Document 7M97443k999pV3rn0oepKgY8R

2Block- a Monit ring fer_ a, Other Chemicals /Present: -J)^LL a^Ai* Person or Area Monitored- Sample ^|0 07518 Type Sample: [Q'i'ersonnel Area Q Excursion Other. L Dato- 12-30-1 SoTJob Classification- _______Description of task performed during monitorin' including any unusual activities. CATtff </ A7us,- &C'J Time Started 08QQ Timo Stopped__ \^l30________ Beginning How Rate C- >'2-S Ending Flow Bote (, ^ Respirator used Q Yes \C/No Calibration Check Prior to Monitoring? [] Yes [] No Calibration: Q Bubblemeter Q Rotometer Other NOTE: Job description must be concise and complete. LOUISIANA DIVISION INDUSTRIAL HYGIENE Type?_ Wind, Temp, and Humidity Form filled in by "p jJc-o if ~X*Z- % V DO A 1106.59 CONFTDFNTIAL Block <3 &P \ C - 4____ Monitoring for.-M o H- Other Chemicals Present: 'kW *' ' Person or Area Moniittoorreedd--__LL____C>cV Sample ^0 07517 Type Sample: f^^Pers nnel Area Q Excursion Other. Date. Job Classification------- ----------------------- _Description of task performed during monitori including any unusual activities____C/)TC H e^-- -k j /7-T Time Started______0 Time Stopped____ O ) Beginning Row Rate___e* 3 Ending Row Rate___ *-3 eL tart Respirator used [] Yes No Calibration Check Prior to Monitoring? [p^Yes No Caiibrati n: Q Bubblemeter QRotometer Other NOTE: Job description must be concise and complete. LOUISIANA DIVISION INDUSTRIAL HYGIENE Type?. Wind, Temp, and Humidity Form filled In by- 7 3*^3 Blocked _^L Monitoring for__ Other Chemicals Present: Person or Area Monitored. di. hhtfC- Sample ^0 07515 Type Sample: [jTenonnel O Area Excursion Q Other Dote /Z ' Z f - Job Classification____ ^ ^ __ LiDescription of task performed during monito including any unusual activities. c/irr/-/ ^ /fW c/u/s//<l tc/'co Time Started 0 7 Jv Time Stopped / Beginning Row Rate. JL9 Ending Row Bote J-/ <? Respirator used Q Yes Q-" No Calibration Check Prior to Monitoring? [] Yes [] No Calibration: Bubblemeter Rotometer Other NOTE: Job description must be concti and complete. LOUISIANA DIVISI N MXJSTRIAL HYOIENE Type?Wind, Temp, and Humidity Form filled in by . fJc- 0Ik - n-d -c T/^T} iS rnwr ti-J 1 66 confidential Bl elc jCL i M nitoring lor A/fo f~f Other Chemicals Present: Person or Area Monitored -0a ^--C 07514--------------- Sample ^0 Typ Sample: Q^Personnel G Area Excursion Other--------------------------------------- Date /Z- ~ *7 ~ &_ Job . O . V Description of task performed during monitorin Including any unusual aclivities- if A/ C/JusT/C 'j V- Moa/ Time Started__ O 7 30_________ Time Stopped / ^CV__________ Beginning Flow Kate O ____ Respirator used Yes B'flo Ending Flow Kate /. 9 ^____ Calibration Check Prior to Monitoring? G Yes G No Calibration: Q Bubblemeter G Rotometer Other NOTE: Job description must be concise and complete. LOUISIANA DIVISION INDUSTRIAL HYGIENE Type?------------------------------------------------------------------------------------- Wind, Temp, and Humidity TL &o~c /^r - 3 7.*/'^- Form filled in h, iJ J ?- Col fl/.uO itMe iitoring for. Other Chemicals Present: ftih&z A/Ci Cf4____ n7?0Time Started. Time Stopped. MS/) MPerson or Area Monitored. / > A. Sample ^J0 Q7512 Type Sample: [^Personnel Q Area Excursion G Other- 3*TJob Classification________ Including any unusual actlvities- Date. .Description of task performed during monitorin 7 U. // ^ Beginning Flow Rate__ __________ Respirator used Yes Ending Flow Rate____ 2- * &______ Calibration Check Prior to Monitoring? Q^Yes G No Calibration: G Bubblemeter G Rotometer G Other NOTE: J b description must be concise mid complete. LOUISIANA DIVISION INDUSTRIAL HYGIENE Type?---------------------------------------------------------------------------------- Wind, Temp, and Humidity TI m k/o c k -- H-d , Form filled In by_ /Jr, f \ .M:. JLL. 7 >// DO A 110661 CONFIDENTIAL DOW CHEMICAL USA LOUISIANA OIVISION ENVIRONMENTAL CONTROL REPORT OF ANALYSIS REFERENCE DATE THIS REPORT----- 2 '5 ~ 8 CHAROE ..tT-- O hlor.n O _. DATE SAMPLES rwi I tKTHL samples roVrgn-4r;iratil cu/Aprv6 Saiunr-rPc ^ Ov-Ct PgrSoNNeli "Ti6w MamOwMn 10 CoN P-gn^ra-li oft I TW.llVq REMARK5 KAOH 07517 0 75IS J 75 1M 07SI2 06.J Nt> i , 037 j______ .02?: 675IZ rib 1 I 1 METHoo-feiJ-g^H___/WejfvJ - 53SI a^LL^eiuS___ qc.'fj g JC4raction *DLO BELOW LIMIT Of DETERMINATION VALUES REPORTEO HAVE SEEN CORRECTED FOR interferences NO - NoNt dLc+ec4<-A . h.ut<uh. - . ooS mj ___. _______________________ WCMAAK& . Sqmjpfl^ .. Atmo UMAJ. '.a^alyzgj HONED.. LflS*TL DO A 110662 CONFIDENTIAL------- f 8986 >>> Contact RANDY COLLARD oranyone in the labfor help logging in samples. < Date (mm/dd/yy) (>1 / .19 / 8Number of Samples: 5______ Emergency (Y or N) N Plant or Project: CHLORINE Charge #*. 25 Outside DOW N Submitted By: LOUISE ALMO Bldg. 3502E Phone: 1635 Report To: LOUISE ALMO Bldg. 3502E Phone: 1635 Problem or Reason for Analysis: CAUSTIC (NAOH) Composition, Hazards, etc.: Sample ID: (Plant Equipment #, Data Book #, etc.) A # 07512 B #07518 C # 07514 D # 07515 E #07517 F GH IJ >> PRESS PgDn (BLUE DOT) TO CONTINUE <<<<<<<<<<<<<<<<<<< IF YOU ARE NOT CERTAIN OF THE ANALYSIS NEEDED, CONTACT RANDY COLLARD (8686, RADIO PAGE - 106) FOR HELP. PRESS PgUp (YELLOW DOT) TO RETURN TO PREVIOUS PAGE. Analysis Needed:NAOH___________________________________________________________ __________________ SAVE ENVELOPES_________________________________________________ Area: X WET/IC _ X-RAY _ GC/MS _ IR Comp: _______ _______ _______ _______ __ NMR _______ _ SEM _ ESCA ___ N DONE YOU ARE FINISHED WITH SAMPLE LOGIN PRESS F6 (GREEN DOT) TO PRINT YOUR LOGIN SHEET AND THEN F3 (RED DOT) TO READY THE SYSTEM FOR THE NEXT PERSON. ... **.- Sample Number:8986 Report Responsibility: Disposal: Last Update: 01-08-88 Time: 11 :49 00 A CONFTDE-NTIAI Tos LOUISE ALMO Dept: ENVIRONMENTAL Bldg: 3502E ANALYTICAL REPORT DOW CONFIDENTIAL INFORMATION La. AS&TL ANALYTICAL LABORATORIES I Request No(e): Bldg. 2503 I 8386 ______________________________________________________ I______________________________ Sample Date: I Prelim. Report Dates I 01/13/88 I I _____________________________________________ ______________ TITLE: CAUSTIC IN AIR. I (Charge Nos I 5 .1_________________ Final Dates 01/23/88 Author(s): J. PREJEAN Phone<s>: 6817 REVIEWER: I Data Archival: I 4815-3 I SAMPLE 07512 07518 07514 07515 07517 Ojgr NAOH (MG/M*) ND LOD=.005 .033 . 083 ND . 131 -- . LITERATURE REFERENCES: MODIFICATION OF METHOD NO. S381, PREPARED UNDER NIOSH CONTRACT NO. 210-76-0123, 7/8/77 METHOD WAS MODIFIED IN ORDER TO UTILIZE A METROHM TITRATOR. DUPLICATE SPIKES OF 0.5, 1.0, AND 2.OX THE OSHA STANDARD OF 2.0 MS/M* WERE MADE. AVERAGE RECOVERIES WERE 33*, 38tf, AND 103X RESPECTIVELY. DO A 110664 CONFIDENTIAL  DOW CHEMICAL USA LOUISIANA DIVISION ENVIRONMENTAL CONTROL REPORT OF ANALYSIS REFERENCE DATE THIS - 2^^*^ y CHARGE --- utPT___ C- h lor ;ne_______ _ . samples rbWn-tial bXpdSure Of ID n;,/tomi CoiJ f.erAr aVt on v rrs. H'. q DATE SAMPLES r.cn 1 rr.Trn Personnel To isSaOH REMARKS KAOH 07511. ^0(*A 0 76IS ND 075 H 037 1 0 7S 1$ .02? 07ZIZ Kb 1 _ i ________ i______ | ! .etmod KJ <x<)a*aus Ateibal__ - gc.Vj ft* Irat+fon GLD PELOW LIMIT OF OETE RMIN ATI ON VALUES REPORTED have seen corrected for INTERFERENCES NO - NfiNe de+e-c-ki MLS SOLVENT. LIMIT OF Nft.OU - determination . OOSmj i WEIGHT/VOLUME i Sorapfit. .foW UXMA ' QruAy2ei LflS^TL DO A 110665 CONFIDENTIAL. . jfgg/sg Alrno. SIGNED- / 898$ >>> Contact RANDY COLLARD oranyone in the labfor help logging in samples. <<< Date (mm/dd/yy) J01_ / J_9 / 88Number ofSamples: 5 Emergency (Y or N) N Plant or Project: CHLORINE Charge #: 25 Outside DOW N Submitted By: LOUISE ALMO Bldg. 3502E Phone: 1635 Report To: LOUISE ALMO Bldg. 3502E Phone*. 1635 Problem or Reason for Analysis: CAUSTIC (NAOH) Composition, Hazards, etc.: Sample ID: (Plant Equipment #, Data Book #, etc.) A # 07512 B #07518 C # 07514 D # 07515 E #07517 F GH IJ >> PRESS PgDn (BLUE DOT) TO CONTINUE <<<<<<<<<<<<<<<<<<< IF YOU ARE NOT CERTAIN OF THE ANALYSIS NEEDED, CONTACT RANDY COLLARD (8686, RADIO PAGE - 106) FOR HELP. PRESS PgUp (YELLOW DOT) TO RETURN TO PREVIOUS PAGE. Analysis Needed`.NAOH_______ __________________ SAVE ENVELOPES _______________ _____ ________________ Area: X WET/IC _ X-RAY _ GC/MS IR _ NMR Comp: _______ _______ _______ _______ _______ _ SEM _______ ,, ESCA _______ N DONE _______ >>>>>>>>>>>>>>>>>> YOU ARE FINISHED WITH SAMPLE LOGIN PRESS F6 (GREEN DOT) TO PRINT YOUR LOGIN SHEET AND THEN F3 (RED DOT) TO READY THE SYSTEM FOR THE NEXT PERSON. Sample Number:8986 Report Responsibility: Last Update: 01-08-88 Time: 11:49 Disposal: Pl? A 11066s CONFroeNTrAL Toj LOUISE ALMO Dept ENVIRONMENTAL Bldg: 35C2E ANALYTICAL REPORT DOW CONFIDENTIAL INFORMATION La. AS&TL ANALYTICAL LABORATORIES 1 Request No(s>: Bldg. 2503 1 8986 1 Sample Date: l Prelim. Report Date: 01/19/88 1 1 TITLE: CAUSTIC IN AIR. 1 \ 1 (Charge No: 1 25 Final Date: 01/29/88 Author(s): J. PREJEAN Phone(5): 6817 I Data Archival: I 4815--3 I SAMPLE 07512 07518 07514 07515 07517 NAOH (MG/M*) 4k ND LOD=.005 . 033 . 083 ND . 191 LITERATURE REFERENCES: MODIFICATION OF METHOD NO. S381, PREPARED UNDER NIOSH CONTRACT NO. 210-76-0123, 7/8/77 METHOD WAS MODIFIED IN ORDER TO UTILIZE A METROHM TITRATOR. DUPLICATE 3PIKES OF 0.5, 1.0, AND 2. OX THE OSHA STANDARD OF 2.O MG/MJ WERE MADE. AVERAGE RECOVERIES WERE 99*/, 98'/, AND 103*/ RESPECTIVELY. ^H0667 CONFIDENTIAL