Document 6bKVqz18d4XjjRExy3574GpB9
LG 3S CODE RT-695-D PKG
. JOl 2 3 1982
G2J60
7"7>AT~>#; i LOT NUMBER')
,EST. WT. 2608* LBS -
PREPARATION NOTES :
DmIE FRI NTEI>: A /Q2./S2
PROCESSES \ ) RT-695--D (0)
APPROV JJG 3/18/81
EWK 12/7/81
COMTYP JOB NAME = 36RT695DM0
TYPED BY: KLW
A.
STANDARD HRS.. ____________ TIME //_
NON-BLEEDING
: "BON* RED DARK
1 USE i N-CODE j ACCT
1 LBS l
i LBS
IF,NECESSARY, CLEAN, DRESS SPARKLER & PRE- I
I
if""-
7AT WITH 15* DICALITE FILTER AID
I'__________ 1 77? ~ A i\,,_
OBTAIN FOR S 6 2-CHL0R0-4-AMIN0 TOLUENE-5 1i
I 740-C !
SULFONIC ACID
ji
1
| OBTAIN FOR S 42 3-HYDR0XY-2-NAPHTH0IC ACID|
! 82-C 1
(732G) WATER INTO V-317
POUR IN SODIUM HYDROXIDE ,, _
Mjjfe ,J@L5LS-X
TURN ON AGITATOR & STEAM & DUMP IN FROM S
J2-CHLQRO-4--AM INQ-TOLUENE-5-SULFONIC ACID
LOT
100%
/-wL
ACTIVATED
DICALITE, FILTER
T TO 214-2/4J3EG. F
WffiTCH FOAM
RECORD: BYT < + >, IF NECESSARY ADJUST
+ BY SODIUM HYDROXIDE
ASSUME 50%
-3 MIN. AT 212-214 DEG. F, THEN SHUT
STEAM
WATCH FOAM
RECORD: SPARKLER PRESSURE 2.,,_PSI
IF HOT ZERO, NOTIFY SUPERVISOR
CIRCULATE 15 MIN OR LONGER THRU SPARKLER
UNTIL SOLUTION IS CLEAR
MAINTAIN AT i90~^'5 DEG. F FOR S 15 ^
RECORD: HT.15d &2.F & RFXGRDER_/$DEG.F. ,
RECORD: START/4fS_TOTAL MINJL^CLARITYjQJCJ
*1 C99GY WATER INTO V--100 WHEN S-13 COMPLETE, PUMP V 317 THRU SPARKLER. MAINTAIN V-317 AT ]90>^5 DEG .F RECORD: START&j?fkfTOTAL MIN.XSf
SAMPLE FROM HOSE. SHOW TO SUPV'R FOR OK
N32582
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MAKING INSTRUCTIONSBATCH UNIT
EQUIP HENT
PAGE 02 OF 04 CG 36 CODE RT-695-D (0)
ItiTI WHEN S 13 COMPLETE, CLOSE V-317 OUTLET 6 ] ' I STOP PUMP
i5-TRUN IN 7* (216G) WATER 6 HEAT TO. 190-195 DEG F
| USE I N--CODE | ACCT
! LBS I
1 LBS
]
CIRCULATE THRU SPARKLER UNTIL SOLUTION IS |
I CLEAR
I
MAINTAIN AT 190-1.25 DEG* F FOR S 19 6
i
RECORD: ,HT_/_t5 _DEG, F & RECORDER
!
V RECORD: STARTZ^TOTAL MIN_^.,,CLARITY_^V<J
WHEN S 18 IS COMPLETE, PUMP V-317 THRU ARKLER INTO V-iOO
ar-| RUN IN 5" <90G) WATER & HEAT TO 190-195
L^ce". F 2CIRCULATE 15 MIN THRU SPARKLER, PUMP V-317
SPARKLER INTO V-iOO
HEN MT,' BLOW OUT SPARKLER INTO V-100 HEAT TO 165-170 DEG- F (TAKE 1 QT. SAMPLE)
(WITH AGITATION ON) TEST FOR CLARITY OF SOLUTION- SHOW 1 QTSAMPLE TO SHIFT SUPERVISOR FOR APPROVAL (EXAMPLE OF ACCEPTABLE CLARIFICATION OF N-740-C IS AVAILABLE IN OFFICE TO COMPARE
3 IE>^23 IS OK,- CONTINUE WITH S 25. IF S 23
S NOT ACCEPTABLE, RECLARIFY THRU SPARKLER IF S 23 IS OK, REHEAT V-IOO TO 165-17 DEG- F FOR S 26
100 TO 16" C1590G)
I
6 EAT V-iOO TO 165-170 DEG. F
I
IN V-324 HYDROCHLORIC ACID THRU
AND RINSE IN
M___
IRECT f.%
I nm
I 28-D I 443
R 15 MIN AT 165-170 DEG- F
I
ADJ TO 50* (4199770G) AT 34-38 DEG- F
I
RECORD: Tt eMmpP__JjJJfdOS?._BEG- F AND IF NECESSARY X330I 57-A i 4^/0 0
'I
RECORD: TEH
,_DEG -
57-A [_
sssssssrsarsss
stssssssjsssssssssssss:::
1 07 1145* (4320G 3 WATER INTO V-107
7 %'7ST\ TURN ON AGITATOR AND STEAM AND DUMP IN
V J-^flSHSANESE SULPHATE - . .
IXPr^MP IN BARIUM SULPHATE
iJ>--rtlEAT TO 150-160 DEG- F AND STIR
I JS^T^ECORD : PH
__(5.0-5-5)
I EF PH ABOVE 5.5, ADJ TO PH 5-5 OR LOWER
. r U-SlJLFURIC ACID^_
'ASSUME 78%
l#r3^REC0RD: PH__<?_4?__..
/P&&\LJ18'TE: IF PH BELOW 5-0, DO NOT ADJ UPWARD
L3rn HOLD FOR S 58
I1
1i { 1400 1 I 250 I
\1 II 1 `I Ii 1t
I i 336-B 1 1400 65-A ] 250
i 27-D 1
-#
DUP050463670
MAKING INSTRUCTION":BATCH UNIT
PAGE 03 OF 04 CG 36 CODE RT-695-D (O)
~7~N-C0i)E 1 ACCT I LBS
RUN IN 47" <1610G) WATER INTO V-322
WEIGH AND POUR IN SODIUM HYDROXIDE M JjJL____
..J _/'
j DUMP IN FROM S 2 -HYDR0XY-2-NAPHTH0IC ACID|
LOT
1
7--D 82-C
470 934
WEIGH 1~HYDR0XY-2-NAPHTH0IC ACID ON POSTAL BALANCE AND ADD LOT Z&7S5I?-- HEAT TO 70-90 DEG. F SIFT IN BLANCOL N IN ONE TO TWO MINUTES 1SUMP IN TETRASODIUM PYROPHOSPHATE & STIR 5 MIN OR LONGER TO DISSOLVE
i ! j
i
WEIGH SODIUM NITRITE & POUFt^INTQ V-____ , .. ... , ,
f o r s so
m_.3L_____,
ADJ V-322 TO 65" (2240G) AT 77-30 DEG. F RECORD: TEMP<fc3L___DEG. F
1 SLURRY TRISULPHOIC SOAP D WITH 3 GALS | WATER IN DRUM. POUR IN AND STIR 5 MIN.
160
130-C i 20 2<
36:
39--A
16
.KIL
| (1) IF CR-, KI- ADD 20* "AS IS" INCREMENTS| .
] HYDROCHLORIC ACID .
ASSUME 32%I______
!
RECORD: CR________( + >, !<!_________< + )
!
(2) IF CR+, KI - ADD 20* "AS IS" INCREMENTS!
SODIUM NITRITE /
ASSUME 33%!______
I __ RECORD: CR..........KI_________________< + >
1-
TEMP_________DEG. F
1
m j COUPLE V-322 THRU UNDERSURFACE DISTRIBUTOR I
i INTO V--10O IN 9Q-1 LO MIN (USE 9/16ppRIFICE5 1
I RECO.RD: STMuMfll___ TOTAL MIN..
I
'#fiEN S 53 COMPLETE STIR 15 MIN.
I
RECORD,: DIAZGr^___ <->; SASEjJt__< + )
!
PH_JKf^<7.0-8.0 5 TEMP^L^sDEG. F *60-65 F) |
NOTE:
I
IF PH IS.5.0-7.0, WEIGH AND DUMP IN I
3* "AS IS* N-7-D DILUTED TO 30 GAL \
AFAFVS'O'DIUM HYDROXIDE
ASSUME 50% iw>rL_
PH ADJUSTMENTS USE ONLY -DILUTED !
N-28-D AND N-7-D)
I'
J TO PH 9.0-9.5 (SEE ATTACHED PH ADJ AID)I
HYDROCHLORIC ACID
ASSUME 32% |_____
! (1) IF PH IS 6.5-7.Q, WEIGH 40* AS IS
i
U N-7-D POUR INTO 50 GAL WATER <1/2
i
P
FULL) IN PT & RUN ItyTG CV 100 IN 15
1
I MIN & RINSE IN mjc /.STIR 5 MIN &
I RECORIRD: PH ____<9.0-9.5)
57-A 28-A 725-A
28-D
DUP050463671
EQU]
EQUI MEN
USE
i USE PAGE 04 OF 04 CG 36 CODE RT--695-D (0) I LBS
2) IF PH IS 7.0-7.5, WEIGH 35* AS IS N-7-D f
POUR INTO 50 GAL WATER <1/2 FULL) IN F'T h |
RUN INTO CV 1G0 IN 15 MIN. & RINSE IN PT. !
STIR 5 MIN h RECORD: PH__________ <9.0-9.5) I
3) IF PH IS 7.5-8.0, WEIGH 30* AS IS N-7-D |
POUR INTO 50 GAL WATER <1/2 FULL) IN PT & |
RUN INTO CV 100 IN 15 MIN. RINSE IN PT.
I
STIR 5 MIN 4, RECORD: PH_____________(9.0-9.5) I
4) IF PH IS 8.-8.'57 WEIGH 10* AS IS N-7-D |
POUR INTO SO GAL WATER <1/2 FULL) IN PT & |
RUN INTO CV 10Q IN 15 MIN. & RINSE IN PT. I
STIR 5 MIN St RECORD: PH__________<9.0-9.5) I
5) IF PH IS 8.5-8.9, WEIGH 5* AS IS N-7-D i
POUR INTO 5 GAL WATER <1/2 FULL) IN PT & I
RUN INTO CV 100 IN 15 MIN. &RINSE IN PT. i
IR 5 MIN & RECORD: PH.___$JL_<9,0-9,5>
!
3) IF PH IS ABpVE 9.5, DO NOT ADJUST
1
RECORD: PH_/.ju___SODIUM HYDROXIDE ASSUME 50% I.
NOTE: ADD N-28-D IN 5* "AS IS" INCREMENTS |
TO APPROACH PH 9.0-9.*5 .THEN USE
!
LESS N-28-D HYDROXHLORIC ACID
i
<CONCENTRATED N-28-D & N-7-D AND TOO LOW j
COUPLING TEMPERATURE CAUSES' MASSTONE TO
I
GO TOO LIGHT) .
!
SHUT OFF AGITATOR
I
.
N"COi)b,saJ ACC1 i N--CODE 1 ACCT i i LBS
i
7-D 1.
DURING S 53 HEAT V-107 TO 210-212 DEG. F !
& SHUT OFF STEAM
I
! NOTE: IF NECESSARY REHEAT V-107 TO 210- !
l/212 DEG. F PRIOR TO START OF STRIKE '
!
H! PUMP V-100 INTO V-107 IN 70-75 MIN. i LET V-107 TEMP DROP TO 200-265 DEG. F
I I
I I DURING STRIKE THEN MAINTAIN AT 2O0-205 DEG.1
I I F FOR BALANCE OF STRIKE WITH AGITATORSHUT 1
I I OFF IN V-100
1
I /"RECORD: START <!ilrMjTOTAL MIN__Z2__
I
STRIKE COMPLETE, HEAT TO 210-212 DEG,FI
TIR 15 MIN AT 210-212 DEG. F
I
I FRLEOCOODRDT: O P1H80__-190, <(163.254-070,.2) AND STOP
AGITATOR
START
FINISH
OPERATOR
&
DU P050463672
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DUP050463673
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