Document 6RVymj82VeEJBMNk4VY1KyQrg

Waste Material Data Sheet GENERAL INFORMATION- ENSCO CLIENT Invoice Address Cert Address fiff N/AD Contact________ Customer Name Address_______ yJ.Hrs*>r*-* City ___ State__________ Zip. Phone # ____ ___ USEPA ID# WASTE DESCRIPTION NAME OF WASTE _LL- PROCESS GENERATING WASTE waste treatment unit SHIPPING FACILITY Contact_____ Facility Name. Address City____ State___ Phone # USEPA 10 #. No. Regional Office Invoice AddressX Cert Address N/AC -jest .Zip. GENERAL CHARACTERISTICS (at 70 F unless otherwise specified) r.oi or Black LIQUID *0 % PHASES odor yes SOLID % (X SINGLE LAYER NONE 8 STRONG SLUDGE % DOUBLE LAYER MILD POWDER % MULTI-LAYER NFPA HAZARD CODE Enclose copies of safety data sheets applicable to waste. Include data constituents of waste and materials used in process. SPECIAL HANDLING INSTRUCTIONS If special handling techniques are required, specify: Use OSHA approved equipment__________________________________ HEALTH REACTIVf fai RCRA INFORMATION W Is this a USEPA hazardous waste? Please give USEPA hazardous waste codes: Oo not include state waste codes in this section. F024 D001 DO 18 D021 -DQ33- jmD02a2. D027 D04Q Describe nature of reactivity it D003 waste: DO 19 D032 Mf SHIPPING INFORMATION DOT hazardous material PROPER SHIPPING name Waste Flammable Liguid, n7o. s. (contains Jfchvlene dichloride.Tetrachloroethene) hazardCLASSFj-^TM^^le io# NA 1993 r/q lib. _-R ANTICIPATED SHIPPING VOLUME_________GAI_______ YDS. 25-*UQCLBS. ------------- DRUM(S). BULK X TANK TRUCK X RAIL X ONETIME WK MO XJYR Type and size of container Tank Truck OTHER GUT ~wSPECIFIC GRAVITY VISCOSITY (centipoise) <0.8 0.8-1.0 [J1.4-1.7 >1.7 (Xl-100 n 37 ectuai 100-1000 1.0-1.2 1.2-1.4 n 1.44 actual 1000-10.000 > 10.000 WT PER CONTAINER:____ ASH (HWT) <0.1 "" SOLIDS (HWT) 0.1-1.0 <0.5 > 20 1.0-5.0 0.S-2.0 aso-2o n ectuai P >20 2.0-5.0 5.0-20 C'" _ WT PER GALLON: 1 4J lbs. BTU's 1000/lb. <2 R?-fi '__ 6-8 a>20 LO actual ,, 8-10_ coniWufil 10-12.5 EK1 012-16 B 1-4 ^ >16 4-6 6-8 actual 8-12 FLASHPOINT (closed cup; SULFUR (HWT) [<100 F >200 F <0.5 >5 100-140 F ________ 0.5-2.0 UNK 140-200 F *** 2-5 U HAZARDOUS CHARACTERISTICS ANO OTHER COMPONENTS HALOGENS (H) Clorine 70 Fluorine. Bromine _ Iodine ~" ' ARE METAL OBJECTS PRESENT IN THE WASTE? YD NR IF YES. DESCRIBE IN SECITON I Reactivity: (X None Explosive Pyrophonc Shock Sensitive Fuming /Smoking Waste Water Reactive Air Reactive Radioactive Biological Asbestos Cyanides --UNK-- (ppm) PCB's ^ 5fl____ (ppm) Acutely Hazardous Waste Sulfides------ UNK (ppm) Phenolics UMK____ (ppm) Dioxins & Furans ||t] METAL TOTAL (PPM) DTCLP (mg/L) Antimony (Sb) UNK__ ____ CHEMICAL COMPOSITION (If actual percentages are not known use ranges) Total should be at least 100% Actual Solids (carbon ____ % Fed? _LL% f.hl nrinateH % HyHrnrarhrvns r % (mlxt-in-p nf Pi % _az% -Hszane .03 % Carbon Tetra- % chloride 0.1% chloroform 0.11% Range -- % --% --% --% 80 - 90 % __Q_--_J__% --% 0- 1% 0 -.... 1 % chlorobenzene 1.4 DCB HCB HCBD EDC Trichlor PerChlor 1,1,2 Tri TCE's 1.1-DCE Actual 0.6 % 0.9 m. 1.1 0*. 5.2 % 3.4 % 0.3 % 8.0 % 3.4 % 4.0 * 0.6 % !^Rta.ct-iiT---ir-T-HaT*u-*-c-iE0n^oUiiC*T/nAla0n&HJE)CwTi$>A&MA CoO*Fu0TTnTMUC>NBt OiFo<WaA4SiTtEH. BNAcV<E >BW&VLOiHBC*LMOQ)IOrfuJifia>t>tMui()(oiiitii44uawcnD' w-H. corPER ENV. CRTL. SPEC. 11-20-91 Range Arsenic (As)Qj_1 Barium (Ba)21 Beryllium (Be) _ UNK % Cadmium (Cd)_ 1- 5% Chromium (Cr). 2JL 1_ 5% Lead (Pb)____ 1Q.Q- 5_10 Ok Mercury (Hg) __ Q.Q2 1 - 10 % Selenium (Se) _ JL_L 1 _ 10 % Silver (Ag)____ 10 _20 % Thallium (Th) _ 5.0 10 __ 20 % Other (Specify) 10_2 (u, 0 _1 % Cu - 8.9 Ail Binu Must Be Completed it meteHsi is/r not pfeeem. indicate "None SL 021465 --LNSTO USE (JNLV------------------ From: American Laboratories and Research Services, Inc. P.o. BOX 15609 Hattiesburg, MS 39402-5609 601-264-9320 Date: February 6, 1991 To: Mr. Gerald L. Perry PPG industries Chemicals Division p. 0. Box 1000 Lake Charles, LA 70602 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: Sample I.D. AA07095 Sample location: 1002GP LabLog 1520 Classifier Solids collected by: GPP Collection date: 01/31/91 Time Laboratory submittal date: 01/31/91 Time: 15:57 Received by: RLH Validated by: RLH Parameter: TCLP Extraction Method reference: SW846-1311 Result: done Date started: 02/01/91 Time started: 16:00 Parameter: Mercury, TCLP Method reference: SW846-7470 Result: .009 mg/L Date started: 02/05/91 Time started: 08:30 Parameter: Mercury, Total Method reference: SW846-7470 Result: 1.25 mg/L Date started: 02/05/91 Time started: 08:30 SL 021466 Date finished: 02/02/9: Analyst: BLM MDL or sensitivity: .0 Date finished: 02/05/9 Analyst: BLM MDL or sensitivity: .c Date finished: C2/C5/S Analyst: BLM 501-863-7173 P*virrnrTvriiaJ svsie^ > jn>oan> JANUARY I 1 , i'yyi -'nencan On Roaa - r' Box ! 957 r I ;raao Arkansas i ' 731 195" PPG INDUSTRIES, iNC . aTTNi GERALD CLARK P.U. RUX 1000 LAKE CHARLES RU 9-------------------------DATE RECEIVED-- 01/14/yi oAMPLE: LA /ObOJ INCINERATOR i LED <bO rPM RCB 'I w AMP LE -r LS OOlGlSyS TESTS SPECIFIC GRAVITY PH BTU/LB & CHLORIDE s SULFATE VISCUSITY PLASH POINT F COMPATIBILITY = YES RESULTS = = = = < = > ' 1.44 4,00 b,y17.00 S4.0W 1.00 i 7.OO 140.00 RAGE E. a. PEDEN TECHNICAL MANAGER . UF 1 Si 21467 * Waste Material Data Sheet no. 13 GENERAL INFORMATION CUSTOMER INFO Invoice Address Cert AddresaJD N/AD GERALD L. PERRY________________ SHIPPING FACILITY Invoice Address!] Cert Address N/A C Contact.._____ GINGER BUSBY_____ ustomer Name PPG INDUSTRIES, Address____ P0 BOX 1000 CityLAKE CHARLES State Phone # LOUISIANA 7.P 70602 318-491-4370 USEPA ID# LAD008086506 INC. Facility Name_ PPG INDUSTRIES. INC. Address______ P.0. BOX 1000 City - LAKE CHARLES State LOUISIANA___ Zip 7Q6Q2 Phone # 318-491-4500 USEPA ID # LADQ08086506 Generator Name (if different) rrnssTEBESCWW1W r" NAME OF WASTE Incinerator Feed<50pptn PCB& 1 PPRROO<CESS GENERATING WASTE WTU MgGeEmNiERAL CHARACTERISTICS (at 70* F unless otherwise specified) COLOR Black________ (3 LIQUID 1 On % FREE PHASES ODOR yRB SOLID SINGLE LAYER Mnfpa hazard code' FLAMMABLE HEALTH REACTIVE NONE HETRONG SLUDGE DOUBLE LAYER MILD POWDER MULTI-LAYER SPECIAL HANDLING INSTRUCTIONS If special handling techniques are required, specify;. Use proper protective equipment. Is a representative sample provided? Yes II No Sample Purchase Order No.. RCRA INFORMATION X Is this a USEPA hazardous waste? Please give USEPA hazardous waste codes: F024 D021 D033 D001 D022 D039 DO18 D027 D040 iribe nature of reactivity if 0003 waste: DO 19 D032 SHIPPING INFORMATION DOT hazardous material x PROPER SHIPPINMGGfmi--a-m---f^W--aste Flammable liquid.n.o.s.* HAZARD CLASS Ll^Tj 6__ ID# ANTICIPATED VOLUMEGAL _____ DRUM(S), BULK 1 RAIL ONETIME WK MO SYR Type and size of container Tank Truck WT PER CONTAINER:____ WT PER GALLON:________ JAUl SPECIFIC GRAVITY <0.8 0.8-1.0 1.0-1.2 K) 1.2-1.4 XXI .4-1.7 >1.7 n dual VISCOSITY (centipoiaa) 1-100 ___ u. 100-1000 1000-10,000 > 10,000 ASH (%WT) <0.1 0.1-1.0 1.0-5.0 sisn-nn n >20 TOTAL8U8PENDE0 SOLIDS (HWT) <0.5 nns-jn 2.0-5.0 5.0-20 > 20 u PH <2 >12.5 2-6 6-8 n R.m -NA------- 10-12.5 PI BTU's 1000/lbs. jQ<1 12-16 XH1-4 >16 4-8 ___________ 8-12 | FLASH POINT (closed cup) SULFUR (MWT) OKIOOF >200F <0.5 0 >5 100-140 F _________ 0.5-2.0 -D- 140-200 F 2-5 |f|AZARDOUS CHARACTERISTICS AND OTHER COMPONENTS HALOGENS (%) Chlorine 70 Fluonne -0 Bromine 0- Iodine 0" Reactivity: $None Explosive Pyrophoric Shock Sensitive Water Reactive Etkkogical Cyanidea (ppm) PC8`s___ ^*50 Sulfides (ppm) Pheoodcs 1 *-i Radioactive Acutely Hazardous Waste t(ppm) Pesticides WOT HJI iXMV D________ (ppm)____________ `PRESAIfT _ Til METAL STOTAL (PPM) EPAEP(mg/Lj Arsenic (As)__ < 0.10_______ Barium (Bs)__ 27_________ Cadmium (Cd). < 0.50 Chromium (Cr) < 2.0 Mercury (Hg) _ < 0.02 (Pb)------- < 10.0 Chromium-Hex (Cr+6) Xl-flot TesrpH Selenium (Se) . 10 CHEMICAL COMPOSITION (MUST TOTAL 100%) I Solids (carbon. iJibM 1,4- Dichlarobenzaie t FeClgA 1 1% Hexachlorobenzene i Chlorinated Hvdrn- 80-90% Hexachloro-1.3-butadiene rarhnns (mixture nf 1 1% Ethylene Dichloride , Ci-G^L i i% Trirh1nrrvrhvl(=n(s 1 Benzene Perch! nrnTphyImp i ------Carbon Tetrachloi=i4e IW-W 1 -1 T2-THrhlnrnpt-h3iv> I thlorofomOilnrobenymp 1 o-i l% 1.1-Dirhlnrnprhanp_____1 I HEREBY CERTIFY THAT ALL INFORMATION SUBMITTE6 IN THIS AND ALL ATTACHED DOCUMENTS IS COMPLETE ANO ACCURATE. AND THAT ALL KNOWN OR SUSPECTED HAZARDS HAVE BEEN DISCLOSED 1 1"5 1% 1 1~5 1% 1 5-10i% 1 1~10|% i i-i rn% l _lQ=26t> i 10-7Rfc 140=206 1 Or! 1% Silver (Ag)____ Copper (Cu) -- Nickel (Ni)____ Zinc (Zn)------Thallium (Ti) _ Other (Specify). M. < 2.0 11. < 5*0. PC / WSE ENSCO USE ONLY AUTHORKED StQNATURE ENV.CTRL.SPEC. -J tttle RECERTIFICATION DATE 02l4gg gnvtomixntu syswms company LAND DISPOSAL RESTRICTION NOTIFICATION FORM SECTION I Manifest No.:_______________________________ Generator Name: PPG INDUSTRIES INC. WMDS No.(s): ^1599 Address:1300 Columbia Southern Road Completed By: Lake Charles, LA_________________________ Title:--F_nvi_Ecinmant-ai USEPA ID No.: LAD008086506_____________ Date: __ ________ (Continuation Sheets may be attached and are numbered accordingly: Page_________________of) Spg^jalj SECTION II SPENT SOLVENT WASTE (268.30) AND CALIFORNIA LIST WASTE (268.32) (Check Here) | 1 A. Spent Solvent Wastes The shipment, as referenced by the above manifest number, contains waste(s) which correspond to USEPA Hazardous Wast Codefs) ______ _________ IThe above referenced waste(s) must be treated to meet the treatment standard expressed as Constituent Concentration in lie Waste Extract as outlined in 40 CFR 268.41 Table CCWE below. Tadte CCWE--Constituent Concentrations m Mam Extract F001-F005 Scant Solvants Acetone n-Butyl aiconoi Carlton aisuihde Caroon tetracniorKle Chtorooenzene Creeota land creaytic acid) Cycionexanone 1 2-DicmoroOeniene Ethyl acetate Ethytoenzene Ethyl etner ISOOUtVNM Methanol Metnyiene chloride Metnytene cnloride nrom tne onarma- ceutical industry) Metrtyi etnyt Ketone Metnyi isooutyl Ketone Nitrooenzene PyrwJm# Tetracnioroetnytene Toluene ' 1 iTriehioroetnane 1 2-Tricnioro-i 2 2 Trifluoroetnane cntoroMrrvtene cmoroiiuorometnane Xylene wuMwttr containing sewm &otvwns 0 05 5Q t 05 05 15 2.62 125 65 05 05 05 so 25 20 12 7 0 05 0 05 0 66 i "2 . 0 079 1 12 i 05 ' 05 0 062 0 05 0 05 Concentration (in mg/ll All Other soont solvent a*i*4 0 59 50 481 96 05 75 75 125 75 053 75 so 75 96 96 0 75 3 33 0 125 0 33 0 05 0 33 0 41 0 96 0 091 0 96 0 15 I I --If indicated by X." any or all of the above specified waste codes are referenced to Certification Statement Section Vl. X" here, it aoDiicaoie SL 021469 SECTION IV LAB PACK CERTIFICATION In accordance with 40 CFR 268.7(a)(7) and (8) and regarding those lab pack wastes corresponding to USEPA Hazardous Waste Code(s) identified as restricted wastes contained in this shipment and referenced by the above manifest no., I submit the following certification statement(s) where applicable: Appendix IV Lab Pack Wastes (Organometallic) i certify unoar oanany o* law mat I oaraonailv nava atammad ana am tamitiar wnn tna waata ana mat tna lao oae* comaTM only ma wavaa toacrtiad m Aoowndu IV to san 266 or unto waataa not suotact to raQuiatton undar 40 CFR Pan 261.1 am awata mat mora ara wgmheant oanamaa lor suommmg a tataa eantttoauon. including ma pooaiouitv of Ima or imonaonman Appendix V Lab Pack Wastes (Organic) unoaf <0 CFR Pan 261. I am awara mat itwra ara aigniticam panamaa nr auomtmng a faiia cartincation. including tna ooaaioility of tma or impnaorwnam Lab Pack Wastes with hazardous waste codes not specified by EPA in Appendix IV or V are referenced in Section III of this form. SECTION V RESTRICTED WASTE SUBJECT TO AN EXTENSION IN THE EFFECTIVE DATE (40 CFR 268 Appendix VII & VIII) Th wastes contained in this shipment as referenced by the above manifest no. which are subject to an Extension in the Effective Date in accordance with 40 CFR Subpart C are identified below: USEPA Hazardous Waste Code/ Treatability Group (NWW or WW) Extension Date (These wastes may be subject to the California List Prohibitions) SECTION VI CERTIFICATION OF RESTRICTED WASTE WHICH MAY BE LAND DISPOSED WITHOUT FURTHER TREATMENT In accordance with 268.7(a)(2) and regarding those restricted waste(s) contained in this shipment, these waste(s) may be land disposed without further treatment. I submit the following certification statement: i candy unoaf oanany of law mat t DdiaonMy nava aaammao and am laminar wim ma waata mrougn anaivaia and tatting or mrougn vnowtooga ot ma waata to auooon mu codification mat tna waata comouaa witnmttiatimtnmanoarataoaciliao map CFR Pan 266 Support D ana ttitcpiicaottoioninitiiint tat Wnn into CFR 268.32 or RCRA aacnon 300410). I oanova mat ma information I auommaa It tma. accutatt and comptatt t am awara mat mara ara aignificant oanaaiaa lor auomttitng a tana eamheation. including ma Signature Title ate (This certification is referenced to the appropriate USEPA Hazardous Code(s) in the foregoing appropriate Sections II or III). Waste analysis is attached where available, otherwise, the information contained herein is based upon my thorough knowledge of the waste(s). I hereby certify that all information submitted in this document is complete and accurate to the best of my knowledge and information. Signature Title , Date GKH 7/90 ensco ccihov>v Sl 2U70 51-701 WASTE analysis report environmental Laboratory PPG Industries. Inc., Lake Charles, La. ^mple: Incinerator Feed from WTU. Location of Sample: Composite made from daily Lab samples. sample Collector: G. P re.lean Sample Method/Device: Composite - bottle Date/Time of Sampling 11-14-90 9:30 am Date All Analyses Completed: 11-30-90 Report Submitted By: Date: Gary Prejean 12-10-90 ANALYSIS RESULTS Test Parameters | Ienitabilitv ( \S) N/A | Corrosivity pH j ( w'f N/A inch/vr | Reactivitv j Standard 140F 2-12.5 0.250 max Lab 1 i i Log (^' N/A TCLP Toxicity (mg/L) A/ W1 N/A | As |Ba |Cd |Cr |Pb j He | Se |A i 1 5.0 max 100.0 max 1.0 max 5.0 max 5.0 max 0.2 max 1.0 max 5.0 max Other Parameters (if needed ) ( ) n/a ND/none detected i 1 CHLORINATED'HYDROCARBONS' ( %) | Chloroethene (VC ) | Chloroethane (EC ). Dichiormethane < MeC12 ) j 1.1-Dichloroethene ( VDC )i 1A1-Dichloroethane ( DCE ) 1,2-Dichloroethene (cls/trans) Trichioromethane (CHC13.) L. 2-Dichloroethane (EDO 1.1.1-Trichloroethane ( MC ) Tetrachioro^^^hane (CC14 ) Tnchloroethene (Trichlor ) 1 * 1.2-Trichloroethane (TCE ) Tetrachlorethene (Perchlor) 1,1,1.2-Tetrachloroethane (unsvm) 1.1.2,2-Tetrachloroethane ( svm i Pentachloroethane (Penta) para-Dichlorobenzene (d-DCB ) Hexachioroethane (HEXA ) Hexachlorobutadiene (HCBD ) Unknown CIHC Total C1HC (% i i Sample , No 1463 ii ii I.,- i. ---- i! ! .... ! 1 ......... | 1 | 1 1 1 | 1 j ......... 1 i | i I PCBs | Heat l j t| j Value I i ... i Chlorinej Water Densitv 1 i i i .. .... i Ash i | Sodium i -------- ! I DDm 1 ! BTl'/lo i .. i %j 1 wt% i .. 4 e/ml ! ..... 1 wt% i wt% ..........| | | | 1 ! I TFST PROCEDURE RAMETER METHOD USED LAB LOG NO. 1463 Ignitabi1ity Penskv-Martens Closed Cup Tester ASTM Standard D-93-79 Setaflash Closed Cup Tester ASTM Standard D-3278-78 Otner (Specif;- Corrosivity (pH ) *A/a ____SW-846 Method 9040 pH measurement . Other (Specify) Corrosivity (inch/yr) wAI/A National Association of Corrosion Engineers Standard TM-01-69 Other (Specify) Reactivity -A/a ( One affirmative answer will classify waste reactive) 1. Normally unstable without detonating? Reacts violently with water? Forms potentially explosive mixture with water? Cvanide or sulfide bearing waste which can generate toxic gases, vapor or fumes under pH conditions between 1 and 12.5? Capable of detonation or explosive reaction if subjected to strong initiating source or if heated under confinement? Readily capable of detonation or explosive decomposition o r reaction at standard temperature and pressure? Forbidden Class A, or Class B explosive as defined in 49CFR 173.51, 173.53, and/or 173.88? TCLP* 1A *Toxicity Parameter SW 846 SW 846 SW 84 6 Method Parameter Method Parameter Method As 6010 Ac Ba 6010 C1HC Cd 6010 Sodium Cr 6010 pH Pb 6010 JiS_ Se 7470 6010 Characteristic Leaching Procedure 6010 5030 3050.6010 9045 PCP LD-1571 C1HC L D -1 5 61 Heat Value LD-2513P Chlorine LD-256CL Water iLD-25 61 Ash iLD-156I LABORATORY IDENTIFICATION Laboratory: PPG Lake Charles Analyst(s): American Labs _____________ Test Parameters Analyzed and Date Total volatile organics11-19-90 Total semi-volatile ora.________ 11-30-90_______ SL 021479 From: American Laboratories and Research Services, Inc. P.0. Box 15609 Hattiesburg, MS 39402-5609 601-264-9320 Date: November 30, 1990 To: Mr. William H. Cooper PPG Industries Chemicals Division P.o. Box 1000 Lake Charles, LA 70602 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: Sample I.D. AA06087 Sample location: PPGHC LabLogl463-Incinerator Feed Collected by: GPP Collection date: 11/14/90 Time: 9:30 Laboratory submittal date: 11/15/90 Time: 19:45 Received by: RLH Validated by: RLH Parameter: Volatile Organics Method reference: SW846-8240 Result: see appended report Date started: 11/19/90 Time started: 22:04 Parameter: Semi-Volatile Organics Method reference: SW846-8270 Result: see appended report Date started: 11/30/90 Time started: 16:06 Date finished: 11/19/90 Analyst: BB Date finished: 11/30/90 Analyst: LWL SL 021473 Mr. William H. Cooper Page: 2 November 30, 1990 Sample I.D. AAou087 (continued) Data for Volatile Organics mg/Kg (ppm) Component Name Chloromethane Bromomethane vinyl Chloride Chloroethane Methylene Chloride 1.1-Dichloroethene 1.1-Dichloroethane trans-1,2-Dichloroethene Chloroform 1.2-Dichloroethane 1,1,1-Trichloroethane Carbon Tetrachloride Bromodichloromethane 1.2-Dichloropropane t-l,3-Dichloropropene Trichloroethene Dibromochloromethane 1.1.2-Trichloroethane Benzene c-l,3-Dichloropropene Bromoform Tetrachloroethene 1.1.2.2-Tetrachloroethane Toluene Chlorobenzene Ethylbenzene Xylene, total c-l,2-Dichloroethene 1.1.1.2-Tetrachloroethane Concentration Not Det Not Det Not Det Not Det Not Det Not Det 600 Not Det 1100 34000 2500 990 Not Det Not Det Not Det 3600 Not Det 120000 300 Not Det 150 80000 74000 140 6200 150 420 Not Det 9200 Component MDL 50 50 50 50 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 Data for Semi-Volatile Organics mg/Kg Component Name Phenol bis(2-chloroethyl) Ether 2-Chlorophenol 1.3- Dichlorobenzene 1.4- Dichlorobenzene 1,2-Dichlorobenzene bis(2-Chloroisopropyl) Ether Concentration Not Det 6700 Not Det 1800 9500 5800 Not Det Component MDL 300 300 300 300 300 300 300 SL 021474 Mr. William H. Cooper Page: 3 November 30, 1990 Sample I.D. AAuti087 (continued) Data for Semi-Volatile Organics (continued) Component Name Concentration N-Nitroso-di-n-propylamine Hexachloroethane Nitrobenzene Isophorone 2-Nitrophenol 2.4- Dimethylphenol bis(2-Chloroethoxy) Methane 2.4- Dichlorophenol 1.2.4- Trichlorobenzene Naphthalene Hexachlorobutadiene 4-Chloro~3-methylphenol Hexachlorocyclopentadiene 2.4.6- Trichlorophenol 2-Chloronaphthalene Dimethyl Phthalate Acenaphthylene Acenaphthene 2.4- Dinitrophenol 4-Nitrophenol 2.4- Dinitrotoluene 2.6- Dinitrotoluene Diethylphthalate 4-Chlorophenyl-phenylether Fluorene 4.6- Dinitro-2-methylphenol N-Nitrosodiphenylamine 4-Bromophenylphenyl ether Hexachlorobenzene P ntachlorophenol Phenanthrene Anthracene Di-n-Butylphthalate Fluoranthene Pyrene Butylbenzylphthalate 3,3'-Dichlorobenzidine Benzo(a)anthracene bis(2-Ethylhexyl) Phthalate Chrysene Di-n-octyl Phthalate Benzo(b)fluoranthene Benzo(k)fluoranthene Benzo(a)pyrene Indeno(1,2,3-c,d)pyrene Dibenzo(a,h)anthracene Not Det 15000 Not Det Not Det Not Det Not Det Not Det Not Det 13000 1400 52000 Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det 11000 Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Component MDL 300 300 300 300 300 300 300 300 300 300 300 300 300 300 300 300 300 300 1500 1500 300 300 300 300 300 1500 300 300 300 1500 300 300 300 300 300 300 600 300 300 300 300 300 300 300 300 300 si 021475 * Mr. William H. Cooper Page: 4 November 30, 1990 Sample I.D. AA0u087 (continued) Data for Semi-Volatile Organics (continued) Component Name Benzo(g,h,i)perylene Benzidine alpha-BHC beta-BHC delta-BHC gamma-BHC Heptachlor Aldrin Heptachlor Epoxide Endosulfan I Di ldrin 4,4'-DDE Endrin Endosulfan II 4,4'-DDD Endosulfan Sulfate 4,4"-DDT Methoxychlor Endrin Aldehyde alpha-chlordane gamma-Chlordane Toxaphene Aroclor-1016 Aroclor-1221 Aroclor-1232 Aroclor-1242 Aroclor-1248 Aroclor-1254 Aroclor-1260 1,2-Diphenylhydrazine N-Nitrosodimethylamine Concentration Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Component MDL 300 2400 300 300 300 300 300 300 300 300 300 300 300 300 300 300 300 300 300 300 300 600 300 300 300 300 300 600 600 300 300 Comments: Reference Lab Report No. R1670. 4 >6