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ACUTE TOXICITY TO FISH TEST SUBSTANCE Identity: N-Ethylperfluorooctanesulfonamide; may also be referred to as U1464, EtFOSA, EtPOSA, F-6309, or FX-12. (1Octanesulfonamide, 1,1,2.2,3,3,4.4,6,5.6,6.7.7.8,8.8heptadecafluoro-N-ethyl-, CAS # 4151-50-2) Remarks: Material is a white solid, lot 505 (cc842-3, F6309, L-1089). Sample purity was not recorded. `The following summary is abbreviated due to the fact that this study has been superceded by a more recent test. METHOD Method: Not provided Type: Acute static GLP: No Year completed: 1984 Species: Pimephales promelas R0 ESOL0 YS 00000000000 O00 96-hour LCsy: 34 (27-44) mg/L (Probit analysis) DATA QUALITY Reliability: Kiimisch ranking = 3. This study was tested in excess of solubility (individual weights above solubility limits) and actual concentrations were not measured. Results were based on nominal concentrations. Additionally, sample purity was not adequately characterized. REFERENCES This study was conducted by the 3M Company, Environmental Laboratory, 1984. OTHER Submitter: 3M Company, Environmental Laboratory, P.O. Box 33331, St. Paul, Minnesota, 55133 Last changed: 5/16/00 006058 eso, spe EST COPY AVAILABLE = CHEMTIOCXALIBCINTYVTESIT:RSOUEMFNMFAERNCYTERSEEFNVOARTLTUAATILON Chemical Tested Jy/2, samsasloe 2-3) Test ype:Detu(nFur ssi soreuc @sysesorcsois BR EL ums ston (7:5, mest Test Species: SARMAN MINNIS, (TIMEPNAUES FLOAMELR Test Date:_</-2- le LR (250 - Analysts): =r ; _ Exposure Type: (Expsure/Test Conditions) Static \/ Are Static Recirculatory. Static/Continuous Orbital Shaking Static Renewal, Flow-Through Diluent: Aerated Well Water (Initial 0.0.4,Zna/1; PHB,2,1 Temp. ZO CU/BF)) Water Hardness:_ Z4//) ppm Hardness Classification:AED _ Dissolved Oxygen % Saturation: Control(s) Lowest Experimental Dose Small Highest Experimental Do"1swaell PH Levels: 48-hr 79 9 8, 96-hr 20 19 B82 EExxptoesnudreed Control(s) Lovest Experimental Dose }Bwaqll Highest Experimental Dose wall Test Temperature C (F): 48-he 2 Bl ar 26x al al oad Extended Exposure Photoperiod: 48-he 96-hr EExxtpeonsduerde oT 2beiny zzeczy sel 006059 Sixteen hours light with a 15-30 minute transition period. _ ' AQEUNAVTIIRCONMTEONXTIACLETYLDAABTOARATSOHREYET DEFINITIVE (FULL-SCALE TEST) : eeemsnN pate e. zane MATERIAL TESTED NUDUGESOS [AO<S) TEST ORGANISMALTMANMMT. BEST COPY AVAILAGE 30,Lofg? no = corm = > -- hl RervicaTs COMBINED + Xs0's . IGsp's (95% CONPIDENCE iImMITs) T+rrostrmwaets %DH mall 24 --49) = &s-nep5i3 (2--a45) +MOVING AVERAGE ANGLE METHOD Hu (rs-48) | a (16-42) LG (oo--t 45 comms 006060 BEST COPY ENVIRONMENTAL AVAILABLEASSIS oxicETy LABORATORY oar seer w 75/250) Pe TesT t, l pre Soe cia Tested yg fps) tot gs st orventenS0me0paun)Sov Figsirs, Nets. buckfara, = fof Batch 45-/5 WE. 23.pypans hug. Size,Ben No. Organisms per do //)s loade ing Factor QO: Slits SN ee sh DiseaseTreatment: st Solution Volune//)Liters/N1-Glass Tank Tank Dinensions: Sm 0na6 as 33ret ge 9p ES EETEETEE Tee Sp (95% contidence Limite) lutionWaterCarbon-filteredwellwater (Temp. Z( C., 0.0. 4, 2 Pem, pH all s: R ark |tnitial] otal THREAT ARALYSIS Alot CAGE SY(2 407Jig BY(15-4 ioc 24fours 48fours. 72Hours. 82/7 ) 56 Hours I lemed=|"5 Tedd o> Jalal 0 bird o Hl .C loz moo 7 bord 5 Bde = bod = hl L& liso [seo]20 latin]+ Bded 5 bod 2 lds TT TTT IT Il 1] LT 1 TTT TTT TTT TJ -- Be s & oe 2 ret | 2/70 pr SNES ODI IRAN OC ER HTUS, Jocd/7C 4 2.8 WR ia |Za| Z7a. 2 es, la A -- condary Effects (other thanMortality) : so________ 00000000000 wll | re Awe |Awe | 6 VV dee[Aone[Awe | dips 2. YT Tr] se|m 2 w |zou | 2z 0 | 2 -- tf 2. 006064 BESTCOPYAVALIBLE romspr veetest tte por Smtr vaveria NE(0.8) tet sus DEFINITIVE (FULL-SCALE TEST) LR_ wV t 0O 3pLlpW raansnAvgd. lSni3)BzS hiem Noy . OrganiNsmses ah &d% [2 Baten 15-5 1 Disease Txestmants_//Z7// perdose_/) Loading Factor 9,2 4igp on 2st Solution Volume/)Liters/All-Glass Tank TankDimensions: BREIIFITZewdery ime Started [2 Sun Date Started [2 [6 DateCompleted 0/8 {ution Water Carbon-filtered well vater (Temp. Z/] _C., D.0, 2.2 pm, p=) Ig, (95% Confidence Limits) 8,2 ) nll s ro Jot ro oes "LIUctosnWAERTANoGSnEsIRS RE eSHl1f5-e 3x7 s? msl Se mt Laced| oe 17 Joi [oad [2 Ni I1 Bh am A > po Jae [eos 70 | 1=20L [cooll0oTeb llyl0oBeliBlo0dBlBd l20d1d 20 p aLo [scol = lolol kdl 7 Llad 1d nS 1 TT 111 ITT Thon Tents TE E 5 T py EASYoy EETALIENLS Dy ENGUIR LAT C7 ita Co VS AI 2 JIT ------ a nw wm ee sem. =soondary Effects (other than Mortality): -- Beso 00000000000 moll Ve |Hae [Apr| Mow AL New | e 1 |r 1] / AV The|1 |2 | 7 MMs|o 2r |2g ,| u 2n| = 006062 AAN NT SS sT ] ----