Document 7OKqoywjM7MJVb01o31Z3mzb8
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C.VX90TV9O3
DATE PRINTED: 5/12/82 D. V. 902/904
oe 3Z, CODE RT-A9S-D RKG___
'MA-M 7~DATEr7~-
_g ?M33.____ "(LOT_NUMiiR)
EST. WT.'^jSIS LBS.
PROCESSES < )RT-69S-D (M>
APPROVED BY EWK2/25/82
TYPED BY: KLW STANDARD HRS. ___________
TIMEM
PREPARATION NOTES:__________________
NON-BLEEDING
WATCHUNG RED B
USE i N-CODE i ACCT
LBS I
j LBS
___ BATCHES SINCE SPARKLER LAST AFTER 4 BATCHES, CLEAN, DRESS
i I.
14
I _i
N PRECOAT WITH 154= DICALITE
Ii
! IN FOR S11 2-CHL0R0-4-AMINQTGLUENE-5- I
1 I
LFONIC ACID
.,
I
OBTAIN FOR S41 3-HYDR0XY-2-NAPHTH0IC ACID |
1 !
INSTALL DV & CV RECORDER & CONTROLLER CHART!
NOTE: RUN 15' WATER INTO V-904. PUMP WATER |
FR0it>V"94 THRU DISTRIBUTOR. IF WATER DOES |
NOT COME OUT OF ALL DISTRIBUTOR HOLES WITH 1
LL FORCE, NOTIFY SUPERVISOR .
1
777-A
740-C 82-C
O' <4150) WATER INTO V~9^ & HEAT-TO
DEG F
8-9 MIN DRESINATE X>
IR 5 MIN & RECORD:
<9.5-1 .5)
STIR 20 MIN OR LONGER TO DISSOLVE FOR S44
\ ! I !
|
OTIFY PRESS ROOM BEFORE ROPING OFF
REA UNDER V-922
<782G) WATER INTO V-922
SODIUM HYDROXIDE IN V-926 & RUN IN
M_lQ_____
ON AGITATOR STEAM & DUMP IN FROM S2 I
L.Sn _ - #t t 110y0y%/i1
- aM.'
TOLUENE
-
9SEv !:3
IC ACID ACTIVATED CARMn
I ___1 AZi
FILTER AID W. 212-214 DEG F WATCH FOAM!!!!
! 10
BY__rfc__< + > if NECESSARY ADJ TO
+BY SODIUM HYDROXIDE
ASSUME 50%
i
STt.3 MIN AT 212-214 DEG F, THEN SHUT QFF1
AM. WATCH FOAM. RECORD: SPARKLER PRES- I
SURE _ Cl __^PSI IF NOT ZERO NOTIFY SUPVR. I
CIRCULATE 15 MIN OR LONGER THRU SPARKLER |
UNTIL SOL'N IS CLEAR. MAINTAIN AT 190-19 F| FOR S19. RECORD: START jMgtei-jAIOTAL MIN,,
CLARITYl^-bft4>HT_Jl3Lk^u^ & REC_J|y&__ F
I i.
I I |
1 1
N32893
DUP050464617
MEKT 1
WV'CVj 1 4 j1
ErE 2 OF 3 CG 32 CODVE RT-698-D (M) ,
2" C5SG) WATER INTO V-Sfflr/CV Ho [ WHEN-Si 7 COMPLETE, PUMP IN V-922 THRU
KLER, MAINTAIN Vf|>22 AT 19~195 DE F D: START_l\.|l.llw TOTAL
USE LBS
N-CODE l ACCT I LBS
4* (1407G) WATER INTO V-92
|
rMP IN CALCIUM HYDROXIDE & STIR TO SMOOTH. !. 53
SL.URBY W^CT SODIUM HYDROXIDEI IINN VV--992266 && RRUUNN IINN !I '''''
W HOLD FOR S41,
M_lCL-____ ,
I
ASUREfeX.jLHWTS IN V-928 FOR S35
HYDROCHLORIC ACID
M.._\.L______,
SODIUM NITRITE IN FT FOR S38
M_^L-______,3&bL____%
I
i Ij CLMI
f, I AIMS,
542-D 1 I i
7-D i
53 i 66
i
28-D 1 I
725-A I
544 367
N JJ19 COMPLETE., STOP PUMP & INSERT V-9221
PLUG
,- I
IN 15* <309G) WATER & HEAT' TO 190-195 FI
ULATE 15 MIN THRU SPARKLER
i
"HP V-922 THRU SPARKLER INTO 'WMtt/CV
|
1'
-9" C177G) WATER INTO V-922 AND HEAT i '-195 F. CIRCULATE 15 MIN THRU SPARKLRI
V-922 THRU SPARKLER INTO N MTY BLOW OUT SPARKLER INTO OUR IN IGEPAL CO-63 HEAT TO 165-170 DEG F FOR S34 .
r
/CV
i
47
I 979-D I
I
CV i . I NOTE: IF N-740-C SOL'N'WAS PUMPED DIRECTLY I
11 I
FROM SPARKLER TO CV, OMIT STEPS 33 & 34- |
133 > RUN t m < fo-cci
-------- 1
134, I WHEN S32 C0MPLEI~4tWW`*,^g9fflr^T""T65-- 1
IHRF UNC^kSURFACE DISTRIBUTOR INTO CV AFAP 1
*2-15 MIN) - MAINTAIN 1 45=^LZl J)EG F liLJLV,
\
HYDROCHLORIC ACID N-28-D FROM S23
*-15 MIN
15 MIN AT 165-17 DEG F-
t*
Lfea__-48" (4536G) AT 32-38 DEG
RD; TEMP_J3*_0__ F, VOLUME
*54X33
N IN SODIUM NITRITE N-725-A FROM S24
AFA'P (-5-1 MIN) & RINSE IN PT
STIR 30 MIN AT 32-38 DEG F MAINTAINING-/Cli
+DR, +KI FOR S40-RECORD: TIME START
CR__-*r-__< + > KI__SC__<+> NOTE: (1) IF CR-, KI- ADD 204 'Up IS" INCREMENTS
HYDROCHLORIC AG*fD
i
RECORD: CR. __<_< + > KI_,,.__( + ) ASSUME 32% l__^
(VjriF CR+, KI- ADD 204 "AS IS* INCREMENTS I
DIUM NITRITE/^
i
RECORD: CR.__<__ < *> KI_,,CC,,(+> ASSUME 33% !
DUMP IN FROM S3 4, STIR iMIN LOT
]
3--HYDR0XY-2-NAFHTH0ICACID
i 1Q3U
! 57-A I
I
i 28-D I.
725-A S2-C
1021
DUP05046461 8
CATE PRINTED: 5/1:
EQUIP MENT .1
902' 14, -12
E 3 OF 3 CG 32 ,JODE-RT-698-D <M> IN AMMONIUM CHLORIDE
USE LBS
221
N-CCDE 165-A
IMMEDIATELY AFTER S41 COMPLETE, WITH V-902
AGITATOR ON PUMP V-902 THRU UNDERSURFACE?
DISTRIBUTOR INTO CV IN 18-22 MIN. LET TEMP,
SE FREELY. RECORD = START&J^U^TAL i __M___
STIR 15 MIN & RECORD: PH
< 9.0-9. &)
TEMP__ 1*Ol DEG F (40-50 DEG F) AND IF- PH
LOW 9.0 ADJ-JO PH 9.0--9.8
TUM HYDROXIMT
/ -. ASSUME 50%
'ECORiD PH_^r__ DIAZO_jj-L_<-> ASSUME 32% .*X!:< + ) HYDROCHLORIC ACID
EJECT
FROM S8 INTO CV
IN I OCTANOL
TO 5 73-175, DEG F IN 55-65 JIN AND
HTAl^b-DEG F & REC_0^st_DEG F
30
7-D 28-D
588--A |
^G S46 HEATING, RUN 10" (268G) WATER
''I NTS' V-902
`
RN ON AGITATOR & STEAM & DUMP IN BARIUM
'HktiRIDE
|-M^I.^HEAT TO 155-160 DEG F 6 STIR TO DISSOLVE
[ I 259
i
i 6~B 25?
WHEjjJ S46 COMPLETE, STRIKE V-902 AT 155-160F!
n.&DUNDERSURFACE_DISTRIBUTOR INTO CV IN
3 MIN
-
I i
CORD: STARTJU.tr_TOTAL MIN,,jJ
|
EAT CV TO 193-195 DEG F IN 16-15 KlN.rt * ^
STIR 60 MIN AT >193-195 F. RECORD .START^OtOil-H.
20 MIN ||&STIR RECORD PH5&4(8.8-9.3> !
NECESSARY Jl|lJ JO PH 8.8-9.3 ASSUME 56% l__38k-
AND RECORD:
ASSUME 32% I
WHEN S52 STIR^IpMPLETE,' FLOOD TO 180-19" 1
(*/--180G) AND STOP AGITATOR
'|
WHEN INSTRUCTED BY PROCESSING AREA HALF WAY i
1
THRU PRESSING, DUMP IN I OCTANOL, STIR;5 T 10 i
MIN 6 STOP AGITATOR. RESUME PRESSING. '
!
I
:^Sk k i
_
FIN1 M2.
OP* a.--
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588-A i 10 I
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