Document 7Odz6DLN1GngNwn8nkM1nRX7o
&iM <* DATE >
...Kgsisa.:. <LOT NUMBER )
EST, WT. 2603* LBS,
PREPARAT ION NOTES: ___ _
( )RT-695-D (0) JJG 3/18/81
EWK 12/7/81
COMTYP JOB NAME = 36RT695DM0 /)
TYPED BY- KLW
-
STANDARD HRS,_____.___________ _ TIME //J/_ _A_M,
______ --
EQUIP MENT
;___ -j____ - 1 ('&&
NON-BLEEDING
I USE
N-CODE
NAME: * BONV RED DARK
1 LBS
----- <
------------ ------ ---------------- ---- 1------------ j ----
NECESSARY, CLEAN, DRESS SPARKLER & PRE- |
J.
COAT WITH 15* BICALITE FILTER AID
777-A
OBTAIN FOR S 6 2-CHL0R0-4-AMIN0TOLUENE-5 j
| 740-C
IRONIC ACID
I|
OBTAIN FOR S 423-HYDR0XY-2-NAPHTH0IC ACID I
! 82-C
_ _ _ _ 1 __ J
| ACCT 1 LBS -
J
\ _s>Z, |'
1 j
I
* (732G> WATER INTO V-317
|!
|
1GH & POUR IN SODIUM HYDROXIDE _
1
^ ' M__#______ \M&3,,\
TURN ON AGITATOR & STEAM & DUMP IN FROM S 21 2-CHL0RG-4-AMIN0-T0LUENE-S-SULFDNICACID |
^L
| '1
) 7--D i
. ,p 740-C 4,
215
: ML-
-TA igajrl
-35LP&
\j233Li
t/t>3
i
i
ON POSTAL SCALE 2-AMINQ-T0LUENE-5-
C ACID & ADD-EOT
IN ACTIVATED CARBON -
FILTER AID
F WATCH FOAM
IF NECESSARY ADJUST
+ BY SODIUM HYDROXIDE
ASSUME 50%
STIR 30 MIN, AT 212-214 DEG, F, THEN SHUT
! 1 OFF STEAM
WATCH FOAM
^
ii
s p a r k l e r p r e s s u r e _CL_p s i
\ 3*?*^ IF NOT ZERO,' NOTIFY SUPERVISOR
i!' CIRCULATE 15 MIN OR LONGER THRU SPARKLER
1 ) UNTIL SOLUTION IS CLEAR-
.
I MAINTAIN AT 190-195 DEG. F FOR SI? RECORD-: HT_/tPLDEG.F & RECQRDEE^.DEG-F
RECORD: STARU:M#rOTAL MINgr.CLARITYf^_
-584-C i13-B 777-A
I________I - ...-7-D
1 i 1
50 10
I
100 3
1
;:UN 41 (99G) WATER INTO V-iOO
I
WHEN S-13 COMPLETE, PUMP V'317 THRU
1
SPARKLER. MAINTAIN V-317 AT 19.0-195 DEG.F i
RECORD: START$<4QPTAL MIN_rf^
!
SAMPLE FROM HOSE. SHOW-TO SUPV'R FOR OK 1
1 rsss
MAKING INSTRUCTIONS: BATCH UNIT
EQUIP MENT
I USE 02 OF 04 CG 36 CODE RT-695-D (0) | LBS
N-CODE I ACCT i l bs;
31? 4
IMS' I WHgW"S 13 COMPLETE, CLOSE V-317 OUTLET 6 f ' J^STOP PUMP
RUN IN 7* (216G) WATER 6 HEAT TO 190-195
II DEG^F
,-
| | I
317 J^mPTc IRCULATE THRU SPARKLER UNTIL SOLUTION IS I
CDNT'DI 4 |-
J CLEAR
I
| MA INTAIN AT 190-/95 DEG * F FOR S 19 6
!
I RECORD: HT^/f *7_DEG. F i, RECORDER
T RECORD START^yfOTAL MIN / SCLARI TY"2?J_
\d^TWHE 100 WHEN S 18 IS COMPLETE, PUMP V-317 THRU
|
5 i^RARKLER INTO V-10
I
20-^1 RUN IN 5` <90G> WATER & HEAT TO 190-195
I
j^Btrr f
[
1 CIRCULATE 15 MIN THRU SPARKLER, PUMP V-317 |
PARKLER INTO V-100
I
N MT, BLOW OUT SPARKLER INTO V-100
I
I HEAT TO 165-170 DEG* F (TAKE 1 QT* SAMPLE) |
I I (WITH AGITATION ON)
I
I I TEST FOR CLARITY OF SOLUTION* SHOW 1 QT* l
I 1 SAMPLE TO SHIFT SUPERVISOR FOR APPROVAL
I
1 I (EXAMPLE OF `ACCEPTABLE CLARIFICATION OF
|
I | N-740-C IS AVAILABLE IN OFFICE TO COMPARE |
1 JUAWFHr
-I
L3**TlF S 23 IS OK,- CONTINUE WITH S 25* IF S 23|
r RECLARIFY THRU SPARKLER I
125^*f*F S 23 IS OK, REHEAT V-100 TO 165-170
i
I DEG* 'F FOR S 26
,
1
ISWr^rtlJJ TO 16" (1590G)
1
IQT^UHEAT V-100 TO 165-17 DEG* F
|
RUN IN V-324 HYDROCHLORIC ACID THRU DIRECT |
a
'LINE AND RINSE IN
M__A ,
\Ct&jL-
-STIR 15 MIN AT 165-170 DEG* F
|
L ADJ TO 50" (49TOG) AT 34-38 DEG* F
||
RECORD : TEMPS^J: >d)EG* F AND' IF NECESSARY 150X330 |
i ADJ TO 34-38 DEyT J,
.I I
RECORD: TEMP_L_____ ;DEG. F
II
""45" (4320G) WATER INTO V-107
'
I
TURN ON AGITATOR AND STEAM AND DUMP IN
I
JGANESE SULPHATE
I 1400 1
IN BARIUM SULPHATE
-
I 250 |
TO 150-16 DEG* F AND STIR
3RE>: PH _^^l_(5*0-5*5)
.V
PH ABOVE 5.5, ADJ TO PH 5.5 OR LOWER
7URIC ACID>>w ,
ASSUME T8%
--JLi
im^fmCORD: PH_JaacjiL`
|fc4^N0TE: . IF PH BELOW 5.0, DO NOT ADJ UPWARD
-0^ } HOLD FOR S 58
-V
-. .
DUP050101944
e b o Jp .TT
HIKING INSTRUCYIONS: BATCH UNIT 7
PACE' G3 OF 04 CG 36 CGDE RJ-695-B (0)
~ 'n -Eq d E
ACCT LBS
IN 47* (T6"10G> WATER INTO V-322 1^K<WWEEICI Gil,AND POUR IN SODIUM HYDROXIDE
' .T /V-
',
V DUMP IN FROM $ .3 3-HYDR0XY~2-NAPHTH0IC
^ihn
i ^MM-
1-HTDR0XY-2-NAPHTHOIC ACID ON POSTAL
CE AND ADD LOT / /
TO' 70-90 DEG, P
i^^flFT IN BLANCOL N IN ONE TO TWO MINUTES
DUMP IN TETRASODIUM PYROPHOSPHATE G STIR 5
i i MIN OR LONGER TO.DISSOLVE
.
|
7-D S2-C
470 934
I 1 80-C .1 ;'R0)
T' ;#
567-B 1 Y`-T?
479-D i
0
313/ \&T\ WEIGHT SODI&M NITRITE & POllR INTO V
302 !
f FOR 50 '
-M.' .___ . 'jt^JSr&VA 1
9i
725-A
A'DJ V-322 TO 65* J224GG)' AT 77-80 BEG,. F RECORD::'' TEMP^Tz .___ DEG, F
SLURRY' TRISULPHOIC SOAP D WITH 30 GALS WATER:'-In d r u m; p o u r in AND STIR-5 min .
I
:UN IN N-725-A .FROM -S 47 AFAP. INTO V-100
STIR 30 MIN AT 36-38 DEG, F MAINTAINING -
t.R, +KI
.'
RECORD: TIME S1WX/&MB-, TEMP 3-b_____DEG, F
NOTE?:
' '
' .'
H ) IF CR-. KI- ADD 20* 'AS IS* INCREMENTS
HYDROCHLORIC ACID . X
^ASSUME 32%
' RECORD : CR
< +-), I__^1__ < +) /-
<2) IF CR+, KI- ADD 20*- `AS, IS* INCREMENTS
So d iu m n it r it e .* /
^a s s u me 33%
RECORD: ,CR_,,_t*l^<+> .. KIL< +0 ' : TEMP...___ ____DEG, F
COUPLE V-322 THRU UNDERSURFACE DISTRIBUTOR
INTO V-100 IN 90-110 MIN (USE 9/1 SACRIFICE> RECORD: STARTo?iOOjHjOTAL MIN../^__
w h en s 53 Co mp l e t e s t ir is min ,,
RECORD: DIA2D_Xr_<-) j BASE_rET_(+ >
(7,0-8.0>TEMRJfe^,.DEG, F (60-65 F)
NOTE;
(1) IF-PH IS 5,0-7,0, WEIGH AND DUMP IN
30* "AS IS"* N-7-D DILUTED TO 30 GAL
AFAP SODIUM HYDROXIDE
ASSUME 50%
(FOR PH ADJUSTMENTS USE ONLY -DILUTED
N-28-D AND N-7-D)
ADJ TO PH 9,0-9,5 (SEE ATTACHED PH ADJ AID)
HYDROCHLORIC ACID
\ ASSUME 32%
(1) IF PK IS- 6,5-7,0, WEIGH 40* AS IS
1 _______
. N-7-D POUR INTO 50 GAt WATER <1/2
FULL) IN PT & RUN INTO CV 100 IN 15
MIN 6 RINSE IN PT/ STIR 5 MIN t,
RECORD: PH ___^d_____(9.0-9,5)
DUP050101945
EQUIP
I USE
N-CODE ! AOCT
EQUIP i KENT
USE PAGE 04 OF 94 CG 36 CODE RT-695-D (0) I LBS
N-CODE
ACCT LBS
2) IF PH IS 7*0-7.5, WEIGH 354 AS IS N-7-D I
POUR INTO 50 GAL WATER (i/2 FULL) IN PT & I
r u n In t o c v 100 in 15 min . Ot in s e in p t . i
STI#5 MIN & RECORD; PH__<9.0-9.5) 1 =
3) IF PH IS 7.5-8.0, WEIGH 304 AS IS N-7-D i
POUR INTO 50 GAL W,ATER Ci/2 FULL) IN PT 4. j
RUN INTO CV 100 IN 15 MIN. RINSE IN PT.
|
STIR 5 MIN 6 RECORD: .PH
_____(9.0-9.5)1
4) IF PH' IS 8.0-8.5, WEIGH 104 AS. IS N-7-D I
POUR INTO '50 GAL WATER (1/2 POLL) IN PT & i
RUN INTO CV i0- IN 15 MIN.^iV RINSE IN P+/.;l
STIR 5 MIN & RECbRD: PH^j^__(9.0~9.5) / I
5) IF PH IS 3.5-8.9, WEIGH 54'AS IS N77-D I
1.4-^
'XS. 3
I
) IF PH IS* ABOVE 9.5, DO NOT ADJUST
RECORD: PH^'il`L_SODIUM HYDROXIDE ASSUME"; SOX L
NOTE: ADD N-28-D IN 54 `AS IS* INCREMENTS 1
TO APPROACH PH 9.0-9.5 THEN USE
,I
LESS N-28-D HYDROXHLORIC ACID
I
(CONCENTRATED'N-28-D & N-7-D AND TOO LOW j
I 1 COjJIMflNG TEMPERATURE CAUSES MASSTONE TO
I
A *J>trT0O LIGHT)
.I
I5an SHUT OFF AGITATOR
,*
|
/-l
DURINGS 53 HEAT V-107 TO 210-212 DEG. F }
ii SHUT OFF STEAM
I
NOTE: s IF`NECESSARY REHEAT V-107 TO210- I
. F PRIOR TO START OF STRIKE '
I
100 INTO V-107 IN 70-75 MIN.
I
07 TEMP DROP TO 200-205 DEG. F
I
STRIKE THEN MAINTAIN AT 200'-2OS DEG. i
ALANCE OF STRIKE WITH AGITATOR SHUT |
^F^>-iO0 ^ `
,,l
-JSlEpBRD: START^rf^^TOTAL MIN~Zj__
|
^Ey^SfRJKE COMPLETE, HEAT TO 210-212 DEG. FI
SPrm^l^MlN AT 210-212 DEG. F
|
OD^TQ- 130-190* (1 8240G).
|
D: PH_^i^___(6.5-7.2) AND STOP
I
AGITATOR'
|
! i
II
. .Ald&LzSiU;,
DUP050101946
DUP050101947
DUP050101948