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SEVERN TRENT STL STL Chicago 2 4 1 7 Bond Street University Park, IL 6 0 4 66 Tel: 70S 5 3 4 5 2 0 0 Fax; 7 0 8 534 5211 www.stl-inc.com SEVERN TRENT LABORATORIES ANALYTICAL .RE PORT JOB NUMBER: 2 3 2 0 8 b Prepared For: Weston Solutions, inc,, 1400 Weston Way Building 5-2 Wegt Chester, p a i938-i499 Pro jact : Conf idential Decatur - FC Investigation Attenti on : Jai Ko sari Date.: 1 2 / 3 / 2 0 4 Title: Project. Manager E - M a i l : r w r i g h t O s t l -.1n e .corn This Report Contains Leaders in Environmental Testing Date STL Chicago 2 417 Bon d Street. University Park, IL 60466 PRONE: (708) 5 34-52 00 F A X . .: (70S) 5 3 4 - 5 2 1 1 ) Pages Severn Trent I abnramries, Inn. WET CHEMISTRY DATA PACKAGE CONFIDENTIAL DECATUR - FC INVESTIGATION JOB# 232885 Data Summary............................................................... 1 Chain of Custody......................................................... 29 Case Narrative............................................................. 36 Raw Data...................................................................... 38 STL Chicago is part of Severn Trent Laboratories, Inc. ; . . S A M P LE -,-,v-,,^ Job Number. : 232885 Customer... : Weston Solutions, Inc. Attn...... : Jai Kesari IM F 0 R M A T I 0 N ; v_ Project Number........ : 20004891 Customer Project ID___ : CONFIDENTIAL DECATUR Project Description___ : Confidential Decatur - FC investigation Laboratory ! Sample' ID . ' Customer Sample ID 232885-1 DFBb-SB-135R-0-0000 232885-2 DF8b-SB-135R-0-0005 232885-3 DF8b-SB-135R-0-0010 232885-4 DF8b-SB-135R-0-O020 232885-5 DF09-SB-131B-0-0005 232885-6 DF09-SB-1316-0-0080 232885-7 DF8b-SB-135R-0-0000 232885-S DF8b-SB-135R-0-0l90 232885-9 DF14-SB-137R"0-0000 232885-10 DF14-SB-137R-0-0005 232885-11 DF14-SB-137R-0-0010 232885-12 DF14-SB-137R-0-0020 232885-13 DF14-SB-136R-0-0000 232885-14 DF14-SB-136R-0-0005 232885-15 DF14-SB-136R-0-0010 232885-16 DF14-SB-136R-0-0020 232885-17 DF14-SB-136B-0-0000 232885-18 DF14-SB-136B-0-0005 232885-19 DF14-SB-136B-0-0010 232885-20 DF14-SB-136B-0-0020 Sample Matrix Soil soi l Soil Soil Soil soi l Soi 1 Soil soi 1 Soil soi 1 Soi 1 Soil soi 1 soi 1 Soi l Soil Soil soi l soi l Sampled. 12/13/2004 12/13/2004 12/13/2004 12/13/2004 12/13/2004 12/13/2004 12/14/2004 12/14/2004 12/14/2004 12/14/2004 12/14/2004 12/14/2004 12/14/2004 12/14/2004 12/14/2004 12/14/2004 12/14/2004 12/14/2004 12/14/2004 12/14/2004 Time sailed 15:15 15:30 15:40 15:50 13:40 13:59 09:35 10:45 14:10 14:15 14:25 14:35 14:50 15:00 15:10 15:20 15:35 15:40 15:50 16:05 Received 12/17/2004 12/17/2004 12/17/2004 12/17/2004 12/17/2004 12/17/2004 12/17/2004 12/17/2004 12/17/2004 12/17/2004 12/17/2004 12/17/2004 12/17/2004 12/17/2004 12/17/2004 12/17/2004 12/17/2004 12/17/2004 12/17/2004 12/17/2004 Received 10:00 10:00 10:00 10:00 10:00 10:00 10:00 10:00 10:00 10:00 .10:00 10:00 10:00 10:00 10:00 10:00 10:00 10:00 10:00 10:00 Page 1 1 CM STL Chicago is part of Severn Trent Laboratories, Irte. Job NkJifcer: 232B85 :CUSTOflE R : ;Weston 1SoE utions , Inc. ; ' ; Customer Sample ED: DF8b-SB-135R-0-0000 Date Sampled..... : 12/13/2004 Time Sampled..... : 15:15 Sample Matrix.... : Soil TEST METHCt Hethod , Lloyd Kahn PARAMETER/TEST 0ESCRIPTION % Solids Determination % Solids, Solid % Moisture, Sol id Total Organic Carbon {Soils) TOC Average Duplicates, Solid LABORATORY TEST RESULT S PROJECT: CONFIDENTIAL DECATUR- Laboratory Sample ]D 232B85-1 Date Received...... 12/17/2004 Time Received...... 10:00 Date:12/30/2004 ATTN:; Jai Kesari : ! SAMPLE RESULT C FLAGS 82.0 18.0 6100 'H D L ..... ' RL DILUTION UNITS BATCH DT DATE/TIME TECH 0.10 0.10 0.10 0.10 1 1 % 138041 12/27/04 1317 daj % 138041 12/27/04 1317 da j ! 210 B10 1 mg/Kg 137664 12/21/04 1328 els 1 * In Description = Dry Wgt. Page 2 i __ co STL Chicago is part of Severn Trent Laboratories, Inc. Job Number: 232385 CUSTCHE R :Wes ton:Sotut ions, Inc. Customer Sample ID Date Sampled..... Time Sampled..... Sample Matrix.... D FSb-SB-135R-0-0005 12/13/2004 15:30 Soi L TEST METHOD Method Lloyd Kahn PARAMETER/TEST DESCRIPTION % Solids Determination % So lids, Soli d % Moisture, Solid Total Organic Carbon CSoils) TOC Average Duplicates, Solid LABORATORY TEST RESULTS F'ROJEC T-::COM FIDE NT TAL :DECATUR Laboratory Sample ID 232885-2 Date Received...... 12/17/2004 Time Received...... ID: 00 Date:12/30/2004 ATTN: Jai Kesari 3 SAMPLE RESULT 82.2 17.8 1500 FLAGS MDL 0.10 0.10 150 FEE DILUTION UNITS 'BATCH! |DT DATE/T.IME' TECH a .1d 0.10 138041 I 112/27/04 1321[daj 138041 \ 12/27/04 1321;daj 570 mg/Kg 137864 12/21/04 1344 els * In Description = Dry Ugt. Page 3 STL Chicago is part of Severn Trent Laboratories, Inc. Job Number: 232865 CUSTOMER : Weston Solutions, Inc. Customer Sample ID: BF8b-SB-135R-Q-0010 Date Sampled...... :12/13/2004 Time Sampled...... :15:40 Sample Matrix..... :Sai l TEST METHOD ; 'PARAHE TER/TE ST::BESCRTPTI Oil! Method % Solids Determination % Sot ids, Sol id % Moisture, Solid Lloyd Kahn Total Organic Carbon (Sails) TQC Average Duplicates, Solid LABORATORY TEST RESULTS PROJECT: CONFIDENTIAL DECATUR Laboratory Sample ID: 232385-3 Date Received........ :12/17/2004 Time Received........ :10:00 Date:12/30/2004 AtTW: Jai (Cesari .SAMPLE RESULT Q FLAGS HH: :M .... =: M - M Rt DlLOT EON UNITS BATCH' DT DATE/T1ME TECH 80.8 19.2 0.10 0.10 0.10 0.10 1 1 % 138041 12/27/04 1324 daj % 138041 12/27/04 1324 da j 310 130 490 1 mg/Kg 137664 12/21/04 1406 c Ls * In Description = Dry Ugt. Page 4 STL Chicago is part of Severn Trent Laboratories, Inc, Job Number: 232835 CUSTOMER: Ueston Solutions,:Enc. Customer Sample ID ate Sampled..... Time Sampled..... Sample Matrix.... D F8b-SB-135R-0-OQ20 12/13/2004 15:50 Soi L TEST METHOD- PARAHETER/TEST;DESCR EPTJOff : Method \% Solids Determination Solids, Sol id \% Moisture, Solid Lloyd Kahn [Total Organic Carbon (Soils) TOC Average Duplicates, Solid LABORATORY TEST RESULTS ' PROJECT: CONFIDENTIAL DECATUR ' Laboratory Sample ID 232335-4 Date Received...... 12/17/2004 Time Received...... 10:00 Date:12/30/2004 ATTN: Jai Kesari SAMPLE RESULT 80.2 19.8 810 FLAGS 0.10 0.10 140 RL DILUTION!;- UK ITS CATCH Jo t DATE/TEME TECH 0.10 0.10 130041 I 12/27/04 13 26 ^da j 13S041 12/27/04 1326 daj 540 mg/Kg 137664 !12/21/04 1443 els ( STL Chicago is part of Severn Trent Laboratories, Inc. Job Nimber: 232865 CUSTOMER; Heston':Soltions, Inc. Customer Sample ID Date Sampled..... Time Sampled..... Sample Matrix.... D F09-SB-131B -0-0003 12/13/2004 13:40 Soi L TEST METHOD Method Lloyd Kahn .PA RA METER/TEST'O E S C R I P H O N % Solids Determination % Solids, Solid % Moisture, Solid Total Organic Carbon (Soils} TOC Average Duplicates, Solid LABORATORY TEST RESULTS PROJ ECT: CNF.J DENTI AL .DECATUR Laboratory Sample ID 232865-5 Date Received...... 12/17/20D4 Time Received...... 10:00 Date:12/30/2004 ATTN : Jai Kesari SAMPLE RESULT ,0 FiGSA: S3.4 16.6 1000 MDL 0.10 0.10 90 RL DI LUTION UNITS BATCH BT DATE/TIME TECH 0.1Q 0.10 13S041 138041 12/27/04 1326 daj 12/27/04 1326 daj 350 mg/Kg 3764 12/21/04 1504 cts * In Description = Dry Ugt. Page 6 STL Chicago is part of Severn Trent Laboratories, Inc. Job Nimber: 232085 Customer Sample ID: DF09-SB-131B-0-00S0 Date Sampled.......:12/13/2004 Time Sampled.......:13:59 Sample Matrix..... :Soi l TEST METHOD Method Lloyd Kahn :p a r a m e t e r /t e s t ;d e s c r i p t i on % Solids determination % Sol ids, Solid % Moisture, Solid Total Organic Carbon {Soils} TOC Average Duplicates, Solid r* LABORATORY TEST RESULTS P R O .lFP T r COTJFTRiP(JT l Al ftPCATI IS ' Laboratory SanrpLe ID: 2328B5-6 Date Received....... : 12/17/2004 Time Received....... : 10:00 Date:12/30/2004 SAMPLE RESULT 82.3 17.7 B30 FLAGS MDL 0.10 0.10 05 RL. DILUTION UNITS CATCH DT DATE/TIKE TECK 0.10 0.10 130041 i 12/27/04 1330 da j 130041 ! 12/27/04 1330 da) 330 mg/Kg 1374 12/21/04 1516 els * In Description = Dry Wgt. Page 7 i II STL Chicago is part of Severn Trent Laboratories, Inc. Job HLjnber: 232885 CUSTOMER: Weston 'Solutions, Inc Customer SanpLe ID: DF8b-SB-135R-0-0000 Date Sampled.......:12/14/2004 Time Sampled.......:09:35 Sample Matrix......:Soi L TEST METHOD : RARAHETER/TEST.'DESCRIPTION Method % Solids Determination % Solids, Sol id % Moisture, Solid Lloyd Kahn Total Organic Carbon (Soils) TOC Average Duplicates, Solid go LABORATORY TEST RESULTS PROJECT: CONFIDENTIAL DECATUR Laboratory Sample ID: 532885-7 Date Received........ :12/17/2004 Time Received........ :10:00 Date: *2/30/2004 ATTN:: Jai Kesari SAMPLE RESULT ':G FLAGS ' 81.6 18.4 980 MDjJ ' 0.1D 0.10 81 -RL ;dilutioij: ' UNITS' ' 'BATCH lot O A W H K E TECH 0.10 0.10 1 1 % 138041 12/27/04 1332 da j % 138041 12/27/04 1332 da) 320 1 mg/Kg 137664 12/21/04 153 P cLs In Description = Dry Wgt. Page 8 STL Chicago is part of Severn Trent Laboratories, Inc. " Job Nunber: 232885 CUSTOMER: Weston Solutions, Inc. Customer Sample ]D Date Sampled..... Time Sampled..... Sample Matrix.... D Ffib-SB-135 R -0-0190 12/14/2004 10:45 Soi l T.EST METHOO Method Lloyd Kahn :PARANE TE R/TEST ?DES CR TRT IGli % Solids Determination % Solids, Sol id % Moisture, Solid Total Organic Carbon (Soils) TOC Average Duplicates, SoLid LABORATORY TEST RESULTS PROJECT:; CONFIDENTIAL DECATUR Laboratory Samp Le ID 232885-B Date Received...... 12/17/2004 Time Received...... 10:00 Date:12/30/2004 ATIf: Ja Kesa'ri; SAMPLE RESULT O FLAGS- 78.6 21.4 540 MDL 0.10 0.10 77 RL DILUT t m UNITS CATCH DT DATE/TIME TECS 0.10 0.10 138041 138041 12/27/04 1334 da j 12/27/04 1334 daj 300 rtig/Kg 138147 12/27/04 1052 els * In Description = Dry Ugt. Page 9 STL Chicago is part of Severn Treni Laboratories, Ine. O H * [n Description = Dry Ugt, Page 10 STL Chicago is part of Severn Trent Laboratories, inc. Job Number: 232885 CUSTOMER: Weston Solutions, 3nc. Customer Sample ID: D F14-SB-137R-Q-0005 Date Sampled..... : 12/14/2004 Sample Matrix.... : Soil TEST HETHOD Method LLoyd Kahn PARAMETER/TEST DESCRIPTION Si Solids Determination Si Sol ids, Solid Si Moi sture, Sol id Total Organic Carbon tSoiIs) TOC Average Duplicates, Solid ri ri LABORATQRY TEST RESUL T S PROJECT CONF IDENT]AL ;DECATUR ' Laboratory Sample ID: 232885-1Q Date Received.... .: 12/17/2004 Time Received.... .: TO: 00 Date:12/30/2004 ATTN: Jai Kesari SAMPLE: RESULT:.; 0: FLAGS 33.3 16.7 3400 MDL ' D. 10 0.10 .: :Ri DILUTION ......... 0.10 0.10 1 1 UNITS BATCH DT DATE/TIME TECH: % 138041 12/27/04 1339daj % 138041 12/27/04 1339:daj' 37 340 1 mg/Kg 138147 12/27/04 1147 c ls * In Description = Dr/ Wgt. Page 11 STL Chicago is part of Severn Trent Laboratories, Inc. Job Nuifcer: 232885 .CUSTOMER: Weston Solutions, Inc. Customer Sample ED Bate Sampled..... Time Sampled..... Sample Matrix.... DF14-SB-137R-0-OIO 12/14/2004 14:25 Soi l TEST METHOD Method Lloyd Kahn .PARAMETER/TE ST.D ESCR1 PT IO R . % Solids Determination X Solids, Solid % Moisture, Solid Total Organic Carbon (Soils) TOC Average Duplicates, Solid LABORATORY TEST RESULTS PROJECT: CONFIDENTIAL DECATUR Laboratory Sample ID 232885-11 Date Received...... 12/17/2004 Time Received...... 10:00 Date:12/30/2004 ATTN: Jai Kesari. SAMPLE.: RESULT :FLAGS 79.9 20.1 1200 mi. 0.10 0.10 9 RL: DILUTION- UNITS BATCH DT DATE/TIHE TECH 0.10 0.10 138041 138041 12/27/04 1341 da j 12/27/04 1341 daj 370 mg/Kg 138147 L 12/27/04 1222 els * In Description = Dry Wgt. Page 12 STL Chicago is part of Severn Trent Laboratories, [nc. Job Htitber: 232335 . CUSTOMER: Weston So l'utions .Iric. Customer Sample ID Date Sampled..... Time Sampled..... Sample Matrix.... DM4-SH-137H-Q-002 12/14/2 m u 14:35 Soil TEST METHOD :PARAMETER/TEST?DES CR IPT ION Method Solids Determination \% Solids, Solid % Moisture, Solid Lloyd Kahn Total Organic Carbon (Sails) TOC Average Duplicates, Solid Fl H LABORATORY TEST RESULTS PROJECT: CONFIDENT fAL DCAUR Laboratory Sample ID 23285-12 Date Received.,.... 12/17/2004 Time Received...... 10:00 Date:T2/30/2DD4 ATN: Jai Kesari SAMPLE:RESULT Q FLAGS: :j 30.1 19.9 1300 :MDL : 0.10 0.10 91 fiL DILUTION UNITS ' BATCH- DT DATE/TIWE TECH 0.10 C.1Q 13E041 130041 12/27/04 1343 da j 12/27/04 1343 daj 35 D mg/Xg 138147 12/27/04 1240 els * In Description = Dry Wgt. Page 13 STL Chicago is part of Severn Trent Laboratories, Inc. Job Nimber: 232885 .CUSTOMER: Weston Sol tit-ions, :Inc. Customer Sample ID: DF14-SB-136R-0-0000 Date Sanpled...... :12/14/2004 Time Sampled...... :14:50 Sample Matrix..... :Soil TEST METHOD Method Lloyd Kahn i;!;PARAMETER/TEST DESCRIPTION % Solids Determination % Solids, Solid % Moisture, Sol id Total Organic Carbon (Soils] TOC Average Duplicates, Solid H LABORATORY' TEST RESULTS PROJECT: COiJFIDEMTIL DECATUR Laboratory Sample ED: 232835-13 Date Received........ :12/17/2004 Time Received........ :10:00 Date:12/30/2004 ATTN: Jai Kesari SAMPLE RESULT 0 FLAGS 01.9 13.1 6 1 DD HDl 0.10 0.10 160 j RL DILUT]0M UNITS BATCH DT DATE/TIME TECH 0.10 0.1D 1 1 % 138041 j12/27/04 1345-daj % 138041 12/27/04 1345 daj 630 1 mg/Kg 138147 12/27/04 1303 c Ls ' i j * In Description = Dry Wgt. Page 14 STL Chicago l's pari oi Severn Trent Laboratories, Ine. Job Humber: 232835 LABORATORI TEST RESULTS Date:12/30/2004 Customer Sample ID: DF14-SB-136R-0-0005 Date Sampled..... : 12/14/2004 Time Sampled..... : 15:00 Sample Hatrix.... : Soil ; TEST WETHOC PARAMETER/TEST DESCRIPTION Method & Solids Determination % Solids. Solid & Moisture, Solid Lloyd Kahn Total Organic Carbon iSoiLs) TOC Average Duplicates, Solid Laboratory Sample ID 232885-14 Date Received...... 12/17/2004 Time Received...... 10:00 SAMPLE RESULT 3 FLAGS 83.2 16.3 2000 MDL 0.10 0.10 120 RL DILUTION UH ITS DAtCH DT d a t e /t j m e TECH 0.10 0.10 1 1 % 138041 12/27/04 1347 daj % 138041 12/27/04 1347 da) 480 1 mg/Kg 138147 12/27/04 1352 els * In Description = Dry Ugt. Page 15 STL Chicago is part of Severn Trent Laboratories, Inc. 11 i Job Number : 232S85 CUSTOMER : Weston Sot ut ions.. \nr.. Customer Sample ID; DF14-SEM36R-0-0010 Date Sampled..... 12/14/2004 Time Sampled..... 15:10 Sample Matrix.... Sai l TEST: METHOD: :PARAMETER/TE$T 0ESCRIPTtON Method % Solids Determination % Solids, Solid % Moisture, Solid Lloyd Kahn Total Organic Carbon (Sails) TOC Average Duplicates, Solid H LABORATORY TEST RESULTS PROJECT: C0MFTDFH7TAI DECATUR . Laboratory Sample ID 232885-15 Date Received...... 12/17/2004 Time Received...... 10:00 Date:12/30/2004 SAMPLE RESULT 82.9 17.1 1600 FLAGS mu, 0.10 0.10 82 RL DILUTION^.-' UNITS BATCH DT DATE/T3ME TECH 0.10 0.10 138041 138041 12/27/04 1349 daj 12/27/04 1349 daj 320 mg/Kg 138147 12/27/04 1418 c Ls * In Description = Dry Wgt. Page 16 STL Chicago is part of Severn Trent Laboratories, Enc. I> H * In Description = Dry tfgt. Page 17 STL Chicago is part of Severn Trent Laboratories, Inc. LABORATORY TEST RESULTS 0 H ]n Description = Dry Wgt. Page 13 STL Chicago is part of Severn Trent Laboratories, Ine. S H * in Descri P* ion = Dry Wgt, Page T9 O (SI STL Chicago is part of Severn Trent Labaratori es, Inc* Jab Number: 232885 .CUSTOMER: Weston Solut ions. 1Inc. ; Customer Sample ID: DF14-SB-136B-0-0010 Date Sampled..... : 12/14/2004 Time Sampled..... : 15:50 Sample Matrix.... : Soi l L TEST NET MOD PARAMETER/TEST D E S C R I P T I O N . . Method % Solids Determination % Sol ids, Solid % Moi sture, So lid Lloyd Kahn Total Organic Carbon CSoils) TOC Average Duplicates, Solid LABORATORY TEST RESULT S PROJECT-: CONFIDENTIAL DECATUR Laboratory Sample ID 232885-19 Date Received...... 12/17/2004 Time Received...... 10:00 Date:12/30/2004 SAMPLE RESULT 9 f l a g s 81.0 19.0 1400 MDL 0.10 0.10 110 RL DILUTION UNITS BATCH DT DATE/TIME t e c h ' 0.10 0.10 1 1 % 138041 12/27/04 1358 da j % 138041 12/27/04 1358 da j 410 1 mg/Kg 138147 12/27/04 1529 els i * [n Description = Dry Ugt. ________________ Page 20 H & STL Chicago is part of Severn Trent Laboratories, [nc. Jab Nunber: 232885 - CUSTOMER: Weston Solutions, Inc. Customer Sample ID Date Sampled..... Time Sampled..... Sample Matrix.... DF14-SE-136B-0-0020 12/14/2004 16:05 Soil TEST METHOD Method Lloyd Kahn PARAMETER/ fEST ;DESCRIP T;LOtJ . % Solids Determination % Sol ids, Solid % Moisture, Solid Total Organic Carbon {SoiLs) TOC Average Duplicates, Solid L AEORATOR'f T E 5T R E S U L T S PROJECT CONFIDENTIAL DECATUR' Laboratory Sample ID: 232885-20 Date Received__ ... .: 12/17/2004 T ime P&cei ved ..: 10:00 Date:12/30/2004 A?Tlf: J'ai Kesari SAMPLE RESULT Q FLAGS- ' 81.7 18.3 1800 .m d l 0.10 0.10 89 RL .' 0.10 0.10 DILUTION 1 1 UNI TS :::B-:AT:C:H :;D:T:= DATE/TIHE TECH; % 138041 12/27/04 1400 da j % 133041 12/27/04 1400 daj 350 1 mg/Kg T3B47 12/27/04 1550 els * In Description = Dry Wgt. Page 21 i STL Chicago is part of Severn Trent Laboratories, Inc. Job Number: 232885 LABORATORY CHRONICLE Date: 12/30/2004 CUST-OMER: West on Solutions, Inc. Lab ID: 232885-1 METHOD Method EDD Lloyd Kahn client ID: DFSb-SB"135R-0-0000 DESCRIPTION % Solids Determination Electronic Data Deliverable Total Organic Carbon (Soils) Lab ID: 232885-2 METHOD Method Lloyd Kahn client ID: DF8b-SB-135R-0-0005 DESCRIPTION % Solids Determination Total Organic Carbon (SoiLs) Lab ID: 232885-3 METHOD Method Lloyd Kahn Client ID: DF8b-SB-135R-0-0010 DESCRIPTION % Solids Determination Total Organic Carbon (Soils) Lab ID: 232835-4 METHOD Method LLciyd Kahn Client ID: DF8b-SB-135R-0'0020 DESCRIPTION % Solids Determination Total organic Carbon (Soils) Lab ID: 232885-5 METHOD Method Lloyd Kahn Client ID: DFQ9'SB-131B-0-0005 DESCRIPTION % Solids Determination Total Organic Carbon (Soils) Lab ID: 232885-6 METHOD Method Lloyd Kahn Client ID: DF09-SB-131B-0-0080 DESCRIPTION % Solids Determination Total organic Carbon (Soils) Lab ID: 232885-7 METHOD Method Lloyd Kahn Client ID: DF8b-SB-135R-0-0000 DESCRIPTION % Solids Determination Total Organic Carbon (Soils) Lab ID: 232885-8 METHOD Method H o y d Kahn Client ID: DF8b-SB-135R-0-Ol90 DESCRIPTION % Solids Determination TotaL Organic Carbon (Soils) Lab ID: 232885-9 METHOD Method Lloyd Kahn client ID: DF14-SB-137R-O-0OQO DESCRIPTION % Solids Determination TotaL Organic Carbon (Sails) Lab ID: 232885-10 Client ID: DF14-SB-137R-0-0005 METHOD DESCRIPTION Method % Solids Determination H o y d Kahn TotaL Organic Carbon (Soils) Lab ID: 232885-11 Client ID: DF14-SB-137R"O'0010 METHOD DESCRIPTION Method % Solids Determination Lloyd Kahn Total Organic Carbon (Soils) Lab ID: 232885-12 Client ID: DF14-SB-137R-0-0020 METHOD DESCRIPTION Method % Solids Determination PROJECT : CONFIDENTIAL DECATUR ATTN.: Jai Kcsari Date Recvd: 12/17/2004 SampLe Date: 12/13/2004 RUN# BATCH# PREP BT #<S) DATE/TIME ANALYZED 1 138041 138041 12/27/2004 1317 1 1 137664 137664 12/21/2004 1328 DILUTION Date Recvd: 12/17/2004 Sample Date: 12/13/2004 RUN# BATCH# PREP BT #(S) DATE/TIME ANALYZED 1 138041 138041 12/27/2004 1321 1 137664 137664 12/21/2004 1344 DILUTION Date Recvd: 12/17/2004 Sample Date: 12/13/2004 RUN# BATCH# PREP BT #(S) DATE/TIME ANALYZED 1 138041 138041 12/27/2004 1324 1 137664 137664 12/21/2004 1406 DILUTION Pate Recvd: 12/17/2004 SampLe Date: 12/13/2004 RUN# BATCH# PREP BT #<S) DATE/TIME ANALYZED 1 138041 133041 12/27/2004 1326 1 137664 137664 12/21/2004 1443 DILUTION Date Recvd: 12/17/2004 Sample Date: 12/13/2004 RUN# BATCH# PREP BT #(S) DATE/TIME ANALYZED 1 138041 133041 12/27/2004 1323 1 137664 137664 12/21/2004 1504 DILUTION Date Recvd: 12/17/2004 Sample Date: 12/13/2004 RUN# BATCH# PREP BT #(5) DATE/TIME ANALYZED 1 138041 133041 12/27/2004 1330 1 137664 137664 12/21/2004 1516 DILUTION Date Recvd: 12/17/2004 SampLe Date: 12/14/2004 RUN# BATCH# PREP BT #<S) DATE/TIME ANALYZED 1 138041 138041 12/27/2004 1332 1 137664 137664 12/21/2004 1530 DILUTION Date Recvd: 12/17/2004 Sample Date: 12/14/2004 RUN# BATCH# PREP BT #(S) DATE/TIME ANALYZED 1 138041 138041 12/27/2004 1334 1 138147 138147 12/27/2004 1052 DILUTION Date Recvd: 12/17/2004 Sample Date: 12/14/2004 RUN# BATCH# PREP BT #(5) DATE/TIME ANALYZED 1 138041 138041 12/27/2004 1336 1 133147 138147 12/27/2004 1129 DILUTION Date Recvd: 12/17/2004 Sample Date: 12/14/2004 RUN# BATCH# PREP BT #(S) DATE/TIME ANALYZED 1 138041 133041 12/27/2004 1339 1 133147 138147 12/27/2004 1147 DILUTION Date Recvd: 12/17/2004 Sample Date: 12/14/2004 RUN# BATCH# PREP BT #(S) DATE/TIME ANALYZED 1 138041 133041 12/27/2004 1341 1 138147 138147 12/27/2004 1222 DILUTION Date Recvd: 12/17/2004 Sample Date: 12/14/2004 RUN# BATCH# PREP BT #(S> DATE/TIME ANALYZED 1 138041 138041 12/27/2004 1343 DILUTION STL Chicago is part of Severn Trent Laboratories, Inc. Job Number: 232885 LABORATORY CHRONICLE Date: 12/30/2004 CUSTOMER: Weston Solutions, Inc. Lab ID: 232885-12 Client ID: DF14-SE3-t3?R-,0-0Q20 METHOD DESCRIPTION Lloyd Kahn Total Organic Carbon (Soils) Lab ID: 232885-13 Client ID: DF14-SB-136R-Q-0000 METHOD DESCRIPTION Method % Solids Determination Lloyd Kahn Total Organic Carbon (Soils) Lab ID: 232885-14 CLient ID: DF14-SB-136R-0-0005 METHOD DESCRIPTION Method % Solids Determination Lloyd Kahn TotaL Organic Carbon (Soils) Lab ID: 232885-15 client ID: DF14-SB-136R-0-0010 METHOD DESCRIPTION Method % Solids Determination LLoyd Kahn TotaL Organic Carbon (Soils) Lab ID: 232885-16 Client ID: DF14-SB-136R-0-0020 METHOD DESCRIPTION Method % Solids Determination Lloyd Kahn TotaL Organic Carbon (SoiLs) Lab ID: 232885-17 Client ID: DF14-SB-136B-0-0000 METHOD DESCRIPTION Method % Solids Determination Lloyd Kahn Total Organic Carbon (Sails) Lab ID: 232885-18 CLient ID; DF14-SB-136B-0-0005 METHOD DESCRIPTION Method % Solids Determination Lloyd Kahn Total Organic Carbon (Soils) Lab ID: 232865-19 Client ID: DF14-SB-136B-0-0010 METHOD DESCRIPTION Method % SoLids Determination Lloyd Kahn Total Organic Carbon (Soils) Lab ID: 232885-20 Client ID: DF14-SE-136B-0-002Q METHOD DESCRIPTION Method % Solids Determination Lloyd Kahn TotaL Organic Carbon (Soils) PROJECT::...CONFIDENTIAL DECATUR . ATTN: Jai Kesari Date Recvd: 12/17/2004 Sample Date: 12/14/2004 RUN# BATCH# PREP BT #<S) DATE/TIME ANALYZED 1 138147 138147 12/27/2004 1240 DILUTION Date Rcevd: 12/17/2004 Sample Date: 12/14/2004 RUN# BATCH# PREP BT #(5) DATE/TIME ANALYZED 1 138041 138041 12/27/2004 1345 1 138147 138147 12/27/2004 1303 DILUTION Date Recvd: 12/17/2004 Sample Date: 12/14/2004 RUN# BATCH# PREP BT #<S) DATE/TIME ANALYZED 1 138041 138041 12/27/2004 1347 1 138147 138147 12/27/2004 1352 DILUTION Date Recvd: 12/17/2004 Sample Date: 12/14/2004 RUN# BATCH# PREP BT #CS) DATE/TIME ANALYZED 1 138041 138041 12/27/2004 1349 1 138147 138147 12/27/2004 1418 DILUTION Date Recvd: 12/17/2004 Sample Date: 12/14/2004 RUN# BATCH# PREP BT #(S) DATE/TIME ANALYZED 1 138041 138041 12/27/2004 1351 1 138147 13S147 12/27/2004 1435 DILUTION Date Recvd: 12/17/2004 Sample Date: 12/14/2004 RUN# BATCH# PREP BT #<S) DATE/TIME ANALYZED 1 138041 138041 12/27/2004 1354 1 138147 138147 12/27/2004 1446 DILUTION Date Recvd: 12/17/2004 Sample Date: 12/14/2004 RUN# BATCH# PREP BT #(S) DATE/TIME ANALYZED 1 138041 138041 12/27/2004 1356 1 138147 138147 12/27/2004 1513 DILUTION Date Recvd: 12/17/2004 SampLe Date-. 12/14/2004 RUN# BATCH# PREP BT #(S) DATE/TIME ANALYZED 1 138041 138041 12/27/2004 1358 1 138147 138147 12/27/2004 1529 DILUTION Date Recvd: 12/17/2004 Sample Date: 12/14/2004 RUN# BATCH# PREP BT #(S) DATE/TIME ANALYZED 1 138041 138041 12/27/2004 1400 1 138147 138147 12/27/2004 1550 DILUTION Page 3 23 Job Number.: 232885 CUSTOMER : Weston Solutions y Inc. QUALITY CONTROL RESULTS PROJECT: CONFIDENTIAL DECATUR Report Date.: 12/30/2004 ATTN ; Jai 'Itesar j-.:v.. Test Method.... Method. Method Description.: % $olids.D eterm ina tion :.Parameter..,.--- : % Moisture QC Lab ID HD* 232885-1 Reagent Units % QC Result 18.60000 Batch.;...... 138041 . Equipment Code.;.-.: . Analyst...: daj' Test Code.: %M0I5T QC Result "" ' True Value Orig. Value 18.00000 QC Calc. F * Limits 3.3 R T . 0 Date Time 12/27/2004 1319 Test Method....... : Method :Method Descript ion.: % Solids.Dtermintion Parameter.. . . . . : % Solids .-. .Eatch._____ -138041 ... 'Equipment Code.'... : ..... QC Lab ID Reagent MB 138041-001 MD 232885-1 Units % % QC ResuLt QC Result 0.1000 u 81.40000 True Value Orig. Value 82.00000 Analyst.. : daj Test code. : %$0LID QC Calc. F * Limits 0.7 R 5.0 Date Time 12/27/2004 1315 12/27/2004 1319 Test Method.'.... . : Lloyd-Kahn Method Des cripti.on. : Total Organic Carbon '(Soils) Parameter...... ...: Organic carbon. Tot-. (TOC) ..... Batch.... ........ : 137664 ' ' Equipment -Code.... ; T0C4 .. Analyst__ : els . Test Code. : TOC QC Lab ID Reagent Units ICV 137664-002 I04LSTTC2 MB 137664-003 LCS 137664-004 I00FSTLK3 LCD 137664-005 100F5TLK3 mg/Kg mg/Kg mg/Kg mg/Kg ccv 137664-016 I04LSTTC2 CCB 137664-017 CCV 137664-016 IQ4LSTTC2 CCB 137664-017 mg/Kg mg/Kg mg/Kg mg/Kg QC Result QC Result 1731.98 32.00 5172.65 3614.82 U 2038.04 32.00 2032.44 32.00 U u True Value 2000.00 4780.00 4780.00 2000.00 2000.00 Orig. Value 5172.65 QC Calc. F * Limits Date Time 87 % 85-115 12/21/2004 0826 12/21/2004 0829 108 % 53-140 12/21/2004 0852 76 % 53-140 12/21/2004 0900 102 % 85-115 12/21/2004 1202 12/21/2004 1208 102 % 85-115 12/21/2004 1545 12/21/2004 1548 Test Method....... : LloyidTKahih-:;: :!!;Method-,Pese ript ion. : Total. Organic Carbon (Soils) :;!Parameter..; ; Organ i.e'Carbon. Tot. (TOC) QC Lab ID Reagent Units ICV 138147-002 I4LSTTC2 MB 138147-003 LCS 138147-004 I00FSTLK3 LCD 138147u005 I00FSTLK3 mg/Kg mg/Kg mg/Kg mg/Kg QC Result QC Result 1879.51 32.00 u 4713.16 3954.88 4713.16 CCV 138147-016 I04LSTTC2 CCB 138147-017 ccv 138147-016 I04LSTTC2 CCB 138147-017 mg/Kg mg/Kg mg/Kg mg/Kg 2038.32 32.00 2043.79 32.00 u u Batch,, : 138147 Equipment Code___ : TOC4 -.Test Code.: TOC True Va Lue 2000.00 4780.00 4780.00 2000.00 2000.00 Orig. Value QC Calc. F * Limi ts 94 % 85-115 199.22 181.56 U 99 u 83 17 102 % 53-140 % 53-140 R 30 % 85-115 102 % 85-115 Date Time 12/27/2004 0911 12/27/2004 0923 12/27/2004 0946 12/27/2004 0953 12/27/2004 1318 12/27/2004 1325 12/27/2004 1609 12/27/2004 1620 Rage 24 * %=% REC, R=RPD, A=ABS Diff., D=% Diff 24 Job Number,: 232S85 QUALITY CONTROL RESULTS CUSTOMER: Weston Solut ions, Inc. PROJECT: CONFIDENCIAL DECATUR ' ' Report Date,: 12/30/2004 ATTN: Ji Kesari Test Method.. .. : Lloyd' KaBn....................... Method Oesc ript ion. .Total ..Organic ;Carbon {Soi Is) P a r a m e t e r . - . T O C Average D u p l i c a t e s .. QC Lab ID MS 232885-S MSD 232885-8 Reagent Units I04LSTTC2 mg/Kg I4LSTTC2 mg/Kg QC Result 1346.36 1675.61 QC Result 1S46.36 Batch......... .. Equipment Code.. . TOCA True Value 2000.00 2000.00 rig. Value 544.74 544.74 Analyst../..: cl.s TOCAV2 QC cale. F * Limi ts 91 85 6.B % 53-140 % 53"140 R 30 Date Time 12/27/2004 06 12/27/2004 1118 Page 25 * %=% REC, R-RPD, A=ABS Diff., D=% Diff. 25 ft S S U R A N : E M E T H O D S N C'E. S A U: "O' NO.-T.ES. Re|lor.t..Date; r*/3/204 REPORT COMMENTS 1) All pages of this report are integral parts gf the analytical data. Therefore, this report should be reproduced only in its entirety. 2) Soil, sediment and sludge sample results are reported on a "dry weight" basis except when analyzed for Landfill disposal or incineration parameters. All other soLid matrix samples are reported dji an "as received" basis unLess noted differently. 3) Reporting limits are adjusted for sample size used, dilutions and moisture content if applicable. 4) The test results for the noted analytical method(s) meet the requirements of NELAC. Lab Cert. ID# 100201 5) According to 40CFR Part 136.3, pH, Chlorine Residual and Dissolved Oxygen analyses are to be performed immediately after aqueous sample collection. When these parameters are not indicated as field (e.g. pH Field) they were not anaLyzed immediately, but as soon as possible on Laboratory receipt. Glossary of flags, qualifiers and abbreviations Cany number of which may appear in the report) Inorganic dualitiers (Q-CoLunin) U Analyte was not detected at or above the stated Limit. < Not detected at or above the reporting Limit. J Result is less than the RL, but greater than or equaL to the method detection limit. B Result is Less than the CRDL/RL, but greater than or equal to the IDL/MDL. S Result was determined by the Method of Standard Additions. F AFCEE: Result is less than the RL, but greater than or equal to the methoddetection Limit. Inorganic Flags (Flag Column) ICV,CCV,ICB,CCB,ISA,ISB,CRI,CRA.MRL: Instrument related QC exceed the upper or Lower control limits. * LCS, LCD, MD: Batch QC exceeds the upper or Lower control limits. + MSA correlation coefficient is less than 0.995. 4 MS, MSD: The analyte present in the original sample is 4 times greater than the matrix spike concentration; therefore, control Limits are not applicable. E SD: Serial dilution exceeds the control Limits. H MB, EB1, EB2, EB3: Batch QC is greater than reporting limit or had a negative instrument reading Lower than the absolute value of the reporting Limit. N MS, MSD; Spike recovery exceeds the upper or Lower control limits. U AS(GFAA) Post-digestion spike was outside 85-115% control limits. Organic Qualifiers (Q - Column) U Analyte was not detected at or above the stated limit. ND Compound not detected. J ResuLt is an estimated value beLow the reporting limit or a tentatively identified compound (TIC). Q ResuLt was qualitatively confirmed, but not quantified. C Pesticide identification was confirmed by GC/MS. Y The chromatographic response rescmblos a typical fuelpattern. 1 The chromatographic response does not resemble a typical fuel pattern. E Result exceeded calibration range, secondary dilution required. F AFCEE:Result is an estimated value below the reporting limit or a tentativelyidentified compound (TIC) Organic Flags (Flags Column) B MB: Batch QC is greater than reporting limit. * LCS, LCD, ELC, ELD, CV, Ms, MSD, Surrogate; Batch QC exceeds the upper or lowercontrol limits. EB1, EB2, EB3, MLE: Batch QC is greater than reporting Limit A Concentration exceeds the instrument calibration range a Concentration is below the method Reporting Limit (RL) B Compound was found in the blank and sample. D Surrogate or matrix spike recoveries were not obtaihed because the extract was diluted for analysis; also compounds analyzed at a dilution will be flagged with a D. h Alternate peak selection upon analytical review I Indicates the presence of an interfence, recovery is not calculated. M Mahually integrated compound. P The lower of the two values is reported when the % difference between the results of two QC columns is Page 26 Q U A L I I ' A S S.U R A N C. E .. M T HO D s R E F E R E MC ES A N D N O T E Report Dater 1L73Q/2004 greater than 25%. Abbreviations AS Post Digestion Spike (GFAA Samples - See Mote 1 below) Batch Designation given to identify a specific extraction, digestion, preparation set, or analysis set CAP Capillary Column CCB Continuing Calibration Blank CCV Continuing Calibration Verification CF Confirmation analysis of original Cl Confirmation analysis of A1 or D1 C2 Confirmation analysis of A2 or D2 C3 Confirmation analysis of A3 or D3 CRA Low Level Standard Check - GFAA; Mercury CR1 Low Level Standard Check 1CP CV Calibration Verification Standard DiL Fac Dilution Factor - Secondary dilution analysis D1 Dilution 1 D2 Dilutions D3 Dilution 3 DLFac Detection Limit Factor DSU Distilled Standard - High Level DSL Distilled Standard - Low Level DSM Distilled Standard - Medium Level EB1 Extraction Blank 1 EE2 Extraction Blank 2 EB3 DI Blank ELC Method Extracted LCS ELD Method Extracted LCD ICAL InitiaL calibration ICB Initial Calibration Blank ICV Initial CalibrationVerification IDL Instrument Detection Limit ISA Interference Check Sample A - ICAP ISB Interference Check Sample B - ICAP Job No. The first six digits of the sample ID which refers to a specific client, project and sample group Lab ID An $ number unique Laboratory identification LCD Laboratory Control Standard Duplicate LCS Laboratory Control Standard with reagent grade water or a matrix free from the analyte of interest MB Method Blank or (PB) Preparation Blank MO Method Duplicate MDL Method Detection Limit MLE Medium Level Extraction Blank MRL Method Reporting Limit Standard MSA Method of Standard Additions MS Matrix Spike MSD Matrix Spike Duplicate ND Hot Detected PREPF Preparation factor used by the Laboratory's Information Management System (LIMS) PDS Post Digestion Spike (ICAP) RA Re-analysis of original A1 Re-ana lysis of D1 A2 Re-ana lysis of 02 A3 Re-analysis of D3 RD Re-extractioh of dilution RE Re-extraction of original RC Re-extraction Confirmation RL Reporting Limit RPP Relative Percent Difference of duplicate (unrounded) analyses RRF Relative Response Factor RT Retention Time Page 27 DUALITY ASSURANCE METHO D S R E F E R E N C E S AND NOTES Report Date: 12/30/2004 RTW Retention Time Window Sample ID A 9 digit number unique for each sample, the first six digits are referred as the job number s c b seeded control Blank SD Serial Dilution (Calculated when sampLe concentration exceeds 50 times the MDL) UCB Unseeded Control Blank SSV Second Source Verification Standard SLCS Solid Laboratory Control Standard(LCS) PHC pH calibration Check LCSP pH Laboratory Control Sample LCDP pH Laboratory Control SampLe Duplicate MDPH pH sample Duplicate MPFP Flashpoint Sample Duplicate LcFP Flashpoint LCS G1 Cel ex Check Standard Range 0-1 G2 Gelex Check Standard Range 1-10 G3 Gelex Check Standard Range 10-100 G4 Gelex Check Standard Range 100-1000 Note 1: The Post Spike Designation on Batch QC for GFAA is designated with an "S" added to the current abbreviation used. EX. LCS S=LCS Post Spike (GFAA); MSS=MS Post Spike (GFAA) Note Z: The MD calculates an absolute difference (A) when the sample concentration is less than 5 times the reporting limit. The control limit is represented as +/- the RL. Page 28 2S CHAIN OF CUSTODY e-3 CHAIN OF CUSTODY / ANALYSIS REQUEST FORM Severn Trent Laboratories T: 708-534-5200 F: 706-534-5211 2417 Bond Street University Park, JL 60466 PAGE 2.3,2 &&S / of 3 PROJECT INFORMATION Client: Weston Solutions, Inc. 1400 Weston Way, Bldg. 5-2 West Chester, PA 19380 T: 610-701-3761 F: 610-701-7401 Project Manager: Jai Kesari email: f.kesari@westonsolutions.com Project Name: Reference No: Decatur, Alabama 02161-129-081-0001 ANALYSES REQUESTED Sampler: T Frinak, A Murphy P.O #: Quotation #: SAMPLE ANALYSIS ExyUMS # \ JL CoJ le ctio n Client Sample Identification Date DF8b SB 135R 0 0000 13-Dec-04 DF8b SB 135R 0005 13-Dec-04 DF8b SB 135R 0010 13-Dec-04 DF8b SB 135R 0020 13-Dec-04 DF09 SB 131B 0005 13-Dec-04 DF09 SB 131B 0060 13-Dec-04 DF8b SB 135R 0000 14-Dec-04 DF8b SB 135R 0190 14-Dec-Q4 DFSb SB 135R 00190 14-Dec-04 DF14 SB 137R 0000 14-Dec434 Collection Time 15:15 15:30 15:40 15:50 13:40 13:59 9:35 10:00 10:45 14:10 X c 'OaS. -ioc-i z CJ S a m p le Matrix SOIL SOIL SOIL SOIL SOIL SOIL SOIL WATER SOIL SOIL CHAIN OF CUSTODY Reti n : Date &^ ------------ 7 / Cooler ID No.: Time Received By: /P&e> Fed Ex Q Cooler Temp. (C): Date Time /?c ' wjhht' ioaO Comments X X X PROJECT REQUIREMENTS Results Deadline: Laboratory Report Options: SampEe Results Only Add Case Narrative Add Quality Control Summary Add Calibration Summary Add Raw Data Other: H e? CHAIN OF CUSTODY/ANALYSIS REQUEST FORM 2 3 3 8 6 5* Severn Trent Laboratories T: 708-534-5200 F: 708-534-5211 2417 Bond Street University Park, IL 60466 PAGE ^ Of PROJECT INFORMATION Client: Weston Solutions, Inc. 1400 Weston Way, Bldg. 5-2 W estchester, PA 19380 T: 610-701-3761 F: 610-701-7401 Project Manager: Jai Kesari em(ail: i.kesa ritS>westonsofution s.com Project Name: Reference No: Decatur, Alabama 02181-129-081-0001 ANALYSES REQUESTED Sampler: T Frinak, A Murphy P.O. #: Quotation #: SAMPLE ANALYSIS ExyLIMS # Client Sample Identification | VO DF14 SB 137R 0 0005 Ll DF14 SB 137R 0 0010 I t / DF14 SB 137R 0 0020 I t DF14 SB 136R 0 0000 i f - DF14 SB 136R 0 0005 [ $ DF14 SB 136R 0 0010 II DF14 SB 136R 0 0020 DF14 SB 136B 0 0000 DF14 SB 136B 0 0005 DF14 SB 136B 0 0010 Col lection Date 14-Dec-04 14-Dec-04 14-Dec-04 14-Dec-04 14-Dec-04 14-Dec-04 14-Dec-04 14-Dec-04 14-Dec-04 14-Dec-Q4 C o lle c tio n T im e 14:15 14:25 14:35 14:50 15:00 15:10 15:20 15:35 15:40 15:50 CHAIN OF CUSTODY Re 1inq Qalf 7J Cooler ID No.: Time Received By: Fed Ex 0, v & Grab Sample 2 a o CL uEc a C `ft. E* zO u0 X1 X1 X1 X1 X1 X1 X1 X1 X1 X1 Sample M atrix SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL Cooler Temp. (C): Date Time tooo Comments O O l- X X X X X X X X X X PROJECT REQUIREMENTS Results Deadline: Laboratory Report Options: __ Sample Results Only __ Add Case Narrative ;__ Add Quality Control Summary Add Calibration Summary __ Add Raw Data Other: CHAIN OF CUSTODY/ ANALYSIS REQUEST FORM on> a. Severn Trent Laboratories T: 708-534-5200 F: 708-534-5211 2417 Bond Street University Park, IL 60466 PAGE 3 of 3 PROJECT INFORMATION Client: Weston Solutions, Inc. 1400 Weston Way, Bldg. 5-2 West Chester, PA 19380 T: 610-701-3761 F: 610-701-7401 Project Manager: Jai Kesari email: i.kesari weston solution s. com Project Name: Reference No: Decatur, Alabama 02181-129-081-0001 ANALYSES REQUESTED Sampler: T Frinak, A Murphy P.O. #: Quotation #: SAMPLE ANALYSIS ExyLIMS # Client Sample identification DF14 SB 136B 0020 3 jO DF14 SB 136B 0020 C o lle c tio n Date 14-Dec-04 14-Dec-04 C o lle c tio n T im e 15:55 16:05 2it Izoo. oeo S a m p le M a trix WATER SOIL Comments CHAIN OF CUSTODY Cooler ID No.: Re Ein Date Time / // A y /? o & // Received By: Fed Ex to t0 Cooler Temp. {C}: Date Time H i i i Jo* CODO PROJECT REQUIREMENTS Results Deadline: Laboratory Report Options: Sample Results Only Add Case Narrative Add Quality Control S ummar y Add Calibration Summary Add Raw Data Other: Sampie Lot#: Sample No. / ~ C .QJ /-IO Analysis STL Chicago internai Sample Custody Transfer Record Client: C<n*f~ Relinquished by: Received by: C _- ff ^ Date Time Comments / ;2 C ? ;*r C3 - CHi-22-11-001/C -im rpjsckl Job sampLe Receipt Checklist Report Job Nimber.: 232885 Location.: 57222 Check List Number.: 1 Description.: Customer Job ID.... : Job Check List Date.: 12/17/2004 Project Number.: 20004891 Project Description.: Confidential Decatur - Fc Investigation Customer...... : Weston solutions, Inc. Contact.: Jai Kesari Questions ? (Y/N) Comments V2 Date of the Report..: 12/30/2004 Project Manager.... : rew Chain-of-Custody Present?......... ............... Y Were samples dropped off at or picked up by STL?.. N Custody seal on shipping container?............ .. Y ...If "yes", custody seal intact?....... ......... Y Custody seals on sample containers?............... N ...If "yes", custody seal intact?..... ......... Samples iced?.... ..... Y Temperature of cooler acceptable? (4 deg C +/- 2). Y 2.7 Samples received intact (good condition)?........ Y Volatile sampLes acceptable? (no headspace)...... Correct containers used?....... Y Adequate sample volume provided?.................. Y Samples preserved correctLy?....................... Y SampLes received within holding-time?........... Y Agreement between COC and sample labels?......... Y Radioactivity at or below background levels?....., Y A Sample Discrepancy Report (SDR) was needed?.... N If samples were shipped was there an air bill #?.. Y Sample Custodian Signature/Date................... Y Page 1 34 U S Airbill Express 1 Frotn Bate / C h' " f ! Failt TrjctTM f l 4 7 % 7 1 4 4 f i 7 5 Sender's ~T * ~ Mame r i ' /IT . r-,_, G'' 1 : Pilon ^ s ; "r - / 7 Cmpany f ; s- ^ .. : S G o - ; - . ,V c . . . . . . . . ____ n A i - . t /:, Address ' 7 i , _s ', : ; . City . / r- J." ' V j-;!L -' r 'G " .! '''s .' V 7' < A ,rStatu / { [ . . ZIP ' " r hft,Rn^fW Uh { } if ! 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G BFfllMd&t h i, lid F ti i.3 u lp Flh iwtorwlSlu&krtraKl Other D sr. A 1 $ SSfoRcciiaal Ftanding - lidukFtaifj.dJchMfeSu*un. |-- SmjRDVDelMen I i * ^ a^ RIlGj^ylF'iiifahbflZlFrruiEcsmJrr i--i HOLDWadoday i Ia[IivFfnewefFdeiCtax*D-L-r'icaticn | Do&tttib OrebojtrnrttswtbtiaajcihtddHiDM.romgodt? --:_iI BhtuFuBfdSBftlLtomcvatran A^*iuntfHenOdMfVedt rE)Fi2iEjxayI n rty u-ufet fccitaru JRTl\ Wo |i-GI V5ehfsf*r"iDgda-^knII-- Il imattreirnrf'iEDsf+tidarric-i: Dnjom [c(evtk>i]EbYlci|cnttb(Ek|fhfoEjc.uftagng. lI~.- DDiryjyl=o.&e.i I -CargaAitraftQn^ 7 P a y ro rt JtBUT\ SAMiaj^lnrjd.inaeltrwii CtmL'iiteep.l I -- ------------- &mafacrrrFBfnaJiCMi*CtLLllKkiicnrtiamtifii tooirbtiUtOa,bqsb*QwW. .... ^ALdWr-trNtun. U I Recipient G ThirdPiarty G CteditCard G Cash/Check TotalPatsg* TooyVMfK 4- i A - T.OuyhtifcvniniianJ4FiMulr^eDtiVluda B Sign lo Authorize Delivery Wi TtftlIMw^aktet J JM ternilla,ibaba:tIrrdettts. ;TtetCherfK Cia-djCardhji. Bpsigiing huu auL-crzs ua iD-dtiM* ttiM ip fr c n l H -ttn i-tQ ttw ra a Etgnmra - ind |rw i m j i t a r i Y a r d hod uehunil i *ira n orp rasjU ig cair* . . n iio iiidwrrT V is rt M - W e s^B atfedB JC tam 6 4 5A..u'rFre,aDlji4I'HI.UG-cPFsirctEHIlEiJlIl'-U-'Sm-SGEhricEa-PF.aJMI h K'A-A'V 4t?J II 10 CASE NARRATIVE Client: Job #: STL Chicago Wet Chemistry Case Narrative Weston Solutions, Inc. 232885 Date Rec'd: 12/17/04 1. This narrative covers the analysis o f the samples in the above Job # for TOC by the Lloyd Kahn Method. The samples were analyzed for TOC in duplicate by furnace combustion and nondispersive infrared detection on a Dohrmann Phoenix 8000 TOC analyzer, after acidification to remove inorganic carbon, and drying. No correction was made, therefore, for moisture content. The average o f the sample bums is reported. 2. The method-recommended holding time o f 2 weeks was met. Refer to the Laboratory Chronicle Page for dates o f sampling, receipt, and analysis. 3, The TOC calibration curve and the initial and continuing verification standards and blanks met acceptance criteria. 4. The method blanks were less than the reporting limit. 5, The LCSs were within acceptance limits, although the first attempt in batch 137664 was very low and the RPD between the repeated LCS and the LCD in that batch was high, at 35%. 6. The matrix QC done on sample 232885-8 was within acceptance limits 7. Sample 232885-1 was initially over-range and had to be repeated. On the first attempt for sample 232885-3, the analyst failed to insert the sample boat into the furnace within the allotted time window, and the burn was manually cancelled. Wet Chemistry Section Manager Date 37 RAW DATA *** RUM LOG *** (V2 ) Total Organic Carbon (Soils) Method code.,. ; TOCS Batch code... : 137664 Status.... RVWd Batch Oats. ..: 12/21/04 Batch Time, 958 user Name,.. QC Code.... ...: TOCS Calc Code... ...: TOCS 12/30/04 12:47 Location code..;: 57222 Equipment Code.:: T0C4 Import Code___ : TEST CODE TTTTTTTTTTTTT 000O0OCCCIII CCCCCcCSSScCC 234AAA 2ASss VVV V 2A 234 2 2 SAMPLE: Grp Pos Sample ID Di Luti on TEST POS Date / Time 1234567111222 789 0 12 11 ___ICAL_I04LSTTCl_ 0 12 ___ICV_I04LSTTC2_ 12/21/04 0826 0 13 ___MB__ 12/21/04 0829 0 14 15 LC$ 100F5TLK3 j__ LCD_I00FSTLK3_4 12/21/04 0852 0 12/21/04 0900 * 16 232884__1_S___ 12/21/04 0910 0 17 232884_1_S_MS_IQ4LSTTC2_6 12/21/04 0936 0 18 232884_1_S_MSD_I04LSTTC2_6 12/21/04 0943 0 19 232883_2_S___ 12/21/04 0957 0 1 10 2 3 2 8 8 3 J S ___ 12/21/04 1014 0 1 11 232883_3_S___ 12/21/04 1030 0 1 12 232883_9,,S___ 12/21/04 1047 0 1 13 232883_4_S___ 12/21/04 1103 0 1 14 232B83_5_S___ 12/21/04 1124 0 1 15 2 3 2 8 8 3 _ 6 _ S _ 12/21/04 1139 0 1 16 __ CCV_I04LSTTC2_ 12/21/04 1202 0 1 17 ___CCB__ 12/21/04 1208 0 1 18 232883^7^5___ 12/21/04 1215 0 1 19 232883_8_S___ 12/21/04 1235 0 1 20 232883_10_S__ r 12/21/04 1246 0 1 21 2328S5_1_S___ 12/21/04 1328 0 1 22 232885_2_S___ 12/21/04 1344 0 1 23 232885_3_S___ 12/21/04 1406 0 1 24 232885_4_S___ 12/21/04 1443 0 1 25 2 3 2 8 8 5 ^ 5 ___ 12/21/04 1504 0 1 26 1 27 232885_6_S___ 232885_7_S__ ,, 12/21/04 1516 12/21/04 1530 0 0r 1 28 ___CCV_I04LSTTC2_ 12/21/04 1545 0 *** RUN LOG (V2 ) 12/30/04 12:47 Page 2 40 *** QC Summary *** (V2 ) Total organic carbon (Soils) Mttod Code.,,: TOCS Bat;h Code...: 137664 Sta t-us...... : RVUD Batch Date.. : 12/21/04 Batch Time.. : 95 User Name,.. : els OC Code. Calc Codei TOCS . TOCS Location code.. 57222 Grp smp sample ID Pos Test Result Known Original 1 2 ___ICV_I04LSTTC2^ 1 TOC 1731.98 2000 1 3 ^__ MB__ 1 TOC -1.80 1 4 ___LC5_I00FSTLIC3_ 1 TOC 5172.63 4780 1 5 ___LCD_ 100FSTL1(3^4 1 TOC 3614.82 4780 5172.65 17 1a 232804_1_S_MS_I04LSTTC2_6 232884_1_S_MSDJ04LSTTC2_6 5 TOCAV2 2349.75 5 TOCAV2 1955.99 2000 2000 693.67 693.67 1 16 CCV I04LSTTC2 1 TOC 2038.04 2000 1 17 ___CCB__ 1 TOC '1.88 1 28 ___CCV_I04LSTTC2_ 1 TOC 2032.44 2000 1 29 ,___CCB__ 1 TOC '2.90 Report Date: 12/30/04 12:47 Equipmeht Cede.: T0C4 Import Cotie___ : Alternate QC Res 87 F QC Res F 2349.75 108 76 128.7 91.3 102 35 27 * 102 Page 1 41 *** RAW TEST DATA *** <V2 > Total Organic Carbon (Soils) Method Code,. TOCS Batch Code... 137664 Status...... KVWD Batch Date...: 12/21/04 Batch Time...; 958 User Name___ : els SAMPLE: Grp Ros Sanala ID 11 ICAL IQ4LSTTC1 12 ICV 104LSTTC2 13 MB 14 LCS I0FSTLK3 15 LCD IO0FSTLK3 1 6 2328S4 1 S 1 7 232884 1 S MS I04LSTTC2 6 1 8 232884 1 S MSD 104LSTTC2 6 1 9 232883 2 S 1 10 232883 1 S 1 11 232883 3 S 1 12 232883 9 S 1 13 232883 4 S 1 14 232883 5 S t 15 232883 6 S 1 16 CCV I4LSTTC2 1 17 CCB 1 18 232883 7 S 1 19 232883 8 S 1 20 232883 10 S 1 21 232885 1 S 1 22 232885 2 S 1 23 232885 3 S 1 24 232885 4 S 1 25 232885 5 S 1 26 232885 6 S 1 27 232885 7 S 1 28 CCV I04LSTTC2 1 29 CCB__ C Code... .... : TOCS Calc code. Location code..: 57222 Dilution TOC mg/tg TOC2 mS/Kg Report Data: 12/27/04 16:35 Equipment Code.: TQC4 Inport Code TOC3 mg/Kg TOC4 mg/Kg T0CAV2 mg/Kg 1731.98 -1.80 5172.65 3614.82 813.51 2349.75 1955.99 1553.41 2653.69 1263.33 868.92 827.70 938.29 816.91 2038.04 -1.88 878.19 346.29 432.44 6481.37 1671.64 800.78 835.75 1134.86 640.69 908.96 2032.44 -2.90 573.84 1014.91 2102.78 1008.78 826.45 544.33 53.85 659.09 750.33 391.56 497.05 5750.30 1310,59 812.41 792.59 856.93 1016.37 1060.09 693.67 2349.75 1955.99 1284.16 2378.24 1136.06 847.68 686.01 496.07 738.00 814.26 168,93 464.75 6115.B4 1491,12 806.60 814.17 995.89 828.53 984.52 Page 1 42 *** RAW TEST DATA *** (V2 ) Total Organic Carbon (Soils) Hethod Code.. TOCS Batch Coda... 137664 Status...... RVUP Batch Date...: 12/21/04 Batch Time...: 95B User Rame___ : d s SAMPLE: Grp Pos Sanale ID 11 ICAL IQ4LSTTC1 12 ICV 04LSTTC2 13 MB 14 LCS IQQFSTLI3 15 LCD IQ0FSTLK3 1 6 232884 1 S 1 7 232884 1 S MS 104LSTTC2 6 1 8 232884 1 S MSD J4LSTTC2 6 1 9 232883 2 S 1 10 232883 1 S 1 11 232883 3 S 1 12 232883 9 S 1 13 232883 4 S 1 14 232883 5 S 1 15 232883 6 S 1 16 CCV I4LSTTC2 1 17 CCB 1 18 232883 7 S 1 19 232883 8 S 1 20 232883 10 S 1 21 232885 1 S 1 22 232885 2 S 1 23 232885 3 S 1 24 232885 4 S 1 25 232885 5 S 1 26 232885 6 S 1 27 232885 7 S 1 28 CCV I04LSTTC2 1 29 CCS__ QC Code...... . : TOCS Calc Code___ . TOCS Location Code..: 57222 Di Lut ion TQCAV3 mg/Kg TOCAV4 mg/fcg Report Date; 12/27/04 16:35 Equipment Code.: TOC4 Import Code___ : TOCR1 ug TQCR2 ug TOCR3 ug 86.5989 -0.2884 178.9736 91.8164 35.8759 183.5151 141.4178 78.1366 178.3283 85.7799 67.7755 61.9122 75.1571 73.9307 101,9020 -0.3007 84.8331 27.2534 41.4281 178.8858 55.6656 33.6327 30.9226 62.6440 38.9539 58.7191 101.6219 -0.4648 36.2094 72.5663 132.6853 84.9389 62.8926 53.5078 43.5094 53.2545 58.9010 34.9269 48.1147 124.2065 48.3608 32.3341 29.6429 50.0447 60.0677 65.9375 -- Page 2 43 *** RAU TEST DATA *** <V2 ) Total organic Carbon (Soils) Method Code.. : TOCS Batch Code.. : 137664 Status....... : RVUD Batch Date...: 12/21/04 Batch Time__ : 958 User Name.*..: cls SAMPLE: Grp Pos Sample ID 11 ICAL I04LSTTC1 12 ICV I04L5TC2 13 MB 14 LCS I00FSTLK3 15 LCD IDDFSTLK3 1 6 232884 1 S 1 7 232884 1 S MS IQ4LSTC2 6 1 8 232884 1 S MSP I04LSTTC2 1 9 232883 2 S 1 10 232883 1 S 1 11 232883 3 S 1 12 232883 9 S 1 13 232883 4 S 1 14 232833 6 S 1 15 232883 6 $ 1 16 CCV I04LSTTC2 1 17 CCB 1 18 232883 7 S 1 19 232883 8 S 1 20 232883 10 S 1 21 232885 1 S 1 22 232885 2 S 1 23 232885 3 S 1 24 232885 4 S 1 25 232885 5 S 1 26 232885 6 S 1 27 232885 7 S 1 28 CCV I04LSTTC2 1 29 CCB 0C Code.* TOCS Cale Code .... : TOCS Location Code* 57222 Di luti on T0CR4 ug WT1 9 Report Date; 12/27/04 16:35 Equipment Code.: T0C4 Import Code UT2 UT3 UT4 gg9 0.05 0*16 0.0346 0.0254 0.0441 0.0781 0.0723 0.0503 0.0672 0.0679 0.0780 0*0748 0.0801 0.0905 0.05 0.16 0.0966 0.0787 0.0958 0.0276 0.0333 0.0420 0.0370 0*0552 0*0606 0.0646 0.05 0,16 0.0631 0.0715 0.0631 0*0842 0.0761 0.0983 0.808 0.0808 0.0785 0,0892 0.0968 0.0216 0.0369 0.0398 0.0374 0.0584 0.0591 0.0622 Page 3 44 *** RAW TEST DATA *** Total Organic Carbon [Soils) Method code.. TOCS Batch Code... Status....... RVWD BHtch Date...; 12/21/04 958 User Name___ : els SAMPLE: Grp Pos Sample ID 11 ICAL I04LSTTC1 12 ICV I04LSTTC2 13 MB 14 LCS I0FSTLK3 15 LCD I00FSTLK 1 6 232884 1 S 1 7 232884 1 S HS I04LSTTC2 6 1 8 232884 1 S HSD I4LSTTC2 6 1 9 232883 2 S 1 10 232883 1 S 1 11 232883 3 S 1 12 232883 9 S 1 13 232883 4 S 1 14 232883 5 S 1 15 232883 6 S 1 16 CCV IQ4LSTTC2 1 17 CCB 1 18 232883 7 S 1 19 232883 8 S 1 20 232883 10 S 1 21 232885 1 S 1 22 232885 2 S 1 23 232885 3 S 1 24 232885 4 S 1 25 232885 5 1 26 232885 6 S 1 27 232885 7 S 1 28 CCV I04LSTTC2 1 29 ___CCB__ QC code... Cslir Code. ____ : TOCS Location Code..: 57222 D i lution DLFAC N/A ICS mg/Kg 3.2000 1.0000 4.6243 6.2992 2.9851 2.0487 2.2130 2.6273 2.4559 2.1039 2.0766 1.8486 0.3603 1.8681 3.2000 1.0000 1.8275 1.9059 1.6615 6.5041 4.5584 3.9120 4.3011 2.8169 2.6689 2.5237 3.2000 1.0000 <V2 ) Report Date: 12/27/04 16:35 Equipment Code.: TOC4 Imort Code * TCS2 mg/Kg TCSAV2 mg/Kg TICS ng/Ks Page 4 45 Method: STLChicago Total Organic/Inorganic Carbon LabNet Batch: / ? 7 ( lf EPA 415.1 EPA 415.1. mod. for IC SW 846 9060 Lloyd Kahn Instrum ent. Phoenix 8000 TOC 4 Matrix: t soil water Standard Curve: Date of curve / ? /(}./<?)________ us C o 10 20 40 80 100 120 200 300 400 measured, us C *2, Y V "2./3 ? r y# (fo r j\M jv b // V/ Corr. Coeff.: V'intercept: slope: )y/ Calculations: soils: mg/kg = u s C from instrument grams sample Soils are dried as part o f the preparation step, so do not correct for % solids. waters: mg/L = mg/L X dilution Standards Traceability: Stock I : Calibration and Curve : Stock II: LCS, ICV, CCV, Matrix spikes Solid LCS : F oe FS ^ ^ T TO / -g W ^ Spiking Levels; LCS ICV CCV MS/MSD mg/Kg ugC ugC mg/Kg mg/Kg mg/L mg/L mg/L mg/L Analyst: f r f aReviewer: Date of analysis: / Z / z C _Date: f ^ J ______ 46 Calibration Report Print Date/Time: 2004/12/21 7:53:52 Cal. Curve ID: SOILCURVE Created: 12/13/2004 13:36 Calibration Factor (m): 9.841 e+04 Y Intercept (b): -250134 r-squared: 0.99935 Standard ID Y X Expected Measured Message Date & Raw Data ug C ug C Tim e 0 ugram C -8891 0.000 2.451 No Sample Det 12/13/2004 11:24 10ugramC 911065 10.000 11.800 12/13/200411:42 20 ugram C 1853385 20.000 21.375 12/13/2004 11:48 40 ugram C 3745719 40.000 40.605 12/13/200412:04 120 ugram C 11194916 120.000 116.302 Endpoint Time 12/13/200412:28 200 ugram C 18654032 200.000 192.099 12/13/2004 12:46 300 ugram C 29462156 300.000 301.928 12/13/200412:59 400 ugram C 39451668 400.000 403.439 Endpoint Time 12/13/2004 13:19 Multiple Analysis Report Print Date/Time: 2004/12/21 15:53:46 Sample ID Result Std. Dev. RSD Mode ALT IGV 86.5989 TC ICB-MB -0.2884 TC LCS 51.5042 TC LCS........................ ........ 178.9736............. ...TC ,, LCD 91.8164 TC 232884-1 35.8759 TC 232884-1........................... 36.2094... .......... TC 232884-1 ms -0.3194 TC 232884-1 ms 183,5151 TC 232884-1 msd........ ............... 141.4178... ...........TC 232883-2 78.1366 TC 232883-2 72.5663 TC 232883-1............... ........... -0.2423... . ...TC . 232883-1 178.3283 TC 232883-1 132.6853 TC 232883-3........................... 85.7799... .......... TC 232883-3 84,9389 TC 232883-9 67.7755 TC 232883-9........................... 62.8926... .......... TC 232883-4 61.9122 TC 232883-4 53,5078 TC 232883-5........................... 74.1571... .......... TC . 232883-5 43.5094 TC 232883-6 73.9307 TC 232883-6........................... 53.2545... .......... TC . CCV 101.9020 TC CCB -0.3007 TC 232883-7........................... 84,8331.,, .......... TC . 232883-7 17.4619 TC 232883-7 58.9010 TC 232883-8................ ...........27.2534... .......... TC . 232883-8 34.9249 TC 232883-10 41.4281 TC 232883-10.............. ............48.1147... ...........TC 232885-1 466.7505 TC 232885-1 178.8858 TC 232885-1................ ...........124.2065... ...........TC 232885-2 55.6656 TC 232885-2 48.3608 TC 232885-3................ ...........-0.4558.............. ...TC .. 232885-3 33.6327 TC 232885-3 32.3341 TC 232885-4................ ...........30.9226... 232885-4 29.6429 232885-5 62.6440 . ...TC . TC TC 232885-5................ .......... 50,0447... . ...TC . 232885-6 38.9539 TC 232885-6 60.0677 TC 232885-7................ ...........58.7191... . ...TC . 232885-7 CCV 65.9375 101.6219 TC TC CCB........................ ....... -0.4648.............. ...TC .. 48 Detailed Analysis Report Print Date/Time: 2004/12/21 15:54:02 Sample ID: ICV Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL Mode: TC Filename: 12210820 .S' Timestamp: 12/21/200408:26 Sample Type: Cal. Verification Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 86.5989 86.5989 8271924 0.942 1.939 282 Sample ID: ICB-MB Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL Mode: TC Filename: 12210827 Timestamp: 12/21/2 Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 -0.2884 -0.2884 -2611 1.505 1483 120 Last Messaae: No Samole Detected aA S y Mode: TC Filename: 12210836 Sample ID: LCS Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL Timestamp: 12/21/2004 08:41 Sample Type: Sample Mode: TC )atFailenaBmeeg:inni1n2g210E8n4d5ing In/tegration ne BasTeliimneestamTipm:e 12/21/20^4 08:52 09 Sa1.m93p0le Ty2p.e9:3S0ampl2e35( y Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 178.9736 178.9736 17638262 1.819 2.818 370 Sample ID: LCD Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL Mode: TC Filename: 12210855 ( Timestamp: 12/21/2004 09:00 Sample Type: Sample \ Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 49 R ep# ppm C u g C RawDataX Beginning Ending integration Baseline Baseline Time 1 53,2545 53.2545 5266458 ^ 3 8 3 3.381 234 Sample ID: CCV Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL Mode: TC Filename: 12211156 Timestamp: 12/21/200^12:02 Sample Type: Cal. Verification Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 101.9020 101.9020 9777878 1.546 2.545 299 Sample ID: CCB Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL Mode: TC _ Filename: 12211205 " Timestamp: 12/21/20IM 12:0ii Sample Type: Sample R ep# ppm C ugC Raw Data Beginning Ending Integration Baseline Baseline Time 1 -0.3007 -0.3007 -3828 1.695 1.637 120 Last Message: No Sample Detected Sample ID: 232883-7 Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL Mode: TC leame: 12211210 Timestamp: 12/21/2 ample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 84.8331 84.8331 8374055 1.692 2.692 289 Sample ID: 232883-7 Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL '/Il/kls J ' J Mods: /^ X F ile n a m e : 12211218 n .^ T im e s ta m p : 12/21/200412:22 L j^i Sample Type:^am ple Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 17.4619 17.4619 1744159 1.962 2.959 \ 208 Sample ID: 232883-7 Method: boat Cal. Curve: SOILCURVE Mode: TC Filename: 12211225 Timestamp: 12/21/2 12:30 50 Operator ID: CAROL Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 58.9010 \ 58.9010 5822114 1.961 2.955 260 Sample ID: 23288^-8 Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL Mode: TC Filename: 12211230 f Timestamp: 12/21/2004 12:35 Sample Type: Sample Rep # ppm C ug C \ Raw Data Beginning Ending Integration ^Baseline Baseline Time 1 27.2534 27.2534 ^ 0 7 7 2 4 2.428 3.425 219 Sample ID: 232583-8 Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL Mode: TC Filename: 12211235 Timestamp: 12/21/200412:40 Sample Type: Sample Rep # ppm C ug C Raw Data Baseline 1 34.9249 34.9249 3462668 Beginning Ending Integration iseline Time .224 3.223 246 Sample ID: 232883-10 Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL M ode\ TC Filename: \12211242 Timestamp: 12/21/200412:46 Sample Type: Sample I j Re p # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 41.4281 41.4281 4102640 6.401 7.396 \ 184 Sample ID: 232883-10 Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL Mode: TC Filename: 12211247 Timestamp: 12/21/200^12:52 Sample Type. Sample Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 48.1147 48.1147 4760651 2.162 3.161 249 ^ Mode: TC 0 Filename: 12211315 Timestamp: 12/21/2004 13:21 Operator ID: CAROL 1* Sample Type: Sample ' ( ' ^iv Rep # ppm C \u g C Raw Data Beginning Ending Baseline Baseline Time 1 4667505 466,7505 45957920 2.150 3.150 Integration 345 Sample ID: 232885-1 Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL Mode: TC Filename: 12211323 f Timestamp: 12/21/200413:28 Sample Type: Sample 1 ^ Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 178.8858 178.8858 17629628 2.645 3.644 280 Sample ID: 232885-1 Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL Mode: TC Filename: 12211331 Timestamp: 12/21/200413:36 Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 124,2065 124,2065 12248724 2,282 3.282 265 Sample ID: 232885^2 Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL Mode: TC - Filename: 12211339 / Timestamp: 12/21/2064 13:' Sample Type: Sample l / Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 55.6656 55.6656 5503725 2.209 3.208 245 Sample ID: 232885-2 Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL Mode: TC Filename: 12211351 Timestamp: 12/21/2004 13:56 Sample Type: Sample R ep# ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 48.3608 48.3608 4784873 1.633 2.632 248 Sample ID: 232885-: Method: boat Cal. Curve: SOILCURVE r a Operator ID: CAROL \ / Mode: TC Filename: 12211358 Timestamp: 12/21/200414:01 Sample Type: Sample ;= S = 3 52 R ep# ppm C ugC (f*aw D ata Beginning Ending Integration \ ( x v - ' U 1Baseline Baseline Time 1 -0,4558 -Q.45f>8 -19085 2,015 1.541 99 Last Message: Canceled Sample ID: 232885-3 Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL Mode: TC Filename: 12211402 Timestamp: 12/21/2004/14:06 Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 33.6327 33,6327 3335504 3.333 4.328 201 Sam plelD : 232885-3 Method: boat Cai. Curve: SOILCURVE O perato rio: CAROL Mode: TC Filename: 12211431 Timestamp: 12/21/2004 14:37 Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 32.3341 32.3341 3207714 1.637 2.636 285 Sam plelD : 232885-4 Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL Mode: TC Filename: 12211438 Timestamp: 12/21/2004 Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 30.9226 30.9226 3068810 1.838 2.837 230 Sam plelD : 232885-4 Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL Mode: TC Filename: 12211450 Timestamp: 12/21/2004 14:65 Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 29,6429 29.6429 2942870 1.708 2.706 269 Sam plelD : 232885-5 Method: boat Cal. Curve: SOILCURVE Mode: TC Filename: 12211459 Timestamp: 12/21/2 Operator ID: CAROL Sample Type: Sample R ep# ppm C ugC Raw Data Beginning Ending Integration Baseline Baseline Time 1 62.6440 62.6440 6190454 1.827 2.825 243 ^I=i!==?=======E===========x:3:X2=================================SS^S:SKS;==^ Sample ID: 232885-5 Method: boat Cal. Curve: SQILCURVE Operator ID: CAROL Mode: TC Filename: 12211505 Timestamp: 12/21/200415:10 Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 50.0447 50.0447 4950579 1.771 2.768 224 Sample ID: 232885-6 Method: boat Cal, Curve: SOILCURVE Operator ID: CAROL Mode: TC Filename: 12211512 Timestamp: 12/21/201 Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 38.9539 38.9539 3859158 3.971 4.970 199 Sample ID: 232885^6 Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL Mode: TC Filename: 12211517 Timestamp: 12/21/200415:22 Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 60.0677 60.0677 5936929 2.520 3,516 242 Sample ID: 232885-7 Method: boat Cal, Curve: SOILCURVE Operator ID: CAROL Mode: TC Filename: 12211524 Timestamp: 12/21/20 Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 58.7191 58.7191 5804212 1.978 2.976 289 Sample ID: 232885-7 Method: boat Filename: 12211530 Cal, Curve: SOILCURVE Mode: TC Timestamp: 12/21/2004 15:35 Operator ID: CAROL Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 65.9375 65.9375 6514565 2.105 3.104 263 Sample ID: CCV Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL Mode: TC Filename: 12211538 Timestamp: 12/21/^004 15:45 N Sample Type: Cal. Verifrcatiqp- Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 101.6219 101.6219 9750314 1.707 2.706 386 Sample ID: CCB Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL Mode: TC Filename: 12211546 Timestamp: 12/21/2004/15:48 Sample Type: Sample i / R ep# ppm C ugC Raw Data Beginning Ending Integration Baseline Baseline Time 1 -0.4648 -0.4648 -19973 2.407 2.111 120 Last Message: No Sample Detected ;;SS?55^====== o IL unicago Page No 110 TOC in Soils Book No ; ' ^ T T T ' Method: Lloyd Kahn instrument Phoenix sooo (TQC4 LabNet Batch: / 3 7 C Y C a lcu la tio n : Date of Standard Curva: /D .-//3 /& 9 : TOC(mg/kg) ug C / grama sample B ook#^ ? ^ ? Paoe# /&/ MS, MSD Known Cone, (mg/kg) 100 ug C fgrams sample MS, MSD Observed (mg/kg) = ug C / grams sample MS, MSD Ree. * fobserved mg/ko - ava, sample result (mo/ko)l x 100 known concentration in mg/kg Standard Traceability: Stock I (Curve) TT) (Note: Working Standards are prepared daily from the noted Stock Solutions.) T T r C / Stock II (ICV/CCV) - L O ^ i S V T ^ ^ LCS Source ID CS True Value V 7 Acceptance Range Sample ID: Sample Weight (g) ugC Comments: V<V' a .cK 'S'M/ O ' i Q j AC *7 ^ 1 --U <ts J-ic / ux o x n h . O lX H o - 3 x m ~ ( _ O- 0 9*4 t 0 ,0 O K I ~ l -CLo G j q . X/ -Q ___ / T f.T liC 9.1 X / o / 3 C f7<r7 X -X iy 1 C2v /><L ^ ^ 7 7, X d fy _ -- ...... I ^ / in C. o -O -J V i J ~ / H Q , <77.2 3 o. 0 0 0 } I f } . K IS / M H T iT XitteLC 7 . V /7 P U m i {#V2-)?C \ f 1C- ! ~ 0 , 0? /(" *72. $ T O _1__ --,, :- /f_- /O7 i Lj ^/yOCJ_____ X C X n 1 J ~J . 0 Gl 9- /7 P 72f 7 ^rv^Hr "T-------------------------------------- 1 -- l c. C O ' } / / - 7 Pc'? ______ 1_____ o, QC 71 .-"S o X , * y r t gO C17 /r r . 'wi S 7 f _ 0 , C i t i ~ Z T fir~ / - v A- O 7 V P Gl c f / l t __ ^ L _ 7 0 .c a fl a . <?roi s~3. 7 , 7<71 Prep Analyst\ Analyst: R ev ie w e d b y :_ /} --- / Jdk^ Date: f^ / /ff / f $ Date: / T . / 2/ / r r______ Date:. CHI*22'12-09S/B48/Q1 STL Chicago Page No.:, 111 TOC in Soils Sock No. 3 7 P 7 Method; Lloyd Kahn Instrument Phoenix 8000 (T LabNet Batch; fWff1 C a lcu la tio n : Date of Standard Curve; TOC (mg/kg) ug C / grams sample B ook#_________Page#, MS, MSD Known Cona (mg/kg) =* 100 ug C / grams sample MS, MSD Observed (mg/kg) = ug C / grams sample MS*MSDRec. * Observed ma/ko - avo. sample result fmo/katl *100 known concentration in mg/kg Standard Traceability: Stock I (Curve) LCS Source ID Sample ID; cc / cfe Sample Weight (g) ugC Q. OZop- V3StffY 0 . 0 qo 7 ^ 7 5 ? 0 , r) Y O, jixrvr a. o< //, 9^ 2^ . f< - 0, 3m7 Comments; a.O % C ^/,%37/ L________ i = L --- J _ 7 ,0 -f-7.% SY, 9ol& 0 , 7JT7 <21 --Y '. OY ? 2 1 H .fiif 1 '~Q O, 0 9SP <i( < f^f y s -- ^s= ^- 0 n <?6Y -fr:-rrrrf-- t. //V ? W4.7m ?-- S*.S 1\-_ . t?. G2S7U J~Sr. &V> -/ - - c 0. 03^5 j'jf/, 2-d?r~ fy, u y te*' - c <> }>(r 7 _ f r. _~ZZ//,'*<r-fLr*Cs3a j _ . .1 ^ n. /*>yxO L- ?- \~ y fc Q2>< T ' 0310 31. flz? 7=7.7 7 V / le, Tz-z _______ L - o. r t i i Prep Analyst_j2>vl A n alyst^ Reviewed by:___ Date: / /^/c f /ijat- ^ Data: / i r / Y ____ 5 7 Date: _____ CHM 2-12*95/0-05/01 112 STL Chicago Paae No.: TOC in Soils BOOR N o, - 7 / / ; Method; Lloyd Kahn Instrument Phoenix 8000 fTOC4l LabNet Batch;. C alculations: Date of Standard Curve:. TOC (mg/kg) * ug C / grams sample B ook#_________ Paa # MS, MSD Known Cone, (mg/kg) 100 ug C / grams sample MS, MSD Observed (mg/kg) ug C / grams sample MS. MSP Rsc. - fobserved mo/ko avo, sample result fmg/kg)1 x100 known concentration in mg/kg Standard Traceability: (Note: Wbridng Stanfty r*lJfepared daily from the noted Stock Solutions.) Stock I (Curve)_____________ ^ J ^ S t t i c k II (ICV/CCV) LCS Source ID / ^ " LCS True Value___________ Acceptance Range. SampleID: SampleWeight(g) ugC Comments: -. 1 1 O, o, rfv ^ 0 O' bor &,C, &/<i *7 o . o sj/ S O fa'll A.-2_'/ - 1 .teVC. Wr/-0 .0 <r\ St v CO,/ n o s ' .r\\ c*C/b O- ( -fo0i,.VO6XYiSf/ \\\\ \\.\\ \V..\\. Prep Analyst Analyst: Reviewed by: Date: 9 / f t " '} ? Date: S S t/z -t/c -r Date: < S l> js j . *** RUN LOG *** (V2 ) 12/28/04 12:00 Total Organic Carbon (Soils) Method Code..: TOCS Batch Code...; 138147 Status....... :RPT Batch Date...: 12/28/04 Batch Time...: 1124 User Name...... : els QC C o d e . : TOCS CaLc Code...... : TOCS Location Code.,: 57222 Equipment code.: TOC4 Inport Code---- : TEST CODE TTTTTTTTTTTTT D DOO CCC 1II CcC0ccCSSs CC0 234AAA 2Asss VVV V 2A 234 2 2 SAMPLE: Grp Pos Sample ID Dilution TEST POS Date / Time 1234 567 111222 78 90 12 11 ___ ICAL_I04LSTTC1_ 0 12 ___ ICV_IQ4LSTTC2_ 12/27/04 0911 0 13 ___MB__ 12/27/04 0923 0 14 ___LCS_IOOFSTLK3_3 12/27/04 0946 0 l5 ___LCD_l0OFSTLK3_3 12/27/04 0953 0 16 232796_5_S___ 12/27/04 1000 0 17 232796_6_S___ 12/27/04 1022 0 18 232885_S_S___ 12/27/04 1052 0 19 232885_8_S_MS_104 LSTTC2_8 12/27/04 1106 0 1 10 232S$5_8_S_MSD_I04LSTTC2_8 12/27/04 1118 0 1 11 232885m9_S___ 12/27/04 1129 0 1 12 232885_10_S__ r 12/27/04 1147 0 1 13 232885_11_S___ 12/27/04 1222 0 1 14 232885 12 S 12/27/04 1240 0 1 15 232S$5_13_S___ 12/27/04 1303 0 1 16 ___CCV_I04LSTTC2_ 12/27/04 1318 0 1 17 ___C C B _ 12/27/04 1325 0 1 18 232885_14_S___ 12/27/04 1352 0 1 19 232885 15_S___ 12/27/04 1418 0 1 20 232885_16_S___ 12/27/04 1435 0 1 21 232885 17 S___ 12/27/04 1446 0 1 22 232885J 8 _ S ___ 12/27/04 1513 0 1 23 232885 19 S 12/27/04 1529 0 1 24 232885_20_S___ 12/27/04 1550 0 1 25 ___CCV_104LSTTC2^ 12/27/04 1609 0 1 26 ___C C B _ 12/27/04 1620 0 Page 1 -- 59 **+ Oc Sunnary #** (V2 ) Total Organic: Carbon (Soils) Method Code..: TOCS Batch Code...: 138147 Status.,**.*-; RVlfl) Batch Date...: 12/28/04 Batch Time...: 1124 User Name____ : els Gc Code....... : TOCS Calc Code*...... TOCS Location Code..: 57222 Grp Smp Sample ID Poe Test Result Known Original 1 2 __ ICV_I04LSTTC2_ 1 TOC 1879*51 2000 1 3 ___MB__ 1 TOC -1*06 1 4 ,,__LCS_I00FSTLK3_3 1 TOC 4713.16 4700 -1.08 1 5 ___LCD_I00FSTLK3_3 1 TOC 3954.88 4780 -1.08 1 9 232885mB_S_MS_104LSTTC2_8 1 10 232885_8_SttMSD_I04LSTTC2_8 1 16 CCV I04LSTTC2 5 TCAV2 1846.36 5 T0CAV2 1675.61 1 TOC 2038.32 2000 2000 2000 544.74 544.74 1 17 ___ CC B__ 1 TOC -2.04 1 25 ___CCVJ04LSTTC2_ 1 TOC 2043.79 2000 1 26 ___CCB__ 1 TOC -6.21 Report Date: 12/29/04 12:22 Equipment Code,; T>C4 import Code...*: Alternate OC Ree 94 F QC Res F 4713.16 1846.36 99 63 91 85 102 17 6*8 102 Page 1 60 RAW TEST DATA *** (V2 ) Total Organic Carbon (Soils) Method Code..: TOCS Batch Code,,.: 138147 Status.... RVWD Batch Date... 12/28/04 Batch Time... 1124 User Kerne___ els SAMPLE: Grp Pos Sample ID 11 ICAL I04LSTTC1 12 ICV I041STTC2 13 MB 14 LCS I00FSTLK3 3 15 LCD I00FSTLK3 3 1 6 232796 5 S 1 7 232796 6 S 1 8 232885 $ S 1 9 232885 8 S MS I04LSTTC2 8 1 10 232885 8 S MSD I04LSTTC2 8 1 11 232885 9 S 1 12 232885 10 S 1 13 232885 11 S 1 14 232885 12 S 1 15 232885 13 S 1 16 CCV I04LSTTC2 1 17 CCB 1 18 232885 14 S 1 19 232885 15 S 1 20 232885 16 S 1 21 232885 17 S 1 22 232885 18 S 1 23 232885 19 S 1 24 232885 20 S 1 25 CCV I4LSTTC2 1 26 CCB 9C Code,.,.... : TOCS Calc Code..,.-,; TOCS Location Code..: 57222 Di luti on TOC mg/Kg TOC2 mg/Kg Report Date: 12/29/04 12i22 Equipment Code.: T0C4 Import Code,,,,; TOC3 mg/Kg TOC4 mg/Kg TOCAV2 mg/Kg 1879.51 -1.08 4713.16 3954.88 14763,43 8034.17 588.97 1846.36 1675.61 5257.61 3831.14 1563.72 1308.87 6331.02 2038,32 -2.04 2601.24 1577.48 989.92 4875.90 2687.02 1613.62 1853.64 2043.79 -6.21 20808.70 5130.B4 500.51 5466.32 2931.89 822.72 1268.09 5778.91 1456.87 1544.BO 1247.73 4632.97 2047.90 1229.03 1671.70 17786.07 6582.51 544.74 1846.36 1675.61 5361.97 3381.51 1193.22 1288,48 6054.97 2029.06 1561.14 1118.83 4754.43 2367.46 1421,33 1762.67 "TM"-- Page 1 ----------------- -------------------- --- -- ------------ - 61 RAW TEST DATA *** <V2 ) Total Organic Carbon (Soils) Method Code.. TOCS Batch Code... 138147 status...... RVWD Batch Date...: 12/28/04 Batch Time...: 1124 User Name___ : els SAMPLE: Grp Pos Sanple ID 11 ICAL I04LSTTC1 12 ICV 104LSTTC2 13 MB 14 LCS I00FSTLK3 3 15 LCD IQQFSTLK3 3 1 6 232796 5 S 1 7 232796 6 S 1 8 232685 6 $ 1 9 232885 8 S MS I04LSTTC2 8 1 10 232885 8 S MSD I04LSTTC2 8 1 11 232885 9 S 1 12 232885 10 S 1 13 232885 11 S 1 14 232885 12 S 1 15 232885 13 S 1 16 CCV I04L5TTC2 1 17 CCB 1 18 232885 14 S 1 19 232885 15 S 1 20 232885 16 S 1 21 232885 17 S 1 22 232885 18 S 1 23 232885 19 S 1 24 232885 20 S 1 25 CCV IQ4LSTTC2 1 26 CCB OC Code... ....: TOCS Calc Code. ___ : TOCS Location Code..: 5/222 Dilution TOCAV3 mg/Kg T0CAV4 mg/Kg Report Date: 12/29/04 12:22 Equipment Code.; TOC4 Inport Code __ : To c r I ug TDCR2 ug TOCR3 Ufl 93.9756 -0,1730 121.1281 111.5275 31,0032 32.1367 35.2206 128.8759 126.3410 329.6523 253.6214 84.9098 71.5951 236.1471 101.9159 -0.3268 108.7319 95.7528 57.2171 173.0943 102.9129 74.3877 99.3550 102.1897 -0.9940 68.6687 45.1514 36.7372 258.5568 152.1652 43.2751 73.9295 153.7190 60,4603 100.2575 80.6035 149.1816 85.6024 62.0662 103.8124 Page 2 62 *** RAW TEST DATA CV2 ) Total Organic carbon (Soils) Method Code.. TOCS Batch Code... 1 3 B K 7 Status...... RVWD Batch Date...: 12/28/04 Batch Time...: 1124 user Name___ : els SAMPLE: Grp Pos Sample ID 11 ICAL IQ4LSTTC1 12 ICV I04LSTTC2 13 MB 14 LCS I00FSTC3 3 15 LCD I00FSTLK3 3 1 6 232796 5 S 1 7 232796 6 S 1 8 232885 8 S 1 9 232885 B S Ms I04LSTTC2 8 1 10 232885 8 S MSD I04LSTTC2 8 1 11 232885 9 S 1 12 232885 10 S 1 13 232885 11 S 1 14 232885 12 S 1 15 232885 13 S 1 16 CCV J04LSTTC2 1 17 CCB 1 18 232885 14 S 1 19 232885 15 S T 20 232885 16 S 1 21 232885 17 S 1 22 232885 18 S 1 23 232885 19 S 1 24 232885 20 S 1 25 CCV I04LSTTC2 1 26 CCB QC code... m ___ : TOCS Calc Code. ,,,, .7 TOCS Location Code..: 57222 Di lut ion TOCR4 US UT1 9 Report Date: 12/29/04 12:22 Equipment Code.; TOC4 import Code___ : WT2 WT3 UT4 999 0.05 0.16 0.0257 0.0282 0.0021 0.0040 0.0598 0.0698 0.0754 0.0627 0.0662 0,0543 0.0547 0.0373 0,05 0.16 0.0418 0.0607 0.0578 0.0355 0.0383 0.0461 0.0536 0.05 0.16 0.0033 0.0088 0.0734 0.0473 0,0519 0.0526 0.0583 0.0266 0.0415 0.0649 0.0646 0.0322 0.0418 0.0505 0.0621 Page 3 63 RAU TEST DATA *** Total Organic Carbon (Soils) Method Code..; TOCS Batch Code.. . : 13S147 Status............ I FtVUD Batch D a te .. . 12/28/04 Batch Tim e... 1124 User Name___ cls SAMPLE: Grp Pos Sample ID 1 1 ___1CAL I04L$TTC1_ 1 2 ___I C V J 0 4 L S T T C 2 * 13 MB " 14 LCS I00FSTLK3 3 15 LCD~I00F5TU(3^3 1 6 232796 5 S 1 7 232796*6 $ 1 S 232885 8 S 1 9 232885*8 S MS I04L5 1 10 232885 S'V m SD IQ4L 1 11 232885 9 S " 1 12 232885*10 S 1 13 232885 ll's 1 14 232885"12 S 1 15 232B85J3 S 1 16 ___CC\M04LSTTc 2_ 1 17 ccb" 1 18 232885 14 S 1 19 232885 15 S 1 20 232S85" 16 S 1 21 232885" 17 S 1 22 232885~18_S 1 23 232885*19 S 1 24 232885 20 S 1 25 CCVJ04LSTTC2 1 26 ccb" 0C Code.............. : TOCS Cale Code.......... : TOCS Location Code..: 57222 D ilu tio n DLFAC N/A TCS mg/Kg 3.2000 1.0000 6.2257 5.6738 59.2593 25.0000 2.4024 2.2923 2.1220 2.9091 2.7096 2.9935 2.8319 5.0078 3.2000 1.0000 3.8415 2.5478 2.6144 4.7267 3.9950 3.3126 2.7658 3.2000 1.0000 (V2 ) Report Date; 12/29/04 12:22 Equipment Code.: TOC4 Import C o d e ..,.; TCS2 mg/Kg TCSAV2 mg/Kg TICS mg/Kg Page 4 64 Multiple Analysis Report Print Date/Time: 2004/12/27 16:34:57 Sample ID Result Std. Dev. RSD Mode ALT ICV 93.9756 TC ICB-MB -0.1730 TC LCS 121.1281 TC LOS........................ ........ 111.5275............. ...TC .. 232796-5 31.0032 TC 232796-5 68.6687 TC 232796-6............... ........... 32.1367... .......... TC 232796-6 45.1514 TC 232885-8 35.2206 TC 232885-8............... ........... 36 7372... ...........TC 232885-Sms 128.8759 TC 232885-8msd 126.3410 TC 232885-9............... ........... 329.6523... ...........TC 232885-9 258.5568 TC 232885-10 253.6214 TC 232885-10............. ............ 152.1652... ...........TC 232885-11 84.9089 TC 232885-11 43.2715 TC 232885-12............. ............ 71.5951... .......... TC 232885-12 73.9295 TC 232885-13 236.1471 TC 232885-13............. ............ 153.7190... ...........TC CCV 101.9159 TC CCB -0.3265 TC 232885-14......................... 108.7319... .......... TC 232885-14 60.4603 TC 232885-15 95.7528 TC 232885-15............. ............ 100.2575... .......... TC 232885-16 57.2171 TC 232885-16 80.6035 TC 232885-17............. ............ 173.0943,., ...........TC 232885-17 149.1816 TC 232885-18 102.9129 TC 232885-18............. ............ 85 6024... ...........TC 232885-19 74.3877 TC 232885-19 62.0662 TC 232885-20.......................... 99,3550... ...........TC 232885-20 103.8124 TC CCV 102.1897 TC CCB....................... ........ -0.9940.............. ...TC 65 Detailed Analysis Report Print Date/Time: 2004/12/27 16:36:31 Sample ID: ICV Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL Mode: TC Filename: 12270904 Timestamp: 12/27/20' Sample Type: Cal. Verifi Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 93.9756 93.9756 6997856 2.006 3.004 368 Sample ID: ICB-MB Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL Mode: TC Filename: 12270920 Timestamp: 12/27/20# Sample Type: Sample R ep# ppm C ugC Raw Data Beginning Ending Integration Baseline Baseline Time 1 -0.1730 -0.1730 8742 2.293 2.195 120 Last Message: No Sample Detected Sample ID: LCS Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL Mode: TC Filename: 12270940 Timestamp: 12/27/2 Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending integration Baseline Baseline Time 1 121.1281 121.1281 11945784 2.146 3.146 284 Sample ID: LCS Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL Mode: TC Filename: 12270947 Timestamp: 12/27/20 Sample Type: Sample 09:53 Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 111.5275 111.5275 11001003 2.362 3.361 280 \ Sample ID: 232796-5 ^Mode; TC Method: boat Filename: 12270956 Cal. Curve: SOILCURVE Timestamp. 12/27/20 Operator ID: CAROL Sampl^ Type: Sample \ Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 31.0032 |1.0032 3076736 3.096 4.095 219 Sample ID: 232796V5 Method: boat Cal. Curve: SOILCURYE Operator ID: CAROL Mods: TC Filename: 12271006 Timestamp: 12/27/200410:11 Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 68.6687 68.6687 678^336 2.274 3.268 259 Sample ID: 232796-6 Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL Mode: TC Jename: 12271017 Timestamp: 12/27/2 >ample Type: Sample R e p# ppm C ugC Raw Data Beginning Ending Integration Baseline Baseline Time 1 32.1367 32.1367 3188282 3.7T5 4.709 210 Sample ID: 232796-6 Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL Mode: TC Filename: 122TM038 T im estam p\ 12/27/2004 10:44 Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Endft Baseline Baseline Time 1 45.1514 45.1514 4469036 3.726 4.719 Integration Sample ID: 232885-8 Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL Mode: TC Filename: 12271047 Timestamp: 12/27/2 Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 35.2206 35.2206 3491762 5.017 6.013 227 Sample ID: 232885-8 Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL Mode: TC Filename: 12271053 Timestamp: 12/27/2004 10:58 Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 36.7372 36.7372 3641017 2.825 3.820 221 :S==?=S37 67 Sample ID: 232885-8ms Method: boat Cal, Curve: SOILCURVE Operator ID: CAROL Mode: TC ..... Filename: 12271101 x '" Timestamp: 12/27/200411:06 Sample Type: Sample ( Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 128,8759 128.8759 12708236 5.132 6.128 264 Sample ID: 232885-8msd Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL Mode: TC Filename: 12271113 Timestamp: 12/27/2i Sample Type: Sample ITI^ Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 126.3410 126.3410 12458780 3.924 4.919 258 Sample ID: 232885-9 Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL Mode: TC Filename: 12271122 Timestamp: 12/27/2 Sample Type: Sample { Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 329.6523 329.6523 32466308 2.439 3.439 360 sam ple ID: 232885-9 Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL Mode: TC Filename: 12271133 Timestamp: 12/27/2004 11:39 Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 258,5568 258.5568 25469920 2.537 3.537 332 Sample ID: 232885-10 Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL Mode: TC Filename: 12271140 Timestamp: 12/27/2 Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 253.6214 253.6214 24984230 2.872 3.871 304 68 Sample ID: 232885-10 Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL Mode: TC Filename: 12271148 Timestamp: 12/27/200411:53 Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 152.1652 152.1652 15000094 2.983 3.982 279 Sample ID: 232885-11 Mode: TC Method: boat Filename: 12271217 Cal, Curve: SOILCURVE Timestamp: 12/27/20 Operator ID: CAROL Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 84,9089 84.9089 8381506 2.191 3.189 269 Sample ID: 232885-11 Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL Mode: TC Filename: 12271226 Timestamp: 12/27/200412:31 Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 43,2715 43,2715 4284045 2.756 3.752 230 Sample ID: 232885-12 Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL Mode: TC Filename: 12271235 Timestamp: 12/27/20 Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 71.5951 71,5951 7071318 2.755 3.755 284 Sample ID: 232885-12 Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL Mode: TC Filename: 12271241 Timestamp: 12/27/2004 12:47 Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Time 1 73,9295 73.9295 7301051 2,495 3.493 278 Sample ID: 232885-13 Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL Mode: TC Filename: 12271256 Timestamp: 12/27/20CM 13:03 Sample Type: Sample V__ Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 236.1471 236.1471 23264616 2.362 3.359 334 Sample ID: 232885-13 Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL Mode: TC Filename: 12271304 Timestamp: 12/27/2004 13:09 Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 153.7190 153.7190 15153003 2,838 3.835 284 Sample ID: CCV Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL Mode: TC Filename: 12271313 Timestamp: 12/27/200413:18 Sample Type: Cal. V erification---' Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 101.9159 101.9159 9779246 2.419 3.417 286 Sample ID: CCB Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL Mode: TC Filename: 12271322 Timestamp: 12/27/2004 Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 -0.3265 -0,3265 -6366 2,408 2.317 120 Last Message: No Sample Detected Sample ID: 232885-14 Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL Mode: TC Filename: 12271346 Timestamp: 12/27/201 Sample Type: Sample I Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 108.7319 108,7319 10725892 2.250 3.249 300 Sample ID: 232865*14 Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL Mode: TC Filename: 12271401 Timestamp: 12/27/200414:09 Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 60.4603 60.4603 5975563 4.031 5.026 226 Sample ID: 232885-15 Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL Mode: TC Filename: 12271411 Timestamp: 12/27/20(J4' 14:18 Sample Type: Sample - Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 95.7528 95.7528 9448638 2.541 3.540 280 Sample ID: 232885-15 Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL Mode: TC Filename: 12271420 Timestamp: 12/27/200414:26 Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 100.2575 100.2575 9891940 2.729 3.728 289 Sample ID: 232885-16 Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL Mode: TC Filename: 12271430 / Timestamp: 12/27/2004 14:35 Sample Type: Sample ( Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 57.2171 57.2171 5656405 3.785 4.779 240 Sample ID: 232885-16 Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL Mode: TC Filename: 12271435 Timestamp: 12/27/2004 14:40 Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 80.6035 80.6035 7957825 4.357 5.351 243 Sample ID: 232885-17 Method: boat C a l Curve: SOILCURVE Operator ID: CAROL Mode: TC Filename: 12271440 X Timestamp: 12/27/20M 14:46 Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 173,0943 173.0943 17059692 3.155 4.153 295 Sample ID: 232885-17 Method: boat CaL Curve: SOILCURVE Operator ID: CAROL Mode: TC V Filename: 12271458 /\ Timestamp: 12/27/2004 15:04 Sample Type: Sample ; " R ep# ppm C ugC Raw Data Beginning Ending Integration Baseline Baseline Time 1 149.1816 149.1816 14706483 2.493 3.492 292 :=====E=====?;===========?=======^====m="S===?==~==SiTSS: Sample ID: 232885-18 Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL Mode: TC Filename: 12271507 X Timestamp: 12/27/2004 15:13 Sample Type: Sample ... \ Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 102.9129 102.9129 10153252 2.512 3.509 289 Sample ID: 232885-18 Mode: TC Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL Filename: 12271516 Timestamp: 12/27/200415:22 Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 85.6024 85.6024 8449758 2.412 3.412 272 Sample ID: 232885-19 Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL Mode: TC Filename: 12271525 X" VTimestamp: 12/27/20(M 15:29 Sample Type: Sample Rep# ppm C ugC Raw Data Beginning Ending Integration Baseline Baseline Time 1 74.3877 74.3877 7346140 3.272 4.268 249 ;-- Sample ID: 232885-19 Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL Mode: TC Filename: 12271532 Timestamp: 12/27/2004 15:38 Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 62.0662 62.0662 6133600 3.544 4.541 253 Sample ID: 232885-20 Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL Mode: TC Filename: 12271545 / Timestamp: 12/27/201 i 15:50 / Sample Type: Sample Rep # ppm C ug C 1 99.3550 99.3550 Raw Data Beginning Ending Integration Baseline Baseline Time 9803128 2.448 3.446 291 :s = = = B q S T ? m ? 3 S a S S S (3 S : 3 C = = S = 3 3 = = = = = = = = = = = = sam ple ID: 232885-20 Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL Mode: TC Filename: 12271554 Timestamp: 12/27/2004 16:00 Sample Type: 5ampte Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 103.8124 103.8124 10241769 2,507 3.503 296 Sample ID: CCV Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL Mode: TC ^ Filename: 12271603 f Timestamp: 12/27/2004 k6:09 Sample Type: Cal. Verification > Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 102,1897 102.1897 9806190 2.552 3.552 291 Sample ID: CCB Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL Mode: TC Filename: 12271609 Timestamp: 12/27/2004/16:20 Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 -0.9940 -0.9940 -72057 2.832 2.217 120 Last Message: No Sample Detected IS t STL Chicago TOC in Soils Method; Lloyd Kahn instrument Phoenix 8000 fTQC4> LabNetBatch: i C a lc u la tio n : TOC (mg/kg) ug C / grams sample Date of Standard Curve: Book# nf 7 Lf l Page# / o f MS, MSO Known Cone, (mg/kg) 3 100 ug C / grams sample MS, MSD Observed (mg/kg) = ug C / grams sample MS, MSO Ree. - fobserved mg/kg - avq. sample result fmg/kgll x 100 known concentration in mg/kg Standard Traceability: (Note: Working Standards are prepared daily from the noted Stock Solutions,) Stock I (Curva) O l L a t i c i stock II (ICV/CCV) T.cySrrc- LCS Source ID , I b f W q LCS True Value P Acceptance Range ^ ~ / Y&K Sample ID: Sample Weight (g) ug C Commente: i O L/ "CO/} 0 .0 ? 0 . tc> <?2 n L ~ / 7 -}<D Le s o . r i e n /X I, IXOr/ le v c i z7? r -c G? 0 Q 2.0/2^ // /, o n <r &. 0*2?/ 3 /. <3? A 0 , 0 n a _ LL, CC?7 O . OO y?) 12, no 7 vL'"- ^ G o- o o oe > ^ T r - T O . ce??' rr, m y . -.^ .7 3 r , / 2joC \n ,Q \- L > Y /? L 5-VY7 4* ____ J ____i i n .o c J Y 0 . n fr f ' O 7<Y 0. o -n 0. 0 V ? 3 3Q ,nm / .<7 / nr.yeoy ` f m 1.71 / 2. 3 V (& t a r , ( / ( Ki^Urt/ -y&. u n " Q f.ff C , { U? . OC?G c -2XLi2(* _ ~ I - G ._0 ~ LL n 0 /A J L /Q ; 4 f of? n . - / 1 > -IL L 0.0 </7 P -/T______ -iL 2 / in 0 r f ^3 0( 0 . ^ c r. 1 r j , 27/$ ^ ' 7 / f f r '/ . a e t. / o 0/ A J , 7 /3 /7 Prep Anafyst^ i? /^ Analyst Reviewed by:_ I'I/A /T a ^ D a te: Date: Date: /% M lO-fo/J/&/ C jC jM CHM-12-9S/B4S/01 ^ STL Chicago TOC in Soils 114 jA Pag Nq.:_ Book No.: 7 7 f 7 Method: Lloyd Kahn Instrument Phoenix 8000 fTOC4i LabNet Batch: C a lcu la tio n ; Date of Standard Curve: TOC (mg/kg) ug C / grams sample Book# ________ ^P djje# MS, MSD Known Cone, (mg/kg) * 100 ug C / grams sample MS, MSD Observed (mg/kg) = ug C / grams sample MS, MSDRec. * robseived mo/ko - avo. sample result fmo/kol known concentration in mg/kg Standard Traceability: (Note: Woi s are prepared dally from the noted Stock Solutions.) Stock I (Curve) Stock (ICV/CCV) LCS Source ID LCS True Value Acceptance Range, Sample ID: cos Sample Weight (g) ug C 0 .oX / ff f / r r Coo o .U ~ 3 x 2 z r r - / 1/ O. 0 ^ 1 7 /7 C X 7 3 < f _ ~ /!l 6. o V f . OG>o 1 O- 0(a<-f 9 /oo. 2s TT . - /C e o .o X? y -/ c?. rm / 7 > 3 :r -r? .o3 r / /7 3 , ? 0 . -f3 ~ /9 r -L - if -l*i - "la a >0 _ 3 2 . ^ O.o'Sft'X Q .O y , HOI o. o w r o .o-^C? . //7 7' * % 4,2.9 7 e/, 3 ?7> M .tC x t t T !>u o Vs - , O O 2-1 fo i, 7 /2 / CQiS O - to X if L \ f & '< L - . - . l i f - - ? r. Commente: Prep Analyst: Analyst: Reviewed by: V f t v i J 0 i7 ,/ & rY\. l7V \g \ , v 2K L p f / MlU J d J jj* . - -- V Date: Date: / i / ql Date: CHt-22>12-096/B-Q6/01 *** RAW TEST DATA *** <V2 ) % Solids Determination Method Code..: SOLIDS Batch Code...: 138041 Status...... : RVUD Batch Date.. : 12/27/04 Batch Time.. : 1436 User Name... : daj SAMPLE: Grp Pas Sample ID 11 S MB 1 2 232885 1 S 1 3 232885 1 S MD 2 1 4 232885 2 S 1 5 232885 3 S 1 6 232885 4 S 1 7 232885 5 S 1 & 232885 6 S 1 9 232885 7 S 1 10 232885 8 S 1 11 232885 9 S 1 12 232885 10 S 1 13 232885 11 S 1 14 232885 12 S 1 15 232885 13 S 1 16 232885 14 S 1 17 232885 15 S 1 ia 232885 16 S 1 19 232885 17 S 1 20 232885 18 S 1 21 232885 19 S 1 22 232885 20 S Report Date: 12/30/04 14:02 QC Code....... : SOLID Calc Code..... : &S0L Location Code..: 57222 Equipment Code.: Import Code___ : Di Lut ion %SQLIC % - 0.0 82.0 81.4 82.2 80.8 80.2 83.4 S2.3 81.6 78.6 85.6 83.3 79.9 80.1 81.9 03.2 82.9 82.7 82.1 85.1 81.0 81.7 IWGT g 10.1458 10.6229 9.9664 10.5455 10.0699 9.9227 9.7563 9.7532 10.1117 10.2622 9.9027 10.4944 10.5549 10.4721 10.0316 10.5283 10.3409 10.5479 10.4413 9.9847 10.4256 9.9818 FWGT g -0.0021 8.7070 8.1127 8.6664 8.1403 7.9594 8.1348 8.0248 8.2535 8.0674 8.4808 8.7411 8.4304 8.3875 8.2177 8.7610 8.5692 8.7193 8.5730 8.4987 8.4431 8.1539 DRYWT g 1.2540 9.9652 9.3692 9.9160 9.4141 9.2327 9.4099 9.3046 9.5338 9.3422 9.7590 10.0230 9.7146 9.6721 9.5022 10.0393 9.8529 10.0042 9.8552 9.7838 9.7280 9.4493 UETUT g 11.4019 11.8811 11.2229 11.7951 11.3437 11.1960 11.0314 11.0330 11.3920 11.5370 11.1809 11.7763 11.8391 11.7567 11.3161 11.8066 11.6246 11.8328 11.7235 11.2698 11.7105 11.2772 Page 1 76 *** RAW TEST DATA k-kif CV2 ) % Solids Determination Method Cede Batch code. Status.... SOLIDS 138041 RVWD Batch Date.. : 12/27/04 Batch Time.. : 1436 User Name... : daj SAMPLE: Grp Pos Sample ID 11 S MB 1 2 232885 1 S 1 3 232885 1 S MD 2 1 4 232335 2 S 1 5 232335 3 S 1 6 232885 4 S 1 7 232885 5 S 1 8 232885 6 S 1 9 232885 7 S 1 10 232885 8 S 1 11 232885 9 S 1 12 232335 10 S 1 13 232885 11 S 1 14 232335 12 S 1 15 232385 13 S 1 16 232885 14 S 1 17 232885 15 S 1 18 232885 16 S 1 19 232885 17 S 1 20 232885 18 s 1 21 232885 19 S 1 22 232885 20 S QC Code....... : SOLID Calc Code..... : %SQL Location Code..: 57222 Dilution TARE g ASHUT g 1.2561 1.2582 1.2565 1.2496 1.2738 1.2733 1.2751 1.2798 1.2803 1.2748 1.2782 1.2319 1,2842 1.2846 1.2345 1.2783 1.2837 1.2849 1.2822 1.2851 1.2349 1.2954 Report Date: 12/30/04 14:02 Equipment Code.: Import Code.... : FASHWT g %MDIST % 100.0 18.0 18.6 17.S 19.2 19.8 16.6 17.7 18.4 21.4 14.4 16.7 20.1 19.9 13.1 16.8 17.1 17.3 17.9 14.9 19.0 18.3 %ASH % Page 2 77
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