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22661177..00000011 E`E2xx6hh1iibb7iitt 2617 State of Minnesota v. 3M Co., Court File No. 27-CV-10-28862 STUDY SUMMARY FOR WORK PERFORMED DURING 1977-1979 TEST SUBSTANCE Identity: Perfluorooctanesulfonate; may also be referred to as PFOS or FC-95. (1-Octanesulfonic acid, 1,1,2,2,3,3,4.4,5,5.6,6,7.7,88,8- heptadecafluoro-, potassium salt, CAS # 2795-39-3) Remarks field: The test substance is a white powder of uncharacterized purity. The attached is anoverviewcreated in 19for7 stud9ies completedfrom 1977 to 1979. Robust summaries have already been submitted for many ofthese studies. Others have not been summarized due to the fact new studies exist that supercede these or they are being repeated. STUDIES Water solubility; biodegradation; soil sorption; octanolwater partition coefficient; Static Acute Toxicity to Bluegill Sunfish (Lepomis macrochirus); Static Acute Toxicity to Rainbow Trout (Salmo gairdnen); AStcauttiec TAcouxtiecTiotxoyicDitayphtoniFaatmhaeganda;MiCnhnroowni(cPFilmoewphTahlreosupgrhomSetluadsy);onStatic Fathead Minnow (Pimephales promelas) DATA QUALITY Reliability: These studies have been assigned Kiimisch rankings = 2. `They satisfied criteria for quality testing at the time performed, but have some deficiencies. In many cases actual concentrations were not measured. The value was determined by indirect measurement (e.g., solubility) or using nominal concentrations (e.g., aquatic toxicity). In some cases, the analytical methodology itself was questionable. Additionally, these studies lack sufficient characterizationofthe test substance purity. OTHER Submitter: 3M Company, Environmental Laboratory, P.O. Box 33331, St. Paul, Minnesota, 55133 Last changed: 5/3/00 2661177..00002 MICHIGAN STATE UNIVERSITY TJ o onsons w-- s say 15, 1993 ar rn wc ann 5b3eH. CCoRomonvbpeearrn,ty D. Hoel alas, 2-38-09 SE. raat, 0 S3144-1000 Dear br. Bowls STEonemccetoomsrmeeedncdoaamrteeinodsnaystirfoeonvrsieSwfaoprrcoomvFmioenrngutrsetherxeesgGeaesxstilciihse,gy otfFhleecnshiesneesrue3dviivTeiewdcehatulhtiesslcsuildadfeRoner,pmoardttniedo,n na 16% oe Wow 1 1 con be of any furcher assistance. "ITihtidsno hfhauevrechreetrca.toemrmeeIsntdeanttfihnoonsssiusbsaFcioisrctiafnlugfluyraesurpTepesossreatszscchyho.purropePofesfroharaltpsstovteo3Hocooiucnladiaacdciiosarcdouarsnmscaecion on tne eovizonaentai fare and behavior of ihe JW products: oTyniecSoanlstulcdSianygsRffeoexRrfeorviEetwheoEvfomraktepreirafiosrmeSadndcToprdeIapcaeratdSsion$o3o,f200sc.ep0eo0ret(ecnheplsussanodme hy Sincerely, pr - "PSrtoefpehsensoAr. Boyd, PK. [rR 2661177..00003 FRienvaileCwomofprTeehcehnnisciavleRReeppoorrtt SFuCmm9a5ry YAnLoucstianngolt-hweateeqruaptairotni:tion coefficient of 10 would predicat supercooled liquid solubility of250 logKoy = -0.862logS. + 0.710 `o`uColndvberesel~y2if8t6h0ewmagt/eLr.solUusbiinlgittyhofeatbhoevesoelqiudaitsi2o8n,6thmigs/pLr,edtihcenttshaeKsuupvearlcuoeoloefdalbioquutid5s0o0l.ubiTlihtey pvraelduiecstesdeveamluiencsoanrsiesqteunitt,edi.if.f,ierfetnhtethmaenatshuermeedaKseuvriesdcvoarlrueects,, Ianwdotuhledmexepecat ashKiu.gh,rearnewdatde,r solubility, andifthe suspicious. measured solubility is correctT would expaehigchetr K... The values look FC 95 defined icsridteisccalrimbiecdelalseacnonacneinotnriactisounrfsaicmtialnatr. If 50, to SDS does it form for example. micelles and exhibit If 50, then I'm not a well certain talking should about water be examined. solubilities is appropriate. Rather behavior above and below the CMC 1`0Tvaablrey2dperpeseenntdsisnooingltshoereptioxn dpataewhviracrhiiiasblvmierstoueaflalymnomuetnatnoinafgslaelisls,.tThyeofppseoriecle,ntvsoorbledoufiswagmtoeienrg, scoorpnticonecnoetfforicfaiFetnCti.9o5Tnh.isYoshuounledebdetdoonmeeaosnurseetvhereaelntsoiirles.soiAlgasoirnp,tiiofnFiCs9ot5heirs maacnondvoebnttaiionnaal micelle CMC. forming T would nsuortfeacxtpaenctt Iliwnoeuarldiseoxtpheecrtmsd.ifferent soil sorption behavior above and below the aApKpr,oprviaatelnoefus4se5ofisthriespvoarltueed, biatssehdouolnd dbateaofbirzoimneadnootnhesrevreerpaolrtd(irfefefreeraetncseoi3l)s. anTdobeevarleulaatteivtehlye constant, or be consistent with K., values predicted from empirical relationships such as: Tog Ke. = 0.904 log Ks - 0.539 (Chiouetal. Environ. 2Sc1i.)Technol. 17:227- UsingtheK.yvalueof10,thepredictedK,,valueisabout 2 whichismuchlowerthanthe v`amleuaessurerdepvoarltueedo.f 45T.heAgKaien, athnids/oproinSt,s tvoatlhueesincmoensaissutreendcieasroef atlhseomebaesiunrgedusKe.dw,St,o,apnrdedKi,c,t abpiporcoonaccehnitfratthieoKn,fyacotrorSs,uvsailnugeesmaprireiaccaclurraetlea.tioAnsshimpsenltiikoe ntehdeaobnoevaebKovxe.anTdhSis, risepaorretaesdosnaebelme: 0 be inconsistent, so I don't have a lotofconfidence in using them to predict other things like BCE. 22661177..00000044 Recommendation 1. (NSeeeedmaenthacocduorlaotgeydeotferCmhiinoautiaonnodfSwcahtmeerddsionlgub,il1it9y8a0n-dgoicvteannoiln-wparteevriopuarstirteipoonrtc.o)efficient 2. Determine the CMC ofFC 95, and recognize that its behavior above and below the CMC will be different. 3. ObtainsoilsorptionisothermsonseveralsoilsandcalculateK.,valuesfromthese. 4. Check for consistency between S,, Kou and K,, values. 22661177..00000055 [femeiana TECHNICAL REPORT SUMMARY 3718/79 TO: TECHNICAL COMMUNICATIONS CENTER -- 201.20N important= ifreportspintedanbothsidesofpapr,snctwocopies fo TCC.) HR EoEnvironmental Leboratory (EE & PC) Fate of Fluorochemicals Final Comprehensive Report: FC 95 wo r053e5 970612643 o11 R. A. Proko TE,ASfu SN EWelter rr 09362 SecURTYD (0LO, contamion oaRuorznion) | "HES> 12 Ba omonos. | cunnewt owecrve: TaohseiseastewSegd oer Final Report: Etnhceomppearsisoeds1a0l7l7 w-or1k979p.erformed during FElEu&oPCroc-hDemiivc.al (A(aqnuaaltyitci)cal) S(BBooerBirslad)atio-n) . [meron[SoenyAeE eTRACT:3 R20R07n R80woErdsToeSrorhe ereraattesa!Soooatdyvy TBT eCornGert D. L. Bacon VR.l PL.othBaophroangada . Infomation LiLgaEen 22661177..00000066 oa Cla -2- Introduction The rationale for performing enviromental effectgstudies on fluorochemicals has been discussed previously . Tiahnseitornsiiubcbujtesicuotrnfafciltnuaontrtho)echweehmniivcciahrlonhmoaefsntathaipssotretenhptioisratlmatfieosrriFaCwlid9e5issp(ruaesnaedd by the chrome plating, and etching industries, both domestically and internationally. FC 95 chemically is the potassium salt of perfluorooctane sulfonic acid. Cg.Fiz SOK FC 95 This material is an off-white powder, having a molecular weight of 538 and the chemical structure shown above. This report consolidates all available information in the areas of aquatic toxicity, soil sorption studies, degradation, water solubility and partition coefficients and defines the probable environmental risk of FC 85. Methods Whaatveerbeseonlubtihleitsyu,bjebcitodeogfratdeacthinoicnalandrepsooritls!gorgfi. onThsetsuedies "specific experimental methodologys have been defined in these reports and should be consulted for specific details. A) Aquatic Testing : The testing protocols utilized for this study ere modeled after that described by USEPA (1975) . B) Acclimation Procedure Tthroeutblu(eSgaiglmlo sgauinrfdinsehri()L,epaonmdisfmaatchreoacdhimriunsn)ow,s r(aPiinmbeopwhales promelas)" used in this study were obtained from private hatcheries. Stock fish were held in fiberglass holding tanks filled with carbon-filtered well water maintained - at 14-15C. A daily 8 hours dark, with a p3h0o-tmoipneurtieodtroafnsi16tiohnourpseriloidg,htwaasnd maintained throughout the agelimation and testing period. The fish 48 hours were fed prior to Taentdrat-hMrion"ughdoauitlyt,he ftoeosdtbepiernigodw.ithheld Fish were so acclimated for 14 days prior to testing. Acute short-term (96-hour) static bioassays were performed on FC95 Lot 583.Carbon-filtered well water of known composition a. Dale Fattig Fish Farm, Brady, Nebraska b. Dennis Fender Fish Hatchery, Baltic, Ohio c. Tetra-Min - a commercial fish food of known composition 2661177..00007 -- w2a0sxus2e0dcma)s, tcheontdialiuneinntg. 16.A1llofgladsislueanqtuaorriadi(l3u5enxt Bpilnunsowtsoxi(cPainntepchoalmepsrisperdomeaiasst)u,dyblcuheagmbielrl. sunFfaitshhead u(nLiefpoormims imnacsriozcehiarnuds)w,eigahntd, rwaeirnebowtesttreodutat(Saelamcho gairdneri), c2hiesmhicwaelrecroanncdeonmtlryatiaosnsigofnedeatcoh vteasrtioumsatetreisatl.chamTbesetrs wwtieetrmhepienmraait3nu0rtemasiinneufdtoersatthfe1o8llfCoawtihrneaagndgetmoix1in7cn5a1o9nw,t awnadhdidlibteliuoetngh.iellrTaeissuntnbfoiwsh dtriosustolvteedstsoxwygeerne lceovnedlu,cteadndatpH1o4fC.allMotretsatlistoyl,utitoenmsperature, wmoerrtealmietaysurheadd aotccu2r4r-ehdo.ur Giennteerravlalsobosreruvnattiilonstotraellative attoopprbboeephragiveaintoeerr.aalllycOhraghnaegnaeilsstmhsyweuraseneddsifmriineleatrholifysdirssteeucadosyred.ewderwehecnonsidered OIrnisotnrupmHenmteatteiro,n AuSsTeMd tihnecrlmudoemdetearsteg<p1gCr.atufroer tceommppeernastautrieng monitoring, and a Yellow Springs Dissolved Oxygen meter. A9l5l% acqounaftiidcencsetudliiemsitwserweererepclailccautleadt.ed IuCs,ifigvatlhueesUSwEiPAth (Duluth) Probit computer program on the 34 TRAC System. ) Aquatic Invertebrates - 48 hour Static Cg, DtaophFnCia95,maglnoat, 52830 aotrgavnairsymisngpecroncteesntt,ratwieornesefxoprose4d8 hfoiulrtse.redFiwrelslt wiantsetra,rswwietrhecchoeumnitceadl aandddedplaacneddsoilnubcairlbiozned prior to the addition of the Daphnia magna. - Test concentrations were 42, 56, 75, 100 and 135 mg/1. LuCy,sevtahleueUsSEwPiAth (9D5u%lutcho)nfPirdoebnicte lciommiptustewrerperocgarlacmuolnated the 3M Trac System. TahfetertestthatprdoetosccorlibuetdilbyizUeSdEPfAor(t1h9is75g)yy,dy was modeled Results Tdaabtlaeob1taliinsetds wuastienrg sroalduiboirl}istbyellaendd pFaCr-9t5i.tionThicsoemfaftiecriieanlt aispwaartteirtiosnolucboleef,fic2i8e6ntppmof 7-'), 10s0}i7g.htlyBasleidpidonstohleubsleedhaatvaing tito caannabpepreccoinacblluededexttehnattFiCn 9t5hweoeunlvdironnomtenbti.oconCchieonutreatteal(o shIanovleutbhidilseistcsyryisbtoefedmaatncheheemamispccearrliibceaaldndrereirltsoartiboiinsoschocinopcnesnbitedrtewareteeidnontwoaftabecetroorn.e oFCrde9r5 otfo mtahginsitpurdoep.osedWhernelaaptpiloynisnhgipthtehisdatcahemgiecnaelratweoduldfor be projected 200. to possess a bioconcentration factor of approximately 22661177..00000088 . --a- TABLE 1 - Physicochemical Characterization of FC-95 . Parameter Solubility PCaoretfittiicotnent Test Veith Method n-octanol/water R2e8s6ulptpsm 7-10 FunCd-e9r5 wtahse tfeosutndcotnodibteiocnosmpleemtpelloyyerdp2g)i.stanTthisto2bi1o/2de-grmaodnatthion schualkteurecsultduerreivbeidodfergormadaacttiiovnatesdtudsyluudtgieliizneodcumlaicroobbtiaianledtesftrom TtwhienwaCsitteiestreMaettmreontplasnytsst.emsDuorfinCghemtohleitpee,rioDdecaotfurt,hisandstutdhye, daevsetlroapi,n hofenmciecrtohbiessmwahteircihalcowuoludlddegbreadeexpFeCc-t9e5d dtiodpnerostist . biyn mtihceroebnivailroncmaetnatbolfiosrm.extended periods of time unaltered iIfn wtohreksiengmatweirtihalfsludoorocdheegmriacdaelse,ithiterhacshebmeiecnallsyuggoerstbeidolotgh-at hiacvaellynevtehratoobnseervdeedgratdhaetifoonrmpatrioodnuctofwoFuCl-d95bebyFCe-i9t5h.er Woef these raonuttiecsi;pattehderetfoorien,crtehaeseeansviraonrmeesnutlatloflevtehelseoxfogeFnCo-u9s5 parreoduncottion `of this material. S(orialngesor1p4t.i6o-n27,s0t)udioefs thheaveFC s9h5ownisthaadtsorabpepdroxtiomattheelyBri1l8l.8% Csoamnpdlyetleoamdessoiolrptuisoend oifn tthheeseFCst9u5diwehsich(Thaabdlebe2e)n(3)a.dsorbed t(oTasboliel2)w.as MaocbciolmiptlyishoefdFCwit95h3i3n sthcreaelcu(l3a)teddesuotripltiizoinngtrials tahree sccohnevmeerteddevitsoeda cbyonsHtamaankter,('K,whewrheibcyh adsorption coefficients reflects the organic mcoonbtielnittyofoftahegsrooiulp. ofHpaemsakteircidesc'haosulsdhowbne dtheattermtihenedreliantive mtohbisilefastohioinmmoabndilethmatateariraellsatiwvoeuldranrkeisnugl,t. movIinngapfprlyoimnghighly this test, FC 95 had a K__ value of 45, being considerably mmoobrielemowbhielne tchoamnparPeadraqtuoaClhloKPfim2be0n,,000K and12.s8l.ightTlhyeseledsasta wienadki,catheenctehatthethcoosmeplfeotrecesdewshoircphtiobninodfmFaCte9r5iatlo asodislorbaered tios htihgehlsyoimlobainlde.s(e3c)o.ndarily the fact that this material Results of (Table 3). the acute `Based on asqtuaattiicc atqouxaitciictytesctrsitearriea teabsutlaabtleidshed bvyerNtIeObrSaKteFsC 9a5ndwoiunlvderbteebrcaotnesiduetrieldizesdligihntltyhistotxeisct(t>t).he Jt is noted that the invertebrate data correlate well 22661177..00000099 Poe . Cs. wsiptehcietsh.oseThdiastaoobbstearivnaetdiownhehnastbeesetningmadboethrewpaeartmedwlayt,er vtahleirdefoprree,dicotnoermaoyf consider Daphnia magna data chemically induced toxicity as to a. warm wwialtlerbeveurttielbirzaetde tsopecviaelsida(t9e,10t)h.is Aconscteaptti.stical analysis Eagngd-ftrhyeirsturdeiseusltswerceomcpornitsreacTtaebdlesto4EaGnGd Bi,onTohmeisces Lsatbuodriaetsory, wleerveelsunodnerthaaktecnhabtioliatsys,esssurtvhievaelf,fecwteigohft a1n%CdFClen9g5thatcshuabnlgeetshal y(oTuanbgleof4).a spIteciiessgeanreeraqluliyteacsceenpstietdivethaitndtihceatoirmsmaotfurecheomrically ithneducpeedrcetnotxicsiutryv.ivalInwatshesptaartaismteitcearlslyundreerduciendves(tPi.g05a)tioant apaFrCame9t5ercsoncweernetrautniaofnfecotfed1.b9ymgt/hli.s cThehmeicraelm.ainiTnhge tmeescthanism hriegshpeosntsibtleestfocrontcheentriantciroenasecdanmonrottalaictcyuraobtseelryvebde adtettehremined bhaastecdhaobnilitthyesweasstundoitesa,ffeaclttehdougaht itthisisdotosebelevneolt.ed that wIans thmeadeconthtartacttihneg filsahborian totrhye's1.9 rmegpo/rlt,tantkhe woebreserevxahtiibointing Astrseismsilbaerhaovbisoerr;vateirornatiwcassmwiamdmeinogf, adafrekwenfeidshcoilnortahteio1n..0 mg/l tank suggesting that the toxic action of FC 65 is cumulative. Baas3e0d-daoyn tehxeporseusruelttso o1f.9tmhge/lhigifoCpatFhCol9o5gidciadlnoetxamcionnattriiobnu,te to abnormal histopathology (Table 5). TABLE 2 - Soil Sorption Test on FC 95 Parameter Test Solution Soil Sorption Adsorption Vater Desorption Vater Koo Results 18.8% 1a0d0s%orobfedamount 45 22661177..00001100 Pe _e- TABLE 3 FC 95: 96 Hour Acute Static Testing Test Organism 26h Leg, wg/1 Fathead Winnow 37.6 51 Bluegill Sunfish 68 Rainbow Trout 1 B. Invertebrate 48 Hour Static Test Daphnia Magna 50 49.2 lower mg/1 1268.4 62 8.6 42.8 38.7 Linits Upper mg/l 5560.2 7a 12.5 56 56.6 22661177..00001111 ve _7- TABLE 4 LPeenrgctehntaagned HAavtecrha,gePeWretceWnetiagghetSoufrviFvaatlh,eaMdeaMninnTootwal VFrayryi(nPginCeopnhacleenstrpartoimoenlsaso)f}diuCriFnCg9E5g%pgsure to 30 Days Post Hatch Concentration Hatch Survival Total Length Wet Weight ng/1 % % om ng 1.9 o5 42 20.5 72 1.0 96.5 86 20 62.5 0.45 ~ 96.5 20 20.5 66 0.28 95.5 0 21 ee . 0.12 97.5 95 20 63 Control 8 o3 to 20 61.5 Solvent Control 89 100 21 64.5 "Work performed by EG&G Bionomics Laboratory, Inc. PS3Mu,mmaStr.y Ptaaubll,e assubmpiatrttedoftofinEanlvirreopnomretn.tal Laboratory, significantly reduced at P = 0.05 : TABLE H(iPsitmoepgahtglheoslogpircoamlelaEsx)ameixnpaotsieodn o3f0 Fdaatyhetaod1M.i9nmngo/w1l|%c FC.95%" Test Material ObNsuembrevratoifons HistoFpiantdhionlgosgical Control Here os 10 , 10 91//1100 bfaacttteyrilailvergilclhandgiesease 9/10 tissue autolysis 2//1100 nfoartmtaylliver change "Work performed by EG&G Bionomics Laboratory, Inc. PSStu.mvaPrauyl,tabaslepsarutbmiofttefdinatlo rEenpvoirrto.nmental Laboratory, 3M, 22661177..00001122 to -8 - Both groups of control, 9/10, organisms and dosed exhibited organisms fatty 8/10. liver changes, Evidence of tissue autolysis in the control group is indicative of a delay in histological preparation of tissues following death of the organism. Discussion The primary purpose of this report is to provide a single source for all environmental data generated relating to FC 95 and to provide an analysis of potential environmental risk. The environment may be considered to be a closed system which can be depicted as follows: . : K mm Setl wu It, therefore, follows that chemicals entering this system may establish an equilibrium, remain within a single environment, or impact on all phases of the depicted cycle. In the specific "of FC 95 in the No Photodegradation Afr Rate? Toxic to Fry 1.9mg/l ---- case at hand we can represent the impact following manner: NE< Volatility ? --_-- Soil___. No Biodegradation - & 19% `Adsorbed Vater" ~~ --_ ------ --> Sediment 286 ppm " J Projected to minimally bioconcentrate, low lipophilicity As schematically represented above FC 95 enters the environment primarily by means of the waterways and secondarily via athdesortberrpeesrtmrainaelntleycostyosteeimthearndsaoitlmosapnhde/roer. sedFiCme9n5t.doesComnoptlete desorpgion of FC 95 from soil did occur in the laboratory moadfealct wh. ichIt asissuumneksnoiwmnpowrhteatnhceerinor lingotht,tohfistmhaetefriinadlingvolatilizes, that FC 95 does not undergo photolysis. Based on the foregoing it appears that waterways are the environmental sink for FC 95 and aquatic organisms are the intermediate 261177..00013 ade Ce. areccteipotnorosf. FCIt95imsayinbethefouanqdu.atic area that a possible deleterious - X A2s5yn"oVteerde rabeocvoer,derdedatucFeCd s95urvciovnaclentrartaetsionosf offath1e8adpmeiannow hT0he.en1c9enopptmhe.effeacTbthoevesleevnedolatteadofmlaFeyCvel9ss5ermvoaefyFibCnea95apsmrsaeuydmiedcitmitpoavcetbefoansahpipaorno,ximately rhautmeasn offoodthessoeurocregabnyissmisg.nificantly reducing the survival oIft F1C5 9t5o mboereempahcacsuirzaetdelythadtesctrheibeesnvitrhoenmdeengtraele with this chemical. ocfonrciesnktraatsisoonciated seimhpalviestmiacdemodseelveursaeld:asisnumoputriocnaslcuwlhaitcihonasr:e basic to the 1) Tiontailtspreondtiurcettiyo.n is at Chemolite and it is discharged 2) No FC 95 is removed by the treatment facility. 3) All effluent is discharged to the Mississippi River. 4) FC 95 is discharged uniformly. +" 5) nRoitversubfjleocwtantdo salelasoontahlerapnad/roarmetcelrismatairce ccoonnsdtiatnito,ns.hence "The formulae used in these projections include: 1) Mo/mtn - {ERiiYvSeEr EFlIowN, CCFEMM)(CoCnomenrvateornsion,ggaalt[/ffet'))((TTiinmee nmiinn)). 2) MG/min X 1440 = MG/Day : 3) Lhs/day = (mg/l X wt. lbs. H,0 per gal)(G/Day) MlioswsifslsoiwppriecoRridverisfl1o0w,00at0 CHFaSs.tings, MN, based on a 10 year TRhiecketro,talComSm-eyrecairalproCdhuecmtiicoanlsfDiigvuirseisonw.ereInpruotviidleidzibnyg Dt.hesR.e DifunirgtiuhnregesMtihansesipesessrtiiipompdaite1dR9i7v3e-en1rv9i7rb8oe,nlmoewtnhtCeahleEmEoCcloinftcoeerntwFraCast9i5coanwlacsuolfactFaeCldc.u9l5ated ttohebeper5iondg/119a7t8-1H9as8t3inigss,proMNj,ectwehdileatth7engE/E1C. proSjienccetedthefor pwirasotdedurectteciroommnip,anretdFmCetn9ht5atwiiasltlthtehneotepnrvpeirsreeosnnemntetnatnaadnlpursnoirjneekacstofenodarblFleCeve9el5nsviiortfonmental risk. 22661177..00001144 Viel . -10- Conclusions UpnhdyesricotchheemtiecstalcoanndditeinovnisronemmepnltoayledprionpecrhtaireascteofrizFiCng95thite has been determined that this material: 12)) h1asswaatnern-oscoltuabnloel,/wa2t86erpppamrtition coefficient of ~10 23)) iiss rheisgihsltyanmtobitloemiicnroBbriialll sdaengdryadaltoiaomnsoil 5) mIinnnaowconftryrawcatesdrsetduudcye,d stuorvaivsatlatirsatteicaofllythesigfnaitfheiacdant eFCxte9n5.t whNeonotthheerepxaproasmueretercsoncweernetraatdivoenrswealsy 1.9 mg/l affected nleovrelw.as abnormal histopathologi y observed at this dose. 6) woofuladpprhoaxviemaatneleysti7mantge/d1 uenndveirroncmoenndtitailoncso,ncwehnetrreaitnionall uFCni9f5orwmelryeimnatnouftahcetMuirsesdisastipCphiemRoilvietre. and would be discharged 7) may not be biological a metabolite degradation, ahsencaerensoulitncorfeascehemiincaelnvoirronmental 8) FlCeve95l,s uofndeFrC 9t5h.e test conditions described will not present an unreasonable environmental risk. Bibliography 1. Mendanedl', SAu.p,porTte"c,hniJcaanluarRyepo1r7t,. 19"7A9n.alytical Methodology 2. Reinoefr,FluEo.Ar.o,carTbeocnhsnic~alIIIR,epoJrutl:y 19B,iod1e97g6r.adation Studies . 3. Welsahn,d SF.CK.1,43TeocnhnSioicla,l Report. February A27d,sor1p97t8i.on of FC 95 4. US/EMPaAcr-oinMveethrotdesbraftoersAcauntdeATmpohxiibciiatnys,TesEtcowliotghicaFlishR,esearch Series 660/3-75-009, 1975. 5. Unpublished data 6. Chioaun,d CRaordygerT.,L.ViKroghinelrtH:. FrPeaerdt,itiDoanvidCoeW.ffiSccihemendtdianngd, BEinovaicrcounmmuenltaatlionScoifencSeeleancdtedTecOhrngoalnoigcyCh1e1m(i5)c:als4,75-478, 1077. 7. HamaCkheerm,icaJl.sW,., Hu"mIannteHreparletthatiaonnd of Soil Leaching the Environment, Experiments" A CCohlelmeicctailonUSAo,f DMoidwlaSncdi,entMiifcihcigaPnape4r8s6,40.Vol. 1, Dow 22661177..00001155 Sona - -11- . 8. Registry of Toxic Effects of Chemical Substances, +76 Edition, ChristenseH.nE,. and E.J. Fairchild, Eds. p-xvand Ci, U.S, Department of Health, Education and Welfare; National Institute for Occupational Safety and Health, Washington, D.C., June, 1976. 9. Welter, A.N., Technical Report: Aquatic Toxicity Studies: FC 214-30 Lot 566, February 18, 1979. 10. Welter, A.N., Technical Report: Aquatic Toxicity Studies: FC 232 Lot 610, January 17, 1979. - ti 11. ToddU,sinJg.W.S,imuTelcahtneidcaSlunlRiegphotr,t: FC Janu 95/Photolysis ary 9, 1979, St udy 26177..00016