Document 7MXw6Gj9wdXm62vYmV3zqY73g
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Sth.Panul.MN 5144-1000 ARL26_ 1039
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MR 5 (0,
3M
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PS -- US Emir Praesion Office of Toxic Substances Agency
401 MStreet, SW
Washington, DC 20460
Attn: TSCA Section 8(e) Coordinator
gen. September 5, 2001 0901-0373
DREO-2O0-373
00041932
Dear Section 8(e) Docket Coordinator:
Re: TSCA 8(e) Supplemental Notice on Sulfonate-basedFluorochemicals
`With this letter, 3M is providing final reports and other supplemental information
related to previous TSCA Section 8(e) notifications. Many of the encloseditems areanalytical reports providing blood serum and liver levelsoftest materials for which the in-lifereport referring to administered doses has already been submitted to the 8(e) docket. In other cases `where the 8(e) notification consisted ofpreliminary data, we are submitting a final study report.
Allofthe enclosed itemsare already in EPA'spossessionand available in TSCA Docket AR-226. We believe, however,that placing these items in the 8(e) docket may allow for more convenient access to information directly related to previous 8(e) notifications by 3M.
The table below lists the enclosed items and references the study or data whichalready has been the subject ofan 8(e) notification by 3M:
Attached Submission
RteSeu Dae Aled
Filed Under 8(e)
|
1. Amended Analytical Study, 2(N-Ethylperfluorooctane
Combined Oral (Gavage) Fertility, |
'
mami inl Po Gein Ro Repco.| Do oc Si Fase Determinationofthe Presence and Concentrationof PFOS, | Reproduction Toxicity Study of Ne
RCeSRrf5LeoCr6DBsFREsNVOoSAnARAeP63us1n1s6dR33P,a0EsAO0REmxApioiestelsaSLpiBovEnOnSTdOEFNOORS5,, ||| IpmPDipScmnacoonnyeSHi4R00es. M556, PFOSAA, PFOSA and EtFOSE-OH in theSeraof | 6316.5, June 30, 1999, full report
. Coma. nnocg -- 5%8 Z5o5HBn
2= g35 8
.
]
TSCA Section 8() Docket Coordinator `Page 2
|
Attached Suubbmmiissssiioon
| ReRellataedter d SSyta udy/ata Already
2. APnraelsyetniccealanLdabCoornacteonrtyraRteipoonrto,fDPeottearsmsiinuamtionof the | CDoevmeblionpemdenOtraall a(nGdavPaegrein)atFaelr/tPlotsyt,natal
|
SPeerrfulmuoarnoodctLainveesroulffoSnpartaeg(uCeA-SDaNwulmebyerR:a2ts75E9x-p3o9-s3e)d
in to
the
| |
iRnepRratosd,ucAtrigounsTRoexisceiatrychStLuadbyoroaftoPriFeOsS,
|| RPeFqOuSevsitoarGParvoajegcet,NLoa.bo3rMatTorOyXRe6p2o9r5t.9N,o.OcUt2o0b0e6r,27, 1999. | I1n0c,. 1S99p9o,nsfourll'sreSptourtdysuNbom.it6t2e9d5.9, June: |
|
February 15, 2000 supplementing |
| 3. RDeepvoerltopAmmeenntadlmeanntd P1e,rCinoamtbali/nPeosdtnOartaall(RGeapvraogdeu)ctFierotnility, | earlier filing
TLoaxbiocraittoyrSietsu,dyInco.,f PPFroOtSocionlR4a1t8s.,0A0r8g,uSspoRnessoera'rschStudy No.
6295.9, April 13, 2000.
4. CAnoanlcyetnitcraaltiRoenpoorftP,eDrefltueorrmoioncattainoensuolftfohneaPtree,senceand P1e3r-fWleueorkoDoicettaanreysuSltfuodnyaomifdNo-EMtehtahnyoll
LPeirvfelruaonrdooScetraaneSsaumlpfloensy,la3miMdeE,nvMiSrSo6n,meanntdalMSLa7b0orianttohrey || (63N1-4M.1e,FCOoSvEa)ncineRSattus,dy3NMo.Re6f3.29N-o2.2T5-,
Ref. No. U2636, TOX-028, February 23, 2001
Jdualtyed2J4u,n2e00300, 2000, Section 8(e) filing
5. A`CnoanlcyetnitcraaltiLoanboorfaPtoFrOyS,RePpoFrOtS,AD,etPeFrmOiSnAatAi,onaonfdthEeFOSE- | FDienvaellRoeppmoerntt,aOlrTaolx(iGciatvyagSet)udyof 2(N-
EOHxipionsetdhetoSeNr-aEaGnFdOSLEi,ver3oMfECnrvli:roCnDmBeRntVaAlF/LaPbloursatRoartys || eEtthhaynloplerifnlRuaotrso,oc3tManReseuflefroennacmeiNdoo.)-T-
RReefp.orNto.NoT.-6T3O1X6-.07,98F,ebLraubaorryat6,or2y00R1equest
No.
U2402,
3M
|
6to31S6e.c7t,ioDnec8(em)bdeorck1e7t,
1998, submitted per etter of
August 21, 2000
6. PAnraelsyetniccealanLdabCoornacteonrtyrRaetpioornotfoPnottahsesDieutmerminationofthe | FDienvaelloReppmoerntt,aOlrTaolx(iScittoymaScthudTyuobef)N-
2Pe(rNf-leutohryolopcetrafnleusourlofoocntaatnees(uPlFfOoSna)moirdoayn-oetthhearnomlet(aNb-olite of |TE-t6F3O16S.E8,inJRaanbubairtys,113,M19R9e9f,esruebnmcietNteod-
EEntvFiOrSoEn)meinntLailveLrabaonrdatSoerryuRmepSopretciNmoe.nsT,O3XM-.097,
AtougSuecsttio2n1,82(e0)0d0ocket per etter of
Laboratory Request No. U2452, 3M Ref. No. T-6316.3,
February 8, 2001
7. FEimnpalloRyeepodratt,tAhlee3xaMndDeerc,aBt.u,rMFoarctiallitiyt,yUSntiuvdeiressiotfy oWforkers | 8P(rce)lidmoicnkaertydiantaletstuerbomfiDtetcteeodmbSeecrti1o5n,
Minnesota, April 26, 2001.
2000
>
2
TSCA Section 8() Docket Coordinator Page 3
[
red Sebi
|
i
Related StdyData Already
Filed Under 8()
|
Fil Repo, Atte Or Toxic See with T3290C0C | Acute Om Toy Sern win T- |
ian Aalbrinoo Rnatso, SeafertyeEcvalNuoa.tiRonALZaAbRorDaSt6o8r,y,SRMikReerference | 3va2l9u0atCiConinLAalbboinroorRaytsR,ikSeafrety |
|
Nvoi. T4-0329900(040L%17K8',PF-OGSRATA3iLno3t%S01E)tONHo,ve1m7%berIP5.A w19s8214{BbieblmiosgratphyTeSntCrAy i8n0DodckoectkA]R-326, final report
|LOaRbEoZraAtRoOrBieGs3,,I3nc., RPerofjeercetnNcoe.No. T= |[13772%90 (h40a%ndK'4P0F5OSHAiA,iLn737%8.EOH,
6mA57i5s.eLtod1t,o5200S10i0Nosonvleeambyderdo5ec,kte1t9t82,
wiih emsneousty efrs 1 avis
rather than rats)
5 Gtiesy,oLP. amnd K.e Kann, AcRcaummualtatFioornaocfhenicls in | r36e)imdiocnkrsyMdaaya 3su6b1m9i9t9ed to Section
Fish Tissue, Michigan State University, June 20,2001. |
10. Giesy, J.P., and K. Kannan, Accumulation of Perfluorooctanesulfonate and Related Fluorochemicals in Mink and River Otters, Michigan State University, June 20, 2001.
11. Giesy, .P.,and K. Kannan, Perfluorooctanesulfonaanted
RFerloamtetdheFlGuoruoocfhMelmeixcifaclos iannOdysCtheers,aCpreaaskseosBtarye,a MViircghiingicaan,
`State University, June 20, 2001.
12. GRNieeisihy,doInPF.aSaoonnrdeoKcU.nhKmeaemnrensalyn,,hnPJFeurnffelu2oi0r,no2og0c0ta1WnaetseulrfBoinadtse,and 13. GPNiaiersnym,eorJ.NpP.oeaaanadnmcKti.tKMoainnctnhaeing,sannAdcScRutemeuelUdantiiFovonoeoorfssheumnic2l0s in
Soon
If you have any questions about this submission, please contact me at (615)737-4795. Sincerely,
Le Milfs
GMeaonrager, `3AMdaCmosrporate Product Responsibility
Enclosures
.
2
`
MR 5167 BEHQ-W 373
ACCUMULATION OF PERFLUOROOCTANESULFONATE AND RELATED FLUOROCHEMICALS IN FISH TISSUES
KuruJnoaochalGaimeeKye*nnan 0 Deparmentof Zoology NationalFoodSaferandTeriatogs Comer rn STTR Environmental Toxicology. a Michigan et Crier.BnLansingM1883 State University, East. Lansing, MI 48824, U4USA
Te 517) 353.200F0a:: 517-U43s2-2310 E-mail: sus com *To whom correspondence should beaddressed:
218C
National
Prof. J.P.
Food Safety
Giesy
and Toxicology
Center
Michigan State University
East Lansing, MI 48824.
Prepared or:
St. Paul, MN
June 20, 2001
D
=
iy
iii
0008118330
LCiLiing No CBE
J.
,
4
SUMMARY
pT(ehFriOfslSir)oe,proorhpteexirasfnaleuscouolrmfopooinclatatatenieos(nuPolFffHroSens)aumliitdnse ofi(fsaFhOmStoiAns)is.uteosrpiefnrrgfolsmuuorrtvoheoeycotUfanSpoeiracfnlduaocrcioedortcat(ianPnFeOsEuAulr)foopneaaantnde
mPcouRusnOctSlrieeisno.GfrfTeiahsthe LfgarrekoaemtseSsftcihsceholwndcatezsnt2Rri9av7teinrogn/Eogsf,tuwPaerFtyOwSiin,foBinuenltdghieiunmmu.fsischlTehweaosfchi9ag2hp3esntfgr/cogom,ncwSeeantgtirwnatat.iwoinn tohfe
dMeitcehcitgaabnl.e Antarctic
cMonucsecnlterattiisounses ooffPfFiOshS.fromSimsielvaerrlayl, ifnilsahndflraokmesthoef fish did not contain any of the fluorochemicals
NMoircthhigPaancidfiidc
bay. nOocteaconntaangdy
PFHS were rarely found in fish,
analyzed. FOSA, PFOA and
INTRODUCTION
(pTePhriFfsOuSro)er,pcohreptxiearnfealsucuoolrmfopooinclatatatenieo(snuFloHffroSens)aumliitdnseofi(fasFhOmStoiAns)is,tueosrpienfrgrfoslmuuorrvtoheoeyoctUfaSnpoeiracfnlduaocrciodeorcat(ianPnFesOuAl)fonaantde
countries.
European
MATERIALS AND METHOD: ~F2is0hCtiusnstuielsawnearlyesicsollected from various locations (Table 1 for details) and stored at
Analysis
fDoertatihlesaonfaltyhseisaonaflyftliucoarlopcrhoecmeidcuarlessihnatviessbueesenwhoiuctlhinaerde sitnastteadnbdealrodw,operating procedures
pPtrheepraratoFrlyuoMreotchhoedmsi.cal
ETSC.o-8m-p6o.0u,nd"Esxtrafcrtoimon
of Potassium Liver for
Electrospray/Mass Spectrometry". 3M Environmental
PAenrafllyusoirsooctuasniensgulfoHnaPtLeCo.r
a(1n)alfyotrictahleswpeockifwiacsrepgoerntesr.a)ted by the 3M Environmental LLaabboorraattoorryy., (RSte.fePrau(l,ReMfNereTehse
fn uo put
lmoentphayirkienrgt-rbeuatgyelntetwhaesr (aMddBeEd).to onto a nitrogen evaporator until
the The dry.
seaxmtpralcetawnadstthreanasnfaelryrteed itoonapcaeinrtrwiafsugpearttuibteioannedd Each extract was reconstituted
imnettohagnlaosls, aauntodvitahlesn.
filtered
through
a3
cc
plasic
syringe
attached
toa
0.2
in um
n1.y0lomnL.ieorf
S3AnhMaeleyEtnPivcuiaorlroonMcmehetenhmtoiadlcsa.Llasboi~rnEaTtLSoi-rv8ye.,r7.SE0tx,.tPr"aaAucnlta,slMyUNssi.isngofHPPoLtCa-ssEilumecPetroflsupoMrraoaoscystaSnpeseucltfroonmaeterpoyr The analyses were performed using HPLC-ES/MSIMS by monitoring a single product
2
ion selected from a primary on characteristic of a particular fluorochemical, For
monitored for quantitative amass `example, molecular
was fragmented furt
ion
her
49
to
9p,rosdeulceecteidonas99th(eFSpOrsi-m)a.ryThieonc
hfaorracPtFerOiSsti(cCp4rFo)d;uScOty-i)onan9a9lywsiass,
Analvtial Equipment
tThhisesftouldyl.owing are representativeof the actual setings used during the analytical phase of
Liquid Chromatograph: Hewlet-Packard Series 1100 Liquid Chromatograph system
Nile phase compensa Analytical column: Keystone
Ambient;
BetasilTM
Cu
2x50
mm
(S
um)
Column
temperature:
FloCCwooTmmaptpeo:on3en0ne0tnAuBtL::iSmmeimtnhManaamlmonium sceate
Injection volume: 10 4L
Solvent Gradient: 16.0 minutes
Tow Time (minutes) %B_
611.000
s1100o0%%
13.0
10%
QMasus aSpecitrolmeter: Micromass APIMass Spectrometer Quattro IITM Triple CCSooolfnlteiwsaiVroaen:lGaMagasesEs3ne0Lr.yg6ny0:xTMV253.-445 ev ESMlooeudcrtecr:eodEeBl.leocZctksropTsrepamrypayerNaetguartei.ve150C 10C Analysis Type! Mulipl Reaction Monitoring (MRM)
[FastATmarlgyetteonsJMPorniimtaorryeTdoinn3(ManLa)bo|raPtorroyducAtnailoyns(exs 07 [[PPcoEzsOeA ----ITTa-- ang--TIiTgYi---- | mo"nTiHtPoOrSf,o gross etment ne Tetra-hydro perfluorooctanesulfonate, is used as a surrogate to
5 6
DO atab Qualj ityectani dDav ta Ie ntegrs ity
The following data quality objectives were indicated in the method performance section of ETS-8-7.0, Analysis of Potassium Perfluorooctanesulfonate or OtherFluorochemicals in Liver Extracts Using HPLC-Electrospray/Mass Spectrometry:
LtLhiienmeicatarlsiibtoryfa:tQiTuohanenctucirotveeaf.tfiicoinen(toLfOdQe)t:erTmhineaLtiOoQn (irs*)eeqquualaltototohre glroewaetsetr tahcacnep0t.a9b8l0e. standard in Aatcc7e0p-t1a3b0l%e fSopritkhee Raenacloyvteircailesu:nMattorbiexvsapliidk.es prepared in rabbit liver must be recovered Blanks: Matrix or surrogate matrix blanks must have a peak area < % the peak areaof the
lowest acceptable standard (LOQ).
Summary ofQuality Control Analyses Results
cLCuiarnlveiaebrriwatetyii:gohnTtheSedtca1on/edxfafriocdfisea:ntsQoiunfgadlneei,tteaortpmieionnniantogifoontrh(etrw)tooafrtbgrehtaecaksnetatlaiynntdgeasrudnwecxautsrrvabecatwseaeddsc>ou0nr.v9ea8s0q,fuoardreaatcihc
group of samples. High or low points on the curve may have been deactivated to provide
a better
areas le
fit
ss
over
than
the
two
curve
times
range most
that of the
appropriate
extraction
to the
blanks
data,
were
Low curve p
deactivated
oin
to
ts with peak
disqualify a
Oddecaactcaatsirivaoanntagelde.ltyh,aQtuaamnsatiniygtlahetaivmoeindb-oerfeannegasecihgcnuiarfnviacelaynpttoeliynwtaaftsfheacbttaewsdaedsbyaonbnaoctbkhvegiroroueussnpdoountlsleieveerlsmoafythheaavnealbyeteen..
rCsaaplencigibefriaoctfiptorhneodsiutncastntdraiuromnde(snst)w(euarspeipnrpgorxetiphmaeartemeudllyttio0p.lr5eu-nr.1e0au0cn0tdiinolgnu/tgm)e.do,niatpoprrionxgimmaotdeelyowfoitfthheoinnmesthtoerralmmieoenrntes
atLthiemleicatassltibtorwfaotQiutoainnmtceuisrttvahetei(aodnneafl(iyLnteOedQp)aes:akaTahsrteeaanLddOaerQtdeciwtsietdehqiiunnalt=h3teo0st%uhomeofglatohtweeestmthaetaorcricetexipcbtalalabnlkvesa.lsutea)nB,deaacrandudsiein.s
low levels of the target
atnhaelsyetecriinteeraiachfomratrLiOx Qis
analytes are ubiquitous in the laboratory. it is
ldiestteerdmoinnatthieonresbueltsobssuemrvmeadr.y taTbhlee. approximate
imperative. LOQ for
that each
eoBuxltcalenipektrss:fwoAirllllonbneloatwnakatsdevrewresbrelelaynbkealffofoewrcttPhFtehHelSiomiuattncdoofmaqleluaocnaftvitithaaitrsiobsnltaufndoykr.sthfeoGricvaoelmlnpwotmuhpenodnusantdoursfe.inotTfehreetsshtee,
samples used as
encompassed by this study, the surrogate tissue for matrix blanks.
well-characterized These surrogate
matrix of rabbit liver matrix blanks were < Y%
was the
level of the LOQ.
tPhreecciosuirosne, oIfnstthirsumsetundtya.l:IInnostthreurm,enstiamlilparrelciivseirofntiwssause nstoutdisepse,ciifnisctarlluymednettalerpmrienceidsiwointhhians
been determined to be better than 7% for all target analytes.
s
7
fMraotmriexacShptiykpeeso:fAatnilmeaalst;
osnpiekessetweorfemaptrreipxarsepdikatesapwparsoxpirmeaptaerleyd6f0o0r
each ng/g.
type
of
tissue
aaRrdeeecqosuvuaemtrmeiaercsaiuzotefidoPniFnsOhASopuplvedanrdbiieexdexwVeiIrdIceilsyeddeinpeinndteirnpgreotinngthtehesrpeescuiletss.aMnadtrmiaxtrsipx.ike Trheecroevfeorriee,s
cpToronepdvauercretidefydintihn2e rwsaetblablti-utcshwaorefarcettheearlilezxeatdcrcasecuptritroaonbglaeatned(m~aa-tn3ra0ilyx%t,)icraaflbobristtyhslotisveeemrs.a,naTmlahytteircimaxaltsrrpiuixnksesspuiswkeeedrsetwuhadelinse,os reporting data for samples and matrix spikes.
Ac`dhDdreiomtmoianotsnotagrlraatcpiohoninfciorfmraSetpteoecrnityfiiotcneisttyst:iwmSeepreecaifnpidecriftmyoarfsmoserdansfapolercyttPreaFliOdSe.ndtaiufgiIhcntaettirhoen iewolanesctdcrehoamsrpoarncastyierrtiaazneaddneombn.y tsmhtaersosanngaeslrpyessciitsgronoafmlteittsrhysanu(etEhsSeaMm4Sp9lM9eSsD)acos>lylset9cet9me.dDtafhretor4ma9nss9iotDmioeanosf>petchi8ee0sPDoFafOaStnriaamnnasaliltsyi,soinsa,ncaHunonwipderevonevtriid.feieidan 9rian9rteeDlrayferotrebansntesriwtviaeosdn,,ptroeseennsturien ctohemp4l9e9teDsaelectiv8i0ty,Daquatnrtaintsaittiioonn.wAalstbhaosuegdh otnhisthient4e9r9ferDeant>js
q7Tu0oanvtneigrt/iagftyiv(telhieavegirrdeeonertmietonytthoetfrotwhteiitsdhseiutene),c~t/e-adt30a%ln.eaalsyttTey,p2iicntarlsalanyms,iptl4ieo9sn9sd9ew9teerarenmdinm4eo9dn9it>to8oc0roentdtraainansnidtPiFosnOshSowwaeterde>
qsmuoaanmnipttlioetraetwdia.vse arOegn-raenteahmleeynoztcecdwaimstoihnointtshoerthriaentpgotrththeeesde4d9tawt9ao1f3trr0oanmtsritathniesoin4tsi9od9ni.9ff9eTrhdeiedstebtryhmiirmndoatrtireoannt,shiatinon30s5h%.owtehed.
ISttaistenmoetntpoosfsiDbalteatQouvaelriitfyy true radiolabelled reference material.
rTehceovoenrylyomfeeansduorgeemneonuts
oafnaalcyctuerafcryomavtaiislsaubclse
without at fs
cciiomtnehse,irdmea+rt/er:di3x0s%es.mpiiqk+ue/as-nt5tui0dt%ia.etsi,vieTn.hdiecaDtreeetctaohivaletsrtioheefs dmfaaatltalricbxaenlsbpoeiwkree5pr0oe%rct,oevderrweipieotsrhtaaerdseadstauetdmamaascrhciouzureladdcyboaf
CfAooprnpceetnnhdteriaxtrieVocInoLsverTrehipeeosrctoeondfcewntethrreaetinsoountmsocgooafrtrPeeFcOtseSd,ndfFoaOrrSdpAur,iotrPyFomOfaAttrhiaexndPFsPpOFiSkHeS
were not comertoind recoveriee. he
attempt relevant
twiasssuemsasduechtoascolrivreerc.t
the
fluorochemical
concentrations
for
msotainsdtaurrde.
coAnltseon.t
m1os,
RESULTS AND DISCUSSION 1C1on0ceVn1traantdiotnhse orfePsFuOsSa,reFsOuSmAm,arPiFzeOdAiannTdabPlFeHS1. inPFfiOshStwisassuedseatreectgeidveinn vin rAppnesnedgigcses
s 8
oooffflfwiihsvihetrefofirrsohme.gtghsMe.uGsrcelAaemt otLinaskgseuse.msuscCcoolnntecaeitnintsersduaetsri,eolnacstairvwpeelrfyerloelmsessScatoghniacnnena4tw0r0aBtainyongscocnwoteamtipnaweredeidunpt(hteotch2go9se7es
cnoengt.aivneqtuawnit.ifiaMbulseclleeveltsissoufesPFoOfS.fishFOfSrAo,m tissues.
PvaFrOioAusanidnlPanFdHSlakweesreinraMrielcyhifgoaunnddiind
not fish
fi{nomuBonednlgginifuifmsihscehsoesnaamnioannlieytdzoerudepdf.(r0om9S2aE3lumrnooenpge,aannwdectooutwnhite.rriefTsih,sihmseusisfcrtloheemofhtihgeaheBfsiatslhtcifocnrcSoeemnatSrdcaihtdeilondnoetzofceosPnntRuaOairSny `quantifiable concentrations of PFOS.
tAhmeoAnntgartchteicsOacmepalnes, fPrFoOmSraenmdotoethmearrfilnueorloocchaetmiiocnaslssuwcehraesntohtedeNtoercttehd.Pacific Ocean and
REFERENCES (1) 3EM00-E1n3v8i6r,on3m1en9t7al, EL0a0bo-r2a4t5o6r,y,E00St-.27P0a6u,l,0M1N011L,IMs Report numbers; E00-1634,
6
7 10
SpVTealeeer.lSenooTmfHcoceruTptivrinsrs Cosskoloen (040) Une
gn tortaogcn PHOS GNoer PnacissGr,r
HUSA,
HOAFw onsd HIS inia sa hseRdop enne
BOI
lhe
oop Gerdes, oman
ae
EY aw
DOT le Gouri, e cume bian WEhme GSoegoeauy nik.
ane imren
an a
aw @ ow
[--
Be GeldMoimaenio, won ao
SW aa
cluoorskinlooon(0-6) MMaolee CHINO Mack
GSewnmiwinienvnoeridnmee. Greldesnmibie,
essrnn roe
ag
S a0a 8
Bom rI0 Made Gronln[ es Homer, rae
an an
aa wa
[Suioentnneiasedy) itBhiomr SShoadit1i7o)ns ood
MNMeeedsmreerrmnoeemnnssseaas Nedreenses
awiaasnen, siaovn e wen we
aa5w 5%
aEwl a
VfToeirtaeoynnn i
Wain MLwilee
[iri ----"
pring Sadiaosain
gn meaas n
EA GE3A a eoa0n nca0e way
|
Vatospecies 0719 Met
po Cuahrmblc
pt Eh acm an
aym aa
VVDreeoasnnseie(0snw9inr TLGownee Virnat) ioe
ld dunid e nkae MeMoindnnn hind
G@ioyan vmx
an @
a3a aoanr
53 3 ar
\
wien
We WR ----m----
Vac io heGtkwe et cle inesfeS TRsTyey
|
18.
Cofgr wt niss in armors
dEaA mEmeElm
Er OWT MMmEE elomtm SmToaErEnNtnT
danmetttenen mow eam
oOwern nn
iia
||
GHHERhEEERR ERDOEMMMRa DWGLnoIEmmMmNEEmNRTeTT
mmioe nmmeoammmese
SEE
eamno amammooonnn
ehnn oSonloo memaianmmn ddSelooim
SWeEiEEn ein
naNem LLln IORGiENSIEERT
mgPeuynemm ne
ddedemi sou
mGmeiunmmd svat
oGiiimin sore
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awn
seoeenm sanageen soorono,
|
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nein ms une GEIL om mia so oa
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SoTRIIMOI Lna Gmiide ten OR er G[eril=e
400000 oom) aco 400(ommn 40000 oom acon w00coom
deo 1WOOD Ls Grid
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oe wooo tooo <toocanm 400000 aceon oan tooo
peer So
NOT Ls Geille MOS lr GWailkea,
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togmenn togwimn
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|
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ooos ave
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| |
=oI &ao
NJBoON. JMMeeecek SSSwwueennwDBOniSMM INE Mek
o0twmm
Gooooaoltioiomnsmdn dSdeeogtteeanr Lonoeoggiloe
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an
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&& QCUFI MJke sSSaIegEBaymMn 0aomomo SAeo0lgQio(eMmnEe 0Ld0ee0vgii0en0m L<ieo1o(od(0oeitemgsmy QQiIiniSm pmovs Mek Goad om oocnm oom
|
|
GGQooummeiims
eogwmmeebumm Geen
wMNekww ww
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ivr WOON Mae Gmidam
oaiGWobneen ow
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aren? iootamm
||
iLDtilenrrn Diets
pmmnme pen
oNMeewdwks tek
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GiGean mamo
lGoooaagilioinmeses Goon
odeoegrgtoeemmnns wien
doLeitooemLm date
| |
mh beommosma eeem homme
wweeweee wk
GGGaoEiuaoGmh GoM
ho
Lo0d0dinimgns Soames
LGogooigooionnw dogoigenow
dSdeeeptngesm Segeiegs
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f booiOTee BeSd Doin
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hoi [TOBE wk
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odoogiaiieeeooww doaieme
Seogigienn LLLoooiotonemmm rSeegiga Loiieem
|
T PpDSorePimesarcm_IeoGmD wwke OGGGHoaeUnnllGe plleMoimmiaSnootae dioibmeomt meens `ooataioieeooeo ows GGSeoeggeuore lLLanoootooitnmna
|
5
Concentrationsof (ul. wet wt urochemicals in ish APPENDI1X
SSeeoakh Swot
SS Bhahy TLLihE eeerrSNeettmcrrmmoniss c<L0aQ(O00R4%0R55)) SHE Live Nelms
T<LO0TQO
SIL)o TLOoT(00sa pl) <Lo0n hohe)
Steerny
SSUaEl
LLemr
MNekeorlmomnsses
<L000oaSnM 000
wl) 0LL0oO0gGgeY
L0Logo0iogrmmis mmen
<LoLgioosgareer Logit
TToostnoin Tun
TMiiss 5)
LLei
MMeedtkrrnosSneas 100o1o0n07) L"0GL(000i0Ev0g A<Lg000OaITeEcewsyy <<LLo0u0m0mm0en8oprtp)
Th lb Mensa
fTromin Tfoay
TTooonn Tan
Lhhee Lhe
NMeellmreomssea Melonsa
e0mw a0m8
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A4g0i0o0s0 Logins
<<LLoLgoigowmgmrtaesns
ons Logie
Taw _lr Mkrwota
toque
Ti
00 Le eberente 0om% a1g0i0n00 oWogontein -lLoosgesiertg
PPHHOSS Rperrtunncncsaanne
HOSA - esorccmstomnids
LQLimoqt les nrc
|i
le
n
Concentationsof (g/mL) Noches nfs ArreNoic
e e EE TH e e em Ree r w
B BBBaulcoiinno 0 TTOOO Wbleeeeddd tlaeonnecs 2UE MS AAc0oUummugm)) o0g0amaem) ooeusn
DaSancoitdasn TTSOOeDM DDMeeeeddd heeeeenn Sd SH Med heen
OGIT MIW
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od0oagsmoe)) 0Gsme)
Lode) toot mm)
dnoont goeile
|
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SSBHS SU
etMeedwds hmmeeaseeens
DUN Weed
0BH DE
GL0000UUmmmmmlt)y o0mml)
Ldoaopsimtel)) oom
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aaonn oats
non
Swodfih Sn beet meeeents GO1M Q uoquUonm)gm 0do0gcasomme)t) bhoose
PPEOSN- Pelbeoteonmncsinne
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Concenmions of ug, we we) crc in ish AvpENDIIXY
T-- TeoImaN -- WT UT W Soh -- s -- Aa LOoe0ro <CTuOo-- gme eroe <s o i g e
sir Sir
OOP Wh OO ws
aw i
c1o0wod8enomn ey
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ao il Eons
cugommnn on ft y si om
xan [rSSeiSan
CORIO Wikio OM tem
in macs-anmia
Loom oodr o
toque ooo
uoowwf euo s
<0 oth
iiSiTTn [hrBa
te UNO te Cte
bw pe--ocs
o odpg yin py
coomamman oven
Aodwwiof o e
colt oth
wel odin o
wl
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OOM CO
te le
mmee---lien
ooddtpoeiynen
om oom coounman
aATa ionai . vanoatitth ohm oti
w[iSdrrraaee
OO CN
SON
te
ome-es -
oopdooeirno py
coowners oommmem
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audit ob
te
wet
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te te
wmee--ii -
oodpiymn ni
oom oon
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10 10
ecm aodfion quem wap
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ofa cob
8
i
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CONE CNS CMOS CERIO COO POV OO CTR CMO MOT CONT
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dn
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Ue we 10we8r 0 ogo wontr h aaownt
a FOR ~ Pru-- ne
L00- Litof gion eipects
|
1
"
APPENDIX v
Concentrations of (g/g. we wh arochemicas in ish
T F EQW N MMeaea deke beong oWsETs m 0we0 LO e ug Wwg 100 hores ey
F T Fh I OGN UWNN
dwkk leek
hgoegann bon
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Fh OWI
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F FEhh W OOmeWr
aakk Mek
ehong sen
Mk bon
par n aooms
oOBR O oQ o) m Lou0 odmaesnsp 0 LOOT a) "L0G BISuy
E F Eh D WI R OWE II
umdke Mk
bgoenn bon
Fh NIWD wk bon
v0a30 ous
o0m0 re
dCoooomnbeeys ones
cog
aoem moors
vy
nose: aoe
oan
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aoow asmy
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oomme LE
qcgHaeoonmtien
gpors hoi
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TFTaCe To
hDeMIomINwIlDD MMMeeeeke MbMguienmen Auc0oo0wiaNnngMmwinn aSooonwmns
opononueer n <oooomonensen Clooames a
E[ h EGIT ONsT Te nr
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0 00G 0M ry
Looms DI
Adogognommeass
0gqmanamnetev)ey aon
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1FE9h GCQhOReCbVeDIiAtL
kMaek Nee
bboeonn ind
2a0us 40010088250
OoQ on) i) 40000050
Lon baineaer m 1ovmwtoosrennhty 00s Sopa
20
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gGorreesds pi
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CCooubtabioec Cubes
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-t<1Lomorgemamatemrt)ts) Se
|
TTeeeendyN Ton CAN
eldee MMucek
CCuobbihc CCoobbbllee
cloOowney <<LLO0O0W0OMMNS wwae)
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2
PS Nerenmentnse
HON esos
Cometrotfi(wog.nwest wt) Morchenicts in sh APPENDIVXI
T FTG Wo md RT 31 ToaaS OT aon oan
TALIS
FL
BONA
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hn
ry Lob
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ge <L00 008 we) <40Q(OaTpT <L00 0005 <Lowey
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tLoirs Lie
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n
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in
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