Document 82YmYrx4ZEGmD4RJJpmE1qG6k
CG 36
CODE RT-444-D
MAY 251982 F2H17
"<"5a t e ")
("l o t ")
PKG ___
ESTIMATED WGT
LBS.
PREPARATION NOTESJ ____ ___________
PROCESSES < )RT-444-D(A) COMTYP JOB NAME: TYPED BY: KLW
STANDARD HRS. ___
APPROVED BY EWK 02/05/82
36RT444DMA
TIME
_M;
EQUIP I MENT ,I
MISC
DUOL CARMINE
FIRST BATCH FOLLOWING WATCHUNGS, CLEAN DRESS SPARKLER 6 PRECOAT SPARKLER WITH
* FILTER AID. RUN 15* WATER IN V-904 & PUMP INTO V-901 THRU DISTRIBUTOR. IF WATER DOES NOT COME OUT OF ALL DISTRIBUTOR HOLES WITH FULL FORCE, NOTIFY SUPERVISOR.
NON-BLEEDING
USE LBS
N-CODE
--I
I
A COT LBS
15 I 777-A | 15
RECORD:_0,,_BATCHES SINCE'SPARKLER LAST
CLEANED. AFTER 4 BATCHES, CLEAN, DRESS r`ARKLER 6 PRECOAT WITH 15* FILTER AID.
OBTAIN 4-AMIN0T0LUENE-3-SULF0NIC ACID FflR SI 8. "
OBTAIN 3-HYDR0XY-2-NAPHTHOIC ACID FOR S35
I 777-A I. I 549.-C |
I . l I 82-C I
29* (59? G) WATER INTO V-932
WEIGH SODIUM HYDROgDE IN
RUN MN
(N ON AG ITATOR~& STEAM"* ~
SJ.3--1 I
"WHILE HEATING, ADD DRESINATE X IN 8-9 MIN .
460 i
-- VT-TO 180-185#F RCD: TEMP.__4f^___*F
30 MIN.., OR LONGER TO DISSOLVE JfiD: PH^JLj JLi S..< l'l ..8712.0) : CF PH BELOW 11.8, ADJ. TO PH 11.8 OR
m
ABOVE FOR S68 RCD: PH______
ASSUME 50%
7-D I ' 58 I.
530-A I 460
1982 1 I 7-D I___.
TIFY PROCESSING BEFORE ROPING OFF AREA EATH V-922. THEN ROPE IT OFF. 64' (1318 G) . WATER INTO V-922 SODIUM HYDROXIDE.
ON AGITATOR & STEAM 4. HEAT TO 85-90*F DUMP IN 4-AMINQTQLUENE-3-SULF0NIC ACID * FROM S4
LOT
24>
7-D 549-C
COMTYP JOB NAME ^ 36RT444DMA
PAGE 2
DATE PRINTED: 2/05/32
EQUIP I ~~T|
~
MENT | I^PAGE 02 OF 04 CG 33
CODE RT-444-D(A)
| USE ~N-CODi' | LBS j
922 \W, \ STIR 15 MIN & RECORD: BY__^EEC<MUSTBE +) I
I
4 ( VL-^y PAPER TURNS RED*
CON'T |San 1^. NECESSARY, ADD SODIUM HYDROXIDE TO + BY
: |- J<RfC0RD: :BY,,.___L.
ASSUME 50%
H9T\ CHECKFOR COMPLETE SOLUTION RECORD:
'l-V;'J^|SULTS___ ________
UMP IN ACTIVATED CARBON .33*T ^DUMP IN FILTER AID .
15 MIN*
^
RECORD: SPARKLER PRESSUREJ_C>____ PSI NOT ZERO, NOTIFY SUPERVISOR
CIRCULATE 15 MIN OR LONGER AT 85-90*F
SPARKLER UNTIL SOL'N IS CLEAR. MAIN AT 85-90*F FpR^-28. RECORD: START
l min _j 55L_. c l a r it y ^_4LZ4s 5i
II II I _______ I
I 22 I 20 I
I I
7-D
113-B 777-A
ACCT LBS
no 20
UN 1* (95 G) MATER INTO V-901 : >/
\ WHEN S26 COMPLETE,^PUMP IN V"922 THRU . I SPARKLER. MAINTAIN `V-922/AT 85-90*F^<
I RECORD: START^^^ftll. TOTAL MlN_r3.$__ `
1
., I
"WEIGH SODIUM NITRITE IN PT.FOR S57 * - m___j L__,
mtiSURE towji^UNITS IN V-928 FOR^ S55
mDROCHLORlCAClD M__jL____
MEASURE
UNITS IN,V-927 ACETIC, ACID
FOR SB0
M,,_i/____ __ jfe*JUL_%
I vl
imi-i-1 lfj> J i.- i
V J y-j* 1
725/A | "216 .* / I
$8-D ( ,268
30-D I 200
'20* (503 G> WATER INTO V-902. "WEIGH..SODIUM'HYDROXIDE V-926^6^RUN^ IN
|34,nLjURN ON AGITATOR N"STEAM"G'*HEAT TO 95-100*1
]35>TDUMP IN 3-HYDRQXY-2-NAPHTH0IC ACID FROM S5
II
...
' LOT,...........
1"
' "tiMShr'
. 3ac_*+
|36T| STIR 30 MIN OR LONGER TO DISSOLVE FOR S67v
7-D | 378
I-
82-C 4,
I I
922 |3T WHEN S28 COMPLETE, SHUT OFF SPARKLER PUMP |
. 8 | Jx ONSERT FOOT PLUG.
- '
I
\mfUmwm 10* (206 G) WATER
I
13^T>PN ON AGITATOR & HEAT TO 85-90*F.
I
[CORD: SPARKLER PRESSURE
___ PSI. IF I
NOT ZERO NOTIFY SUPERVISOR.
I
[4K'|' CIRCULATE 15 MIN OR LONGER AT 8S-90*F THRU I
/SPARKLER UNTIL SOL^ IS CLEAR.
I
\tQA RECORD: CLARITY._iS.Dw_ THEN SHUT OFF STEAM. I
l
& IT"
V
DUP050047800
GOMTl'P JOB NAME = 36RT444DMA
PAGE 3
DATE PRINTED: 2/05/82
USE | N-CODE I ACCT
AGE 03 OF 04 CG 36 CODE RT-444-D (A) LBS 'I
) LBS
1 WHEN S41 COMPLETE, PUMP V-:922 THRU SPARKLER I INTO V-901,
922 10
'
|4*T| WJ^EfS S43 COMPLETE, SHUT OFF SPARKLER PUMP
I ]/ INSERT FOOT PLUG*
)45>n RUN IN 5* <103 G> WATER 6 HEAT TO 85-9*F
I I XHEN,SHUT OFF STEAM,
^
REetiRV: SPARKLER PRESSURE _J/f___ PSI, IF
l J^IOT ZERO NOTIFY SUPERVISOR
.\#T 1 CIRCULATE 15 MIN OR LONGER THRU SPARKLER
I JJJNflL SOL1N IS CLEAR,
4JTTREC0RD: dLARITY_jSj5L____
N S47 COMPLETE, PUMP V-922 THRU SPARKLER
INTO V-901.
I WHEN V-922 EMPTY, BLOW OUT SPARKLER INTO
V`"901 .
;i
1 1 i i - i
1 1V 1;; "> 1 . 1. '
2- (322 G> WATER INTO V-904 ON AGITATOR & ADD CALCIUM CHLORIDE TO ?-80#F. STIR 15-20 MIN TO DISSOLVE FOR S77,
72^"'S1, 20-A 1...
: i*1
r .atm. . j i '
UST TO mm#*F WITH ICE/
URN ON STACK EJECTOR*
1, RUN IN SODIUM NITRITE- <N-?25-A)
Stf 5-1 MIN 6 RINSE IN PT.
ADjBJST TO 74* .<6480
WITH .
^W??TTEER &6 IiCEi C- '
4f7P8-"VyVjf'
IN V-928 HYDROCHLORIC ACID FROM S3
P Ap
.%
IMMEDIATELY ADJ TO42-44F
RECORD:-
ACCURACY - HT#_(VjEti_*F' REC__^2^KF
RECORD: CR2^^X + > CONGO. RED PAPER TURNS
BLUE K*_< + > KI PAPER TURNS BLUE
NOTE: CfTlF^eR*, KI- ADD 200 "AS IS',
INCREMENTS SODIUM NITRITE ASSUME 33%
<20 IF CR-oKI- ADD 200 *AS IS*,
INCREMENJFE^HYDRDCHLORIC ACID ,
' ASSUME 32%
<3^rREPEAT ABOVEAS NECESSARY TO
+CR, '+KI RECORD: CR___.__< + >;
KI_,,_< + )
WEIGH SULFAMIC ACID IN PLASTIC BUCKET 6 -
,._NSE IN
'
STIR 10 .MIN 6 RECORD Kl^hr-- <MUST BE -)
KI PAPER STAYS WHITE*
IF NECESSARY ADJ TO -KI WITH SULFAMIC ACID
Ki__r!!T__<->
'
OFF STACK EJECTOR.
ADJ TO 85' <7560 G) AT
#F WITH WATER
& ICE,
20X330| 1
5 *7-A 7?Mb>
.1 : ' ; '/ ` i. ,,/
ii
1 8X3301
57-A i :i*!: i <
I l11
-
///'
i ii1
'; :/.*. /
1 - -- ' . . l ' /
1j 1I . * -:rv.
i l ;
i___________ 725-A , i
i*i. - l1 . *. v. 28-D
i
J , '
p -
25V'| 395.-D I V/.25:. 11 1 i- -
395-D | /Q 1]1 111 ~~~
57-A
**
DUP050047801
EQUIP MENT
DATE PRINTED: '2/
04 OF 04 CG 36 CODE RT-444-D
I USE(A) | LBS
----I
COUPLE V-902 THRU UNDERSURFACE DISTRIBUTOR J
I INTO V-901 IN 30-35 MIN. MAINTAIN 42-50*F t
' OPEN VALVE jtt___ TURNS RECORD: -
i
ART3iyj?^T0TAL MTM 4| TEMP_JS,___#F r
WHEN S67 COUPLING COMPLETE, IMMEDIATELY
i
STEAM EJECT IN V-932 SODIUM DRESINATE .
i
^___ N FROM SI 3 IN 12-17 MIN, '
- i .
I STIR TO MIN & RECORD: PHUJ&J|<12.0-12.4> ' f '
. DIAZO__--__)
f'
BASEj/&t_<+>
.. i -
IF NECESSARY ADJ TO PH-12.0-12,4 .
'i
RECORD:
ASSUME 50%
- i__--
20___ ASSUME 32%
BASE____ _( + )
IF DIAZO TEST + , STIR ADDITIONAL 15 MIN
RECORD;
. X,-
b a s e .;
(+>
. .H: '
IF DIAZO TEST STILL +, TREAT AS FOLLOWS:
I 11 > -ADD
WATER' TO METAL DRUM
(2) ADD 144 *AS IS* SODIUM HYDROXIDE ' - */^ ASSUME f>0%
I <3> ADD 10$ "AS IS* 3-HYDR0XY-2-NAPHTH0IC
I ac id .
.
.
I (4) Efc-fO MIN TO DISSOLVE
v /
\TXSS PJU4RHTNT0 V-901 & STIR 5 MIN
tfORD: DIAZO
<-) , BASE_____ ( + )
REPEAT S72 AS NECESSARY TO - DIAZO; + BASE
RECORD; DIAZO_____ (-> SODIUM HYDROXIDE ,ASSUME 50%
ASjE___,,< + > 3-HYDR0XY-2-NAPHTH0JC ACID
R 60 MIN RECORD:
.
FTER S74 STIR ROD:. TEMR&'S^F <60-65*F>
HEAT TO 90-94*F
PUMP IN V-904 CALCIUM CHLORIDE SOL'N FROM
P 54 THRU UNDERSURFACE DISTRIBUTOR AFAP
STIR 10 MIN.J i --
CORD:
11 .5-12.2)
RUN IN V-927 ACETIC ACID FROM S31 6 STIR
N-CODE 1 * - I
' v&kiP' i1
?*?* '' J .J. 'vSNJ
V^vL : i1
V !: . : f1 7-D |__ 98-D I.
T-
. V-.f-vV 7-D. I__i
i C. 82-C | __
7-D 82-C
CORD: PHJSL(9.3-9.?> t "
IF NECESSARY, ADJ TO PH 9.3-9.7 RECORD: PH__/xX NOTE: (1) IF PH ABOVE 9.7 ADD ACETIC ACID IN SMALL AMOUNTS ASSUME 70% <5 TO 2$ *AS IS* INCREMENTS) BECAUSE THERE IS A SUDDEN DROP IN PH BELOW 10.5.- (2) IF PH BELOW 9.3, ADD .6$ *AS IS* INCREMENTS SOJUM HYDROXIDE TO A PLASTIC ASSUME 50%
CKET & DILUTE WITH WATER. HEAT/TL4'83-187*F AFAR-* RECORD:. ACCURACY
_Lj01_*F, REC_?__*F STIR && MIN AT 183-187#F- RCD: START. WHEN S84 STIR COMPLETE, FLOOD TO 140* OR L0,,, . SHUHfiFF AGITATOR5
ART.
PIN;,.
o pt r ,
l__ _____
I 30-D |,____
I
'I 1
7-D ___
I,
f..s *?* */*-(
I\
DUP050047802
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DUP050047803
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DUP050047804
DUP050047805