Document 8209pNeeod0wM4bqQEprbRDDy
DAILY PROCESS SAMPLES
Date Time Initials 2D-60 2C-60 DEA 2C2A ^2C2A:S 2C2A 2C-35 '2G3&I 2C35
INLET OUTLET WT% bz/tol
O&G bz/tol tod O&G
IZ.' ZrB, TW
12 ^ 7 -tP TkZ AE2 3m
(rV^ apz
0. tp A -a
Z..U
J.Gz 2.6
AP.I Z<?,/
n--
31/41
3. S'
(V hs
3*4s Z.6>
2/3 A --
2./^
V
=W
2.1
i^!5i Thb --_
/?- 76
_j*2 /7 -V
--2.., &C ShA
3/77
-3f> - .ASS
31
3^3 ? 3/7'*' /&> .2.6
_/9 z-0
on t ^ .tP --
2.7
ivatsr
2. Vo
(p n&_
A. A-*)
7^ tOCw ~),LT>
ia-'3D
7SyS, ^-
V/>L.
jfr~
Km
D,u9 j?.7
7*7K v/U ?.10 ... 'a.M
)
A&
k.t/ z,r
/ '2-96 US.i
2.70
-- 2>0.b
----
litiiiifeii --
3L/_\ 3rSp|
-USD a.s/s,;? f*v 1-- ML
'iifc/uw ...e't'H
2- **v.r
30,7*/
fmm.
--
Z.Vp 0/0 iPiliiii
*h, % _^T iSip D/i.bL *
7. z %,\ tJhK ilMW 3-7 o/tr-i
3.3
vo 3.; ft, 3
JLlr
OF-741 OF-741 OF-711 BZ/TOL TOD BZTTOL
7/7-
Cjs 0/0
..
4/a --
-- /4J^
--
/,e
--
%
-- ___
-___
ofk) 2- /o
/Vr> 6/7?
r>/n
d/o
4.D -------
XK _u>_
9_
0/7)
Z) /37 /p
___
SPECIFICATIONS FOR THE FOLLOWING SAMPLES ARE: 2D-60 strength should be >7% and < 9%
2C-60 outlet should run between 2% and 4 % DEA wt % should run between 28 % and 30 % 2C2A benzene limit is < 300 ppb and toluene limit is <150 ppb. TOD should be < 1000 ppm 2C-35 benzene limit is < 300 ppb and toluene limit is <150 ppb.TOD should be < 1000 ppm OF-741 total TPA Is < 1000 ppb. Oil and Grease should be <15 ppm. TOC should be < 50 ppm
(TOC - TOD / 2.7) OF-711 TOD should be < 15 ppm
CONF T DFN'T T Al DO 008532
N:\Catlett\Word\datalog.doc
DAILY PROCESS SAMPLES
Date Time Initials 20-60
INLET
1-3*
t pu%-r3 Ik.
f
Qui-
____
&.D
/-V- P U^--' --
J-*r 9 O 7
a,/u..
l~L- IC HW nTW 7,7
l~l -iL 07\*& Ten ih
Pg&r, (-7 -
7.3L
/-e T0V J0p, 7 0
2C-60 OUTLET
2.6 y 2.70 2->m 2.la
DEA WT% . 36-2-/
20.z!
2.L7 30,7
*rr--f---- 70 ion 3/. A
2., 44 2.4
4,36- 3713 3
/<f>C
J-9-
/c 1.
/Qp-
/ 70''? (s 1M TEL
&.3C 7P
V 7l./Cp ') 1.
- p-'p'
---- 3c--tJ
Zi.7'7
2C2A 2C2A 2C2A BZ/TOL &*0D.% O&G
J?'3 A. 7 ^ii`t'iYi'i; i1* ^ 2, 0
Z/37
4/9* Vn
fmx mix
2.0 30 2.2s 7" 7
Oft .........
2.L* US /.4
.9,7
---
:/mx. /r*s
/7 Jf- 7
2C-35 2C35 BZ/TOL TOD
...
2C35 O&G
_
/^
/.I,
OF-741 OF-741 OF-711 BZ/TOL TOD BZ/TOL --- --- -----,-------------------
% 9___
-
e/c /> xZp _
9,5^$
<'*7///J?f J3fC V. ------
- --, ........... *
7.0 / 7 tf'l S'. 9
*A Of# Jfd
<4
JUtilA
/& irf / Z?
/0
<5/0
_ </(&> <c?J/<L?
7?At>0
J/*W)
/<?. 5
.......... -....
.4?AL. 3.2s
--
--
--
SPECIFICATIONS FOR THE FOLLOWING SAMPLES ARE: 2D-60 strength should be >7% and < 9% 2C-60 outlet should run between 2% and 4 % DEA wt % should run between 28 % and 30 % 2C2A benzene limit is < 300 ppb and toluene limit is <150 ppb. TOD should be < 1000 ppm 2C-35 benzene limit is < 300 ppb and toluene limit is <150 ppb.TOD should be < 1000 ppm OF-741 total TPA is < 1000 ppb. Oil and Grease should be <15 ppm. TOC should be < 50 ppm (TOC-TOD/2.7) OF-711 TOD should be < 15 ppm
CONFTDFNTT AL DO 00R533
N:\Catlett\Word\datfllog.doc
DAILY PROCESS SAMPLES
Date Time Initials
p /'
/Vz-96
I'/Y /-/z-so J'/S'T6
/-/? 9c, 1 -/7-5C, J-/*-<&
7c4*u
rtk* /zJht7
ft\r7 IW+J /X
-- f-\p A/jljtP k
/-/9*jC
<Cr
/-m '<)(, //'L.
JF 3s
-/*) jfyc. 111
f-i -It
:> t
/-AI-56
Saz
/ 'frm IZEZ
2D-60 2C-60 DEA 2C2A ?'.2C2Av..i 2C2A INLET OUTLET WT% bzttol rtoby. O&G
--
,M C,.2Y LAL
-
P-** z^/ 1A0
3/
----- --
31.7.7 \0.LO
uu
./4& \t>b
*/&*
ao.7</ 9//Cr*
--
3.8
3.3. %-2> as
7.a
--
7 9c &.is
Z'O / n.LA \.7%, 2m
36.77
___ .
21,77
__
--_
'z/y
J3.76
3r 0-7/ 7/9
Me a 7A --
CZ<L* 5 /V/ ^ <1&tk*A V/A
7 V9
79./ ff
Sitf /94 t&fo
3. s' as 3,b 3I 3-1 D.0>
3. &
Z4-&
>L
71
792s
z. 3* S'
....
dH.b Thilnt
3C.7</
SHafe*
V./ Z.o 26,
3.ZP
2C-35 Z;2C35:| bz/tol TOD
--
...
Ov^^JL TtT"
....
.................
'96-^
...
--
/347
--.
49^...
^...
3//^/
3-//F? IFtT"
D//^iP
2C35 O&G -- /5>A
/.7 2.0 -- 3.0
--
A9
A3 -- ^ter
3.6
Jl'O
2. a-
OF-741 OF-741 OF-711
bzttol TOD BZTTOL
--
--
// 0/7/ ^ */
^a
-- --
sTirr ^7Tig
7
z/?/y
V/ _
6?___ /o
>A
---
*>A sc
0/5 y
%
0/3 / 0 /r-
0/-3 & y/
SPECIFICATIONS FOR THE FOLLOWING SAMPLES ARE:
2D-60 strength should be >7% and < 9%
fir f ^
3l
2C-60 outlet should run between 2% and 4 %
s' __
DEA wt % should run between 28 % and 30 %
2C2A benzene limit Is < 300 ppb and toluene limit is <150 ppb. TOD should be < 1000 ppm
2C-35 benzene limit is < 300 ppb and toluene limit is <150 ppb.TOD should be < 1000 ppm
OF-741 total TPA is < 1000 ppb. Oil and Grease should be <15 ppm. TOC should be < 50 ppm
(TOC * TOD / 2.7) OF-711 TOD should be < 15 ppm
^ Qt/viiSiwe c
,,
.
CONFTDFNTTAl. DO 008S34
N:\CatIett\Word\datfllog.doc
DAILY PROCESS SAMPLES
Date Time Initials
/'ll'90 /yC'Z?-m /Xk A Z/-90 7 A
A 2 s '90 a Z2 JC>
/-to - 9o /
l)t
A
J-27 /-2Z- ? *
If, ?%? /
'7 u. jftf cun
/'Z-9'10
iffa
7^ Olh
/' -9C. tft? jpv
/-5A9L 4'1-90 S--'L'QO
t,P? Jr 2-
... ^ /l Am, 7 f ^ JfV A.#* A&.
2D-60 INLET A. 6 Q& .2<* B0
7, 6?
2C-60 OUTLET
2..L XVV 2~,V
DEA WT% 3t-17 34.7,1 3C.~7</ Zc.7<f
27 cO
2C2A 72C2A% bz/tol TOD 9/^ >dT9
o/,,
ASS
2C2A O&G
*-/ 3.X, 2-7 3-0 A^
3x & 0A0. S'
z-z-y
_3,a.
<9, />r. 5L.sU J/.V7 ' &/27 /&/
z.-l ft.32-" 5L.VS
2,.$ ' ^ ` iSzsi; 6.0
1 ? 2-
_^Li\a M 2//9 z>o .<
z.t
S-W ---
__ Z/71,
j2. 5/0 x.t
30*7 --
"V/o
--
. ' j:'
7.(s 1.S
7-91' 2-72'
<7/7
(r.f
2C-3S 2C35 2C35 BZTTOL TOD O&G
V/91 d//c(7 o/>fb *>//*&
.---
... ...........
..y?
.A. 5 Ac*
-2..0
/Z' -----
l^il ^,0 -- #A^| -----0/7-r
&//&?
... sx.
.
3.0 IWiMii
c/308 Hi /* liiiiilti
0//X7
A 2.
OF-741 OF-741 BZ/TOL TOD
V3 //Z3 CJc
*//>
7
// &
70 --
l.Ao --
y
9
2/0 A .... 3/0 ^ 7
9
'Vo
OF-711 BZ/TOL a/c?
c/o e/3 :i> O/ '
e/a
*/*
SPECIFICATIONS FOR THE FOLLOWING SAMPLES ARE: 2D-60 strength should be >7% and < 9% 2C-60 outlet should run between 2% and 4 % DEA wt % should run between 28 % and 30 % 2C2A benzene limit is < 300 ppb and toluene limit is <150 ppb. TOD should be < 1000 ppm 2C-35 benzene limit is < 300 ppb and toluene limit is < 150 ppb.TOO should be < 1000 ppm OF-741 total TPA is < 1000 ppb. Oil and Grease should be <15 ppm. TOC should be < 50 ppm
(TOC - TOD / 2.7)
OF-711 TOO should be < 15 ppm
. '^NFtofn/ttai 008535
N:\Catlett\Word\datalog.doc
c
DAILY PROCESS SAMPLES
Date Time Initials
z-z-9C /2%t Ak 7 9m
Hi''} 6 07) tc/ .fiJ6
z 4- 4b 8** 2 $ f9 ^7K Lc< . 2_- $ Zr-O'W
rk*.
1 -A- *iL
?%
7^. 4 70-9b % II O
j2Vj1-96 Q.'/%-<)(*
fr
<fk\
Su/iA /Ik'
2D-60 2C-60 DEA 2C2A 2C2A 2C2A 2C-35 2C35 2C35 OF-741 OF-741 OF-711
INLET OUTLET WT% bzttol TOD O&G BZTTOL TOD O&G BZTTOL TOD BZTTOL
-- 2/d_
-- Qkt
..n/j.__ Z" /
--
*--** --
-- ....--.........
**
iiu_ TJpX.
.. k-k ..
%*!')
/ ' y<?Y ?>? vhl t<7
............... 3.Z
...............
-- M>
1* j/7 Z,2^ H:J a
LhLCft*- </?^/fL
jf>0 A >08 H> 7,7 <V/^ _ 2 t> _
i>>4 * /<*& 4>&
J2*,; */
4
-- --
30.7?
_
71 .(, 30 7?
3. 7
---
/?? ... --*"*..
o
. V.JT
Azi --
a KskSM*- - .*::*:
2,.
0 --
Vo --
--
6? */<? /o ... A
0,64
.--
o. n. 5 >04
<9 .. 6? 0>
3>C
2-4 / Z>4<b zm Z.ifO
ZO-g
--
&1.SL, 23-6S Zq,4q
7LB.C9
--
*m 4 l f. cJ/0
....
141L /74 /
&7 _ /a&
,--
37.7 _ 3,4 . (yi' 6f3 3-7 /zO
ifllilltli
.. (&$....
0 fC//l7 Jfy
-- ----- -
3.0 _ 'fy/0 _ /*2~
S oif_ 2.0 !V'f
//
--
. 70 & I'Z/&..
/3
"-- f/3 . o/o O.
<?//
SL&.09 V/7 ft
0> C/3!T WArn/mm 2>So 'VO7
//
SPECIFICATIONS FOR THE FOLLOWING SAMPLES ARE: 2D-60 strength should be >7% and < 9% 2C-60 outlet should run between 2% and 4 % DEA wt % should run between 28 % and 30 % 2C2A benzene limit Is < 300 ppb and toluene limit is <150 ppb. TOD should be < 1000 ppm 2C-35 benzene limit is < 300 ppb and toluene limit is < 150 ppb.TOD should be < 1000 ppm OF-741 total TPA is < 1000 ppb. Oil and Grease should be <15 ppm. TOC should be < 50 ppm (TOC - TOD / 2.7) OF-711 TOD should be < 15 ppm
CONFTDFNTTAI.
DO 008*50^ '
H:\Catlett\Word\datalog.doc
DAILY PROCESS SAMPLES
ate Time Initials 2D-60
INLET
WvJ =a'9<,- --/ j?
--. --
2nV'9C,
1& 4/6-VC- 2
fi)\j /W
te-Q
C. Ce V*0 ?
6.8
kllln. 7 -.jUp- 7.22s 7 JPV
_z ~TT~ _
r-L Jj> . 7.3 2,
/ 7-n
/*<**
7cB>
2.-2VOfr 1 yj.
i>o --
2C-60 OUTLET
2.SL z-.fr/ 2.lob
2L-SX. 2.^ X. c> z. /
2.3
DEA WT% --
j2*8-4?9
28. X Z%>
2C2A 2C2A BZ/TOL *TOD;i
;:i< 7/^9
r/,r /2-/&Z- Safe
2C2A O&G V.e> 0.2"
y-r ^7
2.7
s? V.2
7.4. ,/
SL'M 7l. H
X96& HS-oS VzV 2A.09 AZb
Vfr 2J1 b
fi3
j?.y
tv
49-'S' 3/7 3 -- --
2^8 /zn --
dfe&a /so
/ *1.2
2C-35 BZ/TOL TOD
-- w.
&/*r/
//Awt a/ir*
c/x? a
c/&
-.Ki,-:
*//(* -------
............
*/ C ..Zl* . -- *
2C35 O&G
2.7
OF-741 OF-741 BZ/TOL TOD
---
/X
OF-711 BZ/TOL
--
---
ZL.S zr/3
7/
--
a./ z/c
o/<3
10
z.C --O--/O--- s'
a/* --*y//t7--
.0 (0 /a
^?-jA
3.S A /a
3'. G* o/S -----A-'S 0- >it> -- ---
& '--
10
--
o-a
--
SPECIFICATIONS FOR THE FOLLOWING SAMPLES ARE: i 20-60 strength should be >7% and < 9%
2C-60 outlet should run between 2% and 4 % DEA wt % should run between 28 % and 30 % 2C2A benzene limit is < 300 ppb and toluene limit is <150 ppb. TOD should be < 1000 ppm 2C-35 benzene limit is < 300 ppb and toluene limit is < 150 ppb.TOD should be < 1000 ppm OF-741 total TPA is < 1000 ppb. Oil and Grease should be <15 ppm. TOC should be < 50 ppm (TOC - TOD / 2.7) OF-711 TOD should be < 15 ppm
N:\Catlett\Word\dataIog.doc
CONFIDENTIAL DO 008537
DAILY PROCESS SAMPLES
c.cm//
SPECIFICATIONS FOR THE FOLLOWING SAMPLES ARE:
-7 - * * &
"
2D-60 strength should be >7% and < 9%
2C-60 outlet should run between 2% and 4 %
DEA wt % should run between 28 % and 30 %
2C2A benzene limit is < 300 ppb and toluene limit is <150 ppb. TOD should be < 1000 ppm
2C-35 benzene limit is < 300 ppb and toluene limit is <150 ppb.TOD should be < 1000 ppm
OF-741 total TPA is < 1000 ppb. Oil and Grease should be <15 ppm. TOC should be < 50 ppm
(TOC - TOD / 2.7)
OF-711 TOD should be < 15 ppm
N :\Cstlett\Word\datalog.doc
conftdfnttai
N
DO 008538
DAILY PROCESS SAMPLES
Date
Time Initials 2D-60 2C-60 DEA INLET OUTLET WT%
wr F,u Z' f 1-- 1*710
7.00 3`V-9t
k\*J 3Ul.
3-- 9(*
fa
3-V-46 3-sr-9&
&-/J3O^/U71
Mfa
fa.
3S- 9O 7%L, />.
3fa 76 3-6 -96
Ji&L-
3~6~% 3-7 ~90
ilfa
3-9-% 3-&-9G
/S/n /-?C"&C i*t
Afa-
/6 far
7^ 4va
7%r\ /Ut-
2 2- -- 73^ 2.. SZ' 9<*y
&- % /lift*} / jCLf
7A 2-of ----- 77- ZsfalO
As
7.&A 2.70 ---
7.9 Z-'
--
7 2-a
2.a 2.6 2--1Z,
-- 2 09
7. IX 2.Q L.& 2M y.c? 2.
rttf
2C2A 2C2A 2C2A. 2C-35 2C36 BZ/TOL TOD O&G' BZ/TOL TOD
7y/it'} -Aasm Ufa
/p.j ---->
71 #
^nwVi'iyi,i.:'j;;:..;.
---
'V/e> 'IMkM 3.f\ fap^O z-im
------- > "Ail*. -- H.O
/3/z/
/77 .&> fa" . iS/&W --------->
--- . 4.2
v><*
--
riHL
3.a 4.71
vAe> --
*afah --.
fassm .... .
57/9 #S:
S'.9 3.$ S3
fa*> --- 0/,/
&/&
no^ ( ZO
Ip* O fa/` j&X. 6/6 o(fi iiMi
//y 0/39
2C35 O&G /
_ /__________
0
0
2.7 3.7
/& ---
.0
Vf*
7>n *6o
OF-741 OF-741 OF-711 BZ/TOL TOD BZ/TOL
T-nJ/o Ar
Of77
--- --fa*--
<3
<fa
-- fad /c
--1--' %
-- ~3/o
--
fae
/> fao ---- /c fao
fac 7 *fae
c` O to ~7T
Of 0 (0
0/0
7 -1 -
SPECIFICATIONS FOR THE FOLLOWING SAMPLES ARE: J ...
2D-60strength should be>7%and<9%
'
-7 C csM g p*'** // 1)1 - 7'?
' fa- 19'f
2C-60 outlet should run between 2% and 4 %
Tai..
DEA wt % should run between 28 % and 30 %
2C2A benzene limit is < 300 ppb and toluene limit is <150 ppb. TOD should be < 1000 ppm
2C-35 benzene limit is < 300 ppb and toluene limit is <150 ppb.TOO should be < 1000 ppm
OF-74-1 total TPA is < 1000 ppb. Oil and Grease should be <15 ppm. TOC should be < 50 ppm
(TOC TOD / 2.7) OF-711 TOD should be < 15 ppm
______________________
Tc7 0. Q^'.W ,
N:\Catlett\Word\datalog.doc
rnNFT DFNT T Al DO 000539
DAILY PROCESS SAMPLES
Date
3-//' 96
3-n-^C,
+1 90
4r
Time
a *2aA W''rfm //
Initials
?
xcr
2D40 INLET
7.0B 7 if (r-9* 7*S/
2C-S0 DEA 2C2A |2C2a; 2C2A OUT WT% BZ/TOL TDD O&G
*y MbZ' ^/w S#*J$ //
?r.y
p.iJ
%$'* -7191,
^ p/
2'S3jMTt&T-
-
'*7
MON MON
2C-35 l:'2C5iS::' 2C3S
kwmm OF-741 OF-741 Iwwli OF-711
BZ/TOtr. TOO O&G
TOD R2.TOL4E8Z BZ/TOL TOD O&G BZ/TOL ;i<tG|l
eez-
`
%9
0 6/t> tIS
cko jlijL. 3379
/7
/?./$ ................
Vt yAi
(0
C/ 1 ^)i
<* ^ \ '
'
^.yl'lylv.yXy.v.
/.9.Z- ZM7&W:
iQ
*/*3*
'y^:.
3+/S-' 9o (e
W/itnl#
<s*rt/k
r
6^P~x jr^
MM 2-71.
S.S'
yy ,....Z. .A.. t* ;
//
/<>*%ry\
<??
//T <Z`h
JfT-
4&( 270
3/273
it"*- iPi
?i\\wL
x,, v '
7 P-^
4? 3VD z1
hL ,
/Z*
sm yo
'
a -/a-96 . 2.-/9-ho
7^ 7
63V 3,/
?.D
/A.
9.94?
'Vrr
*/.o
Afcitf Z'l
JV7/4 Data
s.o
z/'}9 SM" ^6 %/\ Wri P-9
; v*
y
Vc? /p-
............
//
p?
/v ------- P-----
W?
aA
--
mt
_______ :___
SPECIFICATIONS FOR THE FOLLOWING SAMPLES ARE: ^ f^rJ'
cUc^- ~
2D-60 strength should be >7% and <9% 2C-60 outlet should run between 2% and 4 % DEA wt % should run between 28 % and 30 % 2C2A benzene limit is < 300 ppb and toluene limit is <150 p>pDbb. TOD should be <^lO10O0O0 popmm 2C-35 benzene limit is < 300 ppb and toluene limit is < 150 ppb.TOD should be < 1000 ppm OF-741 total TPA is < 1000 ppb. Oil and Grease should be <15 ppm. TOC should be < 50 ppm (TOC-TOD/2.7)
F*711 TOD should be < 15 ppm
N:\Catlett\Datalog.doc 8/1/95
t
. * u/w>
tA
CONFTDFNTTAI DO 008540
DAILY PROCESS SAMPLES
MON MON
Date Time Initials 20-60 2C-60 DEA 2C2A :2C2Ai' 2C2A 2C4S 2C3S? 2C36 2C36/WW 2C3S/WW:f OF-741 OF-741 ;EPA*74t OF-711 EPA-7J1;: INLET OUT WT% BZ/TOL 1*TQ0y O&O BZ/TOL *TOO:; O&G IP;TOOa.* B240L-EB2 BZ/TOL TOD 060 BZ/TOL I^0::
$ 3L -/7-"C&*m__
&
4.14
//n - >-
ZL-W 9 .tS VV*
7. ft c/rf
3-0
Ink, L-2^- *Ao *3$
3.1 /,3
// // ^
XT
3.3,
iSSmmh .'
773^
/.o ,<T*-
............... ...........
*/?
/o
j--
.'
'jZ'L 3 /,/ : ;vwt-X'X
,
A" ; . , ....-
; - '.
.
3 -2 Z--9& n
------ 3^
n*T /
7- ^ b0-3'
m ~t0{ /,su Z.tV
3'*
Sty 3.0t
PfL
ftjQo' %i>6 3W ~ fJt --. 3.3
`
.........
................
> '--V' 1'
1
........
-------------T"
7Ah'A i-
/tol/liltb ft: yV
,-- S3
i- *
;&S: 2.0 aeee --
' ;^V?V ' --
*/*
SPECIFICATIONS FOR THE FOLLOWING SAMPLES ARE: 20-60 strength should be >7% and < 9% 2C-60 outlet should run between 2% and 4 % DEA wt % should run between 28 % and 30 % 2C2A benzene limit is < 300 ppb and toluene limit is <150 ppb. TOD should be < 1000 ppm 2C-35 benzene limit is < 300 ppb and toluene limit Is <150 ppb.TOD should be < 1000 ppm OF-741 total TPA is < 1000 ppb. Oil and Grease should be <15 ppm. TOC should be < 50 ppm
(TOC - TOD / 2.7) OF-711 TOD should be < 15 ppm
N:\Callett\Datalog.doc 8/1/95
......
. '*
to %
---- --
CONFTDFNTTAl DO 00R541
DAILY PROCESS SAMPLES
MON MON
jvx,- t i l l
DBAte Time Initial* 2040 2C-S0
2C2A
y&SSSSm2C2A 2C-36 "i55ST 2C35 12036/WWI
OF-741 OF-741 EPA-741; OF-711 pM
*
INLET OUT WT% BZ/TOL
0*0 BZ/TOL TOD 0*0 iiiiiiifc:
BZ/TOL TOD li^Op; BZn-OL
' ;.......
,y Vr:^YS"^
U0
V,7V
3. S'
/o*
**
a/m.if,
Ht>
1
2jK5/Z>
f,v> h-Wi .?:<****& .-- i$0r!tU'i
(nffl>
%'S /*07
3.S -p--
o/Tj Ml
' '-'4te4^t^et' `'`V' ,',
cnbf ?.tf
Xk- 6./
29.0a
s*; `M'
%sAi
3./
%rfSl /#
G/e? m&m
Z
C\W
zx
3,(?
^iii'i'1'.'''!^
JzML
n & iCh-
&ef w 2. ei
//& S^.VSfc 1 37
X
lilipi " f/^
/3 s'
wmi*z.
-;'
t-V7'9C i4Cr
73<e Z76 2108 oA
%8
^4. to
0/e,
di'JL-- for
fiyijil:
Vo
$-Z? rrL h a&,
% 11>7 IT
V'''1 (p X
Ws OSB
^273 V// *SMj 3J_ %9
. V/ ML-
y (M(.' ' V
2-7
^r V.l
M ......... iffUM
Olr'h#' 7. oo ?AX
Gitr
p.S/1
OT.0& Mr} if "Li 7 vf,L> {61m 2M
3,6 aluf
[shc> t Q\/l :yj#i3,4v /
7,0 >7 r
-<!^........ ...w^...,, .
W H 7?/ 77/ 3-7 :>.:. .`a*&AV //.*/ *#******'
HJL22x-_- iiz-T'
Vf^ii
oQ'AJ Aft t/f
t*f-)
/W
3, a
i_ H *-
TY --
'-''la
pl^f; &!s,(L Wk-L--
SPECIFICATIONS FOR THE FOLLOWING SAMPLES ARE: 2D-60 strength should be >7% and < 9% 2C-60 outlet should run between 2% and 4 % DEA wt % should run between 28 % and 30 % 2C2A benzene limit is < 300 ppb and toluene limit is <150 ppb. TOD should be < 1000 ppm 2C-35 benzene limit Is < 300 ppb and toluene limit Is < 150 ppb.TOD should be < 1000 ppm OF-741 total TPA is < 1000 ppb. Oil and Grease should be <15 ppm. TOC should be < 50 ppm
(TOC - TOD / 2.7) OF-711 TOO should be < 15 ppm
. TDFNTT Al DO 008542
N:\Catlett\Datalog.doc 8/1/95
Date
V'f G
V&-7C &3-9C
ifs *4 S} O 45 <hr-$L 4-&-1G -4-0? VL i-~T 4 - 7 -s t -&~9C
DAILY PROCESS SAMPLES
Time
Initials 2D-S0 2C-S0 DEA INLET OUT WT%
0-H4m
3.0 ?,7^
2C2A 2C2A BZ/TOL TOO
'f
/iy'
2C2A 040
2C-3S 2Csfi BZ/TO^ ITOD
3? c
2C3S 040
'$&*$&,Isppi OF-741 TOO RZ-TOL-EBZ BZ/TOL
_____
____
*//
P*r 4*r
..................................
MW
ft-
af
Wr/1 .
l,,lb
to.IV *--.
7.0
Gx`0
'
V/ `
/V-3?
......
1
*......
/e
--
IttU
CM-
7-ftA
aw
7.-9
\Jxt9.R
V?
AM
7Ul
> hi.
& :(f 7
.................... ..... ......-...
2/0 *
UO-Vf
j/3t^
V`1
''' T/>
ff/Vty &p
/.? z,$ ........................... ....... 0/0
7*2& //dm
<Ss
3-t
S#VP\ 7(44
Sa*a
''Ilk,-: V //0 (.?!%! h
/r
/. 3
5.7
$nr /./
5/0
"7 j ' 4 V*
SAM
^r(' J./Co 2f.^5 nkl-b
3
IT fl.7> 7.3 if- *
y.>
' i-
/00 / -H52
u
'A*'/V 78/p
ail ^-7 /n # r f
.5 /.(?
..........................': '.v'J..'.... - ........... ...... ?.t/.... ,,n,;";,,,i"m'"'|
MON MON---- p.
OF-741 ^A^4t OF-711 TOD 0*0 BZ/TOL to*ot
/tf /J
>
-:-:-x'*ilnt,~, ,'l! .V
:........ .
/<?
piffTtv: .It t
i _______
f
-o/S
/2.
'
7-3
2 V/ Silt
SPECIFICATIONS FOR THE FOLLOWING SAMPLES ARE: 2D-60 strength should be >7% and < 9% 2C-60 outlet should run between 2% and 4 % DEA wt % should run between 28 % and 30 % 2C2A benzene limit is < 300 ppb and toluene limit is <150 ppb. TOD should be < 1000 ppm 2C-35 benzene limit is < 300 ppb and toluene limit is < 150 ppb.TOD should be < 1000 ppm OF-74-1 total TPA is < 1000 ppb. Oil and Grease should be <15 ppm. TOC should be < 50 ppm (TOC - TOD / 2.7) OF-711 TOD should be < 15 ppm
N:\Catlett\Datalog.doc 8/1/95
CONFTDFNTTAl ,,,,
DO 008543
3DAILY PROCESS SAMPLES
MON MON
Date Time Initials 2D-60 2C-60 DEA 2C2A Tima? 2C2A 2C-35 I5S55| 2C35 iiftttSAlMP p:2C3/WW OF-741 OF-741 EPA741; OF-711 imm*
INLET OUT
WT%
BZ/TOL StOt^: OAO A*y?W '
BZ/TOL ItodA OAO p;
jtoo
B24rOLSZ BZ/TOL TOD OAO . BZ/TOL mx*z
v- r- 9C 7%nt
V'M*
?*ava JUL 2.9^
--""
3J jl*j
/7
*P $|
7:3c y**r S- $.!(? 3.6$ H.tf
. . . * _J3 f 6* #5rA /VI r
X-WkO
ZML
Z'tyJh Jko 8.79
illL
ii if>_
in?
7'B4tfhn far All 3-7 3/a? yv?>
2,$>. %/ SS
s-'isra^:
7/&
f/Ht
/ /' 'A
7-7- J.o
4iT
TfJT TUt
&/?$
4-n-iL.
//-//
tyr ` v -f--
/V
*>
p<\ Z-7 JP> ff-t/W //?,
W
n
3fSJ
M `y. '
> -/S'-96
(r'yf-
l- w
M
7F JA.ZP 2.72. 3/.ft "//S' 7&fc 2-6 c/,y
10. ^
</-//, -9<o
/fr- 7.S'!' 9 .<0. ,72.3- 3//7
o/t?
V-/7-9U ft ft
aLcl, ftof .6/ 30.7^
aQp &.0
?/rlf -'//A
w"
(
fit y.fj. c/n A7.2i $9
jOq. 7.g
3/.r7 V*-/ /fo ,?y
--*
7/TA {I
M. --
W^,
9
m;
SjjL- 5 %a
j5^_ to.;:
$/o ?,
j ' ---- -
.
wifi?- rf
V.- -
" ''
)/"
?A-
n>//r i
iimm
t3#J&3 !0>
%
` ................ ............... .-. :
0/0
0/0
c/t v/C
// y/fpt
' suL- Mas . . c/o
/c
litfiHfe. -...-'-J--Zl~v. --
SPECIFICATIONS FOR THE FOLLOWING SAMPLES ARE: 2D-60 strength should be >7% and < 9% 2C-60 outlet should run between 2% and 4 % DEA wt % should run between 28 % and 30 % 2C2A benzene limit is < 300 ppb and toluene limit is <150 ppb. TOD siKltbbulid be < 1000 ppm 2C-35 benzene limit is < 300 ppb and toluene limit is < 150 ppb.TOD should be < 1000 ppm OF-741 total TPA is < 1000 ppb. Oil and Grease should be <15 ppm. TOC should be < 50 ppm (TOC - TOD / 2.7) OF-711 TOD should be < 15 ppm
N:\Catlett\Datalog.doc mm
conftdfnttal DO 008544
DAILY PROCESS SAMPLES
MON MON
SPECIFICATIONS FOR THE FOLLOWING SAMPLES ARE: ZD-60 strength should be >7% and < 9% 2C-60 outlet should run between 2% and 4 % DEA wt % should run between 28 % and 30 % 2C2A benzene limit is < 300 ppb and toluene limit is <150 ppb. TOD should be < 1000 ppm 2C-35 benzene limit is < 300 ppb and toluene limit is <150 ppb.TOD should be < 1000 ppm OF-741 total TPA is < 1000 ppb. OH and Grease should be <15 ppm. TOC should be < 50 ppm (TOC - TOD / 2.7) OF-711 TOD should be < 15 ppm
N:\Catlctt\Datalog.doc 8/1/95
roNF TDFNTT Al OO 008545
Date Vow
DAILY PROCESS SAMPLES
MON MON
Time
Initials 2D-60 2C-60 INLET OUT
DEA WT%
2C2A BZ/TOL
IcKf 2C2A TOO OAO
2C4S BZ/TOL IW
2C3S O&G
fj2C36/WW! P!i2C3WWWil|; OF-741 BZ/TOL
OF-741 TOO
mWbtmxm
OF-711 BZ/TOL
e*A-^i |Po*pi
' > ....
,Vv >. v;
//&
............
1 Z* t2>VV
A/ tcte
: ,
//o,
mm
4-2v ^
/isfir , X,,
JO a**-
'Ol- 8V Afl.
^.8 Z7
i;:' /,/
0 ........................... T..:...
;1*8$
:. :-V- ; '
- V.
ifwiti
4^AS.-96 S/-.K nf {t to
* A '!<?>/.
`/Lit) `JO y-jr-TL
V..1-
.'...............................
7:/Sf>
8,7Zt J2.7Z^ ?*.?/
e/> #1$*^ ^.0 *7
ym
//0 -- "
/.z- .........
'
/& ^A5iAir^T^;wv;yw!w
7-9///> --* / *
1#
>,V ^.0
hhl fL
//^
mmwmmwmm ^------
h*
. 2 * AivJ ""
IS, ?- --/t,r _-
7-304*, A. 8iif
7//C
&:\*rn
----- 7 <21.
..T.T...V ...
^niinmfi L
t5
.<:----
2.-X 7^
7f?/ "inilwfr--n
/zc
.7
**.1 IMTi^ij rn
o/s
c/e
life .Sf'Ss^W'W.W.ii'
9
--------- -- Ilili'
SPECIFICATIONS FOR THE FOLLOWING SAMPLES ARE: 2D-60 strength should be >7% and < 9% 2C-60 outlet should run between 2% and 4 % DEA wt % should run between 28 % and 30 % 2C2A benzene limit is < 300 ppb and toluene limit is <150 ppb. TOD should be < 1000 ppm 2C-35 benzene limit is < 300 ppb and toluene limit is < 150 ppb.TOD should be < 1000 ppm OF-741 total TPA is < 1000 ppb. Oil and Grease should be <15 ppm. TOC should be < 50 ppm (TOC - TOD f 2.7) OF-711 TOD should be < 15 ppm
N:\Catlett\Datalog.doc 8/1/95
COIMFTDFNTTAI. DO 008546
DAILY PROCESS SAMPLES
MON MON
Oate Time Initials 2040 2C-60 DEA 2C2A ZC2A" 2C2A 2C-3S '..Jess? 2C3S
vvearnttm OF-741 OF-741 EPA-741 OF-711 waTiT
INLET OUT WT% BZ/tOL TOO 060 BZ/TOL TOO; O&O TOO - BZ-TOLXBZ BZ/TOL TOO mm BZ/TOL yoiioil
?. *
T^T A Q ^
3^7/ ^//O mg----
*Mh j
S..0 --
7 ifsiii ~w pllli ' ;'.-.iiw*ir<|:';
iS-tMc
Z'Z-'ik 5-4 5 7s-s-u . * r A 7fa "-"9fa
AAA
1 3z-3 B//o m CL..4 c/oZ/a
M
2,2
& hpy 2,7i.
jcM
fa^/n.i
\oH
A
A/<? loo
7 Mru
V'S
Wt(A>
7X4 l.$L
7 V..... Ad
2-7
w\
SM: *-<? ___--
2- /t}ha 1
.......... ?.c
aliil
QA 7.2- 2,26 zp.yi ijL
> 0/6/4 WMw
7^5,
Um V`2#
A. ft
?/%
Sf*
.4-
761
2-o.Z.f
ftffh ----j-U.---
21,2. o/si/jL w^.
im
M
wm ?*0
alii
7-S a/?
4.U? St.B P.q
fa/'?
0/z^l7 /.ft wm 7 (A
H.^lr j{.& fa/&
% $$
j//y fb.O if?. ZO.T' <0/9
_?.y A^
/6 SUP 3.7
f- -- 1./*... .,. 1.^ ?
7
J - /o ----
--
<3/0 Ml-
*/i
~Cp~ t> i
ipP 0/3. b
rft 0/0
,2-
0/0
<9 v/o
.............................. :.-...'.... A 0J0
.
!0
/o 1,1 4 *</ &/0 -'
/> > c/s 1
7 ............... 9 Ifill c/3
`
St!fe. < *,U' `
?P:f
y:\afih ff\VJ S-Z2&- 7 32*At*
7- >
f,0 2U/L lA
life 3.?
//3
.................. .......... .........
.aJi.
........-L______
>/*
SPECIFICATIONS FOR THE FOLLOWING SAMPLES ARE: 20-60 strength should be >7% and < 9% 2C-60 outlet should run between 2% and 4 % DEA wt % should run between 26 % and 30 % 2C2A benzene limit Is < 300 ppb and toluene limit is <150 ppb. TOD should be < 1000 ppm 2C-3S benzene limit Is < 300 ppb and toluene limit is <150 ppb.TOD should be < 1000 ppm OF-741 total TPA is < 1000 ppb. Oil and Grease should be <15 ppm. TOC should be < 50 ppm (TOC-TOD/2.7) OF-711 TOD should be < 15 ppm
N:\Catlett\Datalog.doc 8/1/95
OONF1OFMT ' DO 008S47
DAILY PROCESS SAMPLES
MON MON
Date Time Initials 2D-60 2C-S0 DEA 2C2A
2C2A 2C4S msm. 2C35
p/wwf OF-741 OF-741 PaS OF-711 ;0F?%j7l^
INLET OUT
WT%
BZ/TOL ;. 0*0
BZ/TOL mm 0*0 litit
TOO BZ-TOL-EBZ BZ/TOL TOD P'O*0 BZ/TOL IgbiGtl:'
S'-l-'tt
rov
s.py
=iA
7;&Jm jQ^ &*
J/.27
/si. /./
O
V-/7.-9V (&>
>tfr
7/9 2-f (\-h 2.? 2*5.7 r/7
732-1
3
TflP j./
>//0 &9* "T^-----
/.*
*4-' /3 '9C
--t 7*
* -J ^ (?
.yy-ft,
a-v A. B-
4L.93
2.<PV
SE2
MLz/p -24_
eA,
3V
0/9 ImIg (,.0 '
5-1 Mio ~7^s
7.84 z-P4 7.9.1$
Mr
A7 tr^^u &
<Ss*. 6-W 2J2C- 3/r0
m 2L2-
jii 7.0
^pil
\4k- /O
0/0
V
M0/0
w (0
0/0
n rr.r^
Jt--
HHI
--
,..,1__:__
3k-- fa
3k--
sjs-- ~z~
aUx
__ -- *//>
a
<Tii
^sm 3k--
-2%.
XL<2-
3*l#yv:i5
f*
Q.iO ~3jc 3/'8
9*7 k&& 2i-
2*2-
'iii 3L-
Z\ 2*K 2,#
/: SAN6mhs.-
C.o _&a.
tit*
0.n 3ii- 3<?-1 'V?3
5.U 4a.
h5 h 2-
tfpil
v .
B T/7T 224
't /# oTT"
SPECIFICATIONS FOR THE FOLLOWING SAMPLES ABE:
*
foritcO
2D-60 strength should be >7% and < 9%
2C-60 outlet should run between 2% and 4 % DEA wt % should run between 28 % and 30 % 2C2A benzene limit Is < 300 ppb and toluene limit is <150 ppb. TOD should be < 1000 ppm 2C-35 benzene limit is < 300 ppb and toluene limit Is <150 ppb.TOD should be < 1000 ppm OF-741 total TPA is < 1000 ppb. Oil and Grease should be <15 ppm. TOC should be < 50 ppm (TOC-TOD/2.7) OF-711 TOD should be < 15 ppm
N:\Catlett\Datalog.doc 8/1/95
/ S/18 f'<
^ *'
Q ttft TXX^ 1
OONFTDFNTTAl DO 008548
DAILY PROCESS SAMPLES
Date
Time
Initials 2D-C0 2C-S0 DEA INLET OUT WT%
-7?> SrT 3,07,
^ ' >- jf- /?& TJ t-<) its <L, 3.C&, __
Tssm2C2A ;>2C2A:?- 2C2A 2C-36
2C3S
BZ/TOL li'TOOJ? 040 BZ/TOL TOD, 040
|i
*
/.* . X
mMtMif: v>jecmNtiB
yiTjM|pl lilTttWsaa:;
of-741 bz/tol
29 rv-'.
W,
X
.X
MON MON
OF-741 WA3iT OF-711 H5* TOD ||40| BZ/TOL pNtOlf
hH
a/a
^7
/
--96
Sz.Bi,
/#
A. 3
&* 7 /&
z-M
yo" 4>7
A4
AM 7rC? -5\2*-f6 y'-oo f/H
tfir.fA
--`1
?// 0/t/fT?. /7
|x</ '.*
-* ' .
(?<h W< Jtfi f'4?
. L? lo
AM
*,9
ti/G fj|$r %i> 7A 2^ ^7Jr, iw t, b
Qh,c\ Vn
isp
l,c7
/ 'in
/
- ; '-
%$r- 3^ 2..^ .Tt> t>
*./vra/r
1
pf' 6Y .2-94 7/-S
0$:
:&lViYfo*fo::
e>/>f
.-r-2.9-7 a
\ / 2- ^Ptr>
K
a}.34 3.v*/
, aQncs
g.SZ^
rh
;
,
eA//&
___
-
' <
/O
'^
sus VtT ipin
Ii7f ^
cy 7
^
0hO c /i>
*tb :0p0&
0/0
.... ._
. -> O/fa
' 0- 0
mSm
>//& ^m.i'-
---------------
A ?/?
wm^m
.........
w. --
---
--
JZt.b
--.....
.------------------ -- ...............
.
SPECIFICATIONS FOR THE FOLLOWING SAMPLES ARE: 2D-60 strength should be >7% and < 9% 2C-60 outlet should run between 2% and 4 % DEA wt % should run between 28 % and 30 % 2C2A benzene limit is < 300 ppb and toluene limit is <150 ppb. TOD should be < 1000 ppm 2C-35 benzene limit is < 300 ppb and toluene timit Is < 150 ppb.TOD should be < 1000 ppm OF-741 total TPA is < 1000 ppb. Oil and Grease should be <15 ppm. TOC should be < 50 ppm (TOC-TOD/2.7) OF-711 TOD should be < 15 ppm
CONFTDFNTTAl DO 008549
N:\Catlett\D8talog.doc 8/1/95
Date
3-St -9/
r-7/-
L- ,c\(o
ir'/f -*V* *
> j 7
if 7- 9b 6-7-9 A
DAILY PROCESS SAMPLES
MON MON
Time
Initials 2D-60 2C-60 DEA 2C2A ?353* 2C2A 2C-3S INLET OUT WT% BZ/TOL -TOD'?. MG BZ/TOL
2C3S MO
CQ,
7 -'Jhv
&,(*/! -
?.o 3^
2,/
.?
Tkf* 3-4
." s
7
S.72-
3^77
-- z.7
f
t1
/4<
Mf c A /.tf
5.ie> Z-CA 9*,H 3/4/3
ofr/+ #f .7
7%
7:0firY\
.Z,*.$g7-
7.7-2-
v.&L v/fA
~7S 2,7
//
j. 5
3.5^ 4's *TS .S'
TOO
.............
p
111
OF^41 BZ-TOL^BZ BZ/TOL
V?
L- -HI _
-... -...->......
OF-741 TOD
? ' To
EPA.741' OF-711 EPA.711:
WMmMO BZ/TOL vr~V;.
of0 6
j <y
O/rt- y^iwl'OOffWwyf
ah
1ilmVi^i ------------- -
6 U--**
2s 7A /V
2'7$> 36.3
Z82_
Uft *i
7-^aJ 7T B,u> Ai& &1S7V s/n/3 />* (rb
n(W\
Y'0t
$c) &M ^.rtS 34-7<f ~7r
73
fiSjps LJL. !<S4l>;'X'X^4,v5
`Ho
,& :|SiP
/&
........................................................................................
....
%
6 Jr1 in 11 rrriYri-- --^--1--
7 ` f//<b Isair! 70 "T7-il?|7
fayj so. 4'*s
c, <-iror fit vj
Sz-bL A-SS
73 %/r yT
7-^thrt a(jl $
A. 96 3 .7/ wt? Sr $.1 ~%J7
7'32v,,,
2. S'
bcte.. L.
>d- Cj %
/s - s </Y
yfs d_
w~
./
At?
wKs*^ -v- - V. . . .v.-.4^
i5L_
~w 7?
__________7
. fiaE
' 'X .*:v.
i..............................
JL 4:!v.v^'}p;v
HSit
SPECIFICATIONS FOR THE FOLLOWING SAMPLES ARE: 2D-60 strength should be >7% and < 9% 2C-60 outlet should run between 2% and 4 %
DEA wt % should run between 28 % and 30 % 2C2A benzene limit is < 300 ppb and toluene limit is <150 ppb. TOD should be < 1000 ppm 2C-3S benzene limit Is < 300 ppb and toluene limit Is <150 ppb.TOD should be < 1000 ppm OF-741 total TPA is < 1000 ppb. Oil and Grease should be <15 ppm. TOC should be < 50 ppm (TOC-TOD/2.7) OF-711 TOD should be < 15 ppm
cNFTOFNTTAI
OO 008550
N:\Catlett\Datalog.doc 8/1/95
DAILY PROCESS SAMPLES
MON MON
'M-i&istMNM &A.HTDate
Time Initials 2D-S0 2C40 DEA 2C2A I2C2AS 2C2A 2C4S 2C36 2C3S 2.C3WWW
OF-741 OF-741
OF-711 :EPA.7ll?
INLET OUT WT% BZ/TOL itob# O&O bz/tol V*M# O&G
B2-TOL^62 BZ/TOL TOD 'io*a >' BOTOL -OAO
,
`,,:, ''.......
-
)r?,F 70 /...-MXm... \r<, V _
__ _
JZl/,s2L_ i __
6-5
--TiWisnfiV~ m sSy'p**4 /Del.
7'% I- XJL
A.L9, o.,A
fft/7 <?AA
3^7if* fa/f
7/
7W
VD 4(v
0/9/6
fiAf
A -//~56
a<- &.6.A 2.lW %S.'W
Wr* hk
-y7 >t?-o^'
2-
..... AMs.
6-70 JZA U2l &/? 24-
.2 mmim................... , >'/ ^ gMBBB
(? ' /.p
- '' 1...................
-tJL- --
M
ne 11 1 *
--
-Ml___
b//9 fillip
-M-- J/y-
.(a fV<: :>' rf J.
':
' ^ s . v av:
.A-- /'s V"* " '
>
.......
/?'A
(o tr 1 h~5b
(I ~/6 '9^6 6'17'14> to~r?
AfL ZC ?U2. 2JB 3l*M W\
MX-
*`2l
wk
mmm
nt
jQl &.%A 2Mk.
*{*!/r>yA
!W\0--
<Z\L
ia/
Vnfo J
1 AJc*-(* 9^ s 7A
___ ________ ......... --
1 HWIII
w
. Q'7 ____
v^O -7, (ft 3 53.1?4 Z/hA
Jf.V MoJ4
--
ClUf
2.7ft
3.5
V?1P^
Joj CIO/
A.7A
l<?
S'
-f
W~
7$
/</* T *7-^
5#
7-^rn- 3E /,9C ml ty/t/t mL 82 SiS
.7 'jSfjs*
____ ^
*
"TTr"".Ji
% JL- ry *% A7M -. ..
"Mm /e>
a/sJs '
W;
-
S-- MM1
0/17J7
- . ;----- ... . ---
_o_ 52
Mi,
^--.
sSt
HEL 6 ...Q-,, HiSl* IW
aS^
Z****?7':
Jb- jL ' *-A' * %0/k
SPECIFICATIONS FOR THE FOLLOWING SAMPLES ARE: 2D-60 strength should be >7% and < 9%
2C-60 outlet should run between 2% and 4 % OEA wt % should run between 28 % and 30 % 2C2A benzene limit Is < 300 ppb and toluene limit is <150 ppb. TOD should be < 1000 ppm 2C-35 benzene limit is < 300 ppb and toluene limit Is <150 ppb.TOD should be < 1000 ppm OF-741 total TPA is < 1000 ppb. Oil and Grease should be <15 ppm. TOC should be < 50 ppm
(TOC - TOD / 2.7) OF-711 TOD should be < 15 ppm
OONFTDFNTTAI DO 008551
N:\Catlett\Datfllog.doc 8/1/95
DAILY PROCESS SAMPLES
MON
MON
Date
Time
Inttialt 2C-60 2C40 DEA INLET OUT win
ZL
Ca'i*. *>U 7*'a~ R -B4 1% T' J < tIe L-l
A W5 Am C-Zst'Oi U
7&i
fp An*
7a-
50.7
c-irlL 6W5 ?l* <V
2>L /
toT,l&
ff'? 7, *5
t, wi*
,260
2C2A $68$ 2C2A 2C-3S
2C30:
BzrroL TOD OAO BZ/TOL TOD . OAO;
/\ '>x
'Sk.*.'
^<r fc.Y oi4s
6.0
v/iv/y
/f?0
$7iV .Tufm.yi 0^O_
k"' -,:t:
W ^1
2C35/WW TOD
2C3S/WW i 0F441 0F-741 BZ-TOL-EBZ KOTOK TODr 080
MM
OF-711: EPA-711,
W^MKOTOL #80||
|t|v
rf; ;;;/V47 aiis
o/0 x$9-*k,?%k tfxHfV
s#s
S;
G-XZ -fiCr
c/l# 7/6 Z-O1# }0,i)
6 T(V\ pf\7
2,S<,
7:3#/Z*r -<0l_
/W
7 '.Oe&rrr Hk
JZiC:
UL
0,96 A'(f!. 9.M
y__ /.***
Ah* e.96 Ud.
f&M %L
2-/
/SX M /<V*
<$7t /+
/ ^ S/
<$> jklh. j3l JjJfL.
:,%ce#WWW\ TjbsANWW
ism._ 7'<* m"MV* t J&&2. J.o
2M
"A
x*p-;' ":: 'litWMssH ;
-
&/l9 ,,,,^ ,,, $hthf . O-,i,,...
' ______ _
......
~$&-
%zA,
____ _J
k^llHy &
SPECIFICATIONS FOR THE FOLLOWING SAMPLES ARE: 2C-60 Inlet strength should be >7% and < 9% 2C-60 outlet strength should run between 2% and 4 % DEA wt % should run between 28 % and 30 % 2C2A benzene limit is < 300 ppb and toluene limit is <150 ppb. TOD should be < 1000 ppm 2C-35 benzene limit is < 300 ppb and toluene limit is <150 ppb.TOD should be < 1000 ppm OF-741 total TPA is < 1000 ppb. Oil and Grease should be <15 ppm. TOC should be < 50 ppm (TOC - TOD / 2.7) OF*711 TOD should be < IS ppm
N:\CatlettVDstalog.doc
CONFTDFNTT A1 DO 008557
DAILY PROCESS SAMPLES
zf.'b MON
MON
Date
Time
Initials 1 2C40 2C-S0 INLET OUT
DEA WT*
2C2A BZ/TOL
v;:>2. ciA.::
2C2A O&O
2C-35 "555SI BZ/TOL TOD
2C36
0*0
2C35/WW TOD
2C35/WW OF4T41 OF-741 IPuiW OF-711 BZ-TOL-EBZ BZ/TOL Top: 0*0 BZ/TOL ^<Sf,
&/za/9C B' *****
HVf
"$r'L
9*) ao& 2.56 ZQhZ
6*6 ~^s ${& l.f
UJb-SU
/> ^'"5 fc 7-/- <U* 7'/ *4 ti
7
.
A5V3
;M 2- "Of. is
"T. r'~ r*?
9.7H
T.$:" *Mr
*>
7<#
7-ZrtC 7r3"96
/Ck nKJD
a-fo
7<$ w* /$!
AA.f' :
/Q, 9.<?
A,A
crtfY ^.*52-
!IU\M
l <0ff 1,
lit* <&*
?o.t>7
7^
: >
Wn, wwy
ytm
/i*
2. *5
w
Wfahk 1 -
o
TFT to 7-77* >
xnr.
to
M
25,
W
**7w
YiA
'
2i3z<?-rawing
l!2l 36.7 ISE //* 7m `At/*.
t$
: V:-:'. : :0.
"...
,.-;^Vv:V :C':v .A ' ---4--- /-
;ws
'r? .....-....
y/*
'0. ,,'S.V<Af,;.j ',
w
f-p-o 2,
V' <
J&L
: -^.
y- &' & 33'"'"' 3^, ---- j 2-
. 4/22^ ^ar-*^
^--- "" -------
f *: S ^ '
"4* ______ :
ItL
L_ fa
V '.'s :5 ' i..<3....
SPECIFICATIONS FOR THE FOLLOWING SAMPLES ARE: 2C-60 Inlet strength should be >7% and < 9% 2C-60 outlet strength should run between 2% and 4 % OEA wt % should run between 28 % and 30 % 2C2A benzene limit Is < 300 ppb and toluene limit is <150 ppb. TOO should be < 1000 ppm 2C-35 benzene limit is < 300 ppb and toluene limit is <150 ppb.TOD should be < 1000 ppm OF-741 total TPA Is < lOOOppb. Oil and Grease should be <15 ppm. TOC should be < 50 ppm (TOC - TOD / 2.7) OF-711 TOO should be < 15 ppm
N'VCstlettNDstatoR.doc
CONFTDFNTTAI. DO 008553
DAILY PROCESS SAMPLES
MON
MON
2C2A benzene limit is < 300 ppb and toluene limit Is <150 ppb. TOO should be < 1000 ppm 2C-3S benzene limit is < 300 ppb and toluene limit is < 150 ppb.TOD should be < 1000 ppm OF-741 total TPA Is < 1000 ppb. Oil and Grease should be <15 ppm. TOC should be < 50 ppm (TOC-TOD/2.7) OF-711 TOD should be < 15 ppm
NACatfett\DataloR.doc
^ONFTDFNTTAI. DO 008554
DAILY PROCESS SAMPLES
MON
MON
Date
Tkne
Initials 2C-60 2C-M INLET OUT
DEA WT%
ZC2A ,;-2C2Ay- 2C2A 2C-J4 'zest'
BZftOL
OAQ: bz/tql TOD
2C3S: 2C3S/WW OAO TOD
2C36/WW OF-741 OF-741 :epa^; OF-711 ip*A*7<*j; BZ-TOL-EBZ BZ/TOL TOO.; 0*0 BZTTOL
?r>G>
7/3^/^/: A 7 ! 1 SJ m VI 1M Vf,0 mh.
7/20/90
7?.2
7# /o-f
fd#
: J7.
Ml
7-2.1*
0 1'<O0 Mfi '7z9i>t* MS&
It'X' 2*<5
"tW"
77,0
*55* ./ 1
$,0:Av;
7*<22^ L?A7Ph*
7Sb ?,-V 2Ao
/7/V 2-//y *53*
3.:2-
.........
y&Zm 0^i^:
Je.zZ
M0
^7/
i/*4;
`^"--J.V'nn,
7*3^'fir* b2-^
7-7-S'9& &>'. is
3cB
*"#r JjWt, &*_
a^VL"-'f^
59-// /W$
fM
z^v
ZjTs
,_.
ZpS -w--
/47 ^wiSl
M, ;
7'ilO^L
l-ZCr'iL 7- Z7~?&
7 78- ?l
/5a r:
/Cb. %(?& M.Ofl z/zdar
w
M
%Z.
%2P
2-1
JL
ifoS
e/rVXE
m.
$& t%G
<77^7/9a
*
*- ^
......... -;,,i
:^L
_-J j!:r. iixik
7$L*s-
C/b/s'
r-
..'^.|..vi:^
W?
11J***
'
SPECIFICATIONS FOR THE FOLLOWING SAMPLES ARE: 2C-60 Inlet strength should be >7% and < 9% 2C-60 outlet strength should run between 2% and 4 % DEA wt % should run between 28 % and 30 % 2C2A benzene limit is < 300 ppb and toluene limit is <150 ppb. TOD should be < 1000 ppm 2C-35 benzene limit is < 300 ppb and toluene limit is <150 ppb. TOD should be < 1000 ppm OF-741 total TPA is < 1000 ppb. Oil and Grease should be <15 ppm. TOC should be < 50 ppm (TOC - TOD / 2.7) OF-711 TOD should be < 15 ppm
doc
CONF TDFNTT Al DO 008555
DAILY PROCESS SAMPLES
MON
MON
mem. mmDate
Time
Initials 2C-S0 2C-40 DEA i 2C2A
2C2A 2C-3S
INLET OUT WT% BZ/TOL freoif OfO BZ/TOL TOO
2C3C
0*0
2C3S/WW 2C36/WW OFJ41 OF-741
TOO
BZ-TOL-EBZ ;BZ/TOL ;;TbOr
0*0
:0F411 BzrrpL ;#o*o#
-
znc.7
7.12-
2??.o
(55 afe
7-zr
w?
Sfa
-O::.
AJ*. l.'Sl' 0JP./A *fajk
7-Z Ztrrrt*.
2.S" Wr.
7-^ .-O/; -7-^pjC^ 'fa e>3t-
36,Zl Wf!
/&?
/A*
/S'? o/7f$ m A.9r
'imz.
1
.....
M&e
2-6> --
to#
7
jT H V 7.57s A9.fi' "SkQzF /&A 7&*P
Pfr^K
2--T
$" sk,
-- --
------
--
::^U:>iillll,i'..'
^mk lliifefik
1 ::!V!!tl!!,!l:::''
`^v-
9-7-*, P-7-9S
av J.OL 36.1)
&0' 2A4 ?/?A MPi
fsA*>t
&<<* __
}>
--
-? s&L
6 -7p9^
/&
A. %*/ 7.f
s>.0B z.r
29='i
Z7.r
vM
Wff
/Wh /*& fV vm
------ --
2ET 7.r ?.*( .7/ '"W6^ /2,3 ok 7$
---------
ft -- 2*6 ---
6 -^r/L
7.2, 2.</ Z?./
13*(> ofy
v.p -=------
Sa
-----------------
-- --
fjfc Z2f. fpJiL jL iMju
--
''2-7':-
ftip:
. Js.k ----
.,g/gL
iiins^Nin^ W
8-S'96 A ,6 96
r-G?-9(n
a-7-10
Z'^SPaA w --
A 2"
7^/V W
M
jUk, & 2-/
/Mmt *UJc S/& m *$0 ?S,/b ik:. . : ..
'a.4'
---
v------
:wSre^.,4**y;,,
{;<;aaMiiiii.fii.
W\ ^TT|rr
: f
SPECIFICATIONS FOR THE FOLLOWING SAMPLES ARE: 2C-60 inlet strength should be >7% and < 9% 2C-60 outlet strength should run between 2% and 4 % DEA wt % should run between 28 % and 30 % 2C2A benzene limit is < 300 ppb and toluene limit is <150 ppb. TOO should be < 1000 ppm 2C-35 benzene limit is < 300 ppb and toluene limit is < 150 ppb.TOD should be < 1000 ppm OF-741 total TPA is < 1000 ppb. Oil and Grease should be <15 ppm. TOC should be < 50 ppm
(TOC TOD / 2.7)
OF-711 TOD should be < IS ppm
OONF TDFNTTA1 ,
D0
N-\CMlrtt\DntiiloR.doc
DAILY PROCESS SAMPLES
MON
MON
Date Tim* Initials 2C-M 2C49 DEA 2C2A mm 2C2A 2C-3S iTCttf 2C3S 2C35/WW 2C36/WW S0F-741: OFr/41. pA.^f OF-Til:
INLET OUT WT% BZ/TOL iroot; OfO 8Z/TOL ;sTpt>!|; 0*0
TOO BZ-TOL-EBZ BZ/TOL TOO 0*0 Btnoi. s|0*0' v|
&S&-90.
V - 7-^
y.'^sTP/n
y`
A%,
&-V
^7 ,272
itt' ;;:v ' ,1^
Wo iSl
^5 arS^ /.a
I;!-:*..
Q-1' r./(.
mj
3 u*ar iff
/ ;,vy
fa/o
yw ote
777; *s>
316
_
1J
5T s
- Y. - 1
w
**'
3.M4 Ttf
1
*-
/
3A 2,4
j/ri*Z8.oS
%'lh9C
JWT
chh
7*2
8 '96 A
Xn '$6 2..P2' ?0.7K
vii
pA P}$9" $?$& ' \:d =
Ihi+Z. *r/ S <*fB 2,^': w*
w&
7;oo 7/11 ft\vj , ^ 2.L
d/3'c/C
b ft. 6 &,5> 29.0"
/H&r
iYZ/6A
7-T's-A. *Chr ft.c.
y** -
~7V
./&
Jfafa
oAZiWik WtEmh
^0
###
/> H 7/
{ft jT'l
3'(? <#,/ zk)s* $pi far?
2.99
msL
3.8
3-{>
-3:
"
----- "
,i:#,
x':-v
.
ISR PM~ likfi
; 3:--f fe-
v:
-----'
SfiWfe o/s/t>
^Sfe
----------
#/<>
Krf-'r
' ir-o
faj/f b/Y/fr 1P1 b/7^ l-i'.F' ' *mi
SPECIFICATIONS FOB THE FOLLOWING SAMPLES ARE: 2C'60 Inlet strength should be >7% and < 9% 2C-60 outlet strength should run between 2% and 4 % DEA wt % should run between 28 % and 30 % 2C2A benzene limit is < 300 ppb and toluene limit is <150 ppb. TOD should be < 1000 ppm 2C-3S benzene limit Is < 300 ppb and toluene limit is < 150 ppb.TOD should be < 1000 ppm OF-741 total TPA is < 1000 ppb. Oil and Grease should be <15 ppm. TOC should be < 50 ppm {TOC-TOD/2.7)
OF-711 TOD should be 4 15 ppm
s - "
" 7//
* " - . ... -
FONFTDFNTTAL DO 008557
MAr'MlrtrtnMntfW Hoc
DAILY PROCESS SAMPLES
Date
Time
Initials 2C40 2C-40 0EA INLET OUT WT%
mm2C2A
2C2A 2C4S:
B2/TOL: # o&o: ez/roL TOO
2C3
0*0
2C3S/WW TOO
2C3S/WW iOF-741 BZ-TOC^BZ
MON
MON
OF-741 P53E'lTI3!T?!WM'7Tr1rT1i.HE*!^!3^33l
7.12 z-y
bt/VSf* 53T,
p,<T
h/t/3 t&ki
oM
Pl-2S~*>C.
s.fid >..32 2>.Z)
^Sp
: :ttm >::i!; ;!:
-jm 7 0
_____
ill
A-l /,WrV) & A.*(s -2.V 23-UP
P0-
3' //>? jfals
3;
fcc^ RS T7
/
S-zi-'ic,
Lh 7W 2.-2/
/C`, 2*0 #> A
1
n*if*
:i i*h !"?
,
SI *Ak j8& 131
w,, : ... - J.i.w'-i; '
It H-8 . . : . .
"" i
& $.$<* AZ,/
1-SC
*A>/n
W'7
bA& 7-lb 2.2$ 3>,2| ctf/ejo
& p/ tt-hj"5&:
t, }6
jr*44L
m:
p3L
M
-y PfcA
7-ZZ
V-TT-JC 7/55-- w
y.t>
oH-2 -*J6
'jfr. 7-9 > Di-IT' J2.9" M/d
7^:
eifcife
Af 7^f
W - ?,<>
--
-- -
1 1
---------
l^:'0r' / - ^ 1 >/<>
a/a/tf O/o/j.
isjdt illili
tlfeS
illiii
_^^**^*^
<^C?:
IlSli
i!?S
j2-
-- ---]
m,,. O'
b ;T1
SPECIFICATIONS FOR THE FOLLOWING SAMPLES ARE: 2C-60 Inlet strength should be >7% and < 9%
2C-60 outlet strength should run between 2% and 4 %
DEA wt % should run between 28 % and 30 % 2C2A benzene limit Is < 300 ppb and toluene limit is <150 ppb. TOD should be < 1000 ppm 2C-3S benzene limit Is < 300 ppb and toluene limit Is < 150 ppb.TOD should be < 1000 ppm OF-741 total TPA is < 1000 ppb. Oil and Grease should be <15 ppm. TOC should be < 50 ppm (TOC - TOO / 2.7)
OF-711 TOO should be < 15 ppm
NACnt1ett\Dataloff.doc
CONFTDFNTTA! DO 008558
DAILY PROCESS SAMPLES
MON
MON
Date
,4.27'^Mi
Time
Initial* 2C-60 2C40 INLET OUT
8i(b'
------u.
.x-
DEA WT%
2C2A 1ma| 2C2A 2C4C 2Cil
BZ/TOt
040 : BZ/TOL TOO
,
%/^A.
.....
53'
/& /Xy: I' v'\'\ .
2C3S 040
2C3S/WW TOD
2C3S/WW BZ-TOL-EB2
OF-741
bzttol
OF-741 "SA-Tir OF-711 0>A.71T TOO 040 BZ/TOL jiO40,
.S' /
' A > , ' A
jf:. ::J':
/j/y 2T
3-Sk> 3- 2-y.*
1T
M?>
S'ZA -9c
81,7 4- cl %-
6,'Vfv. U,G>
'Z.?*2:
y/A- & A. X' 3-0*1
3A f'? &
B-O
V? "X ,
iX,
5>;i
8'3<p'ck r-3i
N\C-
w 8-0 2. Aft
1
!> H-L W-yA
/Wj
Hi
aiissttm;:
tfs/d w
3-2
--*-
As*
&SJL5.k.
g/S ---
1`JLSZ- 7g>9*
J. 7
,*`1itr*" iiV:
,j'
4-/-9C,
7-(l JT ??> 6/
yy# 7-*/ bfofa
'\- 2.--
U p** ii>V / oo/.P" v\yb %>\z
4 <5
02g-i o&ls $ # Ce&~\ Qfo(P 4s& 4t`i,
2.8
: < >,s Mil
**
-i'-v:---'
. y `v.^< 4/m. . ' s>n
jfeL
-v.' 4. y
1 1
C4h A,
...... ! ... .
0q/#/&
:
^-- ,-r-^
'
!
oJ&U i/4
S .. .
y.
`A.V1".%.. v njjji"i i.y ........
ViV.vX-.vi .
_______ ir" A % \
oMfa ,,,o
. x.
, ft-- -ft *
c`% , ft X
6ft qBjtik
'v
rv:'
/afp
.......... .
oM. 0
&kjk
.< . ,
*s*y
"
A%-J'
Qfo/P
.
&/&/&
y^>'r4V. .
.............
SPECIFICATIONS FOR THE FOLLOWING SAMPLES ARE: 2C-60 Inlet strength should be >7% and < 9% 2C-60 outlet strength should run between 2% and 4 % DEA wt % should run between 26 % and 30 % 2C2A benzene limit is < 300 ppb and toluene limit Is <150 ppb. TOO should be < 1000 ppm 2C-3S benzene limit it < 300 ppb and toluene limit is < 150 ppb.TOD should be < 1000 ppm OF-741 total TPA Is < 1000 ppb. Oil and Grease should be <15 ppm. TOC should be < 50 ppm (TOC-TOD/2.7)
OF-711 TOD should be < 15 ppm
N:\Callett\Datalog.doc
OONFTDFNTTAI. DO 008559
DAILY PROCESS SAMPLES
MON
MON
Date
Time
InMeis ac-so 2C40 DEA 2C2A 3SSf 2C2A 2C-3* "?C*ir 2C36 2C3S/WW 2C3S/WW : OF-741 0F-741 mm : OF-711 mm, INLET OUT WT% B2TTOL ^ToOv. 040 BZ/TOL TOD 040 TOD BZ-TOL-EBZ SZTTOt ;;TOD:r 0*0 jBZiroL 0*0'-':;;
:^;:E
9,4 .<) 9
41* fw
# `-r*
a-7 3C.it t'vt1. 1 w /m.Ca f,.Q
t-t
tf/Wd:
^7 -
// t TP
29.<*
r:*. **i w 9- sT" 9 0 & fr*
*7 ^7p?
29J*
S-M'g
1\tp/n 2.' a0*. 0
7. & QzS ?.36
'34 Pm jC
^fo
& sAi*.
5.0D
.
uAi/fo
7* ft
jfi/ *4X
------
_----
ittfVA /> i-
< `f
OB*
J?!*'' '.p-PT
k::;
----
&M70
'S^sW'dtii _______ :T.M:
& ,sv
/V^As
bttokz
9-9-96
rz'y 2,'V) Am w
VaC-- 79A 8'S/prt RS
/3-P/r>
A./*'
RS
r/id/a
M
w , rfyX*. fM*i
: s'' j
29, y/s/k -TT1*
A. 3 JL3_ Pr
&1.&L
,.V^'
.
0Jn/y -o'Agf
______
SPECIFICATIONS FOR THE FOLLOWING SAMPLES ARE: * 2C-60 Inlet strength should be >7% and < 9% ** 2C-60 outlet strength should run between 2% and 4 %
OEA wt % should run between 28 % and 30 % 2C2A benzene limit is < 300 ppb and toluene limit is <150 ppb. TOD should be < 1000 ppm 2C-3S benzene limit Is < 300 ppb and toluene limit is <150 ppb.TOD should be < 1000 ppm OF-741 total TPA is < 1000 ppb. Oil and Grease should be <15 ppm. TOC should be < 50 ppm (TOC - TOD / 2.7) OF-711 TOD should be < 15 ppm
N:\Catlett\Datalog.doc
CONF t dfnt t ai DO 008560
Date
Time
Initll 2C-60 2C-0 INLET OUT
DEA WT%
DAILY PROCESS SAMPLES
2C2A
BZ/TOUEBZ
2C2A TOD
2C2A O&G
2C-35
BZ/TOUEBZ
2C35 TOD
Precaution
See Note
2C35 O&G
BZ/TOUEBZi
OP-741 TOD
L~lh% A-00 fin jfo AUt
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RUN ON MONDAY
EPA-741 O&G
--- ---
------
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Precaution See Note
RUN ON MONDAY
EPA-711 O&G
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--
mmm
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-->
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SPECIFICATIONS FOR THE FOLLOWING SAMPLES ARE: Note: If B nzene, Toluene, or EB2 show up In any of these samples, refer to the EPA 711/ EPA 741 Contamination Procedure. 2C-60 Inlet strength should be >7% and < 9%. 2C-60 outlet strength should run between 2% and 4 % PEA wt % should run between 28 % and 30 % 2C2A benzene limit is < 300 ppb and toluene limit is <150 ppb. TOD should be < 1000 ppm 2C-35 benzene limit is < 300 ppb and toluene limit is <150 ppb. TOD should be < 1000 ppm EPA-741 total TPA is< 1000 ppb. Oil and Grease should be <15 ppm. TOC should be < 50 ppm (TOC = TOD/2.7) OF-711 TOD should be < 15 ppm
CATLETT\DATA\DAILY PROCESS SAMPLES
oonftdfnttai 00 008561
Date
Time Initil 2C-60 2C-60 DEA INLET OUT WT%
it 3%
a.a
9'19% ~7`` An aOl. a t< 3.&
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DAILY PROCESS SAMPLES
2C2A 2C2A 2C2A 2C-35 2C35 2C35 BZ/TOL/EBZ TOD O&G BZ/TOL/EBZ TOD O&G
Precaution See Note
OF-741 TOD
'V9/3
5. ^7 <9/4/?...
MS
2.9
^
7/9/3
A <?/7/r 395 // mm
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RUN ON MONDAY
EPA-741 O&G
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Precaution See Note
BZ/TOL/EBZ
RUN ON MONDAY
EPA-711 O&G
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SPECIFICATIONS FOR THE FOLLOWING SAMPLES ARE: Nolo: If Benzene, Toluene, or ERZ show up In any of these samples, refer to the EPA 711/ EPA 741 Contamination Procedure. 2C-60 Inlet strength should be >7% and < 9%. 2C-A0 outlet strength should run between 2% and 4 % DEAwt% should run between 28 % and 30 % 2C2A benzene limit is < 300 ppb and toluene limit is <150 ppb. TOD should be < 1000 ppm 2C-35 benzene limit is < 300 ppb and toluene limit is < 150 ppb. TOD should be < 1000 ppm EPA-741 total TPA is< 100Q ppb. Oil and Grease should be <15 ppm. TOC should be < 50 ppm (TOC = TOD/2.7) OF-711 TOD should be < 15 ppm
CATLETT\DATA\DAILY PROCESS SAMPLES
00 008562
DAILY PROCESS SAMPLES
Date
Time
7 ;J3
Infill 2C-60 2C-60 DEA
INLET OUT WT% y
7-2- 2, r ft,*9
V vu
$ 'Z.J T>,~>
2C2A 2C2A 2C2A 2C-35 2C35 2C35 BZ/TOL/EBZ TOD O&G BZ/TOL/EBZ TOD O&G
^/C/C /*Y /0, / o/V/ z*?8 J.?
2*# /vy 7-7 o/3/o
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Precaution See Note
OF-741 TOD
' 2*.
RUN ON MONDAY
EPA-741 O&G
--
---
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1TOTW1S EPA-711 SzmnAte O&G Mf/M --------
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SPECIFICATIONS FOR THE FOLLOWING SAMPLES ARE: Not : If Benzene, Toluene, or EBZ show up In any of these samples, refer to the EPA 711/ EPA 741 Contamination Procedure. 2C-60 Inlet strength should be >7% and < 9%. 2C-&0 outlet strength should run between 2% and 4 % PEA wt% should run between 28 % and 30 % 2C2A benzene limit is < 300 ppb and toluene limit is <150 ppb. TOD should be < 1000 ppm 2C-35 benzene limit is < 300 ppb and toluene limit is < 150 ppb. TOD should be < 1000 ppm EPA-741 total TPA is< 1000 ppb. Oil and Grease should be <15 ppm. TOC should be < 50 ppm (TOC * TOD /2.7) OF-711 TOD should be < 15 ppm
CATLETT\DATA\DAILY PROCESS SAMPLES
chit T Al oONFTDt-T'*'
DO 008563
Date
Time
Initil 2C-80 2C-60 INLET OUT
DAILY PROCESS SAMPLES
DEA 2C2A 2C2A 2C2A 2C-35 2C35 2C35 m BZ/TOL/EBZ TOD O&G BZ/TOL/EBZ TOD O&G
Precaution See Note
OF-741 TOD
RUN ON MONDAY
EPA-741 O&G
Precaution See Note
BZ/TOL/EBZ
RUN ON MONDAY
EPA-711 O&G
<)t i 10'f-H
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____________
SPECIFICATIONS FOR THE FOLLOWING SAMPLES ARE: Note: If Benzene, Toluene, or EBZ show up in any of these samples, refer to the EPA 711/ EPA 741 Contamination Procedure. 2C-6Q Inlet strength should be >7% and < 9%. 2C-60 outlet strength should run between 2% and 4 % DEAwt% should run between 28 % and 30 % 2C2A benzene limit is < 300 ppb and toluene limit is <150 ppb. TOD should be < 1000 ppm 2C-35 benzene limit is < 300 ppb and toluene limit is <150 ppb. TOD should be < 1000 ppm EPA-741 total TPA is< 1000 ppb. Oil and Grease should be <15 ppm. TOC should be < 50 ppm (TOC = TOD/2.7) OF-711 TOD should be < 15 ppm
CAILETRDATAVDAILY PROCESS SAMPLES
CONFTDFNTTAl DO 008564
/ Dat
Time
Initil 2C-60 2C-60 INLET OUT
DEA WT%
DAILY PROCESS SAMPLES
Precaution
See Note
2C2A BZ/TOL/EBZ
2C2A TOD
2C2A O&G
2C-35 BZ/TOL/EBZ
2C35 TOD
2C35 O&G
ftzmDOEBZ
OF-741 TOD
RUN ON MONDAY
EPA-741 O&G
Precaution RUN ON Bee Note MONDAY
EPA-711 ;i2/Touet O&G
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--- --
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mtimi
0
- ----------
-- - - - - - - - - - - - - <^>
SPECIFICATIONS FOR THE FOLLOWING SAMPLES ARE: Not : H Benzene, Toluene, or EBZ show up in any of these samples, refer to the EPA 711/ EPA 741 Contamination Procedure. 2C-60 Inlet strength should be >7% and < 9%. 2C-60 outlet strength should run between 2% and 4 % PEA wt% should run between 28 % and 30 % 2C2A benzene limit is < 300 ppb and toluene limit is <150 ppb. TOD should be < 1000 ppm 2C-35 benzene limit is < 300 ppb and toluene limit is < 150 ppb. TOD should be < 1000 ppm EPA-741 total TPA is< 1000 ppb. Oil and Grease should be <15 ppm. TOC should be < 50 ppm (TOC = TOD/2.7) OF-711 TOD should be < 15 ppm
CATLETT\DATA\DAILY PROCESS SAMPLES
rTMFTOFNTr,
00 08565
DAILY PROCESS SAMPLES
Precaution
RUN ON Precaution RUN ON
See Note
MONDAY See Note MONDAY
c Time Initil 2C-60 2C-60 DEA 2C2A 2C2A 2C2A 2C-35 2C35 2C35 INLET OUT WT% BZTTOUEBZ TOD O&G BZ/TOUEBZ TOD O&G
OF-741 TOD,
EPA-741 O&G
; wsyu^w Iztrot/Esz
EPA-711 O&G
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7--
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--'
0 ?0'fjZj/Mii 0
________'
mSM
SPECIFICATIONS FOR THE FOLLOWING SAMPLES ARE: Not : If B nzene, Toluene, or EBZ show up In any ot these samples, refer to the EPA 711/ EPA 741 Contamination Procedure. 2C-60 Inlet strength should be >7% and < 9%. 2C-60 outlet strength should run between 2% and 4 % DEAwt% should run between 28 % and 30 % 2C2A benzene limit is < 300 ppb and toluene limit is <150 ppb. TOD should be < 1000 ppm 2C-35 benzene limit is < 300 ppb and toluene limit is <150 ppb. TOD should be < 1000 ppm EPA-741 total TPA is< 1000 ppb. Oil and Qrease should be <15 ppm. TOC should be < 50 ppm (TOC = TOD/2.7) OF-711 TOD should be < 15 ppm
CATLETT\DATA\DAJLY PROCESS SAMPLES
CONFTDFNTTAl. DO 008566
DAILY PROCESS SAMPLES
Precaution See Note
Dat Time Initil 2C-60 2C-60 DEA 2C2A 2C2A 2C2A 2C-35 2035 2C35
OF-741
INLET OUT WT% botouebz TOD O&G BZ/TOL/EBZ TOD O&G BZnroueBz TOD
fi. //-//-%
* (if* Y l> A.
?. p '7* 30.76 */d/c A3/ 4-t*
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RON ON MONDAY
EPA-741 O&G .3
0
Precaution RUN ON See Note MONDAY ^gp5??7x EPA-711 ZTOUtBZ O&G 7m,
0
> 4'/11 :tV
fehlss`3'^ wZ/f/ms.
Miff 'w&Z/ /? M$MM.
SPECIFICATIONS FOR THE FOLLOWING SAMPLES ARE: Note: If Benzene, Toluene, or EBZ show up In any of these samples, refer to the EPA 711/ EPA 741 Contamination Procedure. 2C-60 Inlet strength should be >7% and < 9%. 2C-60 outlet strength should run between 2% and 4 % PEA vt% should run between 28 % and 30 % 2C2A benzene limit is < 300 ppb and toluene limit is <150 ppb. TOD should be < 1000 ppm 2C-35 benzene limit is < 300 ppb and toluene limit is <150 ppb. TOD should be < 1000 ppm EPA-741 total TPA is< 1000 ppb. Oil and Grease should be <15 ppm. TOC should be < 50 ppm (TOC a TOD / 2.7) OF-711 TOD should be < 15 ppm
CATLETT\DATA\DAILY PROCESS SAMPLES
CONFTOFNTTAI. Dc> 00856 7
DAILY PROCESS SAMPLES
Precaution
RUN ON Precaution RUN ON
Bee Note
MONDAY See Note MONDAY
Dat
Time
Initil 2C-60 2C-60 INLET OUT
DEA WT%
2C2A 2C2A BZ/TOL/EBZ TOD
2C2A O&G
2C-35 BZ/TOL/EBZ
2C35 TOD
2C35 O&G
BZ/TOUEB*
0F*741 TOD
EPA-741 O&G
^ bf-Vlt x EPA-711 %zm>UEB2 O&G
L H'Up
fV; 1.44
IF, a.-// 2
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wmm
SPECIFICATIONS FOR THE FOLLOWING SAMPLES ARE: Note: If Benz no, Toluono, or EBZ show up In any of these samples, refer to the EPA 711/ EPA 741 Contamination Procedure. 2C-60 Inlet strength should be >7% and < 9%. 2C-60 outlet strength should run between 2% and 4 % PEA Wt% should run between 28 % and 30 % 2C2A benzene limit is < 300 ppb and toluene limit is <150 ppb. TOD should be < 1000 ppm 2C-35 benzene limit is < 300 ppb and toluene limit is < 150 ppb. TOD should be < 1000 ppm EPA-741 total TPA is< 1000 ppb. Oil and Grease should be <15 ppm. TOC should be < 50 ppm (TOC* TOD/2.7) OF-7.11 TOD should be < IS ppm
OONFTDFNTTAt
CATLETT\DATA\DA1LY PROCESS SAMPLES
DO 008568
DAILY PROCESS SAMPLES
Dat
Time
Initil 2C-60 2C-60 INLET OUT
DEA WT%
2C2A 2C2A BZ/TOUEBZ TOD
2C2A O&G
2C-35 BZ/TOUEBZ
2C35 TOD
Precaution See Note , ' '
mjambi.2C35 .v;je;op*74t# OF-741
O&G
TOD
RUN ON MONDAY
EPA-741
O&G
Precaution See Note
> OF-711 BZ/TOUEBZ
RUN ON MONDAY
EPA-711
O&G
aMK, 1 ,5/Pm Rs
J?2-33
i3-a 1(4
JVS 3.40
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33-39
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Note: If Benzene, Toluene, or EBZ show up In any of "hose samples, refer to the EPA 711/ EPA 741 Contamination Procedure.
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CATLETTVDATAVDAILYPROCESS SAMPLES
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Date
Time
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SF IFICATIONS FOR THE FOLLOWING SAMPLES ARE: Nc. If Benzene, Toluene, or EBZ show up In any of these samples, refer to the EPA 711/ EPA 741 Contamination Procedure. 2C-60 Inlet strength should be >7% and < 9%. 2060 outlet strength should run between 2% and 4 % PEA wt % should run between 28 % and 30 % 2C2A benzen limit is < 300 ppb and toluene limit is <150 ppb. TOD should be < 1000 ppm 2C-35 benzene limit is < 300 ppb and toluene limit is <150 ppb. TOD should be < 1000 ppm EPA-741 total TPA is< 1000 ppb. Oil and Grease should be <15 ppm, TOC should be < 50 ppm (TOC = TOD/2.7) OF-711 TOD should be < 15 ppm
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