Document 6BKmgN6M6gO8jZGEnxmOxrDX9
GALBRAITH LABORATORIES, INC.
Accuracy with speed - since 1950
LABORATORY REPORT
Barb Holland Gascoyne Laboratories Inc 2101 Van Deman St Baltimore MD 21224-6697
SAMPLE ID
LAB ID ANALYSIS
Report Date: Sample Received: Purchase Order #: Fax Number
10/16/97 10/03/97 Job #9704087 410-633-5443
RESULT(S)
DUPLICATE RESULT(S)
970021039 970021040 970021041 970021042 970021043 970021044
V-6232
Carbon Hydrogen Nitrogen Oxygen
30.99 3.34 < 0.5 * 2.81
% % % %
V-6233
Carbon Hydrogen Nitrogen Oxygen
31.01 3.34 < 0.5 1.96
*
% % % %
V-6234
Carbon Hydrogen Nitrogen Oxygen
30.99
3.34 < 0.5
*
1.56
% % % %
V-6235
Carbon Hydrogen Nitrogen Oxygen
31.08 3.34 < 0.5 2.06
*
% % % %
30.87 3.35 < 0.5 1.94
% % % %
V-6236
Carbon Hydrogen Nitrogen Oxygen
31.09
3.35 < 0.5
*
1.33
% % % %
V-6237
Carbon Hydrogen Nitrogen
31.15 3.37 < 0.5
*
% % %
DO A 049?63 CONFTDFNTTAL
This report shall not be reproduced, except in full, without the written approval ofthe laboratory. Page 1
PAKTNCK$H)P$ ICONTINUC** (MrXOVEMENT
U.S. Mail: P.O. Box 51610 - Knoxville, TN 37950-1610 Other Carriers: 2323 Sycamore Drive - Knoxville, TN 37921-1750 Tel: (423) 546-1335 Fax: (423) 546-7209
/
GALBRAITH LABORATORIES, INC.
Accuracy with speed - since 1950
LABORATORY REPORT
Barb Holland
SAMPLE ID
LAB ID ANALYSIS
970021044 970021045
970021046
970021047
V-6237 Oxygen
V-6238
Carbon Hydrogen Nitrogen Oxygen
V-6239
Carbon Hydrogen Nitrogen Oxygen
V-6240
Carbon Hydrogen Nitrogen Oxygen
RESULTS)
DUPLICATE RESULTS)
1.38
30.99 3.34 < 0.5 1.40
31.03 3.33 < 0.5 1.12
*
30.98 3.32 < 0.5 * 0.96
%
% % % %
% % % %
% % % %
Notes: * Quality assurance data indicates that we cannot be confident in the analysis of your sample below the level indicated. If lower quantitation limits are required, other procedures may be applicable. Check with our technical personnel. We were unable to do a Sulfur analysis on all samples due to high Chlorine content.
ICP:le
00 A 049704
conftdfnttai
This report shall not be reproduced, except in full, without the written approval ofthe laboratory. Page 2
Partnerships FDR CONTINUOUS IMPROVEMENT
U.$. Mail; P.O. Box 51610 - Knoxville, TN 37950-1610 Other Carriers; 2323 Sycamore Drive Knoxville, TN 37921-1750 Tel: (423) 546-1335 Fax: (423) 546-7209
Report No. Report To:
gnmeirr 'SadiQ-'*-
GASCOYNE LABORATORIES, INC. Baltimor , KD 21224
QUALITY CONTROL SUMMARY FOR GENERAL CHEMICAL ANALYSES
GENQC.WS page 1
_=Q
Report Date:
/IMl Page:. / of L
QA/QC Data: Lab Reagent Blank (LRB), Matrix Spike (MS), Quality Control Sample (QCS), Lab Duplicate Results
Detection Percent Recovery Duplicate
LRB Limits MS
PCS
Sample -IB
Duplicate Results
Total Petroleum Hydrocarbons
ND 1
/
Oil and Grease Total Organic Halides
ND 5 ND 0.05
/ /
Water, K.F.
ND 0.1
/
, oti. 7-_____ ND 0,0} fjA 9o.H 9709on -34o9t <0,0/ / <0,01
tfirw fib-
ND
kjA /0Q, 1 Cho`tol-a.in<d, Mco / (, ->
'DinSitL, .`S/CC ND /ja m-A /oft
/,33 , 1,33
lofaj rjklo'Tt'1 ND 0,0% rfA 9AS 9709021'91099 <, /&1_
-ND aIA n/4 Ki A
990*9on -<9/096 /.$ /
ND /
ND /
ND /
Notes: (1) Results expressed as: mg/liter,Xl?pro) .
mg/kile^ram (ppm) i ill'll]
perpdnt (%).
/
00 A 049P65 OONrTDFNTTAL
REVISED 07/94
DEPT. HEAD QA/QC:
SAMPLE ID INC TITRATION:
EQUIVALENCE MV ' 70
dth
TITRANT VOLUME 3. 100
COMPUTATION 3.545E--
TITRATION TERMINATED BY LIMIT ON NUMBER OF EQUIVALENCES PERMISSIBLE. OCT 7 1997 10:37 AM
3
SAMPLE ID: SAMPLE DATA:
+ 0.556
INC TITRATION:
EQUIVALENCE MV
58
TITRANT VOLUME 3. 108
COMPUTATION 7.149E-E
TITRATION TERMINATED BY LIMIT ON NUMBER OF EQUIVALENCES PERMISSIBLE. OCT 7 1997 10:44 AM
SAMPLE ID: SAMPLE DATA:
586 0.0971
INC TITRATION:
EQUIVALENCE MV
47
CV. S3U'/.
TITRANT VOLUME 17.963
COMPUTATION 54. 63
TITRATION TERMINATED BY LIMIT ON NUMBER OF EQUIVALENCES PERMISSIBLE.
7 1997
10:58 AM
00 A 049766 OONFTDFNTTAI
/>
97Oio$7
SAMPLE ID: SAMPLE DATA:
INC TITRATION:
1039 0.0569
EQUIVALENCE MV
66
TITRANT VOLUME 13.774
COMPUTATION 64.85
TITRATION TERMINATED BY LIMIT ON NUMBER OF EQUIVALENCES PERMISSIBLE. OCT 7 1997 11:11 AM
5)
SAMPLE ID: SAMPLE DATA:
1040 0.0636
INC TITRATION:
EQUIVALENCE MV
47
TITRANT VOLUME 13.469
-frf 5*7/
COMPUTATION 58. 35
TITRATION TERMINATED BY LIMIT ON NUMBER OF EQUIVALENCES PERMISSIBLE. OCT 7 1997 11:3 AM
^
'
SAMPLE ID: SAMPLE DATA:
1041 0.0508
INC TITRATION
EQUIVALENCE MV
50
9?o cn <xdi
TITRANT VOLUME 1.353
7'ft- GJl 65 3 /.
COMPUTATION 65. 7
TITRATION TERMINATED BY LIMIT ON NUMBER OF EQUIVALENCES PERMISSIBLE.
OCT 7 1997 11:4 AM
DO A 0497A7 CONFTDFNTTAi
I
^ ji.
^ .1PLE ID: SAMPLE DATA:
1042 0.0608
INC TITRATION:
EQUIVALENCE MV
60
TITRANT VOLUME 13. 855
iri.ee 63.3 l i
COMPUTATION 63. 9
TITRATION TERMINATED BY LIMIT ON NUMBER OF EQUIVALENCES PERMISSIBLE. OCT 7 1997 11:58 AM
$
SAMPLE ID: SAMPLE DATA:
1043 0.0498
INC TITRATION:
EQUIVALENCE MV
58
nowti
A
a.sy-- J/yd-
TITRANT VOLUME 11.628
AA
/.! 4 1
COMPUTATION 61.42
TITRATION TERMINATED BY LIMIT ON NUMBER OF EQUIVALENCES PERMISSIBLE. OCT 7 1997 12:11 PM
SAMPLE ID: SAMPLE DATA:
INC TITRATION:
21044 0.0489
TITRATION TERMINATED BY TITRANT VOLUME LIMIT. OCT 7 1997 12:32 PM
00 A 049768
CONFTDFNTTAl
SAMPLE ID: SAMPLE DATA:
INC TITRATION:
1045 0.0552
TITRATION TERMINATED OCT 7 1997 12:49 PM
torfJL* grabe.
====== ANALYSIS ABORTED ======
3)
SAMPLE ID: SAMPLE DATA:
1046 0. 0499
^ 'Too
id I'H-. ^ rs
m/
ik\^
INC TITRATION:
EQUIVALENCE MV
TITRANT VOLUME
350
15.444
COMPUTATION SB. 40
TITRATION TERMINATED BY LIMIT ON NUMBER OF EQUIVALENCES PERMISSIBLE.
DCT 7 1997
1:02 PM
SAMPLE ID: SAMPLE DATA:
1047 0.0585
INC TITRATION:
EQUIVALENCE MV
262
TITRANT VOLUME 14.057
&7.0 /
COMPUTATION 67. 00
TITRATION TERMINATED BY LIMIT ON NUMBER OF EQUIVALENCES PERMISSIBLE.
DCT 7 1997
1:15 PM
DO A 049969 CONFTDFNTTAI
. (PLE ID: SAMPLE DATA
1044 0.0705
INC TITRATION: EQUIVALENCE MV 49
*770 4W7 Q-^_>
TITRANT VOLUME 14.200
id.ee
SI. 3%
COMPUTATION 56. 32
TITRATION TERMINATED BY LIMIT ON NUMBER OF EQUIVALENCES PERMISSIBLE.
OCT 7 1997
1:26 PM
fUcltcL.
SAMPLE ID: SAMPLE DATA:
1045 0.0524
INC TITRATION:
EQUIVALENCE MV
264
fiO'fOB'l
TITRANT VOLUME 12.125
-fd. Qi U 7 '/ COMPUTATION 61. 73
TITRATION TERMINATED BY LIMIT ON NUMBER OF EQUIVALENCES PERMISSIBLE.
OCT 7 1997
1:40 PM
SAMPLE ID: SAMPLE DATA:
1046 0.0586
INC TITRATION:
EQUIVALENCE MV
258
fyoy-oin
TITRANT VOLUME 12.614
-fd. QL
S7< a '/
COMPUTATION
TITRATION TERMINATED BY LIMIT ON NUMBER OF EQUIVALENCES PERMISSIBLE.
C. 7 1997
1:54 PM
00 A 049770 OONFTDFNTTAl
SAMPLE ID: SAMPLE DATA:
Si044 0.0540
INC TITRATION:
EQUIVALENCE MV
68
srSfet~
TITRANT VOLUME IS.954
iddl
(r$, V y.
COMPUTATION 85.35
TITRATION TERMINATED BY LIMIT ON NUMBER OF EQUIVALENCES PERMISSIBLE.
OCT 7 1997
:03 PM
D
SAMPLE ID: SAMPLE DATA:
/
INC TITRATION:
1044 0.05S
EQUIVALENCE MV
26E
tf?0<+08'7
CLS^~
TITRANT VOLUME IS.700
U cy (.9 /
COMPUTATION 65. 87
TITRATION TERMINATED BY LIMIT ON NUMBER OF EQUIVALENCES PERMISSIBLE.
DCT 7 1997
:41 PM
3
SAMPLE ID:
+
INC TITRATION:
EQUIVALENCE MV
17S
TITRANT VOLUME 3. 500
COMPUTATION O. 1773
TITRATION TERMINATED BY LIMIT ON NUMBER OF EQUIVALENCES PERMISSIBLE.
3CT 7 1997
:43 PM
DO A 049371 OONFTDFNTTAL
ai-lMPLE ID:
+
^ ftitM/L&d. /3 ^|/<*L (e-0{*Jl r/j 0,1 a[ pJad^
INC TITRATION:
EQUIVALENCE MV
TITRANT VOLUME
259
5. 961
COMPUTATION 1.050
TITRATION TERMINATED BY LIMIT ON NUMBER OF EQUIVALENCES PERMISSIBLE.
OCT 7 1997
2:47 PM
00 f* 04 9p7p Nr r^F/vrrAl
Std. /Spike ID
Stock Stock Wt./Vol. Final Final
Prep
ID
Concert. Used
Volume Conceit. Date
Expire Verify Date Date
o, oTV^ W ?>/,;
- / ^ ( Toj 0r ( aS/vf 5 orfi
ydSiofwt > */W %/{47
O.v, 0.1v19?aJ
I'o'f yOrO; , M/ e,o - a 077 7
)9,? X ft.<9. X5/flOrO : 0,0,74 7
|,? x o .o
o.oa'/V
~Lrf Q7 V3?T
Disgard Prepared Date By
%/<?7 fj
ST - /
n.n&d o'.-. /(r i-i* / "7^ /o:y,,/4.6 Uf^ior. 7? -M- irxsA^T. ^
i j>rk. ,xh<
o- /a/ /l.I7j,T-j t-v.c. ion
4<rf lt?oi 0,5.3 -Usi ^ a/O/^A J A/aCj ( >> 9,0 <l) 3C,i> X 070(9 * Jk\ o / c5o. 0 A O./0/9 . o./on
%h.t*n
ihtfar
<5c. t>Y<3o. i 'A 0. 1 070/^
Ll f a ova' /Wd ,:nc.fou3> o. /cvW /00,0 ml. /CDOmf 0,0 to
^iuki yy^
->fc I\cj 0,0/ /JaCX
ZO'Z/Sl&c /(o. o i <o. 01 o
Hcl. y/<diC XO/ft f '0, QJJ2.___ 3io,^&o,o X 0,0 1 ; Q, 0/
FC-0
JJdo~ ld0v J/.<Kl j2?P<3r1. >,(} fr\ pih h/1*
74K/.I / J.7~
ut yf w-- 0Hr\
J J (Tv. C.u-1
i* (\, Srft.ls iOQOftk as
s(fah
eeG,
S-3 U)3-3 iCP-'l
'Ak <?M 3L<22g.
Zk-%0
&0.Z*i.
S-3
nl
<C-.r - O^ ZTQppn S&OlL\
fmoMs looters. jngf
If iOOnh . JfiPaprK
Vttfi7
*r/ftjQ7 sfajv %fahi TW
H%1
y&ki W97
Pi&r P*Qm
DO A 049070 CONFTDFNTTAt.
Std./Spike ID
Stock ID
fY/o ntm H a i|-/Q
Stock Wt./Vol. Concert. Used
/tyJOpjd^v 1.0^
/OucWvr. rf.Os'-l
Final Volume
3.03^1
O.dQfal
Final Conceit.
C-- - r(f*th" .
%1W* ,K
Prep Date
SI fYff/ft Wf>
Expire Date
l3[<i?
m
Verify Disgard Prepared Date Date By
S/f/fi 9W;7 PRft\
Simi
0ik
f^r*. Ph Pb-
!Ooo of>fr~ 0-3 fldl
^J. jIPfjJrT- Pi?-----
fb-1?-
' nfT /039fIpf K-)
ftOrU.
/Op^k/ Pb Tf
lODOfpfQtK <3. OnJL
S.oot*J. t1e,0fQlrpO^ S//S^T $COrid. 0, 0 QffV^ W/W97
?r.. &a?nl /0,D(qpro^ H'4r7-
<dw ih/
ES'S L-?--- --------
O.DI& k\ ~ Ust^ Q<03& M 5bd(o4>^ te?d%r( ,/ 9?7/n0/p3'" ?
19, Y M. 7
xo.
X0-
c
3S*J/<SZ<?,
o
-
'
0.034 0, Oilsf >
?>
at f. a <9^ iO
'9. V X 0, /> iSvt kl/l > :Q.OoVf 3
Oca
(PteS ipea-
m
fr, - (,7 A/aM-W1
fte; VVO_L
w lC,td. SCOydi .... (TP \Mn
/GOO nt< ChtoftsJ y/v(n LUldxr. 0,1 a/ 4J,mx-* hd'&Qlot 02%
xc ,/o ii = <3 S.O A/ c , / o y ^ ' / }
c5S.O xC -#ofl 73^ 0 ' D. 7Z7f7--w~7fr
.............
taiw ?/e^h 9///?7 m
fyfa M2 c. t/ o. n >/<?a) )
DO A 049774 CONF TDFNTTAi.
JOB NO: 9'1q1+0$'7 CLIENT :S&dL
_________________
DATE: ANALYST:
// g-/97 PdQr
SAMPLE I.D: PARAMETER: l7/VlS.'fc^ OrgO^C
"TANDARD NOTEBOOK REFERENCE:_________
/Odt. */0.0<\
*?0
/PCXL /Q-0<=\
'ttrtrL- (ML Scwa>t?,x U.p
a?a/
far&C
l.l3 Cu(ir\cUf'
7'
Sjo*
SUD3l
IZ.$$u//ocs*t'&
I$,3st0\//frcji',&
4,on '!3ir W>3
'/
4>0W /3.
,,s3
-4v,09/ il.wlf//cx^-l-M
^
'7
m3 </oVl
.
<0, o*y li-zanj/o^1^
l3ji3% //c^w
^ IS W / />33
O? / 0
/3 * rug, [/OCjCJ f`i 3
1
JOB NO:_____________________________________ CLIENT:_____________________________________ SAMPLE I.D: PARAMETER: STANDARD NOTEBOOK REFERENCE:________________ -
DATE:_ ANALYST:
JOB NO:_____________________________________ CLI ENT:_____________________________________ SAMPLE I.D: PARAMETER: STANDARD NOTEBOOK REFERENCE:
DATE: ANALYST
DO A 049275 OONFTDFNTTAl
Date Report # !6Ml
Sample
Sample wt.
CU<nt Co K //3-73 in)
Spike vt.
BTU/lb.
omn
UMsL (J/Sfd, rUitoxttl
MIL
ow\n trv\cd/5*iP
0,3&M
Hf>(,3
&io&\ At OHO . AjOW /note
o5W 0,4^
0,444S 0.4$4-O
0,5330 0.3ni3> 0,<3^>37 0;a3^
(p%e{) Lloo
iHoo {e3&0
ohcw3 AioHt
o.5SW> 5.44 {A
0,52/0 0,5543
(j>$ao (eiOO
ohOHC,
o,*n<i? G,$<x>2>
aaafl GSoo 0.533'/ ff^&eo
Sj.o'fj
D.^cA^ e/-
_DW> rvobLAw
o.aa$t
U>Hvo xr
iMLyu{ a.Kxi
0, Qlr>C)Q~ (tHOo
Analyst
00 A 04977a CONFrDFNTTAf
JOB NO: 97o 90$7 CLIENT:.ZE&dt C1SV_-
SAMPLE I.D: PARAMETER:.
_______________ __ Qego^c ,iJm.
DATE: ANALYST:
/0 mk.
STANDARD NOTEBOOK REFERENCE:
fOd<L -,/O.0\
^
HkrO Ch.fil, /OOL, -- /O'a| .
W, act S`
-f'a /OrU
-tarot
I**"
ro va. 13.3^/mo-l 33
//Oc.cJ^ i3 3S(m
41 o V3 1$ 3\?<j/fpeO'M3
Wioyo 13. 337?//IOC-A
A) f3. Z3$*//0<xst`& <2joV7 ym<o i`3^ /i
A/Dm ti.lSlf ffOCCr'l.ll
to US
JOB NO: QnoHQtl _______________ CLIENT: ^4/a^^nlftrtWjgttL^
DATE: ANALYST:
hjYh &,
JOB NO:. CLIENT:_____________________________________ SAMPLE I.D: ._ . PARAMETER: STANDARD NOTEBOOK REFERENCE:
DATE:_ ANALYST:
/>/i
WEIGHS, g
RESULTS, %
Date Joh ft Sample Crucible A
B
ID ID Cntcibl Crucible
& Sample
/0Mcf? Qiovot, -f\dc(jc
35. cm3
&JC# At 041
*
( S/oH# 6yoH& &oW
_____ M31T 53 nto3(* (S te.sm n i<w
7 ft.s IQ.Sl?
-fa -&/
4j0yo>
u
10*47 AA VgV) ft
r^m
M.CRf? 3V,56VC o-W
C Dried Sample & Crucible
D Ashed Sample & Crucible
(B-A) Residue Sample
Wt. A, /o/n'fei fX/* l*r*r
.larvr
Moisture
&.0S?7t. &&&T 3,%</ 111.934? I*WC MM
I7.X4*
mrr<3 ,U(?
aMFT? iq.mas
oertf 3167V/
TVS
ft. 531?
JSflt 3.7355
|7.RWf st,mo
%^o!H hH$pO /.WV7
9 V ` *
Q hr** J
T Mojbj ? 6/ < H$125> 3S*
i? ifootfb </
30,
Ao.TsK ZoJTiC
01. AWtn /,7? /.tea
ILoaS't ?,03fc4 &o.W$ ^.cvc>7 3oAl^o 4W?
Ash Analyst 1
lh
J 1Q.Ol
<0,01 <0,01
<0,o t <OfO/
<0.0/
<0,0/ <0.01
<0.0/ <0,0/
Hsat
40, {
0,1 7,3 <0,/ <0.0/
Z/J
csidite. < = C - A x 100 Total Volatile Solids (TVS), % = C- D x 100
Sample Wi
C-A
Ash, % = D- A x i`00 sample wt,
Moisture, % = B - C x 100 sample wt.
0 A 049?7a CONFlnFNTTAl
Page S
Chain of Custody Record
y
X ---------------------------------------
NO. OF CONTAINERS
PROJECT. l^&cj QJa<z^<.v <L
. '
III ANALYSES
j 1jj
Pago____ ol_
LABOR^TJIRY:
("7c*50e)yi~-*-
I^^IEIrtii/ i / i
PREPAREDLY (Signature>)
.
LAT-Ji ZsJ
c -4---------
Zy
1
FIELE7SAMPLE I.D.
SAMPLE MATRIX
'
DATE/TIME
7yrM/ 7 W/, l
f
-vn^o-f/P-/^3s
- i'-a y
otii
1 o//rd
/
1/
Jr g/sAiA'** _jL
/y
4^
t
<
/ *
74
/_z_0*i y --' i
l
/ r
t 7: /~
______________ AbWE ^
fffe/97_____ 4-
w'
V
/
t
' L 'd /
0*T\ ______________ aa=i4.s^ ___:___
OMij
,3V^' i_______ _1
id-VlS-P^, 1oi|L ______________
_______ J
t
o4] ______________L--3^XJ3r&f
/ V
1
______J__________ /
Lz_\_>k_________
J2fah? I4 f ______ /_________ /
_7_
1
// ly *
,r <.7
c
/ *
LX /t^
/
u/
/ 73 47l'
t/
Ls /
w
u
~
*
1/ u / y
'' ^
REMARKSIV<r<f/
rj^*~J
/-A'd*
ft
//// ////
REMARKS
> (forlabt/se onltf
Sn*~A
ftMrlai--v------------------------ ' Vl / rt.^1 IFFFWT:
*:f
i=
^': #>: .'D .:.
!:: .
##7 7 y.i
; :: x.v.. .,tu.M-'ij....."
;% "F ;v '';W- ;
LLL
DATE
7//9 2*1
RECEIVED3 BY:
date TIME RaiNQUISHED BY::
DATE TIME RECEIVED BY: LAB USE ONLY
DATE TIME M^UfjQUISHEb BY:
ML
DATE TIME
ii..iai
awij *#vf, #7#l
WddSM^ddi -u
DO A 049779 OONFTDFNTTAL