 3r2i6g3s5 FpiopacoeasTzazees 5555) 152 aagzr eos 2SS5ia0c.se0ss000 1s Sess cs 2S5i0e 0x BEST copy AVAILABLE Son 57 FafnFetoaaursznzeeEs 152: ons WBEimeeE rr 0E51s 1ass eerx 366.04 - Ise 4 FeRoaoaeuciaease c1r%o: SmeioEaenrs19 eJBae0N.E2 1333 0 iFaasie eos FEE 002316 N cpoeusrtaNenEe appeoecameEsrt Femocooone wssle: epEoeeaeneeeee ppEfmoeeeerwBsE pmeems sppoaeaeerzeosezs oppnoseesneswseos a pmoesa seee: epfmemeainat mpmoeeensaia Epfaceemesir rppToaaseswvsanreoBersP ppi eele pEwmaerilvtE pmmeeetaaas mfHoeediarstosts raHpoaeemseSesE omuersmoees msEemSet3ab mm HHREETdC bdE3L HEEICE 3% mBmmEEG3Bb REmEEE 3Bb HMMABIRCCREBb IWmMHesEC 3 OL BaMmnERaESE BimiINRLCC SbOSs EmomiNai OB M WmWRGnEC LFod mHHeIHzE HID 0OOSSb MEWECEERDSod EmEmEuNEESoobb EMWLEREELGE HmEEERELCSSOB mE ob wBEzDS 002517 5n=65.ee33 BmBmiruee. 3 4 HS s=wiaem enFPoeyus wnsn wmsrseE62 FiWaEE. BEEweren = mBaE owaallah wsaizeeze nSw=sEe E= BnnEe mEnaxx EEm2eEe= BESTCOPY mFRoei sfent2 AVAILABLE fp B FLiOeeOiLaiIesRrtEs Fone 1oe6e:s: dex fiFrrocaaoairrss oo1e6es0 F`swUiicEre 6BeEF FSSorroaatricaremrss 4oo5ec5 FSSrrooaoascszsee: go3ost frit sFSorosnoaucaemssn oeoisss iiFRhooaaustscaeeessn ao1c0es2 siFropaootiuaasrcees o1ecei:s SiFRorocauczgaeenese boieec:s siFrfoaatasizcnseess oaoeeess SrFraoaioistceied:e oo1ec2s iiForoonunacgioenner oe1s5e:2 FLipooamauicneiee o1o5sc2: Foiirorooouineessr 1oo6ci2 iiFkoeaiaatazazonnre oe1z5zs2: piForFceakvsnigonees e15e5 iirraasazoonse Foouiee ooeess 15 Sivooriadtsanssnr oe2ce6xs2 pFiohrtieeaeacntaeniob1g6ees piaaissitz eeess 3EG2e1E6h2o oeo1e6 p$wregetai e mSRRE:ous sFGreReeer. ae = 3Mesgo ioee W HEE E as s5Ha6sessac.sas WE saves :is sFEreeaa 6os EEmEsaRos.oike spHreeeE s ke WWFEEEE im Hasza eoosie FE HEG oV sie Ge Seisoc soas e msHnaeo ooifse aSBirEsc dfie E Sfieseooie i E SiE hhE ode pmHeEE s ooies 3F01R 5 E 002318 3Sp2ir1e6a2 - sp3e%ed5 333253a.35 - ecaisee 3i365s 8a52 3 se ear5ea]se 3sis0a.2e4e3 36s96.2a541 e2Bleasies 2insienea3 FAprEEes 7EEaenas pFErreiga 3Se1se5is EEHeeae 3nree7gs 3i2E5 322 & BEST COPY AVAILABLE pzSaeihta HSfeesaEos - 3F60.E15 1332 Fipoeanessee 4es2d5 sGoorrees oae e per apor 7 pSeirarz Fiirroaoqinasiiese eo45ie5s Foose ae Fm Seeare re: .ae EEC ae S33e85e2e7e 356 TpFeoraosahote cis sez pve EE Eho Eo.C e Heoe. 3$di5e527 ass iFRroanEitsazEne To15e5 ee GSEnC aoe Bea 002319 - 1333 TW VERE ORALACIET: TOX-ONE STUCY OF FH-I32S4ve 8wFCO-21a4i3cRoInNizPATS STTEOELOCRHYOUF'ISCIBACAANTTEEISNI&TFI2EAM5LAS0L:/E52 LS R TETGHTy OF FULL FOOL TREE ASoneRns veer a2 sEPAaeTs0s4esrs 01s ois Fioroatsisnrgz 101135 Froosnotneg 1r1e5 Fiirrooonastzsetesns 0o11i18s2 iifRapaacset:z ooiiss FLFooounsicRae 1ni1s5 FFaandoess 1n1i2s FiIPoranaatisestsre 1ma1ii5ss ripaniasseess oaiies FiFonnensIaRnE 1bi1s5 FIaFnRnaianrg p1i1s2 r 1roatsas ois FiOFOoDusIaRsE o1i1s5 F1oro0naisnaes 011152 ipPrasosate pi FoirpanaiegssTesesee 1na1ii5ss FioPoanaIzRnRg 1ai1s5 FiioFpnaooiaIczRonesz b01i11s55 FiOFDaO4IcA0Rs p1i1s5 1iFRa0i4Zz00ss o0i1s5 FiDnoeoneanse 1a1iss 1ERFT0az0er ois Fiopoooalzeees o1i1s5 iFRa0s ais rouGseseseeoasiss 0 1 1 Sraamso o1n lBieear. 1om sSuasmeocI1d SSiedse.011 w3i7rge.. oam SFarnea o1n rBriarse.c. 111 BNaeaasno 11 Geizsmoo11 rMeasszroc0 o1111 eexaess o1n dFrsiess 11 Gd7reaec srs 1111 eeSea7sses0c 1111 ESeozer. 1 sGdiavsssoezso 1a11 iSraeesrsaioco a111 EZeCaR. 1 o EE a 1pnaGsoaratonaris 1 ou d3eErimazcocod1 ees + cor -n20o5r505O4u8 stub pseerrie E5r0e 31 : aS1e0is7.e2285 5ie8s s37a7r5es EG0a3 ez 52283727.128673 Hsiazaens 3E67e.2)3 gEseasro2r7 5Se2s.l8a8s aIosL25 23p357r8. 4081 3ESo6s6.p7a8e e5028013 63E1c7d.5d8a 33756a17 6=aa1 BEST COPY AVAILABLE 2Zo8e0 5a3s ES na0ors07son sTuoy 736.03225 13324a 002320 iLrofFnoaeuasiieisrn ao1ii1sss WsEreeedeso 1ooqm Ho0i0ie.sn0 Firoeoictiez s1i1s IFRALs ais 3BS6reaermee0 11om Fa26Ec7 s6s Fronvte 112 104i15 pis EsFrreaee.oO1nn e3E7aas iFroenstcetss s1ias Sraessco ooam 3S4r5a6 Fpooetee 1r12 poate mis EmE1 Iz 1 5336421772s82 FiFoRancies 1a1i3s MFeasroo o1n Fsams7s2 FpioFnaro4Icsezeo pas 115 ZTSaesirdaroo 11 on 30087a7 35sse TiiarFoaseczezsz paiiss o MSeEaEs oq5o1 fEop) I1FFFoaaoaiccszaeas aa1ii1ss5 eBarsaancc 1on 1 Fmrea 32 ar iFaPcaeastoee a2i1ss Fhraoc n HZaar d71 FioFnRoiacnaer 1aias Saseeic o1n 5azs 02 FiioRPooaoarcsrises p1oi1is2s EsEEen-Rs 1I 23365655.27228 FPLoPaoodoscizinilen smaiiissz sDseciaasncc 111 sZeoezee2icn FRioPanaoirsaase 1mb1ii8ss BGpaetca o1n spirreae7sa : FPioarndaeicgzIease oBiiss 145 EfSearrEss Rc ,11 o00rm78 er 1iR84zs os o wees 1o a7s.en Fponrtaen 115 smeez. I1n a31o1s 232 iiFPaniucsaass 6a1i5s Psreez. 1 1a3zo. e2e7 FioFnaoaIcnaRn 81115s JBeratcs 11 F357aa2 FoopaAR n 518.30 602321 1335 Tia VERE GRALCCIETS TON-ONC STUDY OF TECHIE IAN INITIALS FH-352r4 s6 FCo-z1e6a2croInNisRATS FSToEOoXOnRYo-FNSUMRBDTERERTCES.<S0FE-2N25A36L6/E62 : TEIHT OF FULL FOOL JAR:S saokns weer: 42 FisFooacaacrrnsse: docesasss Ffiorroanniiarrntsete 1oau4es FiioFFootiuizenesen 1oai4as Fiiornoaaninrieen:ze 1oai4as8 Fiikroanoirtteeess a04i45ss FiihFroaataaorrnseere 4ooasas FiioRroootaaarzneeese aoo4is Friorooetsorsnrkat1oe4uss FiiForocoatararrnrses 2ou4is2 FiirFooiosr7tsrets 0a4445ss FiioFgoautsrarenr:ss 1co4ausss Fifrorooaatr7irreee 4adscss Fiirpoaanaatzreoesre 1oo4ee5ss iirroaaarreess ooiuss FoiFoaorseesr d14uss LFipaoardareeesns a4aesss iFionFodutuzecere.nr aaoii4s iFiFrooonaar7tieeos i4ais frislrg od JEmriraez.e a as Sieee assc doaa G HeraeE es.c 4 a GiZoaEe:E: 14a aF0r7n5h50 a ie FFeaseleo daas losoiaveda.. daaa ESe0se7es daae BSaeerdca: a as GJprEeeaagsroaoa s1a Gasoiaarc.0 1a8a leuesries... 148a EE azzas 134 E FieLroSa Sa0eca:0 114 MFmeeeamasocadde fWeireemr. daaF S SSoseee az 0d1as War 3H252i22 de0e2 S23e52e2 ea2s ar25e5esec G2247e1 ea1c4 a2300e76.2s535 33276255 7050 2F302r05 76 55 7 f26ad& 2228a7ean e334355%7ae7s d32e65as 54a 3236557a76 i 5215.557 E3z21ids27 =a:e J731si 5032a2 BEST COPY AVAILABLE Zp3o7rro2&s ; 3"Sei%ee oaorcr C1336 iE ozs FaneIRE AFea7az e1a4s5 dsseseorr 0 a44 FpoanneeIese 1e4a5s ieniras eas deesrz0z1 0ca14 rer 0 4 . ipaoraRs aeass iveirse 0az a33041.10z4 144 2asiez oa F1oFnoearAarr e1a4s5 a2ea7z.730ac 1a4 11F0o4a7T9e5s 0044%s zse=s z0 44 pFOansCIoRsR 1ea4s5 esezz 7578 00 4a4 F16O0O302I0R1E 1ea4s5 a2o8s0.0470 144 11rFpaasczoorz eeaass a32s5s.e0s5 co 44 F1OFOaC4IzA0Rs 414s5 232e87..2150 414 FieOnOaDcIaFsE 1e4a5s G26eae6s7 0 144 i1RFoaazsoasr eeaass 226612.3240 44 1FoFoaraIzR0Es e1a4s5 3a2047..3204 0 414 F1OFOaOsIoAsR 1e4d5s eZoes 00 a44 i1FFeaizs1i0t e0a4ss Gzaezs1a07 a4 1FFoooaDEIA1R2 1e4d3s 335257004s 0 414 F1OEon0aIeAsRz 1a4s5 FnRa4zEiLsS aGass Foo IRR 145 1pFaacaEt1s? eeaass 1FFORCa0zIiAsR a14s5 FiOFOo0aIcRiRa c14d5s 1FFOpOaDIzAzRe eas 11FFooaacsazzy eessss F1opoeoaizA2Ry 105555 F1opoooasca2ra e1s5s5 1paaces ess F*1o"0oN4Da6Tp2AzR6r e10s55s5S F1o.n0o4I6A2e6 1S5E5 iFnpaacsaz0s eesses Foooire 17s 1sFpeaasnisz aessss T28e5c.1o4 0 144 d32e2c.a5l6 0 a4 Ire? 0 14 saag2es o a4 33m2m40e11 00 414 a2z331e3s6 a4e 2854 14 27070..6613 55 3s7e4e.e6z0 515 3a7t4e.1s4e 155 34038 0 5 de30e348.5779a 00 5155 3a64me44 535 e37axeatc035 ae 20 15 mezarc0 35 13805. 0077 d30977. 0232 30374.7074 e112 - 22e075.182 0a38 271 239520 5777 228988.7087 a22o5s. 046 339575.185 229684.6278 240691. 2551 20672..3344 237304.331 230858.513 329457.4047 327. 08 329c8.1041 336252.5a61 37187 a2x2e2.8287 332745 0811 422431.3685 2834 - 438797.4813 326608 8623 13704.688 337440..1348 e30x4.5897BEST COPY AVAILABLE 433156.0728 33764a aaa1 0262238 - e 62a38 - 1337 002323 TPmforRamosEsazGe Thmealeimmetaa mmTeaaaamsrlcaekE mem m mesMmoErE oGesEr Imimlaveemasa maDmeecaeerrnne mGDeeRnReEsr rmmwooatEwiaors Erm moMtEEiEEr m Er mmeE h Er Dem E mseGoeseesmseo eorzs mmmmeeemmne ees LmeCoaealimsmratar mTLhieEeegIsssAE mEem smoaimnis ass miEawIaarRie di5ss HWmmEEBED OSodff mEdmaEEEaC 2 8 mE 0b mmmmaeRnnml h8o3db W wmSEeSRnSRsHB3OS HMEHsEHas3 mEREnIC L3GS mSmaSmEEe L33k mSWmiGaarPldk3 mR ok EHmENECC 3OOSL mmNamEaRhrC 3o3sb mm mmaEEac k38kb EEEBMEEEI S33on EmEEuHEnECCEI33b EER mEeEsiLc Sos 002324 a=ewireEae . 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G02363 phme ss mE Od : BEST COPY AVAIL Fn itl bane nen 002364 EFsoeooeoslcaarr os 11s iiirnreoiecuies oi1sz F[oe0dtoer a0i1ss rosaee?s e6seo15 sresssSasodlbeeisl srescaacSseE6rd1C5 x a oe + 6HpOiTgee ou stu 11 e160 + <hSe1toiou stuow a oz + h"oreazoou stuow BEST COGRYPY AVAVAAIILLAZLE 1479 002365 THO VERR ORFLCOHUTC TOX-GNC STUDY OF TECHNICIAN INITIALSS SFHH-352E4x'& W FCo-z1e4i3ckoInNszRATS TSOEDXAYOF'SRDATAST.ESSF1EM2A/L3E/62 LFEOIOGMHTNUOMFERFULSLDF-O3O3L0 JARS S0GRANS ST COPY AVAILABLI week ez 1FArT047SE 045 aR047eEs0o4s, 4 0.10 oNOaT ON STUDY RFAoTars? ass Roars?Sooids a ox: NOTosOu STUDY FioRcaoilresrs 1s9a5s 3Zeso0o4s0 a4a Ses. 0s iFoRoa0iIrAsRs a14s5 aemseetz.caea 3h66at62 RSRAnTi.reo ass prsta eg+cs o ees oNOzT OM STUDY ERReTaTer eas 1R047EZDoo0:45 a oz 0N0aT2on sTuow FiRooniTeese 2114s5 0Z1o6c4o 414 Sos. es iFArTaires 84s 1raa7esGoais 4 ea GNOeTrOn STUDY FiiaRrnogosarlreeesrs 1bb4aa5zs SSpri7iz0e5d 0 1a4 0lsa7oz.r6e5 FiioRRoepoaarreeekrs ab1sa4sss S2S62i247e710 4aaqs 2e824577516 FiRRoooaourzTeeessk pa1ai4ss5 ee2i5ac 5s 0d41s 2S3644i2.a5685 FioRooosa7oom 1644ss d37e5s500 a5 36507.584s FIornairArRs e1a4s5 l357c.0s4 424 63567 67a Rir0as4rr7z d0a4ss ZSeeri3ess 0ca4 2Se6r6. 3365 FRioraoa4oa7ri77e5ak b1aa4es5s 0S7sc.do5ec5 0ccaa1 3pa0r07.51 RFiARoTooabrarre b1a4s5 1R047SS7eo52di0ss35.0 14 0s N5SO2eT3z O4in5z STUDY iRFAkoTao4or0lrer 6s 14s 1Re47S7e7oG.o82d335 0caaa 6.04 5HSeooT0.4O2n2 STUDY A1iRRT0o4a7r7rEs B64ass 1R047e7r5GeoGssas. aa cos c 3Ho6T7e.s6O5u STUDY . 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Ee AVAIi LABLE 143% P Pa E FOfEoroNoiMosEsiscggeed m pmweeemR sEtE pWeEEemESaiE Tmlhoeehemsetse SGeueeentee:r mNmeeeesete EpEeEealr im timgEi heeeetelr eEmeEreRaE m mTeHneEe emTeememae wIfihoeet rs8s2 Tmm DoeisamsE maeirrE TumTeemeiee ren maTieusalem erLeLeewhemnionEe amFeoemmmteet Elbe ase sourT s isawe neon arenes war :B W mRMELodlofb EE WSMLEEEC:LdOE E R mwnak B dd Iemsealllloifk mW W =neE.ldRdod B meall mmdmeaudesldod HmmeEEldod mW mmepaElllBld W mmMnunEloBldi srevSmssRtFElSI35 d1s cos sE mmmEeuR.CB do:f wsmeenea.. i: B wmeisBc Bfod rosE "eCsUSn5ELC. oLd woes sroseE Biesen5En5 dLdf oz TEES ws 002368 oehaedt ou stun Smaae FEn=reeEs i da iFomrga52 BEST COPY AVRAILLAAGG:LE Fanwainnd] nFFoEeau fG=womdaa nSsiaeea emnmayee nFwaeo Rpseeegts BdpfHeEa mPnRoivEeow stow : wH=syeia mnmweaee 3=sh%oaiou stuow %SEwetgn on whobuow sruow 1482 : i reFeomeasmee roseszs aE asssEoeSsis io[rEnhoiautEeeeiss EgsG5z: aseeamsesasa. f5|3ao FHolitpovirwec a5. 6se5: are 1s msirsee. is iiFfroieiod ssaim0e mmrweaamss.s. 33Is THeFersoettteoor 822 esse sroueTTsoo3ee5s. areas & os eco ie eiFroestdcros eetse aeSreiaasn. @6ie fioeresleSerrss bedeeczi aeammmesa:.. &ie Hfireiiresaotlees sW meieeEns.Edc ETirroereeslis soees tressseSestoneis. & ear hCihroeeisoicdet:s staeees CaWmSiEsc. l1ffc oiirrovistsee:s dooieis bBaemoreaasr.. &ie oiiRfooigsiseccss 1one5ss memimessee.. ie fffrroieissetconse mrE aess.ai6e i Fiifooostmieers eaae=s 1rodsTmaaseseorirss Mn 1&c ota + of FrESoionn ses snoacainsessni.s die 012 iFGrelaessoteom;z osaecsst Talireesosi.lfie EfHRSoeatfses oseesr sr0aeeSao3sneoee.s 6ie eer + irSnrcayaastsoss oes es 1n0saNs aodcs s 01 + Fsooasoisises Seoeeiis aswsmaseses. 6i6e FLHRoEooassnes saeess 1roaswshSeas6sc. 8ie ozs 1Re4500 BES 3027 6 002389 mM360E.E5E0 Wm5EH2 BEST Cop o wbSaebnne AVAILABLE SiEmeee Einiaas aRfoarg ou suey pHie7r1E1 FpSirea5 mfHoEa 5 wien hSiottdon seo sEaeersd HSFmoEE w5id5as i heotwon stow Rp$5He5 oHpohrteonn soy 6 fThoor on Stuy oHSleEesR hSo2l.on stuov SSsE mSh - eaons L403 330.27 1453 ' rom ses ser 1s 573 02 poBr i w se 1noas0d ois fae. or + ge RtOYee0ou suey [HiPoeeitisees pdofee Tous oe aEammreas. 8Le deri. f wE4i5e5 BEST COPY AVAILABLE Si wFlaiSroindoens eck ass protiel sros"sUEoSsE rBoeTs ae 00s HmoTeeaon STUY fe Fiworyooteer 6c3 aes fhe: ai 1r0aSs00e6 G6lecs fae ee me. & RSooe7T8ou sTuow pe eiFroooinsies eoas6 mdaaEmmaess.. od1 fmHgee iFEkoeotas:e doie Seemea s. 1e ESEEre iFShoroouistses edbeses RET mnFrsEeRc 150515 oes oie 2f5ra5 oes + Nor on tuo pfootiiiec de seni. ie mESdhE frmoovtinieel ne SE wy ras. ie 1roesN36 oSds E e.00 :EfrigE Hor on sTUOY FWicEheEses ow Sina 1:s we . 602370 = 1484 re BEST COPY AVAI_LA--BLE GHEE EEC : FOODIAR 115 Ser 37 11 002371 sox 37 1485 l . 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S 6S0GRANS veer 100 RFeoiars Gas 1604705Go0s35 a Gea Rares paz Goo a NeOT on STUY aFUO)UIRE 145 1RB4TETeeEas 14 o0 H8.O0T1on sTULY FFAaTerwie daz 1rearssGooids a ee NOToion STUDY FFoaoroIeRse o13i5s 1keiren Gas asissseszt 0 41a "oz 4 2s1s85e7z 6 Gz EFReTr0al pas 1R04760co0i35 ~eez noaelrOu STUDY, EFotcoonle 145 aFeaneSLo0e3s reataesy EE 14 Ger 6mmozou suv Sees IBeRATE Bis 1R047Ee3e0l35 Fouls 145 siese a ~eez oHeOT:On STUDY 1a sie 5% prrartvieasg pai 3s2e6i3s: 4oa Fae3 2 {LSpaormees 1g4a5 eZmeoenr 144 2p7e4 FTrooiorenr a13z5 Tzeecs a1a 5iz0:7 LPaereiss 5a4a SZeeEsdz 4oa s32z e1n8 : FPusabaznk 1B4a5z S saEt 14a fzrare 7s RFATeoaw r 04F 1Fe4TTLso0n4s 4 Sea NOT On STUDY F1L6L0CI4E7E 01a4F5 aso3r :ss 414 2s2o0s 3563 F1ORDECIITATRS G144F3 SEraear a 3aid57 FLART oAw T BaE AF84T7Seee0s4s 4 een -NeOTanOM STUCY 1EAFT047078 045 F1FOeode7I7nEg 104455 1EAETBaT0TT Bad F1O6O8O4I7R7E8 104355 AEaSTaT7E 04E F1aRcGeaITnEeD B14a5 RAsTar0es Gas FFEOTGuT0RE 145 Feariz oii 1F04775Go0s4s 32c5.e71e0 1Re4777Se0x35o Taaips$e5 R47E7 EBaRs 4"7b3e7n0 1Re47EDCeBnisc kaneseobzas cel aa oe 44 1s ee: 4 1a 6.08 4 4 "8.00 a4 o1 4 NOT on STUDY o32o871 HSO4T0 O5%n STUDY p r N4O7T 7On STUDY NooOoTtOM STUDY NoOoTzon STUDY oo 1572 603058 aLF1OaT0SE Gaz presenGee eo Nol on STU FEionun 14g INCEGeo a4 ee mo on STUDY EAErRAeTEsD Baats naSenl 44 #3EN10 Faat dw 143 FarWeise zBaas a4 Ger HaOvTe zOau STUD-Y aEfmoin EE EanesSe8r3s a eT HoOeTr On STUDY EAlbewr fas ARearErGao5zo ez HDTorOu STUDY EFoGnaeTdEaeE B1a4s5 GCoeza o oeorx FEAaTa7Wes 04g FearsCeexas 4 ee @NOTezon sTULY FFAoTneT0Re 145 1Rea7EcRoGcas as ez NoOTxon STUDY E1A8T17050 04% 1Rea7seseBziz 4 e020 NOTezOn STUGY E1AFTBaT0ss Gas R0473S1ee0d4s 4 -e ea 5NOT04OM STUDY pFortoeleve e1n4s seemazn 414 35o7zas F1A6T0TH ban 1ReaTsEGoGoas 4 @ee NOT on STUDY . F1oEmecIlTaEe4 B14i5E p43r3 xe 14 sazz e3s8 e RITESe Bas asiizeer 1a4 kaez e54r 1Ra0at75e7 0B4a3E aa=iesaa 4a33em FOaOrTEsRe B1a4z5 seisr:e 414 S0s3752 EPRToWa G3 rearsboosis ca Bez NoOTeON STUGY 1FOFGGCiIzReEn B14a5Z Ssai7z.aerr 0 4as Enrae) E1ARTeii0es Baz LFeazarRTBEas Ger NaOoTrOn sTUGY 1FEosanzeez 011455 aw%oem s14s 414 aSs0o5 s2e4 F1FoeaISIERLE 1G4a5s 3a8r7ieEss 1a4 437537 eess 11FE8aaiEz6eds BBaaiE e6 z oz 4 o2z13 FEaTsti0ng 148 pe 0277 a4 ez NsOoTs O77H STUDY FrArTv8eega peazosGeBtaso 4 03 NoOoT ON STUDY F1AFT04Z%er eas ReserG0G2is 4 ez HOTozOn STUDY FEOaOsCIeAsR b1i4s5 asseises0 414 464soz ws FpOrOeCsIeArFeg1e4s3 4385570%8 0 41a a5g 012s 11RFeBiEz110L BB4a3s aagsriEers 44 aasre ee7 PreeaztazeGsan apzigz 4Rt a353.5274 F1OROaCET1ATE 1o4a2z FeaEid O45 4ap7i3zii 1as pa) 4ao7n7.3238 az 68 - FRoIooZIAEE 1o4i3s ariereers 1aa a3177 oerx 603059 1575 JFrae rustsGooris Corowaes on STU Wontar wis He ELE Fost. 145 sisson pe SUsrraayaastaiss oa oi sxoasatcbRaTes s ceo [nies SEL r=oen stun 55a FrFoSaooioann Gut awoasSo baas d2 oes "oateo Stoo 0.00 prBprneven sesSsshieolieooos sez oSaeoTrrooim sTuow iJFRroesatirioaag81e65s02 Winaaoelis SWFees Ffpoaeircsedete 153 srasSiSehi5E2, Eas 06s aSaoT2r5on sTuoy nHprites I irescH HisE6E 3s, L oon hHpoLTEow stun Epprraeissttiygiegess arossEetGe05E5 Sof esc mEo7r6Eson stu Faactae 15s SE ws Son a ffsrrreessnztztasgoenss WW saEzESs psaceeig77 aiwFroaeetzsz on oss 1roazEiat 0Ee 5s, . s sez 0NST0:Eou sTuow neFioretaog1e52 srssFsEtEE bbs ooo 5HEoTHon stu SpiFaooscattioznmag o13s2 ESGEEECCE.8is LSGhaaEet: FSRoaaazime o1s%s E mEssI pEregnen riagaeutaa?e ons ons snousaS Etr0ae5 s oon ohoot:on stu rEiortwaultnee oaos:s praofmeons as aez SWoeosT on os sue FFikoraoaacnaeo 652 ass arassViSnEeoscsas o0z + oaNO7eT 5on stu TifeRaaeaattiasz ois ons pFSg EReC 3 coez ipNorst ow STUDY niet EE wa SFsrRaoaiaestaass one oss sroazSas 0oE55,ess oes NoSoat 2o7u STUDY FFpoarsriueinnge 355 1045E4E r5 5s,R oes + NoSoite ou STUD .. AFBasic cos vers sw eo 1574 603060 EFionne 10s JLrhavaesaar Si EFoiounIEe 155 ArFphaazgansn 0g6u2i AFoTouWiee 195 reoaiu 652 EFRoTnel6ne 15: 1FARTGaZ0T: 058 FFapdaezisnae o1e5s5 Fpraiteestonse EFoToel0re 135 1FAFTeaz0sT 03% FFoenaesatRse o1z3s5 1pFroeaszeens sii RFAoToviwae 152 p1RrGiaszta1egBtost FTDoWTRe 155 prersetye FooeaRe 152 Fpases ou rFAsTases poz F1FoiEnEgT 10502 JrRET 0 EFAOTDUTwAR L155 p 1Fa4r sT0 e 055 FonpIeR 155 pedSaheonn as GoEnAoEan A akgazGaesm eonos au Saonarsg keazGeonoBnos am Sivresl o=w treaswnize ozsie0 1m RassERoTot asze1i1nd ciss see5oais-0 5 praes sz 0 13 ReesesreeBnos asii7neeno cafm apsec22 og) reszseannae:os as seBroxo 38) Resswez4z. 02755 13 AsEEaoa70 o8s) Geraco 1s az az 5 rt Goss seseo0z5 155 prCoes os 1redssSsae6z3s 1s asemzazzes 0 5os ear as Cel M on stu ESyean Sees N3O5T0 o=n STUY a eza1 - Bez NdOsTs On STUGY 345ox 75 ez N1O0T.2o5n STULY 1c NOTenON STUDY 432715124 eseesrae e1 NaO0T O5N2 STUDY -oeo HOT ON STUDY assi7s o40o2:52 ex0 NSaOsT. O1n5 STUOY eoeo 77 ee: N22O4T. o2n7 sTULY 7as1s6a1r e111 sez 43 es NOTosON STUDY sesezen Gz eNoOT:ON STUDY ees -eMOTezOM STUDY saomza.3ze 376. a1 1FAFT0as07L oes 1Re4571seBxESs 63 C oNOoTnON STUY 1FOFDeOaIERTE2 015555 STedaeex caee 3208474&3 1o reaaEzrnss ooeisd sSerogee 6og EAT W ReaETd gis eer 0S0161es NOT ON STUDY. rFooeLIeRE 155 EAT 0 452.3o6z 1keasTs ees oaee eo e45e2 3 = MOT ON STUDY oFoaoslaeRse o1e6s5 aszietnr oi6e a502z57s7 603061 1575 aSehs ous Farookriie pvt oass EMFaanteo oes Fpjorriircsilenetgegaasss pFTrovoeie oact pfFrroioossttieitceyy saettt aFaaiaycdhse 3acs FiFarrraeete oes Frioraieostdiecees s1e6t5 rFraoedsiti b1e6ss iareeatiz ses Fhiwueaeeadcs FSSRkoaaaatteemss bo1os5t:s FrRaoetos oaees hisRriGeaaecziser booess EFiroAatsiosss b15i5s FBioRrtaoaelteoso os 15 SEinRraioantsez oss pFErorronweesaics FRooWnaohzTnise bet 16s nIfrreoosct:s bGeest prJFerovrnvitaged ses aed BEST COPYa RUAILASLE 00sveocr FA ood moaroon Stuy sit or aoseSnsPGosbnes ELe 600 + hgSoitt el on stow rngN SeEew 6 ez EaNieOThsou stu E psermeEL HSS2ie2 ll HF SEEE eE fi HfSreEes soasSsdGsbeoisst8 Gos hoSoeLrsEon sto 1rassEiSteEbnes, ae 60 H5eorTeodn sTunY srassetGSEbTios, sue osc N5oOToonon stu skaszazeosebecs oz aMzeoT:eon stu 1reasEioleEbres &ae oes chooaeara:o5n8 smu SLE Tie reaosmewss d15 "oox aaac en HOT ou stu SGLIEses is oSGeiE pro[S toERE 38 . 064 oNTz aou stu EEE presaeoengreAo oe 062 oNaOnoTi oam stow proveeSnshg-elas "oes aNseoTxsoofu Tow srasson0Goxois os ae oor oNooason sue oaseesGoorees e osc ohooorron stun presseensG02260 fac 060 SGNo5ev2zon sTuow 1r04sShEs EE 055 a "oes Eoa Taou Tuo sroasmie oa eon,cdE ole h&ot a on ster EEeSElesi 2&ue eEiesEen 157S. 603062 jFwooirortt0 eedaasde a Efabf oss aFTrihedee easis FrTihleytteirs ess ses SHpheraobuvid mHiaoousmesk m FMhbeieRmoe: TEMeeannriitah La fraAspried HELE a TUFREES ae sssaounseeisebbeiss aressalSGoo6io65. &ae ieasasLSvEaes .ae awossFiSOsUtR5eS5 i aroesmaEsEdiRs iL "E EVEIn NE S LfF HmEIEHS.CYGS sseisHztGEoios t& oor cer Sooo os cers oe eee con eworeeaon smu n3NoTvoon sor stu h.ooraon stow N3ooevson suo hHoraon sic i hfeeron stu SEEaeE FEHEaE pa HroEn sor 602063 1577 Stephen Biystner, DVM. Rose6v8il5e,RoMminaesAovreonu5e5113 Appendix Tten 6 21crReNI~ ol -- April 18,1983 MPaartvhionlogTy.-CaTsoexicDo.lVo.gMy.,PMha.naDger RSkaifeertyLaEbvoarlautaotriyon Laboratories S2t1.8-3Pau3l MCiennnteesrota Dear Dr. Case: OgnrouAppriolf a1p5p,1r9o8x3imaItepleyrfotrwmoedyeaorculoalrd being used in 3M study 0281CR-0012. eSparmaignuaetioDnaswleoyn arats All rats had their eeeyxxeaasmmiinnpearteivtoihneo.usalAnyteFrdiisioolrnateaidnnddiwripetochstte1r%oipohartthioaoclpumilonasercporipsoeergmweatnsot.uosceudlarto pAelrl tfhiendGionogds wLearbeorarteocroyrdePdracitnictehse in this group of animals namely a Alcatb.oTrhaetorcyhanngoetsebooobkseravsed random distribution of crsaauttpsaerrafocfitcsitahliiss kaesgreeae.tnTihtaeisrsenporrwomeabrlleemassogmeeibnugtchrctohhnaeinscegesaugvaeiiinntitswheouclaldseenssbe. oafnedx- pected in a group of animals of this age. No ocular findings cpslotueudalysd.e belIfetobI mseemaryvkendoawn.stwheart waneyre adidnidtiicoantailvequoefsttihoenscomtphoautndyouundhearve Sincerely, SStteepphheent BBrissttnneredDVdMim Associate professor Comp. Ophthal. 603064 J. 1573 _-- Animal No. _-- Contro APPENDIX ITEM 6 Two Year OOrfalFlu(oDireotc)arbToonxicFiHt-y3-92O4ncoIgnenRiactisty Study Individual Opththimologic Findings FEMALES Eve Comment(s) S**I1RR--44558843 S$H*I1RR--44650929 **IIRR--44662106 S 1R-4623 S 1R-4625 +IR-4636 00 ppm LLeefftt RRiigghhtt Left RRiigghhtt Right Bilateral Left ADtirfofpuhsye?corneal opacity CCohrrnoenailc souppaecriftiyc-idailffukseeradtiutlicerated (SDA F(occharloniicrisuvesittaipshylwointah; sceocronnedaalryopeaxcoipthythalmia ADtarcorpyhayd?gnitis Cpoarrnteiaalllyopaccoiltlya,pseednla(rSgDeAd), ulcerated, uIlrciesrasttiaopnhyloma, focal corneal opacity Posterior subcapsular cataract 11RR--44775668 *I1RR--44777965 *I1RR--44881110 +IR-4814 30 oom RLiegfhtt RLeifgtht LRiegfhtt Right AtOcruolpahry?gpacity?. APtorsotpehryi?or subcapsular cataract CPhorsotneircioruvesiutbicsapsular cataract Phthisis bulbi (secondary to bleeding **IIRR--44883222 *+IIRR--44883386 0pon *I*1RR--44590117 _-- NOTES: * RRiigghhtt RRiigghhtt PPhhtthhiissiiss bbuullbbii ((aattrroopphhyy, DPhitfhfiussieslebnuslbiopa(caittryophywith iritis RRiigghhtt DiAtfrfoupshey?corneal opacity with pannas iinnddiiccaatteess abnliomoadl sahamdplipnogssitbalkeenSOfAromvireayles involvement indicates clinical observation sign 605085 1572 _-- Animal No. -_-- Control **1IRR--33553314 S*+IIRR--33553498 *I+RIR--33556625 S**IIRR--33556679 *IR1-R-33557772 00 pon *SIHIRR--33772151 **IIRR--33775572 30 pon APPENDIX ITEM G Two Year OOrfalFlu(oDrieotc)arbToonxicFHi-t3y9-2O4ncoIgnenRiatcsity Study Individual Opthalmological Findings MALES eve Coment (s) LRiegfhtt RLiegfhtt RRiigghhtt BBiillaatteerraall BBiillaatteerraall PPoosstteerriioorr ssuubbccaappssuullaarr ccaattaarraacctt PPoosstteerriioorr ssuubbccaappssuullaarr ccaattaarraacctt DChirfofnuisced uyTeenistisc-aspeaccoitnydar(dhyptoopybolne)e;dincghronic uPvoesitteirsiorwitlhensmicorpoapchitthyainia CPhorsotneirciorsupseurbfciacpisaullarkecraattairtaisct Very pale choroidal circulation RiLegfhtt Diffused Atrophy? hyphemia RLiegfhtt CDihfrfounsiec csourpneeraflicioaplacikteyrawtiitthismicrophthalni **IIRR--33777665 *I*IRR--33778847 1R-3809 RLiefgtht RRiigghhtt Right OOccuullaarr ooppaacciittyy?} AtPrhtohpihsyi?s bulbi (atrophy . Atrophy involved with a mass! 10pom *+IIRR--33883335 RiBiglhatteral OOccuullaarr ooppaacciittyy'? ++IIRR--33883475 RRiigghhtt AOtcruolpahry}gpacity' -- *IR-3853 Right Atrophy? NOTES: * iinnddiiccaatteess abnlionoadl shaamdplipnogssitbalkeenSDfAromvireayles involvement # indicates clinical observation sign 603086 1550 Appendix Item # cer MFLTD.. CGarsieffith 31D. Henderson cFl. EKBe. llLeurd/eDr.annC. Goenner 3W0. Rcl. HNeelCsoornn/iIc.k Porietis RR.. EA.. ONbeelrs/oJn. D. Johnson R. A. Prokop/V. Pothaprogada $GRd. BSitbeifnfsekniLGRLERALAL) TITLE: FPlruootorcooclarbfoonrsTFwio-3Y9e2a4r aOnrdalFC(-D1i4et3) inToxRiatcsi.ty-O(nRciokgeerniSctiutdyy Study of No. 0261CRO012) OBJECTIVE: EFCv-a1l4u3ateinachrotnwiocyetaorxicratansdtuodnyc.ogenic affects of F-39242 and TEST ARTICLES: Fwi-l3l92b4e2saunpdplFiCe-d14a3n%d,,3as afplpuroorporciarabtoen,s.wellThechcaormapcotuenrdiszed Satn.alyPtauilc,allMyN.byAptphreoxCiommametrecliyal1.0ChekmgicoaflsFM-D3i9v2i4sioann/d3M2,.0 kg of FC-143 will be needed for the study. CONTROL ARTICLE: Ground Certified Purina Laboratory Chow #5002. SPONSOR: Commercial Chenicals Division/3M. TESTING FACILITY: SSta.fetPyaulE,valMiunanteisoontaL.aboratory, Riker Laboratories, Inc., DOSING INTERVAL: Fsteubdryuadryire=ctMoarrchwil1l981istsuheroaughdeFteaiblreudarsytu-dyMarscchhed1u9l8e3.befTohree start of stuay. TEST SYSTEM: Trhatrse,e h3u8n-4d2reddayasndotlhdiorntydomsaeledaaynd1.330ThfeemarlaetsCwhialrllesbeRhioveursedCD finrohntasngi(nmgalesta-in1l/ecsagse,stefeelmalceasges- w2i/tchagew)i.re mTehsehrofolmoorwsillandbe 1t2emhpeoruartulrieghatn/ddahrkumicdyciltey. controlled with the lights on a JUSTIFICATIuOsNedFbOeRcaSuEsLeECTofIONbaOcFkgrToEuSnTdSYdSaTtEaM:obtaCihnaerdlesfrRoimveprrevCiDoursatssuwbcihlrlonbiec toxicity studies in that strain of rat. TEST SYSTEbMeIDiEnNdTiIcFaItCeAdTIoOnN:theBaocuhtsiadneimaolf wtihlelcbaegeasasnidgonnedana niunmdbievriduwahlicheawrill tag. 2 2 AFlus-o39c2odetda technical grade as T-2999CoC me-3422 Also coded as T-2993CoC 603087 1581 Appendix Iten H (continued) RANDOMIZ`AGTrIoOuNpsObFyTEuSsTingSYSaTEcMo:mpuAtneirm-aglesnewrialtledberanasdsoimgnnuemdbetro mtehtehovda.rious DIET ANDgOrToHuEnRd cFeOrRtMiUfLiAeTdIONP/uArNiAnaLYLTaIbCoArLatSoPrEyCIFCIhCoAwTI#O5N0S0:2 aTnrdeawtaetderawnidllunbtereated awtevecaskitsl,iabrltdeiecpleaenddiaLnnigdbidotniuentthtwehirloslutgabhboieultipthyytsheiOcfaslttluhdyey.mfiexsetFdreasrehtveircmyliexstounerienstothoeffoutchrhoew. TcPhrheeasrtasucpdtoyenrsioazrneawliytlthliecaptlreostvriedsaeurlttitscheleosnfecatehnesdsattrehyset ataenrsattliyctalirectsailclmeussutpdpiboeetrt mfitoxortwuarredse.d tcohatrhaectetresitzatfiaocniliotfytbheefotreestthaertisctluedsy wwiillll bbee idneitteiramtiende.d pArniaolfyttiocal atunesdsitngatarttrtihiecallecsoblmepinlnde(tdsii)oentoworiflfltrhoebmedthodeseitneFgrimrisintnetdbelrvepanrldi.orfoSrttoatbhtaihelidtodysoisonifgng tihnietnetrevravla:l eRcveoeplrrlyeescet1ne3tdawtebieyvkesthetsahmteperlseteasftfeoarfciealanicdthywditulerlsitnbgearwtseiuecbklmeit3tdeiodret 4tmoiaxnttdhueraepCpowrmioelxrlicmiabatelely uCnhiemfiocramlisty-Aonfa-lcyotinccaelntrLaatbioornataonrayl/ys3esf.or test article content and ADNIDETAARCYCECPTOANBTLAEMINLAENVTESLSITiHOEWRNEOTFO: BENoCAPdAiBeLtEaryOFcoInNtTaEmRiFnEaRnItNsG WarIeTHkTnEoSwTn AtoRTIiCnLtEerfere ) w2biCypt,htheatnhdeveotnredgsoatrnoafprohtxoischplehea.avtyesmH.eotwaelvse,r, aftlheatocxeirnt,ificehdlordiientatehadshybdereoncaarnbaolnysz,ed DOSAGE LbEeVcELaSu,seROiUtTEa,ppeGaRrOUsP,toSIbZeE,anETaCp.p:ropOrriaatle (rdoieutt)e long term toricity-oncogenicity. Also in the dtoosiunseg wfiolrlevbealuuasteidng previous subchronic rat wteorxeicdietmyonsstturdaiteesd.this route was used and at higher doses toxic effects Taensitmalasrtiicnleglamsisxtufroeosd ajnards.theFcroensthrotlreaartteidclaendwiulnltrbeeategdivdeinsttowitlhle be Changed on a weekly basis. Dose Group coHnothroPlu-3924 NLiodw ePuu--33992234 LHiogwh FCF-C1-41343 DosageLevel 1000 ppppmm 3100 ppppmm 30300 ppoomm GroupSize 6s505,, 65502% s5o0s4,, 550082 ossoss., 6350%8 602068 15352 AppIte emn H (cd onti inux ed) STORRS SSIERUE TIEALG GTF TOUIT SSAA, TBoI Egiemsorte,tHiingS} hsnbebmosnss teToe ot oe TeEmA Temaersfa eorioteiontntyofyfnr1p 8eomean)meraisi/srpvusineentes--gfe--reos--wssyetsnun EereeereltanotpA eSnEesaneeCesoippb oeaitDes,OeSJsoEneRoE TomodreoilevE sie,tJavu)riesmmyaat(sfeommeumrpiinne EBhrRenE? fTorm2Sria/eedome grou other visser mars Se SneEseeSresSavoptpt eeneeexantminenoLst cCtrooanhyespyimdimaeeyetreddhmoupymSmipyeveayvrseyeeresdsddnsapaaunTsemofkmtihene d ToF EeiH Br Carpnssiomn, 47 tpihFeTiehowaaspsoypiassocnweiaol8nlfaniSeotmmieetsewsdSrrsetcm0yeesmemeeasect,iteyr ) Bcd report which will be a supplement to the toxicity-oncogenicity eT, CoBOroSeTsiERea:rremePmeiaineetvraitsoehmmoteehsspmadraeveerraTsaisTnevIe,E,bIeuSLswkLeuoetittnmeiigsnoaielpyeaLlriivnmeSltdosnendT3OoFbthecsk T2o27et% omE erpremryotiTT reonuteMs5,r51TbRuE nedmeemnmeacwmieuysRcieanVnediecdbhetsasitwogR inhlsd febeeseerhStsy erocosTrhteheduonnnd L speas Re esrCa semEeind LLeeyae oSefeaIotaste)vIC ocaateL tra iIniacoiannsy oTBmyr3anSndnineednees eeeoSbyhaLHihmEesseLcfoiYrinySsnaen r T mtn t oti0 setoatBeasrkenethFieae fpoetn vewoPn oFi ptisny=aF the 60g, 969 1553 AppIte em n(cd onti inux ed) CLINICAL PAcToHnOdLuOcGtYe:d onThe15cmlainliecaalndla15borfaetmoarlye rtaetsstsfrloimsteeadchbelgorwouwpilalt b3,e 6, 12, m1a8deandby24themonutshes.of Arnainmdaolmsnusnebleercst.ed aBtlooedachwiltlimbeeionbttearivnaeldwivlila be Svteaniinpluenscsturseteeolf mtehetaboorlbiitsamlcasgiensu.s. Urine will be collected in 1. Heam.atoTlootgayl mC obll HHeemmaotgolcorbiitn ea.. DTioftfaelreunntcial 2. Clian.icaTloCtahlembiisltirryubin cbo. ATlobtuanlinProtein Ga.l Gsluuncose 3. uria.nalyosnis bcl. ASlpbeucmiifnic Gravity 4. Glucose 5.. Aclokxaline Phosphatase niln sseeoerr 3. calcium e.. OBcicluilreubiBnlood 5. Ketones ' TISSUE PATHtOhLeOGsYt:udy.GrosAsnynercatropisnieasmwoirlilbunbde ccoonnddiutcitoend osnhoualldl breatsterinminated otfo tIhnesurvearisoautsisftaicsstuoersy wtiilslsuebescamopllleescte(dseefrboemloanwylirsatt).whicShamhpaldes adbiseodluutnelemsisnismeuvneresamapulteoslyosifsliunsg,prelsiveenrt, iknidanetyi,ssuber.ainAsandanany atnudmor15mafsesmawlielslfbreomcoealclhectoefd.theAntwoinhtiegrhiudnosneecgrroopuspysowfil1l5 bmeales odonnceogeatnic1 ryeeasrpontsoedaettertmhiantetiimfe.therAet tisheanendinodficatthieonstuodfy,anall tsiusrsvuievsingtorbaets fwiixleld bien kLiONllbedufffeorredgrofsosrmanleicnropasrye. liSsatemdplebseloowf. oAnt tthheose1 atnidss2uesyeiadrennteicfrioepsdiewsi,thweatn w*eoignht1sS wrialtls/sbeex/ogbrtoauipn,ed Psaeilreecdtioorngaonfsawniilmlalsbebyrecroarnddeodm ansumabecromtbaiblneesd.weiHgehitghatnsdfoirf waenigohrtganwiltlo nbeotwbeeightaekdeni.s in(vNootlev:ed Biondya wleairggehttwuimlolr bmeassd,etearmined oofn rtheelsaetiv1e5 oarngiamnalwse/isgenxt/sg.r)oup prior to necropsy for calculation 158 6039070 Appendix Item # (continued) aoadrrteanal (21% brains (3 sections including LLuinvgers (2 sections) Lymph node (mesentric) garnognltiaal, copratrieextaalnd cboarstaesx mpaanmcmraeraysgland (females) aanndd ptohnasl)amus; cerebellum eyes pSiatluiivtaarryygland Spinal cord/bone marrow (vertebrae) gonaodvsaries Lb ssptloemeancsh hsemaatlrelesrtienstte/setfipndeif(maitsleast 2 areas) uutrrheiyrnruaosrisyd/obprlaardapdrteohsrytraotied/trachea/esophag Kliadgneaysisntestine aannyy ottihsesruegrmoassssesles(isounsspected tumors Hsieccrtoiosncsopiwcillexabeminpaetrifoonrreofd dose groups, including all ffoorrmaalllina-nfiimxaelds stinaicnoendtrpoalrafafnidnbottihssuheigh aninals in these Groups ating or euthaatized uring the course of the study. Irnomaddailtlioann,imatlhse ifnollthoewinlgovtainsdsuemsidwidlolsebegroeuxpasm:ineLdivemri,crKoisdcnoepyi.cally ) GFornoamdsallandlowallandtimsisdusdmoasseselse.velTahneimraelmsaiwniilnlg future reference. Mictoscopic evaluation of bLeisssuaevsed 1ifosrtepdosasbiobvlee additional tissues from bayniemxaplseriinnenlcoawlorfinniddingdsoseatgrtohuepshiwgihlldobsee pseervfero.rmed i indicated 603071 1535 Appendix tem # (continued) DATA ANALuueYslSegIdhStfsAo,NrDpaenFraIclNeyAnsLtisRdEioPOffRfTet:rheencTdeahteafprroaormep:ocsonetdDruosmlteactftioesrstibcotdaeylstHmefetohlroedssnietno be CPDeahrcich-eosnlqtougayrteumvoafrlourebspeearrwicilenlngtabemnoirnctaoalmlspiatraienedds,ttoumtocuromnrtirnoccliodnetannrciaemcsatslisonsalnpidrnobniaoobrmiallities, boFetahngsearusb.srteitth(uoNtdoested:sefeornIfonroasteustehadeppritnoipmrsaidadttiheet,iodnatthaotsoeartehootshteeorbaemlertenhaaodidyssrcaimdtieldl.) St1i5in-3c1s8euemiostnetccthoisuolndasf,ttearktehefuippnraolfpoonse1ec2drompodsnaytcehs(faopr0prtpohrxeoicneafstisenlaylandr>eepsemdrontsihisi she after slide reading is completed- ) E AdvancedS Toxicelogist cs EG TPdhagear, LkaboeratorSyN eAniomh wa,r reeoa Study birector Mediaine and Fathoiosy Ps Taonai gee r STatohooutsroep1pe6xtc/oto0ss once Safety Evaluation Laboratory I ManaFogerG, rToyxi,com ledy Seo rvices s Sponsor Representative BJUCLJtIoie m MA eeeorseniani HE4 Au ie Spor Reprasentat; 603072 1586 Appendix Tem i (concluded) Tuo Year OorfalFlu(odireetc)arTbooxnic-i3t5y-2oncoignenRiactisty Study Anendsents to the protocol Aosnceofavsetruydytdwaoyve1s8k3s,. body weights and food consumption will be recorded CDfuorenotnrtoRoliskteharenLduanbheoixrgpahetcotdreoisdeesl,FeUa-vt3ih9neg24fioanfaniDdr.sFvCev3.104e.3xamHrieanntdaeetriwsoionlnl,ofbotthhepeersftsoaufrrfvaievsvienbtgyerDiFn.arian Steven Bistner, DM, a conediting veterinary ophihalmelogiss, GPoastepravtaitoinonfofrorpoesvsiinblieceltusmioornss:(sasses) vill secur during the veskly Iinnatdevreirntennetcltyo,psynofotrisstuheesHweetraenoitiaskeengrforuopm. the mle rats during the one year 603073 1537 HEPLIOLKITEM1 STATEMENT OF QUALITY ASSURANCE FOR EXPERIMENT 0281CR0012 "Two Year Oral (Diet) Toxicity/Carcinogenicity Study of Fluorochemical FM-3924 in Rats" Study director snd to managment 2c follows: Audits and inspections were performed by the Riker Compliance Audit unit for the above titled study, and reported to the Date Performed Date Reported 5/13/1981 5/18/1981 6/23/1981 11/05/1981 11/11/1981 6/02/1981 5/20/1981 6/26/1981 11/13/1981 11/13/1981 11/20/1981 2/08/1982 2/09/1982 2/12/1982 3/10/1982 12/01/1981 2/16/1982 2/12/1982 3/02/1982 3/31/1982 3/31/1982 4/15/1982 5/10/1982 5/18/1982 8/18/1982 4/02/1982 5/03/1982 5/20/1982 5/20/1982 8/26/1982 11/09/1982 11/22/1982 1/25/1983 2/22/1983 4/12/1983 11/22/1982 12/01/1982 2/04/1983 3/15/1983 5/17/1983 4/15/1983 4/18/1983 4/26/1983 8/04/1983 9/24/1984 5/05/1983 4/21/1983 6/03/1983 8/05/1983 9/27/1984 12/19/1986 3/31/1988 4/06/1988 3/10/1987 4/06/1988 4/06/1988 DR SohleeCorA .mprarvogT nboE c 003074 1533 APPENDIX ITEM J CHEMICAL ANALYSES OF FM-3524 AND STABILITY ANALYSIS OF FM-3924 IN DIET 603075 1522 Internal Corresponrence ce: ME.TG.. CLaasmepre-ch2t17-2212-3 WWLHC. MPceCaorrlmsiocnk- -22230--G2SE--0024 RL.dA:. SPirboiknospki- -2326-1238-33. Appendix Tten J To 0. R. RICKER - 53-4N CAONMAMLEYRTCIICAALL CREHPEOMRITCAL5S318 From L. 0. WINTER - 236-28 Swiwocer tFM-H39242,3,Lo1t982547, PRE AND POST STUDY ANALYSIS Reference: CRiokmeerrcSitauldyCh02e8m1icaClRs00A1n2a,lytCiocmaplounRdequ4e7s-t299#9164C7o4C. and others. AoanndTi1ug2sh/et3d,/80isntrfaoswreveccrohalalorraecsdtteudrwiiaezxsay.tisoonTlhiedanmdlaatabeneralileaydlsiFshM.a-s332Tb4he,iesn lmaoanttael5ry4iz7aeldwaswbyasrGeLacCneailavnyedzded cIo.Rm.plesteivoernaloftitmheestwsoincyeearandstuwdiyl.l be checked several more times till the The sample has been analyzed as follows: Gas Chromatography of sample os received. (14310; Tae AT in r3eaST IE trent Anide 0s cy c allie 10.6 cs [ CgtCy+isoners 88.9 HB. Nil 0a 0s 0.4 0.6 0.6 0.5 1.2 13 1.2 18 7 1.8 1s 1.6 1s a8 a3 a8 88.9 88.9 8.9 0.6 0.8 0.6 AmleletvaQCluesspecaireficwaittihoinns.experinental and integration parameters. Values 3M 605076 1520 Appendix Item J CCD Analytical Report 4318 Elemental Analysis: es C3\ic F 0 by diff. -2- L. D. Winter Based onCg There: + Found. 25.2 iI15es H21H:8]8 56.66 8.4 24.6 57.0 9.0 Melting Point: Initial Recheck 38-48C 38-48C Spectroscopic: sIpnefcrtarree:d spectra 164742, -3, -4 are identical to cach other and match reference 16474-2 was obtained Nov. 14, 1980 16474-3 i. Mar. 31, 1981 16474-4 " Mar. 5, 1982 confined: The. Tsomer a1 bribytron was, NMR spectra H8385, H8387, F8390, F839] 1980. These were to confirm structure found bo ba 89 0% strstone churns were obtained on December 1 and 2, and not repeated. Structure was 10.9% (CF),CF branched, and 19.5% backbone branching. conctusions: FM-3924, lot 547 has an analysis within specifications, is stable and is representative of commercial material. Sf/ l7pLe' n LOW:df 00307 0 1521 imernalGorespondence topendic item 9 To: From `Subject: Oute: comencia cimeas ANALYTICAL REPORT #347 L. J. SIBINSKI - 218-3-3 R. M. PAYFER - 236-28 Kelsie ion Es MID STUDY PURITY CHECK OF FM-3924 (T-2999CoC) FOR RIKER JUNE 22, 1982 3M Reference: Commercial Chemicals Analytical Request No. 18318, A 15ght, strav-cSoloIredEwaxyRsaolird elabeled FH-3920, Lot 547 uss recefved on 5/17/82 for a mid-study purity check. The sample was analyzed by GLC, The results are as follous: IR, and elemental analysis to compare it to earlier data. FGiLetCressData . C3 CCGsGa CH3aanddaCitgenasnd isomers 082(Area 3) 113 2a1.l.2s9 858:.29 Ether 4 Elemental Fou Analysis: Sop aitrerence "5.4 5 Cc 25.2 25.0 H 1.75 1.8 N 2.45 a7 S 5.6 6.1 F 56.66 55.3 003078 1592 fppendix Item J "Ze Melting Point: 38-48C Infrared spectra obtained (18318-1) was identical to earlier spectra. Conclusions: "All2resultnso aF re p within experiimnenFtMa-l392e4r,rorLotof54p7r.evious results, so there RMP/nC 4 de: M. T. Case - 218-2 EJ.. 0G.. LLaanZperretceht- - 218-3 236-1 We. V. C. McCormick Pothapragada -- 223260--G2B-02 Lo 0. Winter - 236-28 603079 1593 Internal Correspondence Appendix tem J WL. STINSKI - 2183.3 ACNOAMLMYETRICCIAALL RCEHPEOMRITCA#L4S12 fom Re ML PAYFER - 236-28 Su ak STUDY PURITY CHECK OF FM-3924 (T-2999CC) FOR RIKER owe JUNE 15, 1983 Reference: Commercial Chemicals Analytical Request 418318, 19330 Analytical Report #318, 347 GoALnC.l4i/g1Ih8Rt,/,83ansdtfroareul-eacmnoenletonardledoafnwaaslrtyyusdiyssopltuiordictolyambacerhleeecdki.tFNt-o3T9hee2a3r,SlaimLeporlted5aw4ta7es. waasnalryesceedivenyd The results are as follows: FLC Data (Area 1) Atmnierdtes c5 30..7316 124 C&cC7go 8 Cg and isomers pi2.le0s0 #5175 gn aeitars 0.76 Elemental Analysis: % Theor. % Found cW fs 0 by difference 2.213575.s2 2210537.3 55.66.66 55.53.2 8.4 9.7 603080 1574 Appendix Item J iting sont: snags Le amiss: Infrared spectra obtained (19330-1) was identical to earlier specta. BS lg LT All results are within experimental error of previous results, so there WCLidad 11. wh 5LnBTEgL. oobsmeae2pt102a,, GSgsuaamnelesB eot 603081 1595 Appendix Item J Internal Correspondence cc: ME.TG.l LCaasmeprecht - 2182 218.3 JMW..DC..oLMacZCeormtmeick -- 222301-L2602 VR.IAP.othParporkaogpada -- 223366.2384 L. 0. Winter - 236.28 LJ. Sibinski - 218-33 From PL J. Colbert- 236-28 Sweet BGlLeCndAendalyTsnitso oGrfouFn-d392L6a4b C(hTo-w2.999CoC) oe april 9, 1981 RCeOpoArntal#y2t0i2cal SM RefReerqeunecset: #Co1m6m9e5r9cial Chemicals Analytical Laboratory Method C4o6m3m0e-0r4c8i1al Chemicals Analytical Laboratory rCFehocouwer,ivseaadlmopnlfgerosnwiotLf.h FJHt.w-o3S9i2bb4liann(skWk.iRG.roonuEnLdF3-O2SL3Ea-)b81Cbhloefwonrdesadanmgpillnyetsso,isG.rwooruenTdhe Lab samples vere labeled as follos: Compound F4-3924 Theoretical pom FU-3924 Concentrate . 200 ppm (blended 3-20-81) Blafnokr cGornocunedntrLaatbeChow 0 ppm FH-(3b9l2e4ndeTdop3-S2a3m-p8l1e) 100 ppm F4-(3b9l2e4ndeMdid3-S2am3p-l8e1,) 100 ppm F4(-b3l9e2n4deBdott3o-m23-S8a1m)ple 100 ppm Blafnokr TGorpo,undMidL,abBoCthtoowm samples 0 ppm aoTnnhael3y-7z24e3-d-38912f.4or CcoTohnencteeTnnotptr,aatnMedida,nSdtBaobbtiltlaointmkyawneondre8tlhaeannakliynizsteaidmapllfeosrsawcneodrnietnegnt difnaory47p(0o32s-.t23-bj8al1re)snd oannwder3e-o2n3p-rw8ee1epkaraen1 dd anbpdlyacp2ilnapgcoisnttghebmltehneidn.GaromuTenhtdealLsaacbmapblCiehnsoewt 603" 082 1596 Appendix Item J ALpJri.t S9,ibi1n8s81ki Page 2 wtfoirtohnaioru.tthe tjThaheresco1 voenarnsd3-3o20n-w8et1ehkeanpjdaorsst4,-b6ll8ee1na.dvinsgaThmeptlheersessuwalemtrpselesatraekoepneans follows: pom (ug/g) FM-3524 on Compound 4-3924 Concentrate 3-23-81 196 3-30-81 - 4-6-81 - FMB-l3a9n2k4 Concentrate 0 - - FM-3924 Top Sample 100 99 9 4-3924 Mid Sample % 9 8s #13924 Botton Sample 99 95 8s F4-S3a9m2pleToBpl,ankWid, Botton 0 0 0 PaF/m0 yfzan7). (olf Sq -- cu _ated1l Jl AJor citineht e loEr piliihe : << 603083 1597