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PESTICIDE RESIDUE AMD
TRACE CONTAMINANT ANALYSIS
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LCAKT M4
In 1964 the Foundation established o Pesticide Residue Anolysis laboratory for the measurement and monitoring of organochlorine pesticide residues in Canadian wild life. The scope of the laboratory hat con tinually expanded since that time and now encompasses analysis of many other types of insecticides, herbicides, fungicides, and residues of other industrial chemicals found in air, water, foods, soils, packaging, and con sumer products.
More recently, with the growing
concern over the presence of heavy metals In the environment, facilities
have been expanded to include analy tical services for troces of mercury,
lead, cadmium, and special fan* f 1km, 'mk m mifMtmikMtet SUfrif
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This laboratory has provided e much needed service In Canada, and Is also active Internationally. It Is the official Canadian representative for OECD programs dealing with uninten tional residues In the environment.
To ensure the highest possible standards of accuracy, the laboratory participates regularly In International as well as notional check sampling programs.
The following is a list of typical analytical services offered.
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Orgonochlorlne Pesticides
Heptaehlor, aldrln, heptochlor epoxide, p,p-DDE, dieldrin, p,p-TDE, o,p-ODT, p,p-DDT,methcxychlor, endrln, technical and gamma ehlordane, Kelthone, endosulfon, mtrex, TedIon,
HCB, a -BMC, 0 -BHC, Y -BHC (Un-
done), etc.
Organephoyhate Pesticides
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Tracer Chromatograph
Diaz (non, porathion, methyl parathion, molathion, ethion, fenitrothion (Sumithion), fcnsuifothion (Dosanft), dursban, etc.
Herbicides
(2,4-0), (2,4,5-T), (2,4,5-TP), MCPA, plcloram, otrazine and other trlasines, chlorinated phenols such as PCP, etc.
Polychlorlnotcd Biphenyls (PCBs) ond Polychlorlnoted Terphenyls (PCTs)
These are classes of Industrial chemicals which, while not used as pesticides, possess many of the charac teristics of the chlorinated pesticides - they are widely distributed, persistent, ond physiologically active, and hence present a similar threat ecologically.
HONS 078693
froci Mttelt Mercury, orgonomercury, leod, codmium, etc.
Oonorol Methodology
The above lists or* Indicative of anolyset frequently required by ORF client*. A now compounds or special problems oro tnceuntiredf the scientific and ttdmlcal staff of thr PerfieUr and Traca Contaminant tnbwlosy oro wall qualified to evaluate known analytical methods end develop new ones. For example, with Increased Interest in carbamates and orgonophosphatet as replacements for the more persistent orgonocMonne pesticides, the laboratory Is extending its methodology studies of these two classes of insecticides.
Special Instrumentation
Hewlett Packard Model HP 5713 gos chromatograph connected to: 43
New linear (constant current) EC detector (Ni ) HP Auto-injector with turntable for 36 samples
Autolob System I computing integrator
Tracor Research Gos Chromatograph (Model MT220) including:
flame photometric detector (Phosphorus end Sulphur)
UnoarNI** electron capture detector (Tamp, to 400X)
Ceuiton dotoetor (Holagen^ Su^pher, Nttropen)
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k Varlen gas chromatographs (Models 1200, 1400, 15221, autoprep)
Gas Chromatograph-Mass Spectrometer-AEI MS30
Waters Analyticat High Pressure Liquid Chromatograph Model ALC 202/401/6000 equipped with:
U.V. Detector R.l. Detector 6000 p.s.i. Pump
Chromatography - Thin layer, column
Atomic Absorption Spectrophotometers including:
Vorian models AA120 and AA5 with carbon rod atomizer for Nameless atomization
Unicom SP9QA Mercury Monitor (Laboratory Data Control)
Spectrophotometers - visible, UV, Nt
NMJt - JEOL. JNM - 4H - 100
Polarograph (Princeton Applied Research, Model 174)
. Low Temperature Asher (LFE Corporation, Model 302)
A list of clients who hove mode use of these laboratory facilities includes numerous Faderol and Pro vincial Government Agencies and Ministries, at least twenty paper companies ocross Canada, and a variety of Industrial end commercial companies, universities, and commercial laboratories.
TKCNNOLOOIKS FOR INDUSTRY
Tho Ontario Rmmoarch Foundation to Canada's moot comprohotf e/re roaouroo for tnduatrla/ Contraat Raaaareh and Deva/opmant.
An tndapondont tnduatrla/taaaarcb organisation. ORF la goaornad If prominent bualnaaamon and aoianttata. ttm capita! funda neve kaon aubaeribad bf Canadian manufaeturora and lira Province of Ontario.
MOHS 078894
ONTARIO HCSIARCH FOUNDATION SHERIDAN PARK, MISSISSAUGA. ONTARIO, CANADA LSK 103 PHONE: <4H>) . .V -Mil