Document 8OOp3GXR8yRawwLe5Dy4m3pxd

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PFOA and Associated Salts t a = [ ec =e] Ee p -- Fed |Perfluorooctanate: Static (fish test) 3M Env. Lab 5/31/95 _|(MSU) -- E =eE [ Mm Eee] i T oe prmemmems--no--n e [Ll E FooonnlTa eo[Eor--) )mz: and survival of Fry of Fathead Minnow (Pimephale |oromelas) and "Summary of Histopathological EEE en [Examinations of Fathead Minnow (Pimephales promelas) June 1978 |Robust summary, |EG&G Bionomics,| and Sept. [copiesoftwo final Es [es eycose" TO en | nen [smo| [Toxicittoy activated sludge - FC-143 ecoueenocnsn Agar;Tost marosF140) | owen tao | 1Ey10n1|mEtor"| |Exposure/Recovery Algal Assay Test method (FC-143) [48-hour acute static toxicity to Daphnia magna - FC-143 |(3 studies on diet) EE Ee Chronic Toxicity of Fluorochemicals to Daphnia magna = providedby AScl Corp., Duluth, MN 3M Env. Lab 3M Env. Lab 3M Env. Lab 3M Env. Lab 6/4/80 [Robust summary, copiesofdata sheets 11/16/81 _ [technical report 5/6/82, 6/2/82 |copies of data [sheets [Robust summary, 8/10/98_ |letter report 96-hour acute static toxicity to fathead minno-w FX-1001 3M Env. Lab 2/2/85 [copy of data sheet| c03732 | PFOA and Associated Salts ;{ Ecotoniciy lomants thor Date Robust summa. 1[2A0cted sudge respration ition (OECD 209) -FC- ar07_|shceoepytsofcata cRoopbyuosft dsautmamary, icroto est. F126 aur [Rsohbeuetsst summary, 48-hour acute statotoioty to Daphniamagna -FC-126 | am En Lab csohpooytos.fdata - [Robust summary, 6hour acutestatic oxitocfattheyad mionow-FC-126 | oMEm tab| 51eRrcoobpsuysotfsdautma ma, frIncivated sug repiaton inion (OECD 209)-FX- 21650 c[sohpeieetss ofdata Robustsummary, Microto est x.1003 ErvioSystems, 0 _|R|oscbhueoassotpfsiudemamtsaary,: SitmateipchAcauitsepTroomxeilteysofFX-100t3o the Fathead Minnow, | HaHmapmtopns,hiNeew| 311590 n[pariotorceoplort, Static Acute Toxic of FX10to0th3e aphid, Daphnia| EHravmrpotSoyns,toNresw, Ronbausrtesra,mmy, magna THRampWsihbiirrey | 4190 _|oroocot iGnrowFtrheasnmdaRteeprrodAgua.cStlieonnaTasxtiuctmycTaepsrtiwciotmhuNt2u8m03-3 and|LMaabrobrlateohreiaeds,, WInAc. nRoabustrespoummary, AcuteToxic of 2803-31th0 Fathead Minnow, |LabToRrtoWriibsi,ync, Robust summary, |Pimephalespromelas Marblehead, MA| 1/24/96_ [final report [acgutneaToitof N28033t0theDaphvid, Daphnia |LMaabToRrr.vatiWoirelihbeusardynAc.,|_ 37706 -- na report Robust surary, icrotos test F143 Meno | 4296 |[Rcsoohbpoiuoetsssotsfudmamtaary, roto est c-118 Menta | 424s [Rcosboeuespstoisfudemamstaary, | irotoxtest -1015x smenuta | 4290 c[sohpeieetss of data 03733i Co i . i PFOA and Associated Salts i Ecotoxity Elements ! [ mc = pe r bate Robustsuma|n. |AcivatedSugeRespiration onionTest- FC-10t5x | cue Toyof 10151 0 Faas Heron, aTmREWmi.buLtayb_| arzsio6 -- sheets |coopfideatsa pimepnales promelas MaTrbRehWeiabdu.ryWa fiat report tGhreForwetshhawnadtReerpArlodau,cSteiloennTaastxriutmy TceasptriwcitohmuFtCu-m1015 and|LMaaborrotiorhees,aWdncA..| 51156_|nRaolbursetposrutmmary, = LabToRra.tWoiribetsr,yInc, Robust summary, [cr ut Toxityof -1015tthe Dapr ,Daphnia magna | MarbleheaMdr A,| 5/15/96 nlrepo E r ms r oe [eeeEeeRIe Room 7 16 [Technical Report Summary- Final Comprehensive I --_-- [Robust summary, i | 1 1 i 03734 | i ACUTE TOXICITY TO FISH TEST SUBSTANCE Identity: Perfluorooctanoic PFOA ammonium acid, salt, ammonium Ammonium salt; may also be referred perfiuorooctanoate, PFO, to as FC- 116, FC-126, FC-169, or FC-143. (Octanoic acid, pentadecafluoro- , ammonium salt, CAS # 3625-26-1) IRte'smpaurrkitsy:wasTnhoet s3uMffipcrioedntulcytclhoatrnauctmebreizrewd,asth8o3u.gThhceurtreesnttsianmfpolrmeatisioFnC-143. indicates it is a mixture of 96.5 - 100% test substance and 0 -- 3.5% Ce, Cr, and Cs perfluoro analogue compounds. METHOD: Method: Not noted. Type: Static acute GLP: No Year completed: 1977 Species: Pimephales promelas Supplier: Not noted. Analytical monitoring: Temperature, pH and DO Exposure period: 96-hours Statistical methods: Graphed LCs Test fish age: Not noted. Length and weight: Average length = 2 inches Average weight = 1.6 g Pretreatment: Not noted. Test conditions: Dilution water: Carbon filtered City of St. Paul, MN water. Dilution water chemistry: `Temperature: Not noted. Dissolved Oxygen: Not noted pH: Not noted. Stock and test solution preparation: Not noted. Concentrations dosing rate: Once SEtxapbiolsiutyroefvethsesetless:t chemical Not noted. solutions: Not noted Number of replicates: one Number of fish per replicate: Not noted. Loading Number rate: Not noted. of concentrations: five plus a blank control Water chemistry during the study: Dissolved oxygen range (24 -- 96 hours): 4.7 5.7 mg/L (control exposure) 40-49 mg/L (50 mg/L exposure) pH range (24 - 96 hours): 03735 7.07.1 (control exposure) 6.4-65 (50 mglL exposure)" Test temperature (24-- 96 hours): 70 - 72F RESULTS NEolmeimneanlt vcaolnucee:nt9r6a-thioounrs:LCBSk0c=on7tr0olm,g1/0L, (2C0.I,. 3n0o,t4c0a,lacunldat5e0d)mg/L Element value based on nominal concentrations CONCLUSIONS The test sample 96-hour LCso for fathead minnow was extrapolated to be 70 mglL. `Submitter: 3M Company, Environmental Laboratory, P.O. Box 33331, St. Paul, Minnesota, 55133 DATA QUALITY Rmeeltihaboidloitlyo:gyK.iimTihsechLrCasnkwiangs 3e.xtTrhaeproleaitsedinfsurfofmicainentindsoufcfuimceiennttantuiomnboefr tohfedata wpoaisntns.otTphreopgeerlnyercahlarhaecatletrhiazendd aangde iot flatchkesfaisnhalayrteicnalotcnoontfeidr.matSiaomnpolfetepsutrity substance concentrations. REFERENCES TSth.isPasutlu,dMyNw,asLacbonRdeuqcuteesdtbnyutmhbee3rM23C4o0m.pany, Environmental Laboratory, OTHER Last changed: 5/24/00 03736 Zr EF AQUATIC TOXICITY WORKSHEET ts o "TeTe ul Stat 2 Tost Orgaaten, A Material Tested, Fecifg dal 15 bis Avg. Weight Loa Size, ches Duty Started, -25-14 Date Completed. J |; TipeStarted, M;000M Plotted LCs uate oeCito,ENeled City ned BEST COPY AVAR ABLE . ~ 24hrs 48 hrs 72 hrs 96 hrs 2 conc. 9 $ H Dpp.m 0 Survi.val pH 0pm.0 Survi`val 0.0 . D.0 ppa Survival pi :pj emer]\po [7087]voJro[za] Ae [2dse]ao[ilu] wal von[75a] Von[7d]5dvo[ula]Neo [ule] ze" | lon a]&2] oo[70[%0] veo [74a] veo [7cfud] "30 | oo els too ez[4a] eo fea]us] too Jeslud 3 0 [aJeglsoltoolela9] Voo feral100Jeglud <aLaolea]aoleslur] golislus] 0ledlus Merage Tmporseuge 72] 70 | 0 13WARJ] 10 56 s 80 Sogou ~ WeyCalculation ~ } HH HHLR hh TET EER Be iliiiinilil R Leith Eo agin einai B Vm panei Poo 50 de 4 i -ocinibiad Loar hdl pu i Piped ip elit LUTE i Poliln Ph cL 2 Rha ep HE wild [EE |b 0 10 20 30 40 50 60 +survival 70 80 90 100 03737