Document 6XL2N5wLdkdDn4QnQkZzvqD9
**----v--------. CG 01
COPE Y-E----6--9--8-----D-
SO,! ^'-''''PROCESSES ( ) YE-698-D (T)
A--P--P--R--O---V--E--D BY: FWP 10/15/82
" //&<%? ', :-M"&,..'-BATE >
< LOT )
5527* LBS..
COMTYP JOB NAME : 01YE658DMT
^< EST WT p ^(U jo / #2_Tsr
'Bl e n d e d b a c k -, c g 01 PQ 98, .JJt^LZZT. <COD>
<LOT)
,e q u ip
me n t
NAME: MOLYBDATE ORANGE
PREP ,1
'1 ^OBTAIN SODIUM SULFATE Foi5Ts~13 yK\ CALCULATE 6 SET ON BADGER1 METER F/t <NITRIC ACID WEAK) OBTAIN SODIUM CHLORIDE Fi OBTAIN SODA" ASH F0Rj\S-37 OBTAIN SO/lUM-SILIcfc FDR S-39 OBTAIN S0DA ASH FGRis-43
OBTAIN ANTIMONY TRIQWDE FOR >
WEIGH SODIUM
E INTO OPTR
OPTR _
____ i
Tp o u n d ST
~usiX 7
_ -~ACCT
LBS 1 N-CODE J LBS
1 84 I 108--A I
84
1 33-D 1 60 ?i4 i 4-A I 734 146 | 3-A i 146
237 [ 32-D I 237 350 | 3-A i 350
7 ! 711-B I 70
:2Sl! 10-D j 1885
WEIGH IN SODIUM
TR
it
//gmpiuR
I iUt-U u l u N _ _ l, ^____, /-______ _ ,,__%j
N 1O`l /<500 G) WAT
V-358
iI
RUN V-359 INTO V-351 G PU IN V-351
I!
*irt ADJ TO 55* <2600 G.) SIFT IN N-1G8-A FROM
:a ,
I OCli 251382
4<K'STIR 5 MIN G RECORD:
0-10.0)
r ! ADJ TO PH 9.8-9.9 S RECORD: PH
^
I |
I |
<CAUSTIC SODA SOLUTION)
ASSUME 50%!________
7-D |______
ASSUME 66%|________
3-D I______
ADD N-33-D FROM S 2 USING BADGER METER
1
1 ADJ TO 66" <3J 2A G) AT /&-69*F
|
I * i RECORD: VOLJ?|?_* h __jLJ_fF
I 18^4-^TIR 5 1MJ3INN A RREECCOORRD: PHHl;ZZj*^<7..4-7.6> &
I
i G/ML fJJLILJzt1.080-1 .083)
i
i NOTE IF G/ML OUT OF LIMITS FILL OUT CHECK
i
! j LIST St ATTACH. TAKE 1 QT SAMPLE
SV .5
RUN 20* <996 G) WATER INTO
t I RECORD N-41-D STORAGE TANK TO PUMP FROM.
! CIRCLE ONE: 402 41 411 420 424 425
I OCT 1 CHECK WITH CU S,UPV -
l j * STORAGE TANK MUST CONTAIN AT LEAST 2376
I j GAL: 402=49*, 410=25', 411=48*, 420=25*,
! } 424=25*, 425=31
I t ^STORAGE TANK MUST HAVE STIRRED AT LEAST
f t 20 MIN SINCE LAST ADDITION OR ADJUSTMENT
i 1 ^STORAGE TANK MUST BE ISOLATED UNTIL ALL
I Jr PUMPING FOR THIS BATCH IS COMPLETE
I2T iJS-Ei METER FOR 300 G i, PUMP TO SV
\2&n AT APPROX 100 G WHILE CONTINUING TO PUMP,
j j CHECK PH J. DENSITY. RECORD BELOW. IF NOT
I I IN RANGE, STOP PUMPING fe SEE SUPV. ,Jlrs\
i j * PH &+.Q. <2.2-3.7)
Wr\
r 1 * DENSITY : A^O-Ti- C/ML <1.270-1 .328)^
k.
DUP050103053
LOT. QUIF! HEHT!
COMTYP JOB NAME: 01YE698DH1
PAGE 02 . f':
DATE PRINTED 10/13/82 | .USE | N-r i ACCT
| 'LBS I CODE ! LBS
IF 5-22 OK 4, WHEN S~21. COMPLETE, RECORD
DENSITY
C/ML ON TRAPPED SAMPLE
COM END OF 2-21 PUMPING..
USING DENSITY FROM S-23, FIND METER SETTING FOR
SECOND PUMPING IN TABLE BELOW. NOTE: TABLE
ACCOUNTS FOR 300 G ALREADY PUMPED IN S-21 .
CIRCLE DENSITY i* SETTING IN TABLE BELOW. .
TABLE *#*
f 1 G/ML SETTING I G/ML SETTING | G/ML SETTING 1
! 1 1.270 1 ! 1 .271
! i i . 272 l f 1.273 i i 1 .274 t 1 1 .275 r i 1.276 i i 1 .277
1678 1670
1 663 1656 1649
1 641 1634 1 627
1 1.291 1 1.292 1 1.293 I 1.294
1 1.295 1 1.296 I 1.297 I 1.298
1534 1527 1521 1 51 5 i 509 1503 1497 1490
1 1 .312 1 1 .313 ! 1 .314 ] 1 .315 1 1 .316 | 1.317 | 1 .313 | 1 .319
1410 1404 1399 1394 1388 1333 1 378 1372
1 f t i 1 i 1 l
! 1 .273 1620 1 1 i .279 1 614
! 1 .280 1 607 ! 1 .281 1600
I 1 .282 1593 i: 1 1.283 1586 1 1 .284 i 580 } 1 .285 1573 r 1 .286 1566 f 1 .286 . 1566 1 T .237 1559 1} 1 .288 1553
1 1.299 1484
1 1.3O0 1478
1 1.301 1473
1 1.302 1467
1 1.303 1461
1 1.304 1455
I 1.305 1449
1\rr1:.W30T6~
1 444 J 43A
| 1.307 1438
i 1.308 1432
1 i.309 1 427
| 1 .320 1 1.321
1.322 | 1.323
1.324 1 1 .325
1.326 1 .327 1 .323 1 .328 1 .329 1 .3350
1367
1 362
1357 1351
1346 1341
1336 1331 1326 1326 1543 1537
1
( 1 i
1 1 1 f i
r
i i
I 1 .289' 1546 ! 1.31 1421 1 1 .290 1540 } 1.311 1415
1 .331 1 .332
1532 i 1526 i
2#I ""SET METER & PUMP
G (RECORD FROM TABLE)
1 i
FLUSH LINE WITH WATER INTO SV FOR APPROXIMATELY
SECONDS
ADJ LEAD NITRATE TO 76* (3625 G) AT 67-69*F.
RECORD:___ _*F IMIN & RECORD PH: jSesSi (2 .2-3.7)
|
NECESSARY ADJ.. TO_ PH 3.0-3 ..1
ASSUME 66%i_____
I i & RECORD PH: SiJCL
ASSUME 50% i _J3L
jUQTE: DILUTE H -7-0 ?0:1 WITH WATER BEFORE ADDINGi
RECORD: /-M< G/ML (1.143-1 .144) IF OUT OF SPEC|
ILL OUT CHECK LIST 6 ATTACH.
i
STIR AT 67-69#F FOR S-31. TAKE. 1 QT.SAMPLE.
f
i li ti i!
i! i1
fo 1 i I i' 1 i!
i! i1
ii i 'i \1 i1 rI i1
i1 i '1
i1 ii if f1 11 i1
I I..... 7 1 i -%v tl 41 -D ! 5110 I 57-A I______ .
.1 33--D
_ I. 7-D |
OBTAIN 1 G)T SAMPLES OF S-1S 6 S.-30 SOLUTIONS
|
& TITRATE TWICE
'` '
1
! I NOTIFY SUPV IF ML N-10-D IS NOT IN RANGE
\
! I 7.1-7.4 OR IF THE TWO TITRATIONS DIFFER BY
j
I ! MORE THAN 0.10 ML N-10-D (IF YES, FLUSH ALL |
EQUIPMENT 6 REPEAT TITRATIONS). DO NOT PROCEED I
IF N-10-D TITRATION IS OUT OF RANGE /fiP -- I i ADJUST V-353 FOR A TITRATION PH OPTO
I I FROM- FINAL IN-LINE TITRATION, RECORD LOWEST
I
PH ______ 6 ML N-10-D _____ _
.
I
vV
'W
i 33-r-T_
.1 7-D |_ .
'<
1
1
'.jIi.-W!*&*!..s-i*lrS*'-'
`S'
DUP050103054
LOT; , /Equip
MEN? I
COMTYP JOB NAME: $1
03 DATE PRINTED10/15/82
USE
N- TAC.CT
LBS
CODE 1 LBS
WHEN S-31 TITRATION OK , STRIKE V-358 THRU
|
syrv }
i BOTH UNDERSURFACE DISTRIBUTORS INTO SV IN
}
6 " I I 16-18 MIN
I
y Lv 1
f RECORD: START I#*ZlkTOTALMIN_,,i/__L__
!
I NOTE: STRIKE TIME UP WHEN 1/2 VAT BOTTOM SHOWS |
BUBBLES APPEAR IN SIGHT GLASSES
|
I IMMEDIATELY DUMP IN .N-4-A FROM S 3 & SET TIMER j
OR 15 MINUTES
i
i><J>WRlNG S 33, WASH IN V-358
I
I38"T STIR 2 MIN 6 RECORD PH_J'ti/,,_.< 1 .8-2,5)
I
l^PBXS,__ t L__ MUST BE + ) STIR TOTAL OF 15 MIN FROM S-33 &
i |
RECORD: TEMP__'ZZ.__*F (67-?3#F)
|
DUMP N-3-A FROM S-4
|
STIR 3 MIN
|
JSO^POUR IN N-32-D FROM S-5
.
I
}>^>^STIR 2 MIN
i
!>f^KRUN IN LIQUID ALUM USING BADGERMETER I4^K|JIR 3 MIN.6 FLUSH ALUM LINE WITH WATER
| I
I^SSr'DUMP IN N-3 FROM S-6
j
I^T.l STIR--4 MIN FOR S-48
I i
734 i 115-DI
I
367
i RUN IN HYDROCHLORIC ACID USING WEIGHT 6 FLOW
CONTROL PANEL
MK______ , I d5>l-X\
IU
MK _______ _ _____%
i&tr\ DURING S-44 SIFT N-711-B FROM S-7 INTO V-39
i I WITH AGITATOR ON IN 1-2 MIN .
\&K\ STIR 1-2 MIN TO MILKY SOLUTION
,U7.-/~5
I 1
28-D
.1 28-D
105
SV
ai
I
I WHEN S-44 COMPLETE, IMMEDIATELY RUN IN N-711-B
I SOLUTION GRADUALLY OVER 5 MIN PERIOD INTO SV ] WATCH FOAM!!? IF FOAMING IS EXCESSIVE, STOP
! i-"" UNTIL FOAM SUBSIDES,
|^>*tr0MP IN BLANC FIXE N 15XT I WHEN SCHEDULED, DUMP IN BLEND BACK LISTED ON
TOP OF PAGE 1 3 U-^RECORD : CODE jk
J5fjUTlR 2 MINw/j /c/0 -
t^>->ReCORD: PHWi.7_^^_<5-S"6-0^
IF NECESSARY, ADJ TO PH 5.8-6.'
ASSUME' 5%
& RECORD: PH-____________
ASSUME 66%
FLOOD TO 153- <7298 G> 6 STOP AGITATOR
i" | START
FINISH
%M(SnRKw
7-D |______ 33-D | ____
DUP050103055