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Ledbetter - B-2-N Steinbach - G-4-E
Stratmeyer - B-2-N Sample - B-2-N Sohwab - JFQ Partlow - JFQ McIntosh - JFQ
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J. R. Kellogg - JFQ
H. L. Minckler -B-2-S T. M. Patrick - Res. 1 R. E, Keller - Res. 1 D. C. Reed - Res. 1
0. J. Marchand - Res, ;
MONSANTO COMPANY Organic Chemicals Division
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To the Qeneral Manager Organic Chemicals Division
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Estimate No. 1908 Dept. No. 76001.0000922 Plant - R6D Laboratories
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PURCHASE BIOMEDICAL GAS CHROMATOGRAPH
Capital Addition
87,000
DESCRIPTION
Purchase biomedical gas chromatograph with all-glass system and multiple flame ionization and eleotron oapturs deteotors for the analysis of thermally sensitive and polar materials,
APPROVAL General Manager
H. l. Minouer
Date
EXHIBIT WBP M-27
HONS 034702
TOWOLDMONOOQ3285
Estimate No. 1908 Page 2
NEED FOR THE PROJECT
Late in 1966 Swedish researchers reported the presence of poly chlorinated biphenyls in a variety of biological samples. Since that time the Organic Chemicals Division has received a number of requests for Aroclor samples from active pesticide research groups. We also know that the U. S. Public Health authorities have initiated studies to evaluate the significance of this environmental contamination.
To assess the validity of these findings, the impact they may have on our Aroclor business, and to avoid restrictive legislation, the Functional Fluids Business Group has begun its own study.
The Applied Sciences Section has been requested to develop the necessary analytical methodology for this project. To do this and to do it correctly, we need to purchase a biomedical gas chromato graph. This instrument is designed specifically for this type of analysis and is used by most pasticida researchers, including the Publio Health authorities.
Any analytical information we generate will be judged in terms of the techniques and equipment used. By using the tools most familiar to these people, we feel any information we provide will be more effective.
The biomedioal-type chromatograph provides an all-glass system with direct injection into a U-shaped glass column which is attached directly to the base of the flame ionisation or elaotron capture detector. This allows high efficiency analyses to be made on pesti cides, steroids, organo metallios and polyfunctional organic chemioals which are thermally or catalytically unstable or have polar functional groups that, in the environment of the ordinary gas chromatograph, cause them to decompose or become irreversibly adsorbed.
The R(D Labe do not at present have such instrumentation. Therefore, we recommend purchase of such a ohromatograph for initial use on the environmental Aroclor project and to broaden the capability of the Applied Sciences Section in the gas chromatographic analysis of unstable organic systems.
HONS 034703
TOWOLDMONOOQ3286
Estimate No. 1908 Page 3 STATUS OF THE PROJECT No commitments will be made until this project is approved. RECOMMENDATION It is recommended that this project be approved.
Submitted by E, M. Emery Group Leader R. E. Keller Research Section Manager Y,'" M/ l,atricX? 'Manager R8D Laboratories
mw 8/28/68
HONS 03A704
TOWOLDMONOOQ3287
A20C-C
Monsanto Company
PROJECT AUTHORITY FOR EXPENDITURE
and/or RETIREMENT
(THIS FORM TO BE USED FOR AUTHORITIES REQUIRING GENERAL MANAGER AND LOWER LEVEL OF APPROVAL)
PLANT
BUDGET ITEM NO.
DEPT. NO.
DATE
ENG. JOB NO.
Org. RSD Laboratories
76001-0000922
DESCRIPTION. REASON AND JUSTIFICATION FOR WORK:
8/28/68
PAGE 1 OF...
AUTHORITY NO.
1908
Purchase Biomedical Chromatograph
PREPARED BY
Marchand
ITEM
REVIEWED BY
GENERAL NCR.
DESCRIPTION
DATS
1. 29-4976, Chromatograph 29-4977, Recorder
29-4978, Integrator
*
PRODi HGR.
APPROVALS
DATE
PLANT MGR. .
.'
DATE
|
OTHER
DATE
EQUIPMENT
TRANS.
NEW
CONTR. WORK
MAT. ft STORES DIRECT SUPP. O'HEAD LABOR
SHOP
O'HEAD
TOTAL
7000
7000
1-1908-29/76001-0000922 Life - 5 years (U Bldg.)
EXHIBIT WkPMv27;l
INFORMATION FOR RETIREMENTS
SUMMARY OF ITEMS TO BE RETIRED I. INSTALLED COST
2. VALUE NOT RETIRED
INFORMATION FOR EXPENDITURES
CLASSIFICATION OP AMOUNT AUTHORIZED
PROJECT SUMMARY
$. CAPITAL EXPENDITURE 9. REPAIR OR OTHER EXPENSE
7000
Ut PROJECT TOTAL (ORIG OR REV.)
......... ' 1--.------ --
IS. LESS PREVIOUSLY AUTH;
S. VALUE TO BE RETIRED 0-2)
10. LEASEHOLD IMPROVEMENTS
4. ACCRUED DEPRECIATION ON VALUE TO BE RETIRED
XU TRANSFERRED EQUIPMENT
|. DEPRECIATED VALUE
f (3*4)
S. AMTi EXPECTED FROM SALE. TRADE-IN; ETC.
12. DISMANTLING EXPENSE [
: I). TOTAL AMT. AUTHORIZED
7000
>. ftHIRI MI NT LOSS <AeS>
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W* `\ U '} IP'-* S.'i P ${*
8 I... UVH IOR LAPIiAI. APPKOVA1
UP- FORM A--823--1 TO DETAIL RETIREMENTS
| IS, PROJECT TOTAL ^ THIS REQ. (U.15)
17. LESS TRANSFERRED EQU1P
IS. NET CASH REQUIRED <16-17)1
1ft. AMOUNT AUTHORIZED = (16)
MON-MT-008602
7000
7000
7000 7000
TOWOLDMONOOQ3288
RSD Laboratories - South Second Street
September 13, 1368 Hewlett-Packard Company
r Eiaery Vo. Tucker
Purcnaso Order AT-9430
Vernon Fox Stores ~ J.F.Q. Plant
Sometime ago an instrument containing a radioactive source material was lost before reaching the Research department At that time we instigated tne following procedure for subsequent orders of like material or equipment:
''This order requires SPECIAL handling. Upon receipt of this equipwenTTn the JFQ Storeroom, please inform:
Dr. Scott Tucker Station 3*# 39
Please deliver this equipment DIRECTLY to:
Dr. Scott Tucker . Lab 213, U Building
DO HOT LEAVE EQUIPMENT AT ANY DELIVERY STATIONS."
Attached is a Xerox copy of the Purchase Order. Since there is not space on the order to type this statement, will you please take action to insure that the procedure ia carried out.
0, J. .Marc hand raw
MON-MT-008603
ktQiiiSi'i iOil TO PURCHASING DEPARTMENT
INSTRUCTIONS TO REQUISITE |R
1. TIKS FORM MUST BE TYPEWk.lTEN
2. PO NOT fill IN SHADED AREAS
3. REMOVE1S1. COPY FOR YOUR FILES __
DU RECTO.
1 ESI. COS1
[ INQUIRY NO.
f/13/08 2 wks. $6785
iii
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knowni
H* ewlett-Packard
~ ^ 812'.STTTrentwood UTvST
. St. Louis, Mo. 63144 ' Attn: 'Mr, Lou Anderson
REMARKS
r PURCHASE ORDER
DATE
V'3/8
IOC.
NUMBER
AT
REQUISITION NUMBER
r oe icoin
FRtlGtU ICftMS
ftouic
EMERY AIR FREIGHT
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p.c.Imc or hem no.) quantity
1. 1
2. 1
3. 1
1
j1 2011 Kosciusko p St. Louis, Mo.
o
63177
UNIT
DESCRIP1ION
NET UNIT PRICE
ea. Model 402 Basic Dual Flame
$4000
Ionization Detector Gas Chromatograph
ea, Model 71-27A Moseley single-channel
recorder
'
$1100
ea, Option 03 Electron Capture Detector) pith high temperature WT63 foil
(installed)
ea, iRecorder Option 07 - Disc Integratoif
(installed)
'
$1000 $ 685
AMOUNT
lA.E.C. License No. 24-01.113-14-Amenc|ment 07
EXH BIT WBPM-27.3'.
NOTE:
CONFIRMING ORDER
This order was verbally placed by our Dr, E. Emery to Mr, ]>. Anderson to recede an instrument; however, no Purchase Order was issued.
SAIES TAX
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``PAPUaCMI APPROvl1
' nc. , R. f
UlARGE NUMBER'
Oiv PH. 13 l-l 15 16 "2 02
MAIN sun Cl ASS 17-19 30-31 ??-34 264 :oo
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--
MAfERIAl TO
S. Tucker,
SEANOAROS APPROVAI
Lab
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1
2E -49'/o
2 -4977 29 -4 9f8
213
OEPI.
176001-0000922
iDAIA REQUIRED
VENDOR NO.
1 Cfiromatog rap h
- Recorder - Integrate r
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i. 1
RECEIVING REPORT PURCHASING APPROVAL
JOB NUMBER
. 1-1908-29 "'
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MON-MT-008604
1 1
ClAOOP.. 7/67
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TOWOLDMONOOQ3290