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Toxicological Summary PFOS Dietary Chronic Definitive Reproductive Study: Mallard Test Substance: Perflorooctanesulfonate (PFOS) Structure: 1-Octanesulfonic acid, 1,12.233.44,5.5,6,678-,h7e,pt8a8decafluoro, potassium salt. CASH 2795.39-3. Test Remarks: TKhneowtnestassuFbCs-t95a.nceTihseaswahmiptlee pwoawsdesror(ed3MunLdoetr #a2m1b7i)e,ntancdondiistailosnos and purity was determined to be 869% by LC/MS, 'H-NMR, and elemental analysis techniques. METHODS Method: OECD 206, FIFRA Subdivision E., Section 71-4, and ASTM Standard E106286 "Type: Dietary Reproduction ear: 2001 in-life phase, 2002-2003 analytical phase, inal report in 2003 Species: Mallard (Anasplatyrhynchos) Experimental Design: Adult mallards were exposed to PFOS at nominal concentrations otrfe0a,tm1e0n,t a50n,docron1tr5o0lpgpromupincotnhteaidnieetd o1v6eprairspoefrimoadlloafrdasp,proonxeimpaaitrelpeyr2p1enw.eeIknsa.ddiEtaiocnh, d4urexitnrgtahpeatiesst.ofTmhaellmaarldlsarwderpaeirmsatihnattawineerde upesredtrfeoraubmleonotdacnodlleucsteidonfdorurbilnogotdhecotlelstecwteirone ntorteatumseendt fgoroauspsebssy Wreeperkodu3c,ttihoen.GeDautcmen{t0 olevveelrwsaisgnrsedoufc(eodxtioit2y0 npoptme.d aTthethe1501/5200ppppm.m reatment group was then terminated at Week 5. The 50 ppm treatment was terminated at Wsiegensko7f,taolxsiocidtyueortoabonvoerrmtasligbneshaovifotro.xiciBtoy.dy AwleligahdtusltwemarlelamredassuwreerdeaotbWseerevkesd2d,a4il,y6,fo6r, afnidomattshteudeyxttrearmipnaaitrioonf. aFdeuletd mcaolnlsaurmdpstiaotnfwiavse-mweeaeskuriendterwveaelsk.ly.AlBlthoeodtwiames coofllacdiueltd termination, blood sampks were collected from all surviving mallards for chemical afnoarltyhsoiss,e efxrcolmudtihneg5m0alalnadrd1s50fr2o0mptphem 1t5r0e/a2tm0enptpmgroturpesa,tmweentregreouutphsa.niAzleld maanldasrudbsj,ecetxecdeptto gfroroshsisnteocpraotphoslyogaitcsatluedxyamteirnmaitniatoinona.nd aAntalytshees.time ofhe necropsy, tissues were collcted AOdnuclet cmagllaprrdosduwcetrioenbwroausghitnitiinattoedr,epergogdsucwteirvee pwheaeskelybyplpahcoetdositnitmouleattsionfoatiWnceuebakti1o1n. Eggs were candied and developmental stage and abnormalities were recorded for cach 1 629994 esemt.bryoRevpiraobdiluictty,ivheatechnadbpiolitnyt,sanevdalhuaattcehldindgurheianlgththaendstsuurdvyivailn.clAudfeed:r heatgcghinpgr,odmuacltliaornd, wcheirceksdewteerrmeinfedd.unPtrrieoartetdo deiutthafnoarsi1a4 odfaytsh.e lAast tghreouepndofofoftfhseprsitnugdy(,LocthiJ)c,kbbloodoyd swaemipglhetss wcheermeiccaollleacntaeldysifsr.om I1n0_acdhdiictkosn,frotimssbuoetsh wteherecoanltsool caonldlc1t0edppfmrotmreatthmeesnet groups chicks for for hailstnoepcartohposlioegidcamlalelxaarmdis,natainodn tahned lcihveermiscaamlplaneaslyswiesr,e cLoilvleerctweedigfhortscwheemriecarlecoarnadleydsifso.r Sadaimppolseestwisesruee,aalnsdo tBaukresnaoofftFhaebrliivceiru,sbfaoirn,hisktiodpnaetyh,olgoogniacda,l perxoavmeinntaritciuolnusf,rogamlladbullatddaenrd, offspring mallards. Test Bird Age: Adult mallards were 24 weeksof agea est nation NanudmbfeemraloefpReerplpiecna.tesI:n Tahdedirteiowna,s41p6aiprasirooffamadlullatrdmsalwlaerrdesmpaeirnttraeiantemdenpterwittrheaotnmeenmtalase part ofa blood monitoring study: Fsteueddy taonbdotWhatadeurl:t mFaololdardasndanwdatofefrspwreinrge. prFoeveiddecdonsaudmpltiibiotnumwadsurmienagsulrledphoanscees of the a week ona per pen bass Asenraal,ytaicnadl Meogngitcoormipnogn:enCtonscenwterraetiodnesteorfmiPnFeOdSbiyn freeedv,ersree-dphbalsoeodHcPelLlC, liavnedr timsassuse asnpedctCrooomket(r1y9.60E)gagncdoSmtpfoannenetrsaw.e(r1e99s0p).ared using a method characterized by Bemardt SwtaastipsteircfaolrmMeedthoodesv:alUupatoenscigonmipfliectaintondiofffetrheencsetsudbye,tawneeannatlryesaitsmeonftvgarroiuapnsc.e (DAuNnnOeVttA')s cmounlttriopllse (cDoumnpnaertit,so1n95p5r;oc1e9d6u4r)e. wTahseussaemdplteo ucnoimtpsawreerePFthOeSintdrievaitdmueanltpgernosupwsithwiintheatcheh tbirreda.tmeStnattigsrtoicuapl,aenxacleypstesofofrbaodudlyt bwoeidgyhtwesiwgehrtes cwohnedruecttehed sseapmaprlaeteulnyitfowramsaltheeainnddifveimduaalle bmoebtwhhoidtefoqlulaoiwlisn.g aPrecrscienntsaqgueardeatraoo(tretprraondsfuocrtmiaotniodna.ta)StwateirseticealxaamnianlyesdisuosifntgheDudnatnaetwta'ss Spoefrtfwoarrmeepdacuksaigneg dAevveilaonpeRdebpyroWdiulcdtiifoen InDtaetranatSiyonsatle,mLid(.ARDS) Software, a validated AbavseirsaagnedDdaiidlynoItnttaakkee i(nAtDoIa)ccoofunPtFpOoStenftoiraleadcihffetrreenactemsenbtetgwreoeunp mwaalseeasntdimfaetmeadloesn waitpheinn ethxepopseun.reduFreaetdiocnonosfutmhpetisotnudaynadndadtuhlet AmaDlIlawradsbcoadlyculwaetiegdhtsdfaotlalowwes,re averaged over the ADI(ogthhe bodySowteigihnidh1teddeasy)) =AA1ve2ra8geFAFovooeorddagCCeoonnBmosudumypmiwpeotinighogngeehscdt)bi ddaayy)), pg (oom FRCS) 2 . C9995 wTeasstuDseid fPorrewpaerlat.iopnreTphareattiesotndoifssthwefrienalprietp.areHdobmyogiesnieintgyPoRfOtSheintteot3Spubsrtaincethiat the diet was evaluated throughout the study. RESULTS: MPeFaOsSurceadmCeonn,cenfterdatisaomnpsleosf PwFeOrScoilnletchtedDainetd:aTnoahaveedr.iy tThheecmoenacnecsatainodnssainndtrhae PdeRvOiaStiwoanssosftatbhlee atnesdt ididetnsotardeeggirvaedne r(Tianblge h1)e. uy.Analyses of the diet also confirmed that "Tab 1. Mean and standard devinion concentrations ofPEOS in the mallrd diet.NCo*omncenaFtRiOnS ~~ WCeosnmewnetdtiPoRnO.S oCfovafrisftieon PeNoeminoaTlhe am om) C0 Concenition Contr501o00l (0) 15W00<aL29Oe50Q2l5"05e4 aos1a0ts3 111000282 T 150 A16T 12156 E 266 , 0s *LOQ indicates limitof quantitation (LOQ= 2.00 ppm) Morcltie an Clinical Observations: No tment relted morales were observed Gdwinhilstllrhevtmachatoelnotxlnreseopldwtoeoirfrobe1nt0dheoptfpesnmefmoeittsnreeoldaetustmiogeonnbhtseogarruoneudstptshom.ceecnastNst-oirwoncetalrlidni.nlcoaalmreTmsnhaielegsnssa.pwpHeeorawereaovnbecsree,nrvndeodnbeaethoa1fv0ihoprpsmos,f emWfxiooputrirhraiirnlnegesttsmhmaeelonlctfaci.rrurdsertslecad7tenbdwtemethkosr5o0tvoapefreptsmtshegcoaacsstctmouufleriyne,ctditgnhtrreyoet.hpeirnWic1ioi5td01eh70ni2tnd0aletphha.pnrmdtDrute3tenswfeeotenhrketssateomgferconuathpe-i.rmeselTtanhtutee-.d iWSietgeneksdo5i,f caonitde,tsuyarlvlaitrveihnmegasimenailndlogasremdsasliinincclteuhdeeidn0trhepehpe1me5d0t3rre0essmpecpnotnrwseeirsmeuelcn,tuwswieegreddcoahota,WseIecokds 5os.ft crouolredidnastpipoenr,adnecper,eslsoiwoen,r tlhimn awpepaekanreasnsc,e,ehlaacrrgiym,atiaodn, scponsvsu.lsions, lower limb rigidity, B(CoaNnsOceeAdnEtoCrna)tciwloanns(cdLleOtsAieEgrnCms)innwedastmodoebreetram10iln,pepdthme50wNpioolmOe.bstehervLaoblweesAtdvOenrsseevaEbffleectACdovnecresnetrEatsiotn 3 12996 Adult Body Weight: Compared to controls, there were no apparentucament related emWfaefleclcaktrsd2so, ntinhbrohedeyw5aw0seiamgnhadtrki1en5d0tha2en0d1p0sotpamtpismcticatarlemlaytesmiegngntirfogiurcpao.nutp e(BdTauascbetldieoon2n).inthHbeooewdeyevlewerec,itgsshttoarnatmibnoogndaygt bweei0ghtp,otmh.e LOAEC was determined be 50 ppm whi the NOAEC was determined fo mFaeleldarCdosnsinumtphteio1n0:orTh5e0repwpemretrneoattmreenattsmewnhternelactoempeafrfeecdtstoonthfeecdonctoronlssum(pTtaibolne f2o)r wHaowseovebrs,rsstdariinngmailnlaWredsekfsro1m atnhed 12,502e20amppemn.te.amheind. rBedyucWteioenki3,fseocdmecornescuomveprtyioinn cfoeendsumcpotnisounmbpeionng nwoatse oinbtsheerve1d501w2i0lhpp3m tsraetaitsmteinctalgyrouspig.nifTihciasntrecionveeryswasinlifkelcyd dtdeuetesettr,omitnthheedrteoLdbuOceAti5Eo0nCopfofmPo.rFOfSeedconccoenntsruamtpioinosniwtahse fe15d0(popmm 1w50hpimth0e.2N0OpApEm.C Awsaas wLieveernWoecidghnt:hWeh1e0npcpommptarreeadtmetontcognrtoruolps,fonoeirtheesremnalteraenladtefdemfaelcetasduolnt bliivredrs w(eTiagbhlte 2) Based on thse results, the NOAEC was determined tobe 10 pin, Table 2. Feed consumption, body and liver weight, and average daly ine (ADD) for adult mallards at study Avera termination. * om "Treatment (ngAhDyIitsy) GeCoondsbuimnpttiinony)~~ Sex @ Body weight Liver weight Control 00 <LOQ" B01 2105353 3MMFoON11S1267S44a416D00e50 a211906.6s40s25i+4036s836l Foollasis 42215102 50 150 6361.05 209720 11245 98s MMF91o10s6 6i1780a90 NAP NA Vi Sormetea 10 po vemos samp WeeckrSrEwhse s0e5mn130 pv D2SC0oe10ortrsSeenyde10d7Fa0OWySkkucepo(cnndgiFW5n. kaOrevSpsneod3l0y.o8rwpoSieasndpdec1o38mppo. e(16) bii wo mk 30 fo RAC nde NA= Not applicable; em ne no sample reported. mh conto sme tp <1 GHrroaowisemvseenPrta,tehflooaltogemyda:lcefNsfeccftrsoompnstythhreeesu11l00tsppooprmm atrleasisumrtevnnitvti,nggrtofhuermpealwwehasesni5ncodmmiapcraktreetddati0ntcthreheraecsownteirneoltshn,eo incidence of small este siz (7 of 16 birds) when compared t controls (2 of 16 bird) 4 29997 hatrawamserneaument related. Al other findings were considered incidental and not related bHfuirrsostmaoptohafethF1oa0blropigpcyim:ustNrweoeartmeeefnfcteo.cntssiIidnnermtehadeletlrimveeaarlt,lmaeKnritdd.snreweyli,attbherdasiinln,liprttoeevsertneta,rlioctnuleousrc,oonaftdfrsioplproi(s1negoimfsas2lu)lea,arndodsr tefudobuuurcltetsir.oenatTiendhet(h4eotnohufemrb7)ceorbnoitrodlsabaesnxedhnicboeintoeefdmtardteeauctrreidenagsbiemrdadtsueprxeehrimbsaiptteoergdmeandteeosgizesonaeacithnearltaahcetteesorepimhziyendioffberytohuaes sisinezmehi,enisfpneeurrmomubasetortgueonfleecseiltslhwlaaaywsearsnsocorhfmaarglaecrtamesirnicazolemdpebpaiyrtehadenloiaubmsc.eonncItenooloftbhmiearrdtsub.rierdTsshewpsieehrareneaddluascedsdeucgriegsaetssse phraotcesPsR.OSBasmeadyonhatvheesaceceelcetra,tetdhepoLsOtrAcEpCrodwuacstidveevreeignreesdsiton,ba 1n0orpmpaml. physiologieal rsRieegapntrimofeidncuta.cnttiBdoianfs:feedrWeonhnceetsnheisnceaoenmeypocatfrset,dhtehteoreNptOrhoeAduEccCtoinvwteoslpadrgeartmoeeurtpme,irnsetdhfoetrroebmaewlel1ra0redpsmn.ion hseiti1s0icpalply 1oO0fffhhseapcrchiolnnitgnrgoGslrso.owrtT1hh4e:-rdeTahyweerlredewaoesfrfoespnnrooinsgeatasiumrsevinicvtaolrryselsiaintgetrdhieeffc1fa0encptispfomeneetnahectemmseenaitn whvheeerbnowcdeyoimgwphetaisrgehodtf uoflf,sprwienagkefnroemd ctohnedi1t0iopn,pmfotoruelaetmleenstiognrso,unp.d sWuhgiglieshcnliensiscawleorbesesrevratvieondsisnutchhe a1s0npeocmk rirsealsisumtsee,dntthneagtNruorOuepA,oEfCthtehiseneoefoffbfsespcertrisvnagitniwoabnsostdhweetcreoenmtirnnooeltdactnoodnbseitdr1es0riempdepnr.tegarmoeupnst,relBiaesdedduoen 1thehsee cChoenmciecnatlraatniaolynssisooffPbFloOoSd ainnd BllivoeordsaamnpdlesLisvheorweodf tAhdautlatdulMtalmlaalrldasrd:sRienshuels1o0fptohme es{treatemmaeietnmaatepirnpoetranot,xgmirelmoniautvteperglraayocnuScdpu-met(uinTlmauasbmtlegedPrF3)eP.OeFSOtWcShhoainncldeutenrhteitrnhmageteriaetoshnwuesraiessndtuamcdyaos.lnxec-sesnptfFeauocrtmitihfoenctrshemdofinr1fe0ff,erpmeapnaltcmeestrhioeenamtmsitesusntudhteye mw`ceaoasnsceusnritmeridaltairoo,nnlsa,yptphirenoxrmiaatmilaoltoaefrldyPsF1rO.5oSmfionrtbhlbeootochdonssteerxroeulsm.atnodStihna1tc0einpclopinmvceernt(trSre:aaLtmieroannttsi,o)ofafoPrqEbuGotSahnwseetxreies dreevlaetlioopnesdh.ip between PFOS exposure and liver or serum concentrations was not s : cna998 s`Ttaubdlyet3e.rLmiivnaetriaonndA serum PFOS concentrations in adult mallards at TTreament (pom) _ LiverCone Sex ge) Serum Conc. (ig/ml) Control TMF <<LLO0QQ 0001692003094 10 MF 610098184955 817636+112230 rGelpoyrtceodrroanlanwedt 0wepipgmhsbaamspsl.esweeanalyzed om ey Allvas ae t#wLa0sQ0=0~4L-im0it1o0f4qu.atiaron: or live it wes 0.02.- 0.0502 gig whiteforserum sMteuadsyuriendmiecnattedofthPatFOPSFOcSoncaecncturmautliaontsedininblmoaoldlacrodlsleicntebdotthhraoutgihmoeutantdheserxedpreopdeuncdteionnt manner (Table 4). d`Tuarbilneg4t.heSestruudym. P*FOS concentrations (g/mL) in adult mallards at various time points T Teme (ppm) Sex 5 Wek 10 1s Control MFM <<0L0QQ <T0Q <L0Q <L0Q <L0Q 10 M Fo 9355265 7695155 125+206 8512392 138180 9303.10 TT 50 W M e 388 s We6k43? TTConcentations are eporeFd ss meas a3nd0s5andr evitons. 633 *L=0LimQitofquantiation:LOQ was 0.01 gi. `BcyonWceenetrkati1o0n,sseixn-spmeaclifeicmdailflfaerrdesnceweirnesesriugmniPfiFcaOnStlycongcreenattreartitohnanbecthaomsee nootbasbelrev.ed.Thien ffermoamlesW.eekPFO10S ccoonncceennttrraattiioonnss itno sweereukm o15f. femTahleesddeeccrreeaasseedinbysearpupmrocxoinmcaetnetlryat8i5on%s `cmoailnlcairddsedwewirtehpatrhteitoinosneitngofPFthOeSegignt-olaeygignsgdpuhraisneg itnhethreepsrtoudduyctainvedlyinadcitciavteesphthaastefoefmatlhee cstoundcye.ntraItnioncobntyraWset,ekm1a0l.eandsdeirdunmotcsotnatciesnttircaaltliyodnisfferrefaocrhtehde raenmaianpdpearorefntthesasttuurdayt.ion CcoolnlceecntterdaattioenaschosfamPpFliOnSg twiemree(Taalbsloe m5)e.asured in red blood cells of blood samples 6 n0399 `Table 5. Red blood cell PFOS time points during the study. * concentrations (g/mL) in adult mallards at various Treatment Week (ppm) Sex. H 10 15 Control M <L0Q <10Q <10Q 10 MFo 21<5L207Q38 21<0L208Q85 <LOQ 58.6443 F 1412490 39.6225.1 3803.94 Week Week 7 50 M 60.6 274 POS concentrationsasr F rteporated 5nm1e1da8nsaandrd devi4a1ti2ons "LO=Q Limit ofquantitation; LOQ was0.01 mg/L. Overall, the `measured iin creodncbelnotroadticeolnls.ofHPowFeOvSeri,n serum was the relative greater than concentrations of PFOS volumes of serum and red blood cells. in whole PFOS in blood blood were could not not given in the analytical be conducted and the report. As partitioning aofrePsuFlOt,Sabemtaswseebnalsearnaceanodf RBC was not between serum evaluated. Furthermore, and red blood cell PFOS there were sex-specific concentrations. At Week differences observed 5, male serum PFOS concentrations were approximately fold greater `while for females this difference was approximately than red 1.9-fold. blood cell concentrations `The trend observed in for PFOS concentration red serum concentrations. blood cells throughout the Sex-specific differences study in red was similar blood cell to that PFOS tchoanncetnhtorasteiomnesaswuerreedaipnpafreemnatlebyfrWoemekthe15sawmitehttrheeatcmoennctengtrroautpi.onsBiyn males Week being greater 15, male red blood cell in females. PFOS concentrations were approximately This trend agreed with serum PFOS 15-fold greater concentrations than those measured measured in these `mallards, aCnodncleinvterrastaimopnlsesoffrPoFmOjSuveinnilBelomoaldlaarndds LiinvdiecratoefdJtuhvaetnPilFeOSMawllaasrdpsre:seAnntaliynsitsheobfirsdesru1m2 pwepemkstrpeoasttm-ehnattcgh.roTuhpeoPveFrOSthactonmceeanstruarteidonisn in both liver the control and serum group, but increased were less in the 10 than the `concentrations adult mallards, measured in adult mallards no sex specific differences from were the same observed treatments (Table 6). in either liver or serum Unlike PFOS concentrations. 7 : 61000 Table 6. Liver mallards * and serum PFOS concentration in 2 week old juvenile Treatment Tiver Cone. Serum Cone. (ppm) Sex (ge) Conwol M__ <LOQ" (g/m) 0.068" 0.037 10 F <L0Q M 307130 <L0Q 44120931 TFConcenmrations 3smean F and standard 3.61126 deviations.Dats gven sswet 4971.12 weight 2 T<hLe.0mQal=eessesruthmanavleirmaigteof(qnu=a3n)tiwtaasticoanlcfuolaitvederus(i5n0gn%g/gt)heaLndOsQerwuhmer(e10s0amnpgl/emsl)were below the LOQ (1-2). `The ratio of PFOS concentrations juvenile mallards averaged 140. in serum to that This value was in liver in similar to both male and female that observed in adult `mallards, Concentrations were measured inofegPgFsOcSollinectEegdgfrCoommptohneencotnst:rolCoanncdent1r0atpipomns of PFOS treatments. in egg Eggs yolk were tsreeleacttmeedntfgrroomup.WeeYoklsk 1(9w,ho2l0e,) acnodmpo2s1itaensdweyorleksthewneraenalsyezpeadraftoerd PaFnOdSc(oTmapbolseit7)e. d by In addition, from the to 10 better understand the distribution of PFOS ppm treatment were also fractionated into in the egg yolk, yolk composites 3 components, Very Low Density Lipoprotein (VLDL), phosvitin, and lipovitellin. determined in each yolk faction (Table 7). ~ PFOS concentrations were then `Table 7. collected Egg yolk and yolk component PFOS during Weeks 19-21ofthe study. * concentrations (g/g) in mallard eggs Treatment 'PFOS Concentration (ppm) Control Yolk Fraction Yolk-Whole. (ug/mD) <L0Q' 10 Yolk-Whole 528+0.58 Yolk- VLDL Yolk-Lipoprotein 422050 8.870057 Results given 35 mans snd standard `Yolk-Phosvitin deviations ona wet weight bass The 3.590014 samdard deviation caprsses p "PTrheecliismiiotnooffqthueparneptairtatai(toLniOoaQn)ndwaasn1a0 polgf/mdyulpsliciatess for the same unique sample, an ggcomposite. yReosluklstsfrionmditchaeteaddutlhtathaetns10asppcmo,mptahrereed wtaoscoantsrioglns.ificNanot PacFcOuSmuwlaatsioqunanotfifPiFeOdSininctoontergolg einggadyuolltks.femTahleesraattiowoefetkhe21cowncaesnt3r.1a,tionThoef PraFtOioSeigngthyeolekggtoyoaldkultto ftehamtaline blliovoerd PseFrOuSm `concentrations at week 21 was approximately 4.8. The greatest concentration of PFOS in 8 7100% ltihpeovyiotlekllnwaansdapshsooscvitatiend with the VLDL fraction (approximately 77%) followed by CONCLUSIONS: tM1r0ael2al1tamrewdnesteskwsew.reereeDxutpeeorsm(ie0ndasttioegdnPasFoOftShoeavetendrdieottaif7rcyiatcyno,dnc5eandwutelrteaktmisao,lnlsreaosrpdfesc,tiinv10e,tlhy5e.05a0Wnhdane1dn501co3pm0pp2ma0rfeoprdpustpo catohbnestrererovwlsea,ds 1wa0nheinPnFcraOdeSua-lsrteemilnatltelhdaerdiefsnfceiwcdetersnecoefneodfasd1mu0alltplpbtmoedstiyns twsheieziegfhaetneddodr(eTcafrbeeleaedse8cd,osnTpsneurmampauttiloognemanwlceeisri,es apthys1i0olpoogmica(lTabplheen8)o.meTnhouns,iwnhibliredse,adlPypFOo.stmreapyrodhuacvteiveaccpehlaersaetesde.prhcsssiopnroscaesspowhme!n cfeormtipliatry,edhattochaunbtirletayteodr obfirfdssp.ringFihneaallltyh, otrhesruervwievarle innotthree1a0tmpepntmreelaaitmeedntr.eduBctaisoends o1nm tmAhadelvsleearrsedefsfeEacftfnsed,cttohfCefosnpNcreoinntgOrbawsteaiorsnvad(beLlteOeArAmEdiCvn)eerdfsoetro mEfbafeleec1tm0aClpolnpacrmednstwwrhaiatlseiodnethte(erNLmOioAnweEedsCt)0Ofbboesre1rf0veampbapllmee j((uTNvaeObnlAieEleL8).)tisaPsunRedsOSaLrocewosenucsemtnmtaOrrbaistezireovndasibanlseTsaoAbcildaevtee9rdsweitEhfftehcetNLoevOeblse(rLvaObAlEeLA)dvienrbsoetEhffaedcutltLeavnedl Table 8. Measurement endpoints and associated dietary NOAEC and LOAEC values for PFOS in a chronic study with mallards and their offspring. * ADULT Endpoint Dictary NOAEC Diary LOAEC BMoordtaylwietiyght Feed consumption 110 5500 50 150 GLirvoesrswpeaitghhotlogy Male10<s 10 Males = 10 HiRsetporpoadtuhcotliovegy. Femal11e00s = 10 Females = 50 OFFdSaPyRsIuNrvGivability 10 HaJtucvhenliilneglijvuevrewneiilgehbtodyweight TOAECwas based ov cress dens afsl ee 1100 decreed em TeFeo Fo rIOpoiner lia ty estrone pe en Ae ford rs _ } . 9 611.002 c`Tharbolneic9.diNeOtaAryEsLtuadnydwLitOhAPEFLOSv.alues in various matices in adult and offspring mallards in a "MeAaDsUuLrTesMoAfLPFEOSS Exposure * NOAEL LOAFL" ADoDsIe((mpgpmP)FOSkg body weighteday) over 21-week period 11.409 LSievreurm((uuggPPFFOOSS//gm)La)t sattusdtyudtyertmeirnmaitniaotnio(n21(-2w1e-ewkese)ks) 873 609 ADDoUsLeT(pFomE)MALES 0 SAeDrIum(m(g1gPPRFOOSkS/gmLb)odayt pwreei-gthetpordoadyu)ctoivveerp2h1a-swee(e5k-wpeeerkiso)d 149 769 LSievreurm((uuggPPFFOSO/Sg/)mLat)sattudsytutdeyrmtienramtiinoanti(o2n1(-2w1e-ewkese)ks) 166 108 OFYoFlSkP(RuIgNPGFOS/mL) 27 SLievreurm((uuggPPFOFSO/Sg/)mL' 436399 TOCoRncEenLtrawtaisonas esonpcdaornloy pwocestewpedriogfhucaisv.e phase regression Sa mle om Top even AT NmoeasnudrLeoewstcfcvavacl.uesfor die and ADI rebasedon dictayconcnaion. Serumandfiver ff valuesar. Offpin vrand serum LOAEL ales are averagesofeal nd mleconcnttions. DATA QUALITY: Reliability: Klimish ranki=n1g REFERNCES: `Bemardt and Cook. 1960. BBA 44: 86.96. `Dqeucakleer,ggEy.oRl,k.FlEaxhyergteyn, RJeMp.ort2N0o0.3.0A2n3a-l0y7s0i.s of perluorooctane sulfonate in mallard and wDuintanhec,ontCr.oWl.. J19A5m5.er:ASmautlst.iplAesscooc.mp$a0r:is1o0n96p-r1o1c2e1d.ure for comparing several treatments 4D5u2n.n4e9t1, C.W. 1964, New tables for multiple comparisons witha control. Biometrics 20: sGatluldaygwhietrh, Sma.lPl,arVdsa.n HFionvaelnr,epRorLt., WBiealvdeirfse,I1nBt.emaJtaiboenra,l,M.Li2d0,03P.rojPecFtOSN:o.A45r4e-p1r0o9d.uction 10 . ---__ g"003 GCeallllsagahenrd, SS.er2u0m03.forEAxntarlacytsiiosnuosfinPgotHaPsLsCi-uEmlePecrtfrlousoprroaocya/tMnaesssulSfpoencattreomfertormy.RedExBylgoeond Research, Exygen Study Number 023-066. RYoelakg.en,ExWygKe.n R2e0s0e2a.rch.AnaElxyysgiesnoRfepPoerrtflNuoo.ro0o2c3i-a0n7c0s.ulfonate in Mallard and Quail Egg `Smtaelvlearnds.on3,ML.EAn.vi20r0o3n.menAtnaallyLtaibcaolrapthoarsyeSrteupdoyrtNof.orEPOFIO-1S2:56A. reproduction study with the St~ifcaongin,aSt.e, Nliigmapnfd,s Ja.,nSdchonoeciydteer,reWcJe.pto1r9s9-0t.heVibtienldliongegnessitiesifnoXrevnioteplulsogelninaiasenldovccahtiiecdksoenn ipovitelin-L.. Biol. Chem. 265: 882-888. `Wildlife Intemational, Ltd. 1994. Avian Reproductive Data System (ARDS), Version 2. OTHER Last changed: 5/05/04 - -- n pram