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. o4mm. TECHNICAL REPORT SUMMARY [T7307 - 7 vo. vecumica. couunicarions ceuren - o120n [ER T---------------- ~ Tee JAAnH | Central fescorch = Mnalvedeal| esp 1 rrse--22 0, andCharacterization. : Siz A977 Smmery FoR te _Nigpolde To JonBelisle and D.F. Hagen soz re doo 2608 mh 442R9O0D comin Soames |SSP 5 Bram onTM Continue to develop methods and analyze incoming samples.| GCehnetnriaclalR/eNsaeiayracths TFrlaucoer/oacnhaelnyisciasl ./|E REPORT ABSTBu RoAeCT (B20e0s.75A0marciaTmhiyssSaiactHinRfSDor.m4 2 attribiutoednby theTechnicsComemunicationsGCoon w : acM{sheeeet'nmhvioiicdnrasolntsmhaereeFntCpa-ral2ov6cae/iss1lts4au3bdlioeefasn)dLf.eoirFnCgT-th9he5aepmpiaelnntiahelsodyedsrsiutsmohaowovfniednfebAl;buecocerTrov-aenrd, | 5f3o0raaCovtoahmieplraobulnbedi.olFoHg-i3c4a2l2 sinampulreisn.e anIdn sadedriutmiosnh,oul4dmesvoohned | | ] we peiyr | aM CONFIDENTIAL 114488..000011 EExxhhiibbiitt mmm| 111148 State of Minnesota v. 3M Co., Court File No. 27-CV-10-28862 wows FWtelouoctrohoencthipenrnuoiejceactltosd"eiDvneetlteohrepmiEmnenatvthiiorodonsnmaenandntd"C.haanarlayczteeriszaamtpiloens orfelTartaicvee Definitions Fi 3422: CyFy75028 (Calis) Ctlgon Fe-26: cyRpscoon FC-143: CyPysco0Ny FC-95: CoR1psogK it Report i fhp(all1)sausomrbaieT,deoanttaselaedrpupfmdll,riuieondarkniidntneoglaiawvnadektrneoirwsn,naomrpgulareinniecdowsfnalmupotloreid0eb.u0t1inGppuame.whtoolTentheebmleouocedhs,edof {5 is approximately 1 ppm. the background inorganic fluoride if (2) FC-26/143 in serum down to 0.1 ppm (3) FC-26/143 in "xine down to 0.1 ppm (4) FC-26/143 in zat liver down to 0.5 ppm (5) FC-95 in serum down to 1 ppm C1CAo03n0Ppc/9u2eCm0nOb0t0o)rHr,atoiifFnoCn-sr4ee3orl/fuamtCFe-Cd(7-G03aC5nicanolflryousrmmeansturlh1iai0nvveee.r1b/8efernossmcnat-roorxciieccdaolnoeogu/itP.coarlasFiosirt-udceyxamapnlde, Of FP 3422 from blood and urine by diWreechtaveGCboengunCartbhoevaasmai2y4eis ZH3eeH,atchtoainddon1a) cwiciteshptbeaPd-sedffoorolnlpouwPbeadlrircbayotxiyGoCg.nen bybItomAbnhaaslcyobtmoibocunasltWiroBinitotacenhnde,mitscrtlireeyst:ehiydlsibrlanol mMeetthhaondes a2n-4d) Gearxe based on hexane/ether extracts followed by diazo- fsNuoelrtfmhoaontdyilo5n)cohiflsorbtihadeseedphferonnoymlotthheeesrtesruelxaftnordnaicctGCi.oancidandusitnhge pHorleyparfaotliloonveyofbythe 11114488..00000022 3MAO0016496. A nunber of experiments have been done with lic labeled FC~95 The following is a list of the analytical requests completed the " Attached are 2 letters from the toxicology lab to emphasize the { Ae pT. | G5o:n Belisie D. F. Hagen i} 11148..000003