Document 8O7LD4bNQw1MeQM859nzLer0K
3'j ?/.1982 . L2J16 <224,
("DATE >
< LOT )
( EST WGT >
< > KY-908-D (G) FWP 10/05/82
COMTYP JOB NAME: 03KY908DHG
STANDARD HRS*
TIME _____ -M
DRY*
DRY NO. PKG TOTAL ACTUAL
UOCATN CG CODE PQ == sssssssssss ==
LOT*
WEIGHT CONT PKG WGT WEIGHT USE LBS ====== $S;SS Sitz-tz szszsz
14 YC-3 93
... v.
14 93 4juaAL ~TT7i?
14 rc*z 93
'T.,;i; 14 YC-3 93 ---<--
----- ,
EQUIP----- 7
-
MENT j
i NAME : "KROLOR* YELLOW-LIGHT i -- ------ --*-
1 ----1
BEFORE USING SV MAKE SURE N-28-D LINE ( HYDRO
CHLORIC ACID) IF ANY IS BLANKED OFF,*
203 &
205
1
RUN 60* (990. .G) WATER IN V-203. SET AGITATOR ON HIGH SPEED*
WEIGH IN DRUM & POUR IN (SODIUM SILICATE)
DUMP IN AND STIR 5 MIN (CHROME YELLOW > . RECORD: START2/^#J2_ LOT
i I ! 420 ] 32-D | 42
I 63X501YC-3-BI 3150
1
v/T ADJUST TO 75* (1275 G) *NOTE: VOLUMES HIGHER HAN 75* MAY CAUSE DUSTING IN EXHAUST HOOD.
WITH AGITATOR ON LOW SPEED PUMP V-203 THRU
MOG AT 2400-260 PSI INTO V-205
WHEN V-203 MT, WASH COLOR THRU HOMOG WITH MIN
F HOT WATER AT 2400r2600 PSI INTO V-205
RECORD: V-205 VOL
& ADJ TO 60* (2100 G)
HOMOG STRAINER & CLEAN IF NECESSARY
I
"205 SV
N 10* (514 G) WATER INTO V-g&M START AGITATOR
I PUMP V-205 THRU HOMOG AT>4800-5200 PSI INTO SV. | RECORD: TIME START /^ZS&raOTAL MINUTES I NOTE: IF HOMOG PRESSURE FALLS BELOW 4800 PSI,
-WAY VALVE WILL RECIRCULATE SLURRY TO V-205 WHEN V-205 MT, RUN IN 5* (240 G) WATER 6 PUMP THRU HOMOG AT 4800-520 PSI INTO SV
.*1
SR|\2<\ SP STEP 1 - SET FORMULA SELECTOR TO POSITION
2 (V-243) OR POSITION 7 (V-244)
HPRESS SV CAM RESET PB - SET 22 TC IN AUTO REMOTE (TEMP IS SET AT 19-194*F) 3 Mj M" RECORD'LEVELS & SET R/M COUNTER *1 AS FOLLOWS:
!
\ Jrf 11 LG
PRESET si
95 GAL (LIQUID ALUM)
SET ^STRIKE FLOW CONTROLLERS AS FOLLOWS: Cl (N-27-D CONTROLLER - SULFURIC ACID 60%)
MANUAL
0.65 GPM
(N-27-D WATER) IN MANUALLOCAL 5.2 GPM
(N-27-D/WATER) RATIO
0.8
(N-32-D CONTROLLER) `IN MANUAL- 0.87 GF'M (N-32-D WATER) IN MANUAL LOCAL 4.8 GF'M
(N-32-D WATER) IN REMOTE
(N-32-D/WATER) RATIO
1.1
II
MOV 5 198^
1115-D 1 504 11 11 ! 27-D 1 218 t1 11 11 I 32-D 1 1476
<4
-GT- ___ _ _ COMTYP JOB NAME: 03KY908DMG PAGE 02
DATE PRINTED : 1 0 7,05/82
EQUIP MENT
I PAGE 2 CG 03 KY-908-D
-A
'ERATOR STEP PB
RECORD LEVEL 2Lg '2LZ-% "1F <352 FOLLOW SOLUTION
1 L-HAKE-UP PROCEDURE FOR N-27-D
( erj^wjusT s v ;f p a t > <2400 0 `
RECORD PH LlJC ADJ TO It.0-11*2 WITH N-7-D
I (CAUSTIC SODA SOLN) AT 52 (1 PARTS WATER TO 1
J | PART N-7-D)
- '
I J^XlPHQN INTO SV. RECORD: PH fQjtt ' ASSUME SOX
Jv\ OPERATOR STEP PB
USE LBS
6o
ACCT LBS
1ST I SP STEP 06/39. AFTER HEAT-UP RECORD: PH
SV \32rT SWITCH 3FC20, 8FC10, & 8FC2 TO AUTO
SP 123'^T^.OPERATOR STEP PB i^Kl` SP STEP 10/43. WHEN 3FC20, 8FC10 6 8FC20 FLOWS
I |,.ARE IN LIMITS, SWITCH 3FC19 TO AUTO'& PB
\yHf\ SP STEP 11/44. WHEN 3FC1 & 3FC20 FLOWS ARE IN | I^LIMITS, SWITCH 3FC20 TO REMOTE 126.C OPERATOR STEP PB
|2^T DURING STRIKE RECORD: .r
| SP STEP
.
& ***"
V-243/V-244
- . PH RANGE . TIME:,
13/46 <30 MIN)
9LST 9.3-10.0 <T/_^V
14/47 <60 MIN)
J5LSL 9.3-10.0
15/48 (2 HRS)
*.3-10.0 Ta^syP
1 6/49 <2 HRS, 25 MIN) _2i3 *.3-10.0
17/50 (FINAL 3 HRS)-^^^. 7.5-8.5 z Z&EsL
NOTE: IF PH NOT IN RANGE, NOTIFY ,SUPV & NOTE
IN LOG. IF FINAL PH >8.5, ADJ TO 7.5-8.5.
6 RECORD: PH ____
ASSUME 772
SIFT IN (BLANC FIXE N)
ADD 42* (320 G) WATER TO V-385
ADD 6 STIR FOR 2 MIN FOR S 57
ASSUME 502 I -260-),bO
Tk 'T DURING STRIKE CHECK LEVEL IN V-387.
387 T32 | IF LOU LEVEL LIGHT IS NOT LIT, GO TO S-35 7 133 1 IF LOU LEVEL LIGHT IS LIT, VERIFY BY CHECKING THAT LOU LEVEL PEG IN VAT IS- ABOVE SURFACE IF VISUAL CHECK CONFIRMS LOW LEVEL, FOLLOW
STEARATE MAKE-UP PROCEDURE.
7-D
RUN IN 25* (244 GAL). DO NOT MAKE UP THIS SOLUTION MORE THAN 30 MINUTES IN ADVANCE. DELAY BETWEEN END OF STEP 41 HEAT-UP AND START OF STEP 48 HOMOGENIZATION SHOULD BE LESS THAN 30 MINUTES.
'Tu r n o n s t e a m k a g it a t o r
"ADJUST TO 32' (317 GAL) AT 178-182*F *
KW | SET BADGER METER FOR. 466* fesHTPUMP IN FROM V-387 THRU UNDERSRFCE DISTRIBUTORS
Tl AS FAST AS POSSIBLE (ISOBUTYL STEARATE, BUTYL I . L.STEARATE, EMCOL P-10-59) _T40"T SHUT OFF PUMP 1^1 STIR 30 MIN AT 178-182*F FOR S 48 1,42 I DO NOT SHUT OFF AGITATOR
378 44 44
. 'P&'TJ ` .
169 378 155 444160-A -j 44
DUP050059994
LOT=
. COMTYP JOB NAME*. 03KY9O8DMG PAGE 3
BATE PRINTED:10/05/82
I PAGE 3 CG 3 KY-908-D
WENT | - |
'- '
&?r
l^_________________ _________________________ ^ :_____________________
WHEN S28 COMPLETE HEAT SV TO 198-200 DEG F IN TO 1 MIN
.1
CLOSE WATER LINE i. DISCHARGE . VALVES AT STEARATE)
PUMP
|
OPEN V-388 DISCHARGE VALVES TO STEARATE PUMP
INLET
-
OPEN WATER VALVE AT STEARATE PUMP 6 RUN WATER
^4w,.;v-' .1
-THRU HOMOG AT 2900-31OOPSI, TO SEWER | WHILE HOMOG WATER AT 2900-310 PSI, OPEN HOMOG
| DISCHARGE VALVE TO SV AND CLOSE VALVE TO SEWER
IMMEDIATELY OPEN STEARATE PUMP DISCHARGE VALVE, TURN ON PUMP & HOMOG V-388 TO SV AT 2900-310
PSI* MAINTAIN SV AT 198-20*F.
WHILE HOMOG V-388 TO SV, SHUT OFF WATER VALVE
AT STEARATE PUMP ASAP
WHEN HOMOG COMPLETE, RINSE IN V-388 WITH HOT
WATER FROM HOT WATER MIXER
WHEN S50 COMPLETE TURN OFF HOMOG 6 STEARATE
PUMP'
&IUSTIR 5 MIN AT 198-20*F
I5TJU SHUT OFF STEAM 15<> WHEN S53 COMPLETE, OPERATOR PJB
]pgr\ SP STEP 23/53 RECORD PH_3V<?,,(3 .3-3.7)
f56 I IF NECESSARY, ADJ^PH TO 3*3-3.7 (DOWNWARD ONLY)
& RECORD: PH^l.
NOTE: USE LIQUID ALUM, N-115-p. ADD TO SV VIA
BADGER METER. STIR 5 MIN AFTER EACH
ADDITION.
ASSUME 507.
RUN IN N-7-D FROM S-30 IN 10-12 MIN 6 STIR 5MIN
RECORD: PHjyL. (4.2-4.4) G IF, NECESSARY, ADJ
TO PH 4.2-4.4 tf RECORD: PHjSi?. ASSUME 50%
(DILUTE 10 PARTS TO 1 WITH WATER) ASSUME 78%
| J_- SIPHON N-7-D INTO SV
l^i<J__IJPERATOR STEP PB
1d'*rTDPERAT0R STEP PB
16j^T SP STEP 60 - BATCH COMPLETE
USE LBS
.JSJ3L,
N- |ACCT CODE | LBS
.I"
115-D I______
I
7-D |_JZo 27-D I___
I
START TIME,* SP : TEP
FINISH
OPERATOR
SP STEP
DUP050059995
DU P050059996
No. 215A144
DUP050059997
-2>0-
Sr-- r-
4-
i i
4--
r~ 5 ' yr !
|__
tIAlk,,,
* 1 <?
-f f--
,1K1a;w/f%
-f
,4
fJ2; ...
j ... jlw
12*iO
-250-
1
iwf)~ * *.
y- - - - - : $*
--
,.li!A
k
/
. . V* iJr
11zt% I;Ml
:
/Ur*
j
4JI
ul
f
--4.
-t
"Hi##\{u% .
iHfIlf
fe .
i-- r
--r~
--
--1-- 0i
pamiKO in QAA* ..
" OrfO)'
r~j--
4*.
g* ^--J---
^0
1L S '
. No. 215A250
1 L,.
i
3
--
K
-j
.fit 1V
i
-
-r -/
i 4k
. '*
DUP050059998
WV 9
DUP050059999
DUP050060000