Document 8O6q1rrz8jddN4VdGpbwyR9e
STL Burlington Colchester, Vermont
Extended Data Package
SDG: 117702
Case Narrative Chain of C ustody........................................................................................................ Sample Report Summary - G eotechnical............................................................. Supportive Documentation - G eotechnical.......................................................... Sample Handling......................................................................................................... Last Page of this Document......................................................................................
1 2 12 34 41 43
Case Narrative
i
SEVERN
TRENT
STL
December 4, 2006
Mr. Charlie Young Weston Solutions 1400 Weston Way West Chester, PA 19380
STL Burlington 208 South Park Drive, Suite 1 Colchester, VT 05446
Tel: 802 655 1203 Fax: 802 655 1248 www.stl-inc.com
Re: Laboratory Project No. 26000 Case: 26000: SPG: 117702
Dear Mr. Young:
Enclosed are the analytical results for the samples that were received by STL Burlington on November 17th, 2006. Laboratory identification numbers were assigned, and designated as follows:
Lab ID
Client Sample ID
Sample Date
Sample Matrix
Received: 11/17/06 ETR No: 117702
692810 692811 692812 692813 692814 692815 692816 692817 692818 692818DP 692819 692820 692821 692822 692823 692824 692825 692826 692827 692828 692829
DL3I01CFW0010041216 DMCI01CFW0010041216 DL2I01CFW0010041216 DBCI01CFW0010041215 DL1101CFW0010041215 DOUI01CFW0010041216 DL2F01IPW0050041215 DL3F01IPW0010041130 DL3F01IPW0020041130 DL3F01IPW0020REP DL3F01IPW0030041130 DL3F01IPW0040041130 DL3F01IPW0050041201 DOUF01MSF0040041216 DOUF01MSF0050041216 DOUF01MSW0010041216 DOUF01MSW0020041216 DOUF01MSW0030041216 DOLIF01MSW0040041216 DOUF01MSW0050041216 DL1F01IPW0050041216
12/16/04 12/16/04 12/16/04 12/15/04 12/15/04 12/16/04 12/15/04 11/30/04 11/30/04 11/30/04 11/30/04 11/30/04 12/01/04 12/16/04 12/16/04 12/16/04 12/16/04 12/16/04 12/16/04 12/16/04 12/16/04
TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE
Documentation of the condition of the samples at the time of their receipt and any exception to the laboratory's Sample Acceptance Policy is documented in the Sample Handling section of this submittal.
Leaders in Environmental Testing
1.1
Severn Trent Laboratories, Inc.
STL
December 4, 2006 Mr. Charlie Young
Page 2 of 2
Lipids: There were no exceptions to the method quality control criteria during the analyses of these samples.
The analytical results associated with the samples presented in this test report were generated under a quality system that adheres to requirements specified in the NELAC standard. Release of the data in this test report and any associated electronic deliverables is authorized by the Laboratory Director's designee as verified by the following signature.
If there are any questions regarding this submittal, please contact me at 802 655-1203.
Sincerely,
Ron Pentkowski Projct Manager
Enclosure
1.2
Chain of Custody
2
CHAIN OF CUSTODY / ANALYSIS REQUEST FORM
EXYGEN RESEARCH SAMPLE RECEIVING
T: 814-231-8032
F: 814-231-1580
3048 Research Drive
State College, PA 16801
PAGE
/ of f
S E S B lB lP iii
Client: Weston Solutions, Inc. 1400 Weston Way, Bldg. 5-2 West Chester, PA 10380 T: 610-701-3761 F: 610-701-7401
Project Manager: Jai Kesari email: i.kcsarj@wostonsol utions.com
Project Name; Reference No:
Decatur, Alabama 02181-129-081-0001
Sampler:
Chartes Young
P.O. #; Quotation #:
SAMPLE ANALYSIS
Fish Samples
ExyLIMS # Client Sample Identification
Collection Colction Oat# Ttame
Sampt#
oo
zo
M atrix
Comments
w
DL2 F1 IPW05 041215 15-D0C-4 9:05
FISH
DL3 F1 IPW001 041130 30-Nov-04 10:30
FISH
X
DL3 F1 IPW02 041130 30tNov-04 10:35
FISH
X
DL3 F01 IPW03 041130 30-Nov-04 10:40
FISH
DL3 F01 IPW004 041130 30-NOV-04 10:45
FISH
DL3 F01 IPW005 041201 1-Dec-04 10:00
FISH
CHAIN OF CUSTODY
Cooler ID No.:
Cooler Temp. fC );
Relinquished By:
Date Time
Received By:
Date Time
Charles Young (Weston) 12/17/04 12:00
Tim Frinak (Weston)
12/17/04 12:00
//a j c f~ 7
"y-Ziic
/ C /fW
1-1
% Lipids to be analyzed by STL {Analysis of sample homogenate) Call Charlie Young with Questions
at 610-701-3787
I
ES33E B B S 1 S
Results Deadline:
Laboratory Report Options: Sample Results Only Add Case Narrative Add Quality Control Summary Add Calibration Summary
Add Raw Data Other.
CHAIN OF CUSTODY / ANALYSIS REQUEST FORM
EXYGEN RESEARCH SAMPLE RECEIVING
T: 814-231-8032
F: 814-231-1580
3048 Research Drive
Slate College, PA 16801
PAGE
l..Q f f
Client; Weston Solutions, Inc, 1400 Weston Way, Bldg, 5-2 West Chester, PA 19380 T: 610-701-3761 F: 610-701-7401
Sampler:
Charles Young
Project Manager: Jai Kesari email: .kesari@westonsolutions,com
Project Name: Reference No:
Decatur, Alabama 02181-129-081-0001
P.O. #: Quotation #:
ANALYSES REQUESTED
SAMPLE ANALYSIS
Fish Samples
ExyLIMS #
Collection Collection
Client Sample identification
Dote
tim e
DOU F01 MSF004 0 041216 ie-Dec-04 13:15
DOU F01 MSF005 0 041216 16-Dec-04 13:20
DOU F01 MSWO01 041216 fe-Dec-04 13:30
DOU F01 MSW002 041216 16-Dec-04 13:35
DOU F01 MSWG3 041216 16-Dec-04 13:40
DOU F01 MSW004 041216 16-Dec-04 13:45
DOU F01 MSW005 041216 16-Dec-04 13:50
DL1 F01 IPW005 041216 16-Dec-Q4 14:15
DL2 FG1 IPW003 DL2 F01 IPW04
041201 1-Dec-04 13:30 041215 15-Dec-04 0:00
zl u
Sample
Matrix
1 FISH
FISH
FISH
FISH
FISH
FISH
FISH
FISH
FISH
FISH
CHAIN OF CUSTODY
Cooler ID No,;
Cooler Temp. f*C):
Relinquished By:
Date Time
Charles Yount! (Weston) 12/17/04 12:00
Received By: Tim Frinak (Weston)
Date Time 12/17/04 12:00
Zy/yz*---t--"- / * *
//zzfasri/ ,r
% Lipids to be analyzed by STL (Analysis of sample homogenate) Call Charlie Young with Questions
at 610-701-3787
_______ _______________
Comments
X
PROJECT REQUIREMENTS
Results Deadline:
Laboratory Report Options: Sample Results Only Add Case Narrative Add Quality Control Summary Add Calibration Summary Add Raw Data Other:
I
CHAIN OF CUSTODY / ANALYSIS REQUEST FORM
EXYGEN RESEARCH SAMPLE RECEIVING
T: 814-231-8032
F: 814-231-1580
3048 Research Drive
State College, PA 16801
PAGE
4- o f y
Client: Weston Solutions, Inc. 1400 Weston Way, Bldg. 5-2 West Chester, PA 19380 T: 610-701-3781 F: 610-701-7401
Sampler:
Charles Young 610-701-3787
Project Manager: Jai Kesari email: i.kesan>westonsolutions.com
Project Name: Reference No:
Decatur, Alabama 02181-129-081-0001
P.O. #: Quotation it:
ANALYSES REQUESTED
SAMPLE ANALYSIS cism Semples
ExyLIMS # Client Sample Identification
ICoHection Collection
D ate
Tme
L 3 $01 CFW001 0 041216 16-Dec-04 10:30
DMC 101 CFW001 0 041216 16-Dec-04 14:30
DL2 101 CFW001 041216 16-Dec-04 9:00
DSC 101 CFW0Q1 041215 1S-Dec-04 16:30
X
DL1 101 CFW0D1 041215 1S -D b c -04 11:30
DOU 101 CFW001 041216 16-D 8C-04 8:45
Sam ple Matrix
Clam Clam Clam Clam Clam Clam
Comments
X X
CHAIM OF CUSTODY
Cooler ID No.
Cooler Temp. (C):
Relinquished By:
Date Time
Charles YpiiPiFtVVdor.} 12(17/04 12:00
Received By: Tim Frjnak (Weston)
Date 1Time 12/17/04 ! 12:00
*^
/ "s2t*x. >
'/fce
f//U r //X /
NOTES:
u I ) A -> /< * , o ^ S
% lipids to be analyzed by STL {Analysis of sample homogenate) Call Charlie Young with Questions
at 610-701-3787
PROJECT REQUIREMENTS
Results Deadline:
Laboratory Report Options: Sample Results Only Add Case Narrative Add Quality Control Summary Add Calibration Summary Add Raw Data Other:
3058 Research Drive
State College, PA 16801
H
Phone: 814-272-1039 Fax: 814-231-1580
Loain
Login Group: L0004253
Login #: Project:
Company Name: Submitted By: Login Type: Started: Date Start: Due Date: Login Initiated*:
4363 P0000760 Weston Solutions, Inc. Jaisimha Kesari, P.E., DEE Immediate Receipt of Samples True 01/13/2005
01/13/2005
Conform COC Sample: Conform COC: Conform Sample: Conform Request:
False True True True
* Dates entered into "Login Initiated" field prior to 1/5/06 reflect dates of receipt. The field was formerly called "Received Date"
Received By:
Robb, Shawn
Spread Sample:
Label:
Exygen SD/PI: Flaherty, John
Project Title/Type: Analysis of Perfluorooctanoic Acid (PFOA) in Water, Soil, Sediment, Fish, Clams, Vegetation, Small
Mammal Liver and Small Mammal Serum Using LC/MS/MS for the 3M Decatur Monitoring Program /
ROUTINE
Login Notes:
Conform Notes: There were 2 samples that had the same id on the bags but different weight marked on the bags. Called client and resolved the issue
with the weight on the bags. (DBC F01 (MSF003 OR MSF004) 0 041216) SLR 1/13/2005 Talked to Charles Young.
Packaae PK0005104
Carton
Date / Condition
Packages / Containers
ShiDDer/ ID
Received Date: 1/13/05 15:33 Package & Contents Uncompromised
FEDEX 847967144820
TemD. Control/TemD.
Dry Ice 0.0
Direction / Handled
RECEIVED Robb, Shawn
Container #
C0056354 C0056455 C0056456 C0056457 C0056458 C0056459 C0056460 C0056461 C0056462
Gross Weiaht
43.30 g 603.00 g 780.00 g 719.30 g 655.30 g 331.70 g 673.80 g 648.30 g 154.50 g
dH
Container TvDe
1 gallon zlploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag
Preservative
NONE NONE NONE NONE NONE NONE NONE NONE NONE
Mfa. Lot
Mfa. ID
PK0005105
Container#
C0056463 C0056464 C0056465 C0056466 C0056467 C0056468
Received Date: 1/13/05 16:21 Package & Contents Uncompromised
Gross Weiaht
180.40 g 528.00 g 422.70 g 162.30 g 120.40 g 131.30g
dH
Container TvDe
1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag
FEDEX 847967144886
Preservative
NONE NONE NONE NONE NONE NONE
Dry Ice 0.0
Mfa. Lot
RECEIVED Robb, Shawn
Mfa. ID
11/16/2006
Loain. rat
Report Version: Oct 25 2006 8:30AM
Pane 1 nf 4
6
Instance:
R0299342 iuni iii mimumiinnmuinnmii
Login
Login Group: L0004253
Login #: Project:
Company Name: Submitted By:
4363 P0000760
Weston Solutions, Inc. Jaisimha Kesari, P.E., DEE
Conform COC Sample: Conform COC: Conform Sample: Conform Request:
False True True True
Login Type:
Immediate Receipt of Samples
Started:
True
Date Start:
01/13/2005
Due Date:
Login Initiated*: 01/13/2005
* Dates entered in to ' Login Initiated" field prior to 1/5/06 reflect dates of receipt. The field was formerly called "Received Date"
Received By:
Robb, Shawn
Spread Sample:
Label:
Exygen SD/PI: Flaherty, John
Project Title/Type: Analysis of Perfluorooctanoic Acid (PFOA) in Water, Soil, Sediment, Fish, Clams, Vegetation, Small
Mammal Liver and Small Mammal Serum Using LC/MS/MS for the 3M Decatur Monitoring Program /
ROUTINE
Login Notes:
Conform Notes: There were 2 samples that had the same id on the bags but different weight marked on the bags. Called client and resolved the issue
with the weight on the bags. (DBC F01 (MSF003 OR MSF004) 0 041216) SLR 1/13/2005 Talked to Charles Young.
Packaae PK0005105
Carton
Date / Condition
Packages / Containers
ShiDDer/ ID
Received Date: 1/13/05 16:21 Package & Contents Uncompromised
FEDEX 847967144886
TemD. Control/TemD.
Dry Ice 0.0
Direction / Handled Bv
RECEIVED Robb, Shawn
Container # C0056469 C0056470 C0056471 C0056472 C0056473 C0056474 C0056475 C0056476 C0056477 C0056478 C0056479
Gross W eiaht 215.50 g
dH
Container TvDe 1 gallon ziploc bag
502.60 g
1 gallon ziploc bag
202.20 g
1 gallon ziploc bag
198.40 g
1 gallon ziploc bag
196.50 g
1 gallon ziploc bag
235.70 g
1 gallon ziploc bag
188.20 g
1 gallon ziploc bag
133.40 g
1 gallon ziploc bag
2,496.00 g
5 gallon plastic bag
1,797.40 g
5 gallon plastic bag
2,062.80 g
5 gallon plastic bag
Preservative NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE
Mfa. Lot
Mfa. ID
11/16/2006
I nnin rnt
Report Version: Oct 25 2006 8:30AM
D ana 0 nf A
7
Instance:
R0299342
iiiiiiiiiiiiiniiiiii iiiiiiiiiiiiiiiiiiin iii
Sample ID L0004253-0001
Container C0056455
Matrix SOLID
L0004253-0002
C0056470
SOLID
L0004253-0003
C0056464
SOLID
L0004253-0004
C0056465
SOLID
L0004253-0005
C0056459
SOLID
L0004253-0006
C0056479
SOLID
L0004253-0007
C0056472
SOLID
L0004253-0008
C0056463
SOLID
L0004253-0009
C0056460
SOLID
L0004253-0010
C0056456
SOLID
L0004253-0011
C0056458
SOLID
L0004253-0012
C0056461
SOLID
L0004253-0013
C0056462
SOLID
L0004253-0014
C0056477
SOLID
L0004253-0015
C0056478
SOLID
L0004253-0016
C0056457
SOLID
Login
Fraction Fish
Samles
Sample DL2F01 IPW005 0 041215
Fish DL3F01 IPW001 0 041130
Fish DL3F01 IPW002 0 041130
Fish DL3 F01 IPW003 0 041130
Fish DL3F01 IPW004 0 041130
Fish DL3 F01 IPW005 0 041201
Fish DOU F01 MSF004 0 041216
Fish DOU F01 MSF005 0 041216
Fish DOU F01 MSW001 0 041216
Fish DOU F01 MSW002 0 041216
Fish DOU F01 MSW003 0 041216
Fish DOU F01 MSW004 0 041216
Fish DOU F01 MSW005 0 041216
Fish DL1 F01 IPW005 0 041216
Fish DL2F01 IPW003 0 041201
Fish DL2F01 IPW004 0 041215
11/16/2006
I n n in rn t
Report Version: Oct 25 2006 8:30AM
D o n a *3 n f A
8
Date SarriDled 12/15/2004
Date Due
11/30/2004
01/13/2005
11/30/2004
01/13/2005
11/30/2004
01/13/2005
11/30/2004
01/13/2005
12/01/2004
01/13/2005
12/16/2004
01/13/2005
12/16/2004
01/13/2005
12/16/2004
01/13/2005
12/16/2004
01/13/2005
12/16/2004
01/13/2005
12/16/2004
01/13/2005
12/16/2004
01/13/2005
12/16/2004
01/13/2005
12/01/2004
01/13/2005
12/15/2004
01/13/2005
Instance:
R0299342
Illllllll III Hill Mill Hill HIMMill Hill lili Illl
L0004253-0017
C0056354
SOLID
L0004253-0018
C0056474
SOLID
L0004253-0019
C0056475
SOLID
L0004253-0020
C0056468
SOLID
L0004253-0021
C0056467
SOLID
L0004253-0022
C0056476
SOLID
L0004253-0023
C0056473
SOLID
L0004253-0024
C0056469
SOLID
L0004253-0025
C0056471
SOLID
L0004253-0026
C0056466
SOLID
Login
Fish DL2 F01 MSF005 0 41216 Fish DBC F01 MSF003 0 041216 Fish DBC F01 MSF004 0 041216 Fish DBC F01 MSF005 0 041216 Fish DBC F01 MSF005 1 041216 Fish DMC F01 MSF001 0 041216 Fish DOU F01 MSF001 0 041216 Fish DOU F01 MSF002 0 041216 Fish DOU F01 MSF002 1 041216 Fish DOU F01 MSF003 0 041216
12/16/2004 12/16/2004 12/16/2004 12/16/2004 12/16/2004 12/16/2004 12/16/2004 12/16/2004 12/16/2004 12/16/2004
01/13/2005 01/13/2005 01/13/2005 01/13/2005 01/13/2005 01/13/2005 01/13/2005 01/13/2005 01/13/2005 01/13/2005
Login Reviewed By: ____________________________________________ Date/Time:
11/16/2006 I n o in rn t
Report Version: Oct 25 2006 8:30AM Ponn A nf A
9
Instance:
R0299342 Illllllll IIIMill lllll lllll HIMHilllllll llll INI
3058 Research Drive State College, PA 16801
Phone: 814-272-1039 Fax: 814-231-1580
Loain
Login Group: L0004254
Login #:
4364
Conform COC Sample: True
Project:
P0000760
Conform COC:
True
Company Name: Weston Solutions, Inc. Submitted By: Jaisimha Kesari, P.E., DEE
Conform Sample: Conform Request:
True True
Login Type:
Immediate Receipt of Samples
Started:
True
Date Start:
01/13/2005
Due Date:
Login Initiated*: 01/13/2005
* Dates entered into "Login Initiated" field prior to 1/5/06 reflect dates of receipt. The field was formerly called "Received Date"
Received By: Robb, Shawn Spread Sample: Label: Exygen SD/PI: Flaherty, John Project Title/Type: Analysis of Perfluorooctanoic Acid (PFOA) in Water, Soil, Sediment, Fish, Clams, Vegetation, Small
Mammal Liver and Small Mammal Serum Using LC/MS/MS for the 3M Decatur Monitoring Program / ROUTINE Login Notes:
Packaae PK0005106
Carton
Date / Condition
Packages / Containers
ShiDDer/ ID
Received Date: 1/13/05 17:20 Package & Contents Uncompromised
FEDEX 847967144886
TemD. Control/TemD.
Dry Ice 0.0
Container # C0056480 C0056481 C0056482 C0056483 C0056484 C0056485
Gross Weiaht 277.40 g 405.00 g 366.40 g 363.20 g 279.20 g 553.20 g
pH
Container TvDe 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag
Preservative NONE NONE NONE NONE NONE NONE
Mfa. Lot
Direction / Handled Bv RECEIVED Robb, Shawn
Mfa. ID
11/16/2006 I n n in rnt
Report Version: Oct 25 2006 8:30AM Pano 1 nf 9
10
Instance:
R0299343 IllllllllIIIMilllllllHillHillII UHIllllINI
SamDle ID L0004254-0001
Container C0056480
Matrix SOLID
L0004254-0002
C0056481
SOLID
L0004254-0003
C0056482
SOLID
L0004254-0004
C0056483
SOLID
L0004254-0005
C0056484
SOLID
L0004254-0006
C0056485
SOLID
Login
Fraction Clams
Samples
SamDle DL3 101 CFW001 0 041216
Clams
DMC 101 CFW001 0 041216
Clams
DL2I01 CFW001 0 041216
Clams
DBC 101 CFW001 0 041215
Clams
DL1 101 CFW001 0 041215
Clams
DOU 101 CFW001 0 041216
Date Sampled 12/16/2004
Date Due
12/16/2004
12/16/2004
12/15/2004
12/15/2004
12/16/2004
Login Reviewed By: ____________________________________________ Date/Time:
11/16/2006
I nnin rnt
Report Version: Oct 25 2006 8:30AM
Do Oa O
11
Instance:
R0299343
ilimili inmil mumumil innmil mimi
Sample Report Summary - Geotechnical
12
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DL3I01CFW0010041216
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117702 Lab Sample ID: 692810 Date Received: 11/17/06
Method
LIPIDS
Parameter
%Llpids Determination
Analytical Analytical Run Date Batch
12/02/06
Units %
DF RL
1 0.1
Cone.
1.5
Qual.
Printed on: 12/04/06 08:11 AM
13
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DMCI01CFW0010041216
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117702 Lab Sample ID: 692811 Date Received: 11/17/06
Method
LIPIDS
Parameter
%Lipids Determination
Analytical Analytical
Run Date Batch
Units DF RL Cone. Quai.
12/02/06
% 1 0.1
1.8
Printed on: 12/04/06 08:11 AM
14
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DL2I01CFW0010041216
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117702 Lab Sample ID: 692812 Date Received: 11/17/06
Method
LIPIDS
Parameter
%Lipids Determination
Analytical Analytical Run Date Batch
12/02/06
Units %
DF RL 1 0.1
Cone. 1.0
Qual.
Printed on: 12/04/06 10:34 AM
15
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DBCI01CFW0010041215
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117702 Lab Sample ID: 692813 Date Received: 11/17/06
Method
LIPIDS
Parameter
%Lipids Determination
Analytical Analytical Run Date Batch
12/02/06
Units %
DF RL Cone. Qual.
1 0.1
1.5
Printed on: 12/04/06 08:11 AM
16
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DL1I01CFW0010041215
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117702 Lab Sample ID: 692814 Date Received: 11/17/06
Method
LIPIDS
Parameter
%Llpids Determination
Analytical Analytical
Run Date Batch
Units
DF RL Cone. Qual.
12/02/06
% 1 0.1 1.0
Printed on: 12/04/06 08:11 AM
17
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DOUI01CFW0010041216
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117702 Lab Sample ID: 692815 Date Received: 11/17/06
Method
LIPIDS
Parameter
%Liplds Determination
Analytical Analytical Run Date Batch
12/02/06
Units %
DF RL
1 0.1
Cone.
0.9
Qual.
Printed on: 12/04/06 08:11 AM
18
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DL2F01IPW0050041215
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117702 Lab Sample ID: 692816 Date Received: 11/17/06
Method
LIPIDS
Parameter
%Lipids Determination
Analytical Analytical Run Date Batch
12/02/06
Units %
DF RL Cone. Qual.
1 0.1
10.5
Printed on: 12/04/06 08:11 AM
19
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DL3F01IPW0010041130
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117702 Lab Sample ID: 692817 Date Received: 11/17/06
Method
LIPIDS
Parameter
%Liplds Determination
Analytical Analytical Run Date Batch
12/02/06
Units %
DF RL Cone. Qual.
1 0.1
4.6
Printed on: 12/04/06 08:11 AM
20
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DL3F01IPW0020041130
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117702 Lab Sample ID: 692818 Date Received: 11/17/06
Method
LIPIDS
Parameter
%Lipids Determination
Analytical Analytical
Run Date Batch
Units DF RL Cone. Qual.
12/02/06
% 1 0.1 8.0
Printed on: 12/04/06 08:11 AM
21
GEOTECHNICAL / GENERAL CHEMISTRY
Duplicate Sample Report Summary
Client Sample No. DL3F01IPW0020REP
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117702 Lab Sample ID: 692818DP Date Received : 11/17/06
Method
LIPIDS
Parameter
VoLipids Determination
Analytical Analytical Run Date Batch
12/02/06
Units
%
Sample
Duplicate
Result
Sample Result
Cone. Qual. Cone. Qual. RPD*
8.0 8.4
* Control Limit for RPD is + /- 20%, unless otherwise specified.
Printed on: 12/04/06 08:11 AM
22
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DL3F01IPW0030041130
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117702 Lab Sample ID: 692819 Date Received: 11/17/06
Method
LIPIDS
Parameter
%Lipids Determination
Analytical Analytical Run Date Batch
12/02/06
Units %
DF RL Cone. Qual.
1 0.1
3.3
Printed on: 12/04/06 08:11 AM
23
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DL3F01IPW0040041130
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117702 Lab Sample ID: 692820 Date Received: 11/17/06
Method
LIPIDS
Parameter
%Lipids Determination
Analytical Analytical Run Date Batch
12/02/06
Units %
DF RL Cone. Quai.
i 0.1
1.6
Printed on: 12/04/06 08:11 AM
24
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DL3F01IPW0050041201
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117702 Lab Sample ID: 692821 Date Received: 11/17/06
Method
LIPIDS
Parameter
%Llpids Determination
Analytical Analytical Run Date Batch
12/02/06
Units %
DF RL
1 0.1
Cone.
4.8
Quai.
Printed on: 12/04/06 08:12 AM
25
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DOUF01MSF0040041216
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117702 Lab Sample ID: 692822 Date Received: 11/17/06
Method
LIPIDS
Parameter
VoLlpids Determination
Analytical Analytical
Run Date Batch
Units
DF RL Cone. Quai.
12/02/06
% 1 0.1 0.6
Printed on: 12/04/06 08:12 AM
26
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DOU F01MSF0050041216
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117702 Lab Sample ID: 692823 Date Received: 11/17/06
Method
LIPIDS
Parameter
%Lipids Determination
Analytical Analytical
Run Date Batch
Units
DF RL
Cone. Qual.
12/02/06
% 1 0.1 0.6
Printed on: 12/04/06 08:12 AM
27
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DOUF01MSW0010041216
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117702 Lab Sample ID: 692824 Date Received: 11/17/06
Method
LIPIDS
Parameter
%Lipids Determination
Analytical Analytical
Run Date Batch
Units DF RL Cone. Qual.
12/02/06
% 1 0.1 1.4
Printed on: 12/04/06 08:12 AM
28
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DOUF01MSW0020041216
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117702 Lab Sample ID: 692825 Date Received: 11/17/06
Method
LIPIDS
Parameter
%LIpids Determination
Analytical Analytical Run Date Batch
12/02706
Units %
DF RL Cone. Qual.
1 0.1
1.7
Printed on: 12/04/06 08:12 AM
29
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DOUF01MSW0030041216
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117702 Lab Sample ID: 692826 Date Received: 11/17/06
Method
LIPIDS
Parameter
%Lipids Determination
Analytical Analytical Run Date Batch
12702/06
Units %
DF RL
1 0.1
Cone.
2.7
Qual.
Printed on: 12/04/06 08:12 AM
30
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DOUF01MSW0040041216
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117702 Lab Sample ID: 692827 Date Received: 11/17/06
Method
LIPIDS
Parameter
%Lipids Determination
Analytical Analytical Run Date Batch
12/02/06
Units %
DF RL
1 0.1
Cone.
2.7
Quai.
Printed on: 12/04/06 08:12 AM
31
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DOUF01MSW0050041216
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117702 Lab Sample ID: 692828 Date Received: 11/17/06
Method
LIPIDS
Parameter
%Llpids Determination
Analytical Analytical
Run Date Batch
Units
DF RL
Cone. Qual.
12/02/06
% 1 0.1 1.6
Printed on: 12/04/06 08:12 AM
32
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DL1F011PW0050041216
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117702 Lab Sample ID: 692829 Date Received: 11/17/06
Method
LIPIDS
Parameter
%Llpids Determination
Analytical Analytical Run Date Batch
12/02/06
Units %
DF RL Cone. Quai.
1 0.1
4.9
Printed on: 12/04/06 08:12 AM
33
Supportive Documentation - Geotechnical
34
ST LS E V E R N
TRENT
PERCENT LIPIDS
35
Percent Lipids Calculations
D ate: Tim e:
12/2/2006 1445
A nalyst: ETR (s): C lient:
RH /JRM /JH 2 117702
W ESTN2
Sam ple ID
692810 692811 692812 692813 692814 692815 692816 692817 692818 692819 692820 692821 692822 692823 692824 692825 692826 692827 692828 692829 692818DP
Sam ple W eight
(g ) 5.03 10.02 10.05 9.97 6.51 10.05 9.97 10.01 10.04 10.02 10.00
10.01 10.01 9.98 10.00 9.99 10.02 10.02 10.01 10.05 10.02
D ish
(g ) 1.0145 1.0186 1.0277 1.0029 0.9877 0.9999 1.0282 1.0155 1.0109 1.0222 1.0072
1.0243 1.0473 1.0266 1.0029 0.9787 0.9837 1.0133 1.0147 1.0244 1.0312
D ish/R esidue
(g ) 1.0294 1.0365 1.0375 1.0181 0.9978 1.0091 1.1331 1.0617 1.0908 1.0557 1.0235
1.0720 1.0535 1.0323 1.0164 0.9953 1.0105 1.0402 1.0310 1.0736 1.1149
E xtract F inal V olum e (m L s)
5 10 10 10 6.5 10 10 10 10 10 10
10 10 10 10 10 10 10 10 10 10
A liq uot U sed in D eterm ination
( mLs )
1 1 1 1 1 1 1 1 1 1 1
1 1 1 1 1 1 1 1 1 1
% L ipids
1.5 1.8 1.0 1.5 1.0 0.9 10.5 4.6 8.0 3.3 1.6
4.8 0.6 0.6 1.4 1.7 2.7 2.7 1.6 4.9 8.4 # D IV /0 ! # D IV /0 ! # D IV /0 ! # D IV /0 ! # D IV /0 !
STL Burlington
117 7 02 M B 120206AB
36
12/4/2006
Percent Lipids Calculations
D ate: Tim e:
12/2/2006 1445
A nalyst: ETR (s): C lient:
R H /JR M /JH 2 117702
W ESTN2
Sam ple ID
M B120206A 692810 692811 692812 692813 692814 692815 692816 692817 692818 692819 692820 692821 692822 692823 692824 692825 692826 692827 692828 692829
692818DP
Sam ple
W eight
(g ) 10.00 5.03 10.02 10.05 9.97 6.51 10.05 9.97 10.01 10.04 10.02 10.00 10.01 10.01 9.98 10.00 9.99 10.02 10.02 10.01 10.05 10.02
D ish (
g) 1.0290 1.0145 1.0186 1.0277 1.0029 0.9877 0.9999 1.0282 1.0155 1.0109 1.0222 1.0072 1.0243 1.0473 1.0266 1.0029 0.9787 0.9837 1.0133 1.0147 1.0244 1.0312
D ish/R esidue
(g ) 1.0290 1.0294 1.0365 1.0375 1.0181 0.9978 1.0091 1.1331 1.0617 1.0908 1.0557 1.0235 1.0720 1.0535 1.0323 1.0164 0.9953 1.0105 1.0402 1.0310 1.0736 1.1149
E xtract Final
V olum e
(m Ls)
10 5 10 10 10 6.5 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10
10
A liq uot U sed in D eterm ination
( mLs )
1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1
% L ipids
< 0 .1 1.5 1.8 1.0 1.5 1.0 0.9 10.5 4.6 8.0 3.3 1.6 4.8 0.6 0.6 1.4 1.7 2.7 2.7 1.6 4.9 8.4
#DIV/0! #DIV/0! #DIV/0! #DIV/0!
STL Burlington
117702MB120206A
37
12/4/2006
Percent Lipids Calculations
t^
O
'S
N*
Date : !'> : " O ' I ' o G
Y)\j-c
Time: m s
Analyst: / p$i t .
e t r (s
Client:
H2-
Sample
Weight
Sample ID (g )
irti m(
Kill'iiofiW0
A
lb^UsU
tm
l>9
7
i%-\Ht
*6.00
i . %
s . nio'c> LSI
5)
0 i
il
\l
'
1
io . i wn I. i
L
L
Hv 9A
H
iV I ^2) <kh
l o . X)H
>16..0b6\ 6.05
Dish ( Dish/Residue
g) (g)
l.<A9o
i.oiHS
r. b
V f io \9>L
i.fcV)
D 1
>, 9W999
[i.,6iSmS
iiL--tcb>Qi`oVAl.'kV
f, Th3>
/. o -i*i 0
/. /.
og 3MfcHC
I. o 3 7
*..
c
i
i8
Hi
1
t
Lf . tn3o3i1 1
r{..
O
o
lek'l
He t
(( .
(
-.
a.0i
^7tVc2;tT0
UKi* s
Um^fUo* UQ
ID.*
lo-c/o
O -t/V
i1i-i%~ lo.c
Ui . pWm f oo^i o LAonm(v^) i;6i Mh 1. b%MH
il ,oc ^?32C7
f,r
Ol a
(M
1t-. Oo 7(oIO2 , o7 te
`c i ^ gAitr
9l8inp 10.0%
t. nq<?
t
Extract Final Aliquot Used in
Volume Determination
(mLs) ( mLs )
10 1
- w10- >-l
1 1
10 1
10 1
t10- .s :
1 1
10 1
10 1 ,
10 1
10 1
10 1
10 1
10 1
,10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 1
10 10
11
10 1
10 1
% Lipids ##DDliVy//00!! #DW/0 ! ##DDIlVV//00!! #DIV/0! #DIV/0! ##DDIIVV//00!! #DIV/0! ##DDIIVV//00!! #DIV/0! #DIV/0! ###DDDIIIVVV///000!!! #DIV/0! #DIV/0! #DIV/0! ##DDIFV///00!! #DIV/0! ##DDIIVV//00!! #DIV/0!
STL Burlington
LIPIDCALUPLOAD 1
38
f)
/2 /2 /0 6
/
Percent Lipids Calculations
D ate: Tim e:
12/2/06 1445
A nalyst: ETR (s): C lient:
RH / JRM / JH2 117702
W ESTN2
Sam ple ID
MB 120206A 692810
692811 692812 692813 692814 692815 692816
692817 692818 692819 692820 692821 692822 692823 692824 692825 692826 692827 692828 692829 692818DP
Sam ple W eight
(g ) 10.00 5.03 10.02 10.05 9.97 6.51 10.05 9.97 10.01 10.04 10.02 10.00 10.01 10.01 9.98 10.00 9.99 10.02 10.02 10.01 10.05 10.02
D ish (
g)
1.0290 1.0145 1.0186 1.0277 1.0029 0.9877 0.9999 1.0282 1.0155 1.0109 1.0222 1.0072 1.0243 1.0473 1.0266 1.0029 0.9787
0.9837 1.0133 1.0147 1.0244 1.0312
D ish/R esidue
(g ) 1.0290 1.0294 1.0365 1.0375 1.0181 0.9978 1.0091 1.1331 1.0617
1.0908 1.0557 1.0235 1.0720 1.0535 1.0323 1.0164 0.9953
1.0105 1.0402 1.0310 1.0736 1.1149
E xtract Final V olum e (m Ls)
10 5 10 10 10 6.5 10 10 10 10
10 10 10 10 10 10 10
10 10 10 10 10 10 10 10 10
A liq u ot U sed in
D eterm ination ( mLs )
1 1 1
1 1 1 1 1 1
1 1 1 1 1 1 1 1
1 1 1 1 1 1 1 1 1
% L ipids
< 0 .1 1.5 1.8 1.0 1.5 1.0 0.9 10.5 4.6 8.0
3.3 1.6 4.8 0.6 0.6 1.4 1.7 2.7 2.7 1.6 4.9 8.4 #DIV/0! #DIV/0! #DIV/0! #DIV/0!
STL Burlington
117 7 02 M B 120206A
39
12/2/06
O fr
STL BURLINGTON
% LIPIDS
Sample Handling
41
STL BURLINGTON
SAMPLE RECEIPT & LOG IN CHECKLIST
Client: V v y f 'S T - A / 'c ?
fDate Received:
1- i
ETR: { ! -> n o "3
Time Received:
SDG:
J TR.Received By:
#Project: alArOOO
Coolers Received: \
Sam ples Delivered B y:'X S h lp ping Service a C ourier a Hand O ther (specify)
~'0Q>
Log In Date:
By: "\
,
Signature: ^ CAtS* r - U
PM Signature: A / , . / L t - f r ' ~J
d s : ir
^'
List A ir bill Mumber(s) or Attach a photocopy o f the A ir Bill:
f
COOLER SCREEN D '
'-^
There is no evidence to indicate tampering
Custody seals are present and intact
Custody seal numbers are present
If yes, list custody seal numbers:
`~
YES / INO - :NA- - -1 ` - COMMENTS - - '
yY1 '
Thermal Preservation Type: a Wet Ice Blue Ice o None Toother (specify) c k f \ A \ t . P ,
IR Gun ID:
( 2 .
Correction Factor (CF) = r f S
"C
O
,
Cooler 1:
\ C Cooler 6
"6 Cooler 11
C Cooler 16
C
Cooler 2:
*C Cooler 7
"C Cooler 12
C Cooler17
C
Cooler 3:
"C Cooler 8
C Cooler 13
C Cooler 18
C
Cooler 4:
"C Cooler 9
C Cooler 14
"C Cooler 19
.C
Cooler 5
C Cooler 10
C Cooler 15
C Cooler 20 .
C
Unless otherwise documented, the recorded temperature readings are adjusted readings to account for the CF o f the IR Gun
EPA Criteria: 0-6C, except for air and geo samples which should be at ambient temperature and tissue samples, which may be frozen.
Some clients require thermal preservation criteria of 2-4"C or other such criteria. The PM must notify SM when alternate criteria Is specified.
S e s i -in o ,- NA 1
Sample containers were received intact Legible sample labels are affixed to each container CH AiN lO i^iU STQ D /i^
X
X
y e s :; : NO il'NATi
w
COC is present and includes the following information for each container:
.
Sample ID / Sample Description * Date of Sample Collection
I XT
Time of Sample Collection Identification of the Sampler Preservation Type Requested Tests Method(s) Necessary Signatures
,
x
y y
X X
Internal Chain of Custody (ICOC) Required If yes to above, ICOC Record initiated for every Worksheet
The sample container matches the COC Appropriate sample containers were received for the tests requested Samples were received within holding time Sufficient amount of sample is provided for requested analyses
X
-YES'- ilN O NSi T^ S ^ comments-^.>
X y
e e 'oevtA/
V
X
VOA vials do not have headspace or a bubble >6mm (1/4" diameter)
Appropriate preservatives were used for the tests requested pH of inorganic samples checked and is within method specification
X
If no, attach Inorganic Sample pH Adjustment Form
ANOMALY/NCRSUMMARY
"
A /r > -Vx ' w l NC'S-Vec^
-'Co/^ K_T5rvS ^O'T \nq tVs1 e>-F
S'Vv\71Y1>wnnpJ' Ya.lof' l L/vxrvi"5 0vT'tC'Vc'a c
ck U
X
V XI
-
'
^ r~ \cOa^S / L /S L c i 5 r.svnp \<5 , TKC
1
** .
42
Last Page of this Document
43
