Document 82LZzZG0872VQe5v7JVR9wJae

*f. I* ' ,I * *fV> . .** : *. V. 'ii >.V -V- ' VV'V; 'Y;*, V?* *.* * * c;***^* ; / ;,v. : y i. /. i * f. ./ . *\: -RAW MATERIAL CHARACTERISTICS ND TESTING. - 7<-Gdc?Name:-.3&gi^.Silic^.oOeadJX__ No....M.^5^4-' *K^**&|Km **! * - :* > ' * Chemical Name -.SilAP.p^^o.llJ/$- __________ Card No--X.-- Previous No_(?_A.JL. . Composition Sub-Class^flQ"6802-- - : /*' Usage (Name & No.)..S*si..Ee?.tfi.-R&n$!S_______ Most-Similar Classified No. Bulk--3-o.Q.JSals./ (GO lbs. Ibs./Ga!.......... ............ Related Nos.--18. dry.. r; Expan. Cosff. 0.000--I.-..perF Flash Pt........ .F (TOQStorage Loss...... .--.Tanks............Drums r:vV;>frv, .. ROUTINE TfeSiS (Run on Ecch Shipment) SECONDARY TESTS (Ren Qirrerant One Each Shipment) TEST MIN. STO. MAX. METHOD TEST MIN. STD. MAX. METHOD V ': " Color Texture Equal"to Std. Lead Oxide Si02 325M Res. .* Oil Abs. SOo k7-9% U7-9% 0.1% |15 . U.2* v: lao U19.3 i - < t -v . . * ! '* v J: *>' i t'jr V*' ?y*.*r`>\*.f ': V. f'*-. * ,' * ??M-* vv''; VV.V* i * \ ... N15815 % -* . 1 0 7-SWP-0048428 ; - y v., . *.* *. I % . ; '. , *. * v ; ...\ . * ,: , -* _ * . -v - , * A f' .> *'* l * * * f. / c 5 ' .V : ` v f. **.'.'* ' * * * % , ' * # ' - : * . ? <i 1 V . ' '*' : > '. .. \ ; v:!;/ j'* v ' . .. i- MATFRIAf nHARAfTTFRISTIfiS^ ANn:TPftT!NA ;P-.n - '.' Hv:VVv ; .::i`--SllicatQ .Of lead u s ag e c n ame & no.?-ejrQ.pas_te_ Faints. BULK-JLi9-GALSV100 Lss. / inRJOA1. ~ .COMPOSrnONSUB-CLASS: 6801" .- i.MOST SiHILAR ClASSlFiEb NO -H--RELATEV VD .N-Os`l--` lO ERPAH. COEFF. 0.000____- PFR FFLASH PT.'. _F (TOC) STORAGE LOSS. v.-ii -TANKS- --DRUMS ROUTINE TESTS (RUN ON EACH SHIPMENT) ' - - TEST 4 min . ST0.` MAX. METHOD SECONDARY TESTS (RUN DIFFERENT OtlE EACH SHIPMENT) i TEST MIN. SID. MAX. METHOD fje.'/ * *` >*.* i v\ A* v; * ' v^Vr.ov-* N15815.01 ** ' t r ^07-S WP-0048430 * - . i- * ;v . . *vV'- ; / ; *< 4 **. fr-; ^ *7 i* 4 '* **** * ' '* .:x'\ -v v.,- ' :7 '-V ; .y. ; ; '/ j'v^i > * - v-.-;- GENERAL DEAsScCrRIiPpTt IiOo Nn : {s h o w c h emic al an al y s is . ;'.'. if av aiias l 4 e }**. .:^W-A * :.\ . V-;.:' . i /** t .* - > ' V * : - ;: . .* ^ * <. ;* c*'- , * J. !>7. : . 4`.. ' 7P'''7;3\vV;V I;4.*;<^>7*3 * . . U' V ' *$0%**% V \ * . *{ \lf r &&/&$ 'V rO -| '\ . S. -V?,;, :/ < I .-* 5VV ' '] X'-X^S-.X it'*&A* i'.. 1 ~ 0 <<,;#/ *. 1* i . i-*- . 4 .*/ *1 ,* . . t -v . * J * * ;\Vio * Vi 68 01 00 RAW MATERIAL CHARACTERISTICS AND TESTING 6 * TRADENAME--Was*ft nf Load. lift p a t e !t--.n o J>Q1_____________ CHEMICAL NAME;________________________ ______ ___________________CARO NO--U_____ PREVIOUS NO. .COMPOSITION SUB-CLASSt USAGE (NAME & NO.). BULK--3___GAIS./100 LBS. LBS7GAL9________________ .MOST SIMILAR CLASSIFIED ML. .REUTED NOS________________,, 30>AN. COEFF. aOOO-------------- PER ? FLASH PT.(TOC) STORAGE LOSS___ :_____ TANKS______. DRUMS ROUTINE TESTS (BUN ON EACH SHIPMENT) TEST METHOD SECONOARY TESTS (RUN DIFFERENT ONE EACH SHIPMENT) TEST METHOD Color Texture Equa!. to . Std. PbO,* S102i% 1(6*0 1(7-5 1(6*0 325M* Bos* 1% 0*1 Oil Abs. lii.O 16 so3,* fc.l L*2 1*9-0 1*9-0 D185 18.0 D281 l*-3 Moisture Loss . 0*20 D280 f?-fe;S! -&T U&k'YSFri* I'v^irjW?5 :W' , ' -1 * * -** .* y> ^ * ** /i. * *.. vr-..V-V- ';." '' ' \t ' i.,'f\ >/.;'<< . Uri.-tVi'V*V . v-` ' ; ?; * *` v~TV-` r S:-: y c ': i V * ; . * i * . . ' '' * -J\' ' * ` .. - N15815.03 0007-swp^48434 '* * ft.': / / * % a . 4 ,4 * . ' * *. * A, , i . * * - ** . 4- . 1 %'JV \\T *V* V** t * if; .' V * v * '4 -VV/ k / '* *- >.*-* , * ` NAME OF SUPPUER National Lead Co* SUPPLIERS CODE NO. OR NAME Basic Lead Silicate, k$X SAMPLE REPO ftifevSe v ,/ .t> *-' (- -2'"^.*? `fe A >,* > . f ^ * # V A' > 4*; i> GENERAL DESCRIPTION: (SHOW CHEMICAL ANALYSIS IF AVAILABLE) card revised to show suppliers new Spec. 6S 01 00 s t d . s a mp l e is s u e o a t s Jb.21s52____ d is t r ib u t e d nv_.Cleveland Tech Service PURCHASE SPEC'N. DATE fc?2U55 -------REFERENCE lAB-Jl-----------iFREP'D. Bt-.jAPp.wlgy.. iL/ I . -36fl SPECIFICATION FOR PURCHASED MATERIAL Ma+flr;at Basic Silicate White Lead_________________ nat<> 3/12/70rnri(, __ Supersedes Specification General Description: Date____ 9/21/61*Code A Mhite pigmeht designed for use in exterior paints. 68 01 QQ 68 01 00 CHARACTERISTICS 1. Specific Gravity 2. Oil Absorption G/lOOg 3. Color It. Residue 32$ Mesh % 5. Lead Monoxide (P6o) % 6. Silicon Dioxide (SiOg) % 7 Sulfur Trioxide (SO^)^ 8. Moisture (Loss at 105C) % 9. Dispersatility MIN. 3.90 lit STD. It.00 16 MAX. It.10 18 Equal 1 o Standarc It6 U7.5 0.1 It9 L6 lt7-5 it9 It it. 2 lt.lt Equal to Standai d 2 TEST METHOD ASTM D 1$3 ASTM D 281 ASTM D 332 ASTM D 185 Supplier's Method * Supplier's Method * or ASTM 718 Si plier's Method # ASTM D 280 ITM li21.U * Test methods can be obi ained fror National jead Comps ny SPECIAL TESTS ANO/OR CHARACTERISTICS. .4 M15815.04 0001-SVff-O"48436 68 01 00 PRACTICAL REOUIREMENTS: The material shall remain constant in successive lots or shipments with respect to unspecified characteristics to the extent that the seller warrants that no known changes are to be made in raw materials or processing methods of this material without due notification of the buyer. 28320 t0-8 34733 68-01-00 ..... .... ................. Code 3/12/70...... Date RAW MATERIAL CHARACTERISTICS AND ASSIGNMENT REQUEST FORM 1NTRA COMPANY CONFIDENTIAL This Side fir S-W end Affiliated Ceapany Perteanel Only TRADE N AM E__l____________________________ CHEMICAL mimf Basic Silicate White Lead .Card No. 6801 Prev. Code FORMULATING PARAMETERS 3.00 Ga, Cwt.@ 25 C 33.33.....Lb./Gal. @ 25 C "TOO .Wt. % NVM -----100 .Vol. % NVM ..... 100 .Wt. % Pig. 100 .. .Vol. % Pig. SUPPLIERS (Pfimtry) National Lead Company COOE White Lead, Basic Silicate, Oncor ii$X OTHER CHARACTERISTICS ..................Coeff. of Exp. TOC Flash _______ Pt. F. ______ .. .Price Lb. HANDLING Shipping Containers. Safety Label Codes___ 11?_____________ _________ Age Limit.__^one. Protect from Freezing ". Protect from Moisture *es Flammable Material----.Explosive Material__ ________Hazardous Material ^es SAFETY; PRECAUTIONS AND OTHER HANDLING INFORMATION , Contains Lead. Avoid Breathing Dust. Wash hands after use USES Product Name Type or Rex......... I&Q.. H ,_C12--- ------------------------------ .--------------------------------------- ... Line Item________________________Customer Specification?------------------------------ -----Experimental....... Reason for Assignment or Revision___To transfer to large card and assume control Similar Codes................... ...?..9J."20______________Codes Which May Become Overstock Advantages Over Similar Material.....iain_.fontrol___________________________________ ... SPECIAL TESTS: #5 Lead Monoxide #6 Silicon Dioxide #7 Sulfur Trioxide Nat. Lead. Test X126 X127 X128 INSTRUCTIONS 1. Fill out as completely as possible. Refer to Routine & Policy Bulletin No. 145. 2. Enumerate all tests on opposite side in consecutive order. The following test numbers are to be run routinely.____9 Tentative Reference Sample to be sent to Cleveland Tech. Service................. Person Requesting Assignment.......... tv. K. Morse Laboratory Coordinator Approving...... J. H. Piel '______________ Received and Approved in Cleveland 2*320 10-68 36735 gy J. Tillman/E. Gardiner 0007-SWP-0048437 Yes_ n,,. I ah. No. 3/12/70 n2. Chicago Forest CD Products,....... .Date_ -10-70 oo Tu b Sh e r w in -Wil l ia ms Co . CORPORATE PURCHASING OEPT. 101 PROSPECT AVE., N. W. CLEVELAND,-OHIO 44115 rOBM 11315 SPECIFICATION FOR PURCHASED MATERIAL CODE. 68 01 -22---- DATE --------------7/J.0/73~--------- CARQ NQ --------6------- SUPERSEDES SPECIFICATION DATED 3A2/?0 CHEMICAL NAME AND/OR DESCRIPTION BASIC SILICATE WHITE LEAD J -.l. /^Kl J:v;' TEST NORMAL CFJALITY LIMITS 1. Specific Gravity 2. Oil Absorption G/lOOg 3. Color 1 4. Residue 325 Mesh 5. Diapersability * Grind Clean TECHNICAL DATA 1. Lead Monoxide (PbO) % 2. "isilicon Dioxide (Si02) ulfur Trioxide (SO3} 9 4. Moisture Loss at 105C QUALITY CONTROL METHOD MININUM STANDARD ASTM D 153 ASTM D 281 3.90 14 4.00 16 ASTM D 332 ASIM D 185 ITM 421.4 Equal to Standard -- : f 5h bH Supplier's Method ** 46. Supplier's Method * or ASTM D 718 46 Supplier1s Method * ASTM D 280 47.5 47.5 4.2 MAXIMUM 4.10 18 0.1% - 49 49 4.4 2% * Te'st Methods can be Obtain sd fro ra National Lead Company NORMAL QUALITY LIMITS ANO CRITICAL QUALITY LIMITS WILL PE RUN ROUTINELY *iPlAL TESTS ANCi/O* CHARACTERISTICS N15815.05 0007-SVVP-0048438 'RACTICAL REQUIREMENTS: The material shall remain constant in successive lots or shipments with respect to unspecified characteristics o t e extent that the seller warrants that no known changes are to be made in raw materials or processing methods of this material without lue notification of the buyer. & \ ro*M iisss CODE 68 01 00 CARO 6 DATE 7/10/7 FLASH p t . t .c .c . N/A -F FXASM PT. T.C.C. N/A .r SHIPPING - HANDLING - STCIRAGE INFORMATION LOWER CXPL. LIMIT u p p e r c x p l . l imit .V VOL. N/A % ,vvot- N/A % TED. STD. 313 COOES 0 HAZARD S HAZARD S REACTIVITY S HAZARtf bMt None PPM VALUE TLV VALUE MQ/M3 0.2 LOSO SINGLE DOSE,. MO/KG Unavailable ACE LIMIT-MONTHS 36 PROTECT FROM HEAT 0 FREEZING0MOISTURE0 UC GALS/100 LBS. V 77*F LSS./GAL $ 77F - COMPOSITION DATA NVM 1 BY WEIG HT n v m l aV VOLUME 3.00 PIGMENT IDENTIFICATION Basic Lead Silicate VEHICLE JOENTirtCATION 33.33 100 100 PIO'MT C00E-6 DIGIT PIGVMT X BY WT. p ig 'mt s ar vi 68 01 00 VEH. C00E-6 OIGIT 100 VEH. NVM % BY WT. 100 VEH. NVM X BY V N/A SOLVCNTStS) IDENTIFICATION N/A N/A $OL.(S> CODE-6 OIGIT SOL.(SI X BY WT. N/A s o l . s> % b y vs BOILING PT. N/A N/A F v a p o r PRES.tmm-Hol VAPOR OEN. (AIR = tl N/A N/A N/A PHYSICAL DATA EVAPORATION RATE (ETHERS II (BUTYL ACETATES*; U N/A N/A N/A PH N/A N/A 9 MAX, (OLEFINSI MAX. % BY VOL. N/A AIR QUALITY 8 MAX. (C6 AROMATICS) MAX. % BY VOL. N/A BRANCHED KETONES-MAX. X BY VOL. N/A TOTAL NON-COMPLYING MAX. X BY VO N/A COMPLIES TO PULE 66 gjj YES 0 NO HEAVY METAL & WATER QUALITY DATA MATERIAL ANTIMONY Sb ARSENIC As AZIDE N3-1 BARIUM Ba CAOMIUM Cd CHLORIDE CI-1 CHROMIUM Cr-3 CHROMIUM Cr-6 COPPER Cu MAX. % BY MAX. H2o SOL WEIGHT BY WEIGHT MATERIAL LEAD Pb MANGANESE Mn MERCURY Hg NICKEL Ni PHOSPHORUS P SELENIUM Se SILVER Ag SULFIDE S-2 THALLIUM T-1 MAX. % BY WEIGHT 44.1 MAX.H20 SOL BY WEIGHT MATERIAL Silicon Sulfur -- CYANIDE Cn-1 TIN Sn FLUORIDE F-1 ZINC Zn IRON Fe PERSON RtuufcSilNk* ASS ItfNMtNT WILLIAM K. MORSE/dj OTHER OATE 7/10/73 LABORATORY COORDINATOR APPROVING r^F^D. GALAYDA RECEIVED AND APPROVED IN CLEVELAND BY J. Tillman/ J. Woo DATE 1/9/7U REASON FOR REVISION to Up Date Specification MAX. % BY MAX. H2o WEIGHT BY W0G 23.0 1.7 .01 .001 - l AB SUPPLIER __________ __________________________ SUPPLIERS CODE National Lead Company White Lead* Basic Silicate Oncor 45X 0007-SWP-0048439 . - \; > TECH;pROUm The Sherwin-Williams Company C3*'1tATE PWCHASNO 0OT 101 PROSPECT AVC. N.W. <XV*LM<J. ONpiluj _ ffonnitsssa-re - :- PURCHASED MATERIAL\ ` ...' \ - - *,.__ A .. c o d e.68 01 QQ_ OATS #>rf v It /17/79----IT c a r o n o). 7 ' ' ;-'-g'PBKPnPS SPECIFICATION DATED '7/10/7^ :x(MICAk MWC AMO/OK OCSCAIPTION ............. Basic Silicate White Lead Qncor U5X '; -=. " ` - 7 TEST SHERWIN-WILLIAMS QUALITY CONTROL ACCEPTANCE TESTS METHOD MINIMUM STANDARD ' : yam PER CLASS CHAIRMAN, A. OGURCHAK - NO CONSUMPTION - v - ' '* 'll-'n1:*'-'-- " ' . . .. MAXIMUM ... ' ' o-' N15815.06 ' 007-SWP-0048440 NORMAL QUALITY LIMITS AND CRITICAL QUALITY LIMITS WILL BE RUN7__________________________________________________________ 3PCCIM. TUTS ANO/Oft CMAAACTCKIITtCS ' '! "* ' ' "' ' D. L. Brenner , 1 Chicago Chem. Ctgs. Lab `- P . J. D. Baldwin/ J. Woo Cleveland Technical Center o PRACTICAL REQUIREMENTS: The malarial shall remain constant in successive lots or shipments with respect to unspecified characteristics to the extent that the Sellerwarrants that no known changes are to be made in physical or chemical properties of this material without due notification in writing to the Corporate Purchasing Department of The Sherwin-WHSams Company.