Document 6BaqXnx9OqwYz2KxB7o4qwqQd

AR 226 -077 MICROBICS MICROTOX TOXICITY TEST IESTSUBSTANCE Identity: ArefmeirxrteudretocaonstPaiFnOiSng,pFeCr-f9l5uo,roorocatsanaescuolmfponoanteen,twhoficFhC-m7a8y7aolrsoFCb-e 787X. (1-Octanesulfonic acid) (CAS # 2795-39-3). Remarks: 787. Current Tihnfeor3mMatpiroondiuncdtiicoantelsotitniusmabmeirxtwuarseo1f010..7T3h%e test sample PFOS, 10% is FC- pdireotphaynleenSeugllytcoonl fmooanmoebru,ty0l.7e3th%ers,o7d9i.um74o%ctwyaltseurl,fa5te%, 0et.h7y3l%enseogdliyucoml,de1c.y4l7% sulfate, 0.75% xanthan chloroallyi)hexaminium gchuimo,rid0e.,7a5n%dm0a.g0n5e%sibeunmzosturlifaatzeo,le0..10% N-(3- Tchhaerafcotlleorwiiznegd scounmcmeantrryataipopnlsieosftiompaumriitxiteusr.e Dwaittha imnacyomnpoltetaeclcyurately reflect the toxicity of the fluorochemical component of the test sample. METHOD: Method: Microbics Microtox "BASIC" Procedure Tost type: Acute static GLP: No Year Completed: 1990. SAnpaelcyiteisc:alPmhoontiotboarcitnegr:iupmHphaonsdpohsomroetuicm condition. Exposure Statistical pmeertihodo:ds3:0-EmCin5u0tevsalues calculated by statistical linear regression pTersotgroarmgparnoivsimdesdofuorrcMei:crMoitcoroxbics' Reagent. Test coDnidliuteinotn:s:Microbics 2% NaCl solution TSetsotckteamnpdertaetsutrseo:luNtoitonnoptreedp.aration: A primary 2000 mg/L. stock - sooflMuitliloinpowraesMiplrle-paQrTMewdatbeyrd.isTsholevipnHg 200 mgoftest material in 100 of the stock solution was then mL. `awdajsusmtaeddefruosmin5g.52t0o06m.8guNsianCgl ddiilsusteolNvaedOHin. 10AnmLosmstootcikc saodljutuisotnm.enAtll tEexstpossoluurteiovnesswseerles:ma4dmeLbcyupvreotptoerst.ional dilutions. a NNumu berm ooffrb ceopnlce iecnattr resa:tiotnwso: Four plus a blank control Element basis: Percent light loss. RESOWTS 002617 Nominal concentrations: Blank control, 125, 250, 500, and 1000 mg/L Element value: 155--mmiinnuuteteEECCsso==332050(3(02040--~36207)0)mgm/gL/L 30-minute ECso = 210 (200 -- 230) mg/L Element values based on nominal concentrations. RSuebmsatraknsc:e TReesmtianrgkwsafsielcdo. nTduhcetveadlouensthreepmoirxtteudraepapslydetosctrhiabtemdixitnutrheeaTnedstnot the fluorochemical proportion alone. CONCLUSIONS Tdehteetremsitnseudbtsotabnec2e1300-mmgi/nLutweitEh Cas9f5o%r Pchoontfoibdaenccteeriinutemrvpahloosfp2h0o0retoum23w0as mg/L. Submitter: 3M Company, Environmental Laboratory, P.O. Box 33331, St. Paul, MN, 55133 patAQUALTY tReeslitaibnigl.ityH:owKeiviemri,scthhreasnkaimnpgle2. The purity swtausdynomteeptrospterhleycrcihtaerriaactfoerriqzueadliatynd the study lacks analytical confirmationofthe amountoffluorochemical proportion in the solution. REFERENCES This study was conducted by the 3M Environmental Laboratory, St. Paul, MN, Lab Request number H1608, 1990. OTHER Last changed: 6/28/00. 002618 e-- e --B-- EST c-- opy A-- VAIL-- ABLE ------ LR H-- bo --R--| Environmental Laboratory ! Musoror Tocivy Testing Resolvs i Test Substaraes _FC= 787. Lot Joi rr 135 Percent Light Lo: ag 32 34 aso 42 Hq #4 S00 t3 70 76 Coes | 76 22 st Eo Non i EL RR |to EC 330 3 250,bikGo Alo Ea a a lL BT EE REE 7 RS {200-72 TELLER Ca CER bE URE TM ieSB EGeNiEs ns : a 3 He wo Alig bDeidae aLonid TR ERI E a iE is Yae Ee pg fd pecs Ba Se it ir Pal ERE EE i regis 002619 AILABLE EWHOWEITAL LISOMTORY MICROBICS ann MICROTOR SYSTEM TestsussTance: C=787 LotJo) wast: TEST DATE:, - 1b" Pach wHIb0S Pads aa ouPLICATE ql 59 [53 5 u 135 49 45 |aa | 35 2 Duplicate. q3 |45 36 [33 . As0 92 134 [46 | a2 a Duplicate az |3b [22 | a == | DSo0pi0aate lo] 24% 170 3 q7 | Aussi! ISEEo E | oeRsRetAE ig. emeaweeaa2g S| Sirtiaien a8: Is allo | ze TeHoroSolbiiadnie 52oStiocdk.t6oltn.s+ e200nmg, sleorWd Weilliph E WBE oe il ce DOTsmiotiecrrAdkiyssEtmeRnO t:NAddEedA "2200m0S a Mcackl ThE 3oicnd ernie SoS BLich: RE 4 eat AlEL TiH+aiallDDiilulhuiteinosne!ae:TriTalomaohconcentratiAonRs RweIrLe dyocvbwliespshoem i fipCURaliasssty iosyRE, i immre r r AnReSN SA ER BEST i A ARR 1 002620 BESTCOPY AVAILABLE Lo rag "ICROTCOrN DATA SHEET corr smn exeosue esierse ses cma co. torte Tamm wvEe 2I ies 125.000 9v3a.l0o7r s45a.s0 5aE5o 2Do5S0oe.oo0o0mw0m o9ii3o.ee0s,o7 s3de6e.nin0se & 000.000 0718 sEtoonne rpaoisoenrs0. 9oe3s s eo oes am 00.333a3 0.nVE6iX6se7 - 33 cso = 3.22 (02.950 0 397.795) 0.99=42330SLOP(E3=000.-9533960)ImNT3ERCJESLT = 45.7967 ET Lgl Less eT IgFa fA 0.367 433 2u8a 0.11733h5sae2 s 2i55x303 vie 3 . _6:0bs yo (eots +1) ps RE a a Ea wToeeonsla.en eeenMe d Phen Hd :L;; e SDooOboeme ooam ii :or nb eriin 767o.0i.0s92iiie4r0. t1d5> e i g ns 76 LR c8 ao ban tuye 9 TL Cm RB r --m-- hABeE Na R E b oaa r Looo o aaE le aERe ET By a bE TonE eR ro M EEEtEee nheg iSaoae8 g SEEoCa ALonR : 2ERE e CI Saas Nae a Ss AEs RICO TCC e dE siCerVs EREao Crasl hae rariVof E R lgon eed aiER a CESEGER Laorl Bae feEel s. ai Sel SER Bt i A sspi ni 002621 . Y AVAILABLE ra33444 HICROTOX tr) DATA SHEET covey ism EXPOSWRE 6/16/90 sas aim w cone. torte TT HSo 1ml25e.a0n0m0 w3932.00o77 3eo6l.o0 iSo BHoolbo o2n30e7 2187.00 .T 5 n5S0i0o.e m00.0on 97.5R0570Es17.1A00.0 cane gosst= 93/83 BLANK. RATIO= 0.569% a-ous 0st.ao4ia72 02150s8. 2.2a8520Es ccs = 2sism (237.907 10 265.931 K =0.99=784250SLO(PE24= 00-.8287500) mglL INTERCEPT = 5.5277 ses LJ LassDy o0.4m56 01995 a =3y 3= 30 " S0.9e08 770 3 Mh) 2113E 608283 R3 82 o [2 (Gost Ld o1 reose.s : Gloss erodso.s ea 1ii | =:; PiS oooolssss aoame a1p0 S"ai3gg: LI~fTi The "7C. U0.E083 Tt 9N4 ocaAR nPgEEeamdiGeoRBEn on OsTeen Ba"iImdLieE a E % nSRi E EE FLSR 0 R e Sa LT TT Ai nne : rs aed ot) i OOO eC MRkEE S S S GR SAp ERCS A RE 3. oc n L GLA vd islie s 4 BBailsiasl e Ees G tld E oe id ae de SRTR ON Seea a= i CEaTeE SeoSin | CEE EE R gaTyO SRO a cob a Gg a8 y RT E d r74iMoICmKOoTnOX t1ss Ssieg iissi tas nTordadsedeMar PB ae er sil EE API rCIREE CE Fel 8 EL R) e a oeA SERE REEteh hE HOS ieo Sei Aa ssa REsab 002622 BEST COPY AVAILABLE . ra gy AICROTO(rK) DATA SHEET For? SO-MINUTE EXPOSURE 0/16/70 SAD PAIR # cone. torte 32T i Z1E12E255o..mo00o00o00 FF95935e.000r77s 323253a..0000 SSo GSeooows0e0 oroors 1133000 a7 %i1o0o0o0..000000 9e8o.0s/ 8T.e0 oElkan raBotsimoess0.5933761% 5-088 G-esT Ligfosst 7 00V1..6552821315 00.11.523525024707 55 3323 s3y4 3 oz 221778000 7%) os5.586 _ hs 6.405 3 8b [oDGy roBS 4 00 (6c rr) cso = 210.768, 197.73 10 233.388) z 210 (200-2M3ma0l)L "0.99507 SLOPE = 0.0238 INTERCEPT = 45.36% rip a oi | 002623 owookehs. eoss.e Matdsptrt piPooooororsk wameoe So oloen a i Pl T LIT d 1-1 en <8 D55 odoooaomr wCceeaess i> i JHE adfac a H N Pa FC a | SE GLRo Ai G na Lo ao d Bi L EERISEES LeSaaGl tan mas t ASgna a GEEpRa o> Buro itsee oSRU aCEri wR r2 e pit SEE EGk ahsia SHR F SPE saEhnRR REER tEe TrTir rra RRA EA PER TH wa in e TITTTARLRoge Bete 1 [h oki we = FM aa EJi S 4CR T Ge eesE Se RR TN BR3IECol RE]i SaRo1ii:n L psi aat id LHibCROTOMo INaToe lfecisteraga Tradeemarke ofilct roblceiboT greratiH on. bh ARE C S CoL EERRIR mER LRaE D L ne LR L R NE EAe aR es