Document 7ObbEDjXLJoNokEmg65kmj4Le
1-184 (SOM)
~e,,o tehneco CHEMICALS, INC
'^To H.B. Carr frm jqy. Kanzler
Subject LUCldol 223M
at Burlington at Burlington
d*te April 26, 1972
copy to
R.S.
E.
J..C. 'ile
Cole
Gallagher Siegel
The recent shipment (4/20/72) of the subject initiator showed rather high differences in the assay analyses. Previous exper ience of similar nature (shipment of 5/5/71 to Flemington, high out-of-specification with 44.0/ and 43.6/ assay) was explained by Lucidol with difficulties in their initiator mixing system. While changes in reaction rates may not he noticed., it is desir able to get our money5 s worth as well as a relatively constant product quality, therefore, Lucidol was notified via Purchasing (J.F. Bubnis) of the situation. Furthermore, the certificate of analysis listed lot MMGC015 only.
Attached is a list of the assay results obtained with samples from the shipment of 4/20/72. It is noted that the rerun of re samples (taken from another bottle of the same box previously analyzed) from lot MMGC015 show good reproducibility of the in itial results. This indicates that the same quality level was maintained throughout a given box. Lucidol5s reply will be made available as soon as it is available.
Attachment. FWK/jt
F.W. Kanzler
COLORITE 015116
TABLE I ASSAY RESULTS OF SHIPMENT FROM 4/20/72
Lot Number MMGC015
MMGC081 MMGC082 MMGC061 MMGC031 MMGC021
Number of Boxes/Lot
70
19 51
28
%
30
15
Assay 41.3 40.2 40.7 40.4 39.4 39.4 39.4
-
40.9 41.1
41.1 41.3 . 41.5
40.4 39.8
40.9 40.6 40.7
40.0 40.7
Resample A,
39.4 39.8 39.8
COLORITE 015117