Document 8ZxdYmJKpY1OKnnQXMLj0QYd
ACUTE TOXICITY TO FISH
ARIEO3F6
TEST SUBSTANCE
Identity:
Perfluorooctanesulfonyl fluoride;mayalso be referred to as
POSF, or FX-8. (1-Octanesulfonyl fluoride, 1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,88-heptadecafluoro-, CAS # 30735-7).
Remarks: The test substance is a clear liquid of uncharacterized purity. It is described as FX-8 (cc842-2) Lot 1 F-10101, L-1407 washed sample.
METHOD
Method: Not given
Type: Static acute
GLP: No
Year completed: 1984
Species:
Supplier:
PDiamlpehaFaltetisg,prBormaedly,asNebraska.
Analytical monitoring: Temperature, pH and dissolved oxygen. Test
substance concentration not measured.
Exposure period: 96-hours
Statistical methods: Not needed.
Testfish age: Not noted.
Length and weight: Average length = 3.88 cm.
Average weight = 0.366 g
Loading: 0.61 gfish/L
Pretreatment: None
Test conditions: Dilution water: Carbon-filtered well water, 3M well #2, St.
MN Dilution water chemistry:
Dissolved Oxygen: hardness:
9.2 mg/L 240 mg/L as CaCOs
pH:
82
Paul,
Stock and test solution preparation: The test concentrations
were prepared by transferring appropriate weightsofthe test
substance directly to the test chambers. Concentrations dosing rate: Once Stability of the test chemical solutions: Not noted
Exposure vessels: One gallon wide-mouth glass jars containing
3L of test solution.
Number of replicates: Two
Number of fish per replicate: Five
Number of concentrations: Four plus a negative control
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Water Dcihsesmoilsvterdy odxuryignegntrhaensgteud(y0:-- 96 hours): 6.69.2 mglL (control exposure) 52-9.2mg/L (1000 mg/L exposure)
pH ran8g0e -(08-296(choonturrosl)exposure) 7.8-82 (1000 mg/L exposure)
Test temperature: ranged 21-22C
RESULTS
Nominal Element
concentrations: value: 24-hour
BK control, 10, LCso => 1000
100, 500, mg/L
1000
mg/L
48-hour LCso = > 1000 mg/L
96-hour LCs= > 1000 mg/L
All element values based on nominal concentrations
Statistical evaluation of mortality:Not applicable. No mortality seen in the any concentration tested.
wSuebrleestuhraflaceifnfgecatts:eaAcfhtecro4n8c,en7t2r,atainodn 9t6es-theodu,rbsuotfneoxtpionsutrhee,cosnotrmoelsf.ish
CONCLUSIONS
The test sample 96-hour LCso for fathead minnow was determined to be >1000 mglL.
Submitter: 3M Company, Environmental Laboratory, P.O. Box 33331, St. Paul, Minnesota, 55133
DATA QUALITY
dReeltiearbmiilniatty:ionKioifmtihsechtersatnksiunbgst2.ancTehicsonscteundtyraltaicokns iannatlhyetictaelstdsaotlautfioorns and determination of the sample purity. Its estimated that this study was run in excess of water solubilty.
REFERENCES
This study was conducted by the 3M Environmental Laboratory, St Paul, MN, Lab Request Number B1229-2
OTHER
Last changed: 5/18/00
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CHEMICAL EENVNIRVONMIENTRALOELAFNBFOENRCATTESOERNYVALTUAATILON
TT TOXICITYTEST: SUMMARY REPORT
Chemical Tested ES A (rsia:2) h Lg7/ Seppo) Test eeeue(aye
BL
5
semen
TestSpecies: Srey) Mita) {FIMECHAES TH mers)
Test ate:
RS H-2-8Y J --(-8
L.R. #:
Bl229-2
waste PRure sy =
Exposure Type:
(Expdsure/Test Conditions)
Static Recirculatory
Static Renewal,
Plow-Through,
Diluent:
Aerated Well Water (Initial 0.0.2,2mg/1; pH 3,2 Temp. 20 *CLRF))
Vater Hardness: _22() ppm Hardness Classification: AML
_
Dissolved Oxygen % Saturation:
Control(s)
.
Lovest Experimental Dose 10mgll
Highest Experimental Dose |000wq
48-hr
B80.
v8
0?
96-hr 1 Mo
EExxptoesnudreed .
pH Levels:
Control(s)
Lowest Experimental Dose 10wall Highest Experimental Dose 1000wgf
sche s6che EExxpteonsduerde
al 80
al 429
80 M9
Test Temperature C (F):
she 96h EExxptoensduerde 2z0ctn) zzctz) re) 00662
Photoperiod: Sixteen hours light with a 15-30 minute transition period.
SESTCOPY AVAILABLE ....umvrue. casonsron
EXPLAOQRUAATTOIRCYTO(XRIACNIGTEY-FIDNADTIANGSHETEESTT)
wBIZ29-R
ype nese Alte Spr dassria Tasted SK=
0523) ,
Tost Organ pui)sSovm vesBEAAIlr,TNaEssQDD ate Rec'd,
Ag We 0, 3/p( grams AVE. S12e3BGCH No. Organisms per dose
btoots/ (F tons) Batch No.3 _5
Test Solution Volume3Liters/All-Glass Tenk Tank Dimensions:WIDE-HOUTH 1 GALLON GLASS JAR Time Started_//[()ysu{ Date Started A264 Date Completed_2(//z/B5
Dilution Water_Carbon-filtered.well water (Temp, 20 C., 0.0. Z 2 ppm, HAZ)
TE TE 2 erent Dig, (95% Confidence Lites) >Lotoud? (Full Signat;
xNo. emea [=] oo lad7ll No, Dead| pH| p 0lei No,Dead | pl pp 0bipdll No,Dead pH | ppm| 0 ld |No, Dead ppm
wo =oll Bild oJallbdl 0 kde8ll 0 Fda oo (=oo II 0 WTI oo leche o hkl okd To soo [Il0 Rilz@l 0le.owl 0hdpzll o ke [ooo zac 0 leAl 0 ROR 0 aszll o law Corr rr r tr rrr rr 1
r nme, _|| z/r 0 || 2290 ||r 22C || J24 ves HoSAAT of]HEISES(SBN ls
coments: Xoo
oes, Cle Lui,
FE
--
Effects other than Mortality
ECgy,
melt IMAowe Mowe [| Aone | Tank No.
| Symptoms or Reactions
24-Hr,
Total No, Affected
48 Hr,
72-Hr,
96-Hr,
Tl TZ
7
NCwi zz 1 2 |
m o> I 2 e [212 |
= 7 JTRS
=z T= 1
rc Js Ts1 =
:
1
Come
-
006626 -
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z
BESTCOPYAVAILABIE on ons EXPLAOQRUAATTOIRCYTO(XRIACNIGTEY-FDIANDTIANGSHETEESTT)
wWRIZ29-2
oe TostJost Au Src Material Tested -T4-e4222, sot2/ (F-p/rpoe]d Tost Organism7 Jy ur IMAa CkSou0 rcs, all Nee paterolaSLsand No.357
AVE. Weo 0 Bfefr _ gress AVR. SizeZAECH No. Organisms per dose _5
Test Solution Voluse_3 Liters/All-Glass Tank Tank Dimensions:WIDE-OUTH 1 GALLON GLASS JAR
Tine Started [00pa(_ Date starved _2Y/2 [5 Date Completed_o/ //n/FY
Dilution Water_Carbon-filtered well water (Temp.20 C., 0.0._%,2 pom, M5,2)
e Invest s % te Oo(95% Confidenccoenics Livnite)t 1000 tall
.
No. Dead| pit | pp || No.Desd| pit | pm'| No.Dead pit | ppm |[No, Deadbi op
lemen[= 9 lel 0lealoll ledogll 4 Kd
Alo N=o lo RILAL lewd o bind 0 ide
Wlico
Aloo
Nzco 10
(spol 0
Billed
l/l
0 andl
lededl
0 Ulbell 2
Viel 0
bes
Edy
Alinco
{lmmoll 0 kIpZ0 0 180 IL J VASA 0 hd
Lnrr er r rrrt
rr rr r TE 1
rrrrr TT
11
rere || 27C || 207, || 227 | 22
g vee [ISSA I/HS RTSYsa
coments: lop mui. woe eres. (ems Liquin
_--
Effects other than Mortality
eg
I=No. ||| symptoms or Reactions|| z4-hr. 48 HrT,otal No, 7A2f:fected 6-tr,
lel
|
ise hoe |Mage |
All Ni z Tz r 1 7 1
` A =ebvae
Al
[Zz Ts T= 1
NS re Ts|
TAIN
Jw== 1T ~/ |
[1 Ce
006627
----------_--_------
4-12-84
ENVISONMEANLTLAL RLESAUSLOTRSATOTREYNTASTTIAVTEUS REPORT
LAB REQUEST NO. 81229
REQUESTER NAME: ANW/EAR JPERPOTJ:ECT053N5O: 9970012600 DATE RECEIVED: 2-21-84 DESC: FX-8 (CC 842-2)
CONTRACT LAS: CONTRACT LAS COST:
0
3M E-L HOURS: 46
EST CMPLT DATE: 5-01-84
DATE COMPLETED:
SAMPLE NUMBER TWO WILL BE GENERATED FROM TWO EQUAL VOLUME WASHES OF SAMPLE NUMBER ONE.
SAMPLE DATE
coe DESCRIPTION
TEST
RESULT
1
FX-8
SNPL-PREP COMPLETE
2
WASHED ~~ SAMPLE
96=HR-LC50 C-BOD-05
#>1000 MG/L SEE REPORT
C-B0D-10
SEE REPORT
c-B0D-20
SEE REPORT
SOLUBILITY
BIOSORP
SLUDGE-T0X
# *
= =
UCPODNATTREADCT DALTABA
006628