Document 6B1DZz6z87mYEpDRNx9JqVQEm

:- AR 226 _ 0696 ACUTE TOXICITY TO AQUATIC INVERTEBRATES (ACARTIA TONSA) TEST SUBSTANCE Identity: A mixture containing perfluorooctanesuifonate, which may also be rOecftearnreesdutiofoansicPFacOiSd,) (FCCA-S95#o2r7a9s5-a39c-o3m)ponent of FC-201AF. (1- Remarks: The 3M production lot number was not noted. The test sample i1s8F.C5-92%01dAiFet.hylCeunreregnltycionlfbourtmyaltieotnheirn,di3c7a.t8es1%it wiastaerm,ix1t4ur%e eotfh3yl%enPeFgOlSyc,ol, 83.%25tr%ieAtchraynlioclafmoianmee,r6, %9%suslofodniautmedocatlyklylsueltfhaetre,sa0l.ts3,%asnodd0i.um05l%autroyllyisturfiaaztoel,e. The following summary applies to a mixture with incompletely crhefalreacctttehreizteodxiccoitnyceonfttrhaetifolnusoorofcihmepmuirciatliecso.mDpaotnaemntayofntohteatcecsutrsaatmepllye. METHOD: Method: lethal toxicity tIoSOm/aDrIiSne14c6o6p9e-p1o9d9s7:(CWoapteeprodqau,alCirtu--sytDaecteear)m.ination of acute Type: Ace static GYeLaPr:coNmopleted: 2000 Species: Supplier: Acartia tonsa Test organisms cultivated from eggs supplied by Marine Biological ALnaabloyrattiocrayl,mUonniivteorrsiitnyg:of pCoHpaenndhadgiesnso,lvDeednmoaxrykg.en ETexsptosourrgeanpiesrmioadg:e:48-Lhaorugrescopepoites and adults Statistical method: LCs values calculated by PROBIT analysis, National SNwOeEdCisbhyEsnivnigrloenfmaecnttoarlAPNrOotVecAtifoonllBoowaerddby(VBeornsfieornr2o.n3i,s1p9r9o0c).eduCrael.culation of Test coDnidliuttiioonnsw:ater: Filtered natural seawater (34 ppt salinity) from an unpolluted site Dilution water icnhBeymfiisotrrdyo:utNsoitdegiovfeSnt.avanger, Norway. Lighting: A daily photoperiod of 16 hours light and 8 hours dark was `Smtaoicntkaainnedd ttehsrtousgohlouuttiotnheprteesptairnagtipeorni:odA. 999.4 mg/L primary stock solution was prepared by diluting 0.4997 gramsoftest substance in 0.5 L of water. Aliquots were then added directly to water in test vessels to create test solutions. Exposure vessels: 28 mL rolled rim vials containing 25 mLoftest solution Number of replicates: 4 000231 NNuummbbeerr ooff acnonicmeanltsrapteirornesp:lifciavteep:lu5s a blank control Water pchHermiasntgrey(d0u4r8inhgoutrhse):study: 8.18.1 8.08.1 ((c1o0n0trmogl /eLxpeoxspuorseu)re) TDeimsspoelrvaetduroexyrgaengner:an2g0e+(10-4C8 hours): 75..2677..67 mmgg/lLL ((c1o0n0trmogl/eLxpeoxspuorseu)re) b+ e1c0a0usmeg/thLe(hiingtheersmtedtiwaoteccoonncceennttrraattiioonns)uesxepdosruesruelvteadluienstoutsaledmortality by 24 hours. RESULTS NominaRlefceornecnecnetrsautbisotnasn:ceBk(3c,o5n-tdroilc,hl1o0r,op3h2e,no1l0)0,at3210.,0 and 999 mg/L. mg/L. Element values: 24-hour 48-hour LCso LCso = = 52 34 (37 mg/L 71) (CI mg/L. not calculable) 48-hour NOEC = 10 mg/L Element values based on nominal concentrations Remarks: Substance TReesmtianrgkwsafsielcdo.ndTuhcetveadlouensarmeipxotrutreed as described apply to that in the Test mixture and not the fluorochemical proportion alone. CONCLUSIONS TOhbseeFrCv-e2d0E1fAfeFct48C-ohnocuenrtLrCastoiownawsadset1e0rmmgi/nLe.d to be 34 mg/L. The 48-hour No Validity criteria fulfiled and reference substance was in normal range. `Submitter: 3M Company, Environmental Laboratory, P.O. Box 33331, St. Paul, Minnesota, 55133 DATA QUALITY tReesltiianbgi.litHyo:weKvieirmi,scshamrpalnekipnugri=ty2.wTahsisnosttupdryopmeereytschtahreacctreitreirziaedfoarnqduatlhietystudy lacks analytical confirmationof the amount of fluorochemical proportion in the solution. REFERENCES 000232 Treesqtuewsatsofc3onMduNcotregde,byLaRbFreRfoegraelnacnednuRemsbeearrc9h3,12of-1S,ta2v0a0n0g.er, Norway at the OTHER Last changed: 6/26/00 000233 L5a9b3r1e2f.r1o.: Pagel of31 odSEwe A2EERAER "FC-201 AF Light Water Brand AFFF" Toxicity tests Report RF-2000/001 [=Tabet no: 931241 No.of pages: 31 [Eee Aunor: .| Ein Horve Gents: 3M Norge Version No./ date: Vers. 1/05.012000 Research Program: [me Summary: "The following tes results were obtained with "FC-201 AF Light Water Brand AFF: Todcty: Skelotonema costatum Acartia tonsa Corophium volutator 72h EC, 48h1LC, 10dLC, (mon: 50 (mon: 34 (mgkg dry weight): 3020 The resuts relate to the product as supplied by Novatech. Keywords: Toxicity, Skeletonema cosiatum, Acartia tonsa, Corophium volutator. - Topartof idocumentmaybaropoducednary om WAU persioninwitngby FF - Rogaland Research woAirs Inger Lisa Andersen bn. A Ht orFF- Rogaland Research Kare Netland 000234 : L9a3b1r2e-f1ro. Page20f31 CONTENTS: 2. TEST FOR TOXICITY WITH SKELETONEMACOSTATUM vrs 3.TESTFORTOXIWICTHIACTARTYIATONSA criss 10 4. TEST FOR TOXICITY WITH COROPHIUM VOLUTATOR srs 15 5. DATA SHEET(S).crcrsssimmsssssmsssssssssssss 20 000235 La9b3.1r2e-f1o. Page 30f31 PREFACE: ENocvoattoeiccho.logTihceaslatmepstlsewiesraecpoenrcfeonrtmraetdeotnha"tFCn-o2r0m1alAlFyLiwgilhlt bWeatuesreBdriannda A1F%Fs"oliuntiaognr.eeTmeesntst wweitrhe conducted in accordance with the "Harmonised Offshore Chemical Notification Format" (OSPARCOM 1995 /SFT 1998). pTehrefporromjeedctbwyaRsFca-rMriilejdoloaubt.atStRudFy-dRiroegcatloarnwdaRseSseenairocrhEfnogri3neMerNoIrnggee.r LAilslatAhnedteersstsenw.ere The test results arepresented in separate sections. The results relate to the product as supplied by Novatech. _ TThhiesatcecstrerdeiptoarttioins istsastueesdtbhyatatlhaebloarbaotroartyoarcycmreeedittsetdhbeyNNAorrweqeugiiraenmeAnctcsrecdointcaetironnin(gNAc)o.mpetence, Ietqaulispomestnatteasntdhawtorthkeinlgabporroacteodruyrheassfoarsaaltlistfhaectteosrtymqeutalhiotdysacsosnutraainnceedsiynsttehme,acwchriecdhitiantcilound.es internal certified quality control schemes, reference materials and participation in interlaboratory secondary reference materials. comparisons, and the use of The testsperformed are covered by the accreditation. This test report may not be reproduced in anyform other than infull, without thepermission in writing by RF - Miljolab. 000236 . LaSb.oriefnno. Page do3f1 TEST FOR TOXICITY Marine alga: Skeletonema costatum " 000237 L9a9b3r1e2f1ro: Page sof31 TEST REPORT `GROWTH INHIBITION TEST WITH THE MARINE ALGA Skeletonema costatum a lil NeJrorogrras RREOSGEAALRACNHD TEST SUBSTANCE: "FC-201 AF Light Water Brand AFF" TEST RESULT: The 72 hours ECsp was calculated to ~50 mg/l. The test substance was supplied by Novatech, and the test resultsrelate to this product. TEST DETAILS: METHOD: NS-EN ISO 10253, 1998: Water quality - Marine algal growth inhibition test. `with Skeletonema costatum and Phaeodactylum tricornutum. TEST ORGANISM: Skeletonema costatum, strain NIVA BAC 1. A stock culture ofthe test organism is kept at RF - Rogaland Research. PREPARATIONS: Naastbuarsails sfeoarwtahteegrr(oswaltihnimtye:d3i4um%.o)TfhreomwaatnerunwpaosllfuitletderseidtethirnoBuygfhjaorGdFw/aCsfuilsteerd, andbriefly heated to about 75C prior to use.The seawater was enriched with nutrients according to ISO 10253, and recommendations from the: Paris Commission. Test solutions were prepared from a stock solution. Astock solution of 511.2 mg/l was prepared by stirring 0.5112 gramsofthe product in 1 litre of growth `medium. Other concentrations were prepared from this stock solution. INCUBATION: Test cultures of 50 ml were incubated in 100 mi flat-bottomed flasks on an orbital shaker, 3 replicates for each concentration. Test cultures were inoculated to about 2000 cells/ml from an exponentially growing inoculum culture. The test was run under continuous light (> 50 pE/m" sek) from fluorescent tubesofuniversal natural white type, at a temperature of 20 2C.. tThheetteessttfwlaassksrucnacfhordaabyofuotr7g2rohwoturhsm,eaansdurseumbesnatmsp.leAslgoalf5gmrlowwtehrweatsakmeenasfurroemd by fluorescence. pH measurements were performed as indicated on data sheet. 000238 Lab. refro. ' 99312-1 Page 031 DATA ANALYSIS: CALCULATIONS: Growth rates were calculated by log linear regression on biomass (fluorescence) `versus time, as described in NS-EN ISO 10253. ECs: Tcohneceinnthriabittioornyoefaffecptroodnuctthegigvrionwgth5o0f%Skreedluecttoinoenmoafcgorsotwatthumraitse e(xEp.Crseos)s.edThasisthe effect concentration was calculated by interpolation between 32mg/l and 100mg/l.. NOEC: Calculation of NOEC (No Observed Effect Concentration) is done bysinglefactor ANOVA followed by Bonferronis procedure for comparing each. concentration mean with the control mean: TESTRESULTS:TTae ble 1. EC and NOEC values abiained ith Skeletoner ma cosay tum. ---- Testsubstarce ECo ECa Cn "WFaCt-e2r0B1rAanFdLAiFghFtF" - 50 - ae NVVOaatEceCsr:naecce1o0councetnraeronrs gpin.g 17N%OE$C09anaendco0l7e%ubaebiydninofghreocwotmhpruattee. pUrnoigsrainmmmeg. Graphpd nr 3.0 COMMENTS: The results arebasedon growth ratesforthetime span 0 - 72 hb,the period during which the growth is considered to be exponential in the control cultures (see growth curves). VALIDATION: The validity criteria given in the test protocol are fulfilled, in that the control cell density increased by a factorofmore than 16inthe test period (corresponding to a growth rateof more than 0,9 d"), the control pH did not vary by more than 1,0 units during the test and the 72 hours test. results with. 3,5-dichlorophenol was in the range normally found. Lab. ref. no.: TSeasmtplpeeriroedc:eived.: Report date: 99312:1 04.2007..0190.9999 05.01.2000 SU Nor EEnlgininHeoervre Analytical technician Ftd SeniAorgeReMsoelavrecrhsSmcyiernti|st Quality Assurance E EThnicsleotseredp:orDtatoacsdhebeytsbortory Secreied by Norwegiap n Accreiaion (A). Th report may not be reproduced in ay orm aber han ul, hos heprison in wring by RF -Mili. 000239 La99b3r1e-f1 Page 7of 31 PRIMARY DATA: Growth inhibition test with Skeletonema costatum Test substance: "FC-201 AF Light Water Brand AFF" Lab. ro: 99312:1 Start date: 04.10.99 Conc. unit: Measurement: mThoel biomass was measured by fluorescence; values i fluorescence units fm04e.1099]__05_.1_09_9]_0--6._10_.98-- ] 0_ 7.10] 99 Core: atPeHnd Concentration | 1405 | 0925 | 1030| 10:40 Jaton oltest 00 0o111s || oossse || 92 | 79 | s 218| 0997 209 | 0399 o0 001134 || 0o6es2 || 9 64 | 5 47 211 | 0sss 204| 1.000 0 0 o14 | ot2 | os2 | orn | 3| 71 | s48s | a2t0e4| (1.100000 01 01 016 | 013 | ora | 061 | 7525 || e5o5 220172|| 01.90090 01 ota | oss | 83 | 214 | 09% 032 032 01 | oa | 074 | oes | 87 | 86 | = e& 211| 0999 214| 0999 84 032 ota | oes | 92 | e 213 | 099 ota | 015 | oss | oss | 82 9 221110|| 10.900%0 013 | 093 | 89 215 | 099 0o1t6a || oosrss || 82s || 0099999 84 01s | oes | 73 | @ 09% 1100 00116s" || ooddss 527 220065|| 00.999%4 8s 0 016 | 04s a 200| 0995 014 | 0s | 34 | 25 01s | 03 | 27 | w 116626|| 0099991 013 | os | 44 | 3 1.94| 0997 100 100 01s | 0 018 | oor | 0 00s 000 000 84| 82 100 03 | o o 000 Reference substance(3.5dichlorophenol): Tsmgl | 014 | 047 | 185 779 | 09% 11.5smmggh | 001166|| o0e4s3|| 1144s5 110016 | [o0s99s6| 83 Mean values: 0.01 031 2 32 210 0011a3 || o0s5 57 = 221110 [[0099%% ootaa|| 0097 s9 861 221132|| 00399998 01s | 0oi6e || os ooss | 8 64 | 6 214| 1.000 =2m | | 210240 || o09s9s5|memmsen000244C | oboe. reser GROWTH "rom ar gh CURVES: Growth WaBrAaFF inhibition test `with at: 839121 Skeletonema costatum iNee i Iab ,he won enim tl --- i ia oe on Kg 7 032 mg! I:1..So o tot rate hous) nae I 2 iSAT a) stare pom I7 1 mgn ii . Le a) testduration our) een 5 | ibi octon 7 32 mg i ii.EE ioFa-- n 7 100 mg i f |"E Ne= e-- n 000241 LaSb3r1e3fno. Page dort | iLeneibition of the growth of Skeletonems costatun mg/1 (FC-201 AF Light Water Brand APE) Experimental data: CCo5nacTeSn0itraAtFioLnighitn Water Brand AFFF" Growin Tate Inhpiebricteinotn CCCooonnntttzrrooonll 123 CCCooonnntttrrroeal &3 contro. mean : 00.11100 ol 000.33222 111.00000 3.3325k0 101100:..00000 23E23t.00]00 301100000...000000 22200as ne ::: : 2 Zo :: 2.10 0 i23.a0n7 foalylo 2a21n 0oa.ll0o | 3 2 2s 0oa.ls0 i2m.1mn6 0aB.lx0o) 2a.2l0s8 - 13ise 1ii0cs2ee H1E3e.dim 000..000000 211000000.0.000 | | . 000242 Labrefro: Page 100f31 { 993121 |' { TEST FOR TOXICITY Marine herbivore: Acartia tonsa | i 000243 | Lab refro.: Page 11/31 {| 993121 TEST REPORT ACUTE TOXICITY TEST WITH THE MARINE COPEPOD Acartia tonsa flQ\iil || > odiiriwe EEESRERREER i TEST SUBSTANCE: "FC-201 AF Light Water Brand AFF" | TEST RESULT: "TThhee 4te8sthsouubrsstLaCnscepwwaasscsaulpcpulliaetdebdytoNo3v4amtegc/hl, and the test results relate to this product. TEST DETAILS: METHOD: 1toSOm/aDriInSe1c4o6p6e9po- d1s99(7C:opWeaptoedraq,uCarliutsyta-cDeae)t.erminationof acute lethal toxicity TEST ORGANISM: Acartia tonsa (Dana), supplied by the Marine Biological Laboratory, UniversityofCopenhagen. CULTIVATION: `Twihtehttehset o"rPgarainsisCmosmmwiesrseisounpp-lRieidngasTeegsgts",Praontdocwoel"re(VcKuIl)ti.vaLtaerdgien caocpceoproddaintcees and adults were used in the test. PREPARATIONS: N2astbuarsailssfeoarwtahteedri(lsuatliionnitwya:t3er4.%T)herowamtearnwunapsoflillutteereddstitherionugBhyafoGrFd/wCafsilutesred |{ prior to use. | Ti uetstioswonalsuwtapitorenersp.awreOertdhebepyrrescptoianmcrieenndgtfr0ra.to4im9o9na7ssgwterocrakemsspoorlfeutptiahorene.pdArfordosutmcottchikinss0osl.tuotclikoensooolfuf9ti9o9n..4 i |bi| INCUBATION: T2h5emtlesotftweasstrsuonluitniognlaasnsdc5onatnaiimnaelrss,(428rempilircoaltleesdfroirmeavicahlsc)onecaecnhtrcaotnitoani.niTnhge Vials were 201C. kept pH undera 16t8h light/dark photoperiod at a and oxygen measurements were performed temperature as indicated of on the, Zl | data sheet. 000244 st 875000,Fa ed 5) 875200.Eerieumber: 950884800. La9b3r1e2f.r1o. Page 120/31 DATA ANALYSIS: CALCULATIONS: The effect a product loetnhatlhe10su5r0vi%vaolftohfeActaerttaanitmoanlssa is expressed (LCs). The as the concentration combined mortality o f p{eCratgevstacloensceanntdratthieo9n 5we%rceounsfeiddefnocrecallimciutlawteirone.caTlhceul2a4tehdobuyrsusainndg4t8hehours standard procedure PROBIT Analysis, on Board (Version 2.3, 1990). National Swedish Environmental This programme also calculate test `Protecti concentrations lethal to 10% and 90%of the test animals. NOEC: CcfaaoclntccouerlnaAttrNiaotOnioVonfAmNefOaoElnlCwoiw(teNhdobthOyebBscooennrtfvreeordlrmEofenfaiencp.troCcoendcuenrterfaotricono)mpiasrdionneg. ebaychs.ingle- TESTRESULTS: VALIDATION: Table 1. LC and NOEC values obtained with:"FC-201 AF Light Water Brand AFFFTM `Acarta tonsa 24 hours 8 hous Co a 20 (10-29) 5207-1) nm ui) cn 130 (92-260) 509.) NOEC: Fnesear 10 30%2nids0a%nd 55a%lcyonaffidren22c4etard48lhoaurrse,inUdincitsedm.NlO.ECVaal1ru0eescaareeulatd by hecompute programm GraphPad Stat 1.0. Tohxyegveanlicdointycecnrtirteartiiaogniavetnhienetnhdeoftetsht eproetsotcwolasargerefualtfeirlltehda,ninoftheaqtutahle1d0i4ssmogl/vle,d LthCespeorfce3n,t5a-gdeicmholrotraolpihteynionl t(hreefceornetnrcoel)s wwaass ilnestshethraanng1e0%n,oramnadltlhyefo4u8ndh.ours. i | | | | | | || i 1 LSaabm.plreef.rnecoe:ived.: Test period: Report date: 290903912.-919 0608.10.99 05.01.2000 Elin HNorvee t Engineer Analytical technician TAege MWoloveorsnmyr, `Senior Research Scientist Quality Assurance Enclosed: Data sheets top idfl, ywhutBhae pyrmiesionrn wiynNgobryweREinMAiclriis (VA). To pur may not be repro ay 000245 X* 9L9a3b1r2e1no Pege 130/31 | PRIMARY DATA: Acute toxicity test with Acartia tonsa i Testsubstance: "FC-201 AF Light Water Brand AFF" { Lab.ret: 93121 i! SMteaartsudrateem:ent: N06.u10m99obfdeeard | |I Toul | Nsupmebciemreonf number | pr. vessel NUMBER OF DEAD 24 hours 48 hours | | |_ Concentration mon | Scpeocinmeen|| A 8 C 0 E F | A |B CDEF | Tom | ABCDEF| Tow Gonrol 000001 010010 | 2 I| sss 5 | |I 5555 {| 44a 5 17 I {| 5 | | 99 | Referencesubstance(3.5dichlorophendl): | 020 { 100 The result wit th reference substance is within the range normaly found. eee | | 000246 | | [ow| won awe f Testsubstance: "FC-201 AF LightWater Brand AFF" | \ Lab. ref.: 993121 Measurementsof xygen andpH. | 1 (mg) (mg/) - (mg) - (moh) -| | To[|o|o = =] =|v oo[==| 1 {--1 [we[ew] || Reference substance(3.5dichiorophenol): _ _ | | | | se Labrefro: Page 15 of31 1! So3iid |ii | TEST FOR TOXICITY - || Marine Amphipode: Corophiumvolutator | | | || : 000248 Labrefro. Page 16.0f31 \ 993121 ds TEST REPORT | Q AMCAURITNEETOAXmIpCHIITPYOSDEDCIoMrEoNTphTEiiSuTmWIvToHluTtHaEtor moNwOdRrSeKm. s R RRSEERFRER |i TEST SUBSTANCE: "FC-201 AF Light Water Brand AFFF" | i TEST RESULT: "The 10d LCsp was calculated to >3020 mg kg dry weight sediment. | The test substance was supplied by Novatech, and the test results relate to this product. | TEST DETAILS: METHOD: ASTM E1367-90, Standard Guide For Conducting 10 day Static Sediment { Toxicity Tests with `Marine and Estuarine Sediments. TEST ORGANISM: Coraphium volutator, from an unpolluted site near Trondheim. | CULTIVATION: Taehreatteesdtsoeragwaantiesrmastw1e5reC.suApplsimeadllaamaoduulnttso(f4-n8atmuurmalisnesaizwee)eadnwdawseurseehdelfodrin | || feeding. PREPARATION: | Natural seawater (salinity: 34 %) from Stavanger was used for dilution water. an unpolluted ste in Byfjorden outside Sediment collected at an `unpolluted site was used analysed for for oprrgeapnaircincgonttesetatseadnidmepnrtosp.orTthioensseildtifmoernetaicshatmesut.ddy sand and was | Boafdchamtepstsceodnicmeennttrantiaonplwaasstipcrbeupcakreetd. b2y0a0dmdilongftsheeapwraotdeurcwtaisn 6a0d0degdraanmdmtehse i `4b0u0ckmetlwoafssesahwaakteenrfwoars3 ahdoduresd.toTheaechs,edainmdenthtewbaesakdeirvsidweedreinatoertahtreedeobveearkers, ntihgehtd.am1p0asneidmiamlesntwewraes, tahneanlyrsaenddfoomrlwyasteelrecctoendtefnotr, each and `be all aker. A sample of concentrations are 1 calculated as mg kg sediment dry weight. INCUBATION: The test was run sediment, app. 4 in 00 mgllaosfssceoantwaaitneerrsan(6d001:0maln)iemaalcsh,c3onrteapilinciantges20f0orgocafcthes kers were kept under continuous acration at a t - "toenmcpeenrtartautrieono.f T1h5e+b1eaC. pH and oxygen `measurements were performed as. || || indicated on the data sheet. 20 ox 43 ery 9)SgNery 757000Fr27 000249 37520, rg rb SSR L5a9b3r1e2f1no.: Page 170f31 DATA ANALYSIS: (CALCULATIONS: tT`rmhaoetriteoafnlfioetcfytp2oeprnrtotehdseutcsctuornlvecitevhnaatllratootfi5Co0onr%wooefprtheihuuesmetdvesoftlouartnaciatmloacrluilsa(teiLxoCpnsr.)es.TsheTedhae1s0ctdohameybciLonCnecsden PVaRlOueBIanTdAtnhaely9s5is%,cNoantfiiodneanlceSwleidmiitsahrEencvailrcounlmateendtably PursoitnegcttihoensBtaonadradrd(Version 2.3, 1990). This programme also calculate test concentrations lethal to 10% and 90%ofthe test animals. NOEC: CfaalctcourlaAtiNoOn VofANfOoEllCow(eNdobOybBsoenrfveerdroEnfifsecptroCcoendcuernterfaotricono)mpias rdionngeebaychsingleconcentration mean with the control mean. TESTRESULTS: TTO aablee11.LLCCaannd NOEC values obtained withe : "F--C-201 AF Light Water Brand AFFFTM Corophium volutater 104s Co 50 Ln >3020 w0 NOwEC:0000000 w9e50000 eVelteuss nveiccea10%eb30y%PRaOdBI9T0%naesbbsal.ityNaOfeErC1a0rdeaycsa.lcUunliastbiendmgheAcgomspeudiemrenptrorgyrawmeimgeht GraphPad inti 3.0. VALIDATION: Tpehrecevnaltiadgietymocrrittaelriitaygiinvethneicnotnhterotlesstwperroetolceosls atrheanfu1lf5il%leadn,dinattheastttwhieth Folxuyogreanntceonnece(nrterfaerteinocnew)awsaslesisn tthheanrranegceonmomremnadlelyd f(o6u0n%d,)biuntotnheeodfitsshoelvteesdt `coofntcheentrreaptliicoantses(3af0t2e0rmtegn kdagy"s.drTyhweeisgehdtimseendtimuesnetd)iasffteorufnidvetodbayeswaitnhdiinn one `accepted limits for organic content but the silt fraction is recommended higher. TTaabbllee22..CChhaarracatcertiestricssooff thheesseediment used for testing Organic content (9) Sit fraction (6) er es Lab. ref.no: TSeasmtppleeriroecde:ived. Report date: 99312-1 032103..0192..9999 05.01.2000 S\- Nove L. [rr ``EElningiHnoerevre SeniAogreReMsoelavrecrhsSmcyierntist = Analytical technician Quality Assurance Enclosed: Data sheets wed iTosmtceshterehpnriinsflel,dwbiyhtbhoerprnmiascicroendiitnewdrbiynNgorbwyeRgFan-AMcilrjeoaiba.ion(NA). Thereport may no be rroduced n a0ny00250 LSaobrseaino: Page 180/31 PRIMARY DATA: Acute toxicity test with `Corophium volutator Test substance: "F201 AF Light Water Brand AFFE" SLuabt. doatte: Measurement: s03a.12z99 Numbofederad [ | nTuomubler|| Nspoprmevbceeisrmseeolnf NUMBER OF DEAD soars Todas I || (rcoorncaeanrtryawtaiognhy||sopeocinme:n|| A8 FE Tol Toul | Control T1o0 010 1100 000000 | { | a4 10 10 10 | || ww |e| ver | | re | | lfeeroenceessuubsstanceG(oorratnieherne): epee "Tharosutwithth afrancesubstance iwith he rangenormal found 000251 L9b9r3e1f2r1o. Page 190/31 Test substance: "FC-201 AF Light Water Brand AFF" SLtaabr.trdeatt:e: 90331.122-919 Measurofeoxmygeen anndtpsH. || (`Comnceanortyrawnteiioggnht| Oxy(g%)en pH - Oxygen [2 PH - Oxygen () pH I - PToomT[eow w[nowwllo =w|v] t | 1 Cw[[vonw[[wv=anow] --1 7 | --rr 1 rr eoonce substance toramboney em 000252 Lsabsreifro: Page 20of 31 DATA SHEETS 000253 L9a9b31r2e1pro: Fuge su on _ F45->3TASLAD (Helse-, Miljo- og Sikkechetscatablad) Doosks:amenaetrar.: 100-34/11415/-368 USzkgrietvees ut :: 0141//0111//9998 VSeirdesjon l~~av: 06.01%1 Teieon: 63 84 75 00 / Telefax: 63 84 17 88 | i| 1 IORNTIFIEASION AV KIEHIKALIET OG ANSVARLIG FIRMA. | Importer: IN Norge A/S | dandelcs-n6a0vn2: LIGHT WATER BRAND ATC PLUS oeiazoeasjzo.n:sa0u3m5m3e3s7,. Produkcregisteret: Zetefo2n2,'sGif1i3in0f0ornesjonssencralen: | e 2 0Pr ILYSmNINGeER n OM KrIZMe ImSKntmSNOMmmEeNeSe eTTrNeIaeNGm.emanet aman mim e ea nennnnne | | szorexan casas verr-proseNT i| .- : 1,2-zTav0r0L rrr 107-211 =a 2-(2F-a3UrTeOsKySaYoZlTeOsK/SsYi)s-iEkToAsNeOtLni/nger: Xn; R:22 112-38-5 -u (DIEFTYaLcEeNsGyLbYoXlOeLrM/OzNiOsBiUkToYsLeEtTnEiRn)ger: Xij Ril6 FLUORALKYL, OVERFLATEAKTIVE STOFFZR Trade Secze 1s SYNTETISKE OVERFLATEAKTIVE STOFFSR Trade Seczet 1s MTRAErGSNaTEEESRRIeUAMVSUOLRFGAATNISKE FLUORKJEMIKALIER tTeraa7dd4ee87-SS8ee3cc-zr9eett I0k.k5e -=kj1e1n5t 1|| | 000254 Labrefro. 99312.1 Page 220f31 FC-602 LIGHT WATER BRAND ATC PLUS 3 VIXTIGSTE FAREMOMENTER. To Vikeigsse skadevizkninges Kea irsitere oynene, huden og luftveiene. stikeshes: iljotae: Ssestalaviall. 4 rorstzassiasTILTAK. - 1i Tilzek oyne: Scaiiydldlelssuezresk.s oyneze med rikelige mengder vara. Kontakt lege konzaks Lege. Titelkviisnntsnydnipncgo:mer oposthz, bring vedkommende bort fra ekoknszpaoknsesilnegges.kilden. Sorg for frisk lufc. Hvis symptomene vedvarer, TilakKonstvaelkgtinlge:e uniceisart. Fremkall brekainger kun i samcdd med pemezdsiosni.nsk pesonell. Gi aldri noe giensom mussen til ea be.visstles TILTAX VED BRANNSLUKNING. Zgnes Prborcaunkncseltukneringestmibdrdaenln:slukkingsmiddel. Ikke egnet branaslukningsmiddel: Eksponeringszisiko ved brann: 00255 La99b3r12e1r. rage 3031 FC-602 LIGHT WATER BRAND ATC PLUS _--Forazenniagsprodukzes ved bramn: Prosedyzes ved sluking av brana: i - i Taimax veo urzLsIRIT UTSLIR. : sessonSetigveervneescnielseielkeaukd:e: andre punkter i dette EXS-casablades. | ZileakVevnesdituessilomscihkdtee:s.uzSspiiilcle:avgrenses umi: ddelbare. Dexk til med ec : ihsorserende mazezisls. Spill samles opp umiddeloart. Rengjer ; omridet med vana. Plasseres i en egnet beholder med lokk. Se punke 13, Fieraing av kjenikalieavall. | 7 5ANDTERING OG OPPITVARING. i | Th Tir Setingelser foTrigrseiskkerocnpcpbbaeevrarhivnogr: produktet kan komme i kontext med 1| mCDaeeclhsoietuldsle,errenLalgecogeeecsmtidvlleueeks.et:eLmapigerrreastpurvroeeddsukttoeevtmepreir0kaktegursaedreu:nidecbrerlusk4.i9usg.radFeorld +? Utozenelige mesesiates: venziloapssiboenv:as emb-allssjen ph et godt ventilert sted. ii Sikkezhesstileak for & forhindre braan: | SikkeTrkhkeesbsrteinlntbaaks.for 4 forhindre eksplosjon: Sikkerhetstiltak for & forhindre statisk elektrisizet: foholfdoslzdegalnebrelvleasdjeberakt:est Produkter kan soyking Lfuokrkberts.akeRoyfkoirnugrenfsonrbiundgs:aUntdoebrakkberaukoasv/eller CStoikbeinliocgetfoagrlirgeeskdteixvoitmepso,nersiknagdseplriogdeukdteekrospkoannendteearn.es. Se punks 10, |! | ! || i J00256 L9ab3r1e2f-n1o.: Page 240f31 + FC-602 LIGHT WATER BRAND ATC PLUS - | | % ZXSI0NIRINGSKONTROLLS CG PERE SONLIG VERNrEUaTsSwTwYRu.sesssntrsasmnanunass i} OvevesUsn:ngt & 4 damp, spray elles thks i oynene. Bri teste |i vezaebriller med vencilez. stadve3s2n4:k esnede verneneaskes ev hensikcsmessig materiale ved ahnicaedfeaelreisn:g aBvucypirgoudmuakit.et. Vernehansker av folgende materiale(r) AnnesUnheusdvternnedeknonnahkisn.dvazn: . Andecsesssvazn: i| SaUvvnsaegL(dusf)icnignoodrdnukdrjieennngs:aiavdngaelcsuefdtizbeiasrraebvteeirdmnas:teetrmhioaasllfveam.arseknBeavsemelezsdtespfdielntkeoranvsmeonfttorlagsejnodneen | orzanisie damper of vaskeforaige pestikler: A/22ST. pDertocanriseirk.keVesspkiseust,setdcreikkoemsshdeelrlergrurnoydkiessmeunddesrkpeasobgeidvanmne.d Vesk Renders etter hinctering og for spising. Anbefaflvsisvecaitsiulgansijnognssvensilasjon ikke er tilstrekkelis, md egnet VgoedniskijieanssjionndesdLrikestatavedrenmpkboennysietnetsr.asjSoenxesnsforholtdielsssruenkdke:eliagnbefalte Siainisiraive nommet og/eller kentroller spray eller tke. Adm. normes for foruzeasning i arbeidsatmosfare, Febriar 1936: van A(s7s73e2r-i1n8i-n5g3)es: Tagen adm. nora. 1,2-EaT-RcbiImOeLss (v1e0r7d-i21p1m):- (stv) Taa-icviecezsdsi pvoemr:di25mg/m(3d:amp1)0 (stev) Takvezdi ag/ad: - (amp) 2-(2-BUTOKSYETOKSY) -3TANOL / (DIETYLENGLYKOLWONORUTILETER) (112-34-5) A8-nceiznkenrisngveerr:dlAompemr:ika35nsk grenseverdi enbefalt av produsenten. (Ingen norsk eda. nozm). FLUORAALnKsYeLzkOaViEngReFrL:ATEIAnRgTeInVEadmS.TOFnForEmR. (Trade Sectet) SYNTETAInSsKeEsinOiVnEgReFsL:ATEIAnKgTeInVEadmS.TOFnForEmR. (Trade Seccet) . . 0257 LSawbariefnro Page 250131 FC-607 LIGHT WATER BRAND ATC PLUS TT Amerkainger: Ingen adm. norm. TeRVERAEeme(rTkrnaidnegeSsescteitn)gen ada. norm. -) RISTIAS-AcVinaOrRsGANvIeSrKdEi FmgL/UaOdR:KJE0,M1IKALGrIeZnRse(vTerraddei aSencbreefta)lt av 3. | pyp---------- Tilstandstors, Sfasse, luke: uvgifseknensonvsaiskee.ig, ravissvet, ot: aos Sokepunke/ intervals ca. 93.00 C (3egynnence) Snelzepunke/-intesvall: Zkke zelevans Flassegunice: Ingen (Secetlash cc) Setvantonnelighet: ike selevant =ksalosjonssrensez, nedze: Ike relevant | Skasiosjonsgrenses, ove: Ikke celevant Dampteyik: co. 16 mmig (Ralkulest v/20 ) Loselisher vana: Slandbaz. Soestei ves: ce. 1.06 (vanael) desprescher: co. 0.85 (luteal) (ralwless | vi20 ) | Flykeise organiske forbindelser (VOC): =no319g/L SCAQHD (Kelkulest Fordanpningahastighet: <1 (buylacetatel) viskosices: Tike Kent frpm-------- : 0025! Lawbareiflro: Page 260f31 Fc602 LIGHT WATER BRAND ATC PLUS Fornote som skal umngha: MaseriTshteeerKseonms.skal unnghs: - FasiigeehosnpmaelstncitnagtssproodgukKcaerrb:ordioksid. Hydrogenfluorid. Gifsige damper, SGaasnsdeirngellfeorrvepnacretsikliekrk.e TberrmaipsrkesdeenkcoemrpsonneoreisngTisaivkob.ruksferdig | StasilSietaseisleo,g Fraecsikissiviptoelsy:merisasjon vil Like forekosse. 11 Gercvsnincza on aziszrans. | | 2ttekzieseayosvee:izzizasion: symptoser kan vara rocker, hevalse, smerter og threx. stteksTeirdhmuestizzicasion Cymscona kas veze T(oetcnceesr, lhaenvgevlasreigogellKeirse.gjentat koncake): |i Sttekses iankading: Sn enkele overskssonering som overstiges asbefslte administrative i | nocez, ken fore sil: S2Cciehvieikrse,kjonrissneegvvaniaesv,nestse,nitomrraaanltgnleceranvldee,ssyssktoveoimrmedmtie:nlahsesjytomnpostgeovmiiee:e,kksatnnreedvmsaeartettihlofdeelplienre, SZveaslisc,asihoonsti(asgveeogluafyesvienige.r): sympuomes kas vase sizhet i nese og || 2ttekziSevsreeestvoerplsrgoeidknugka:isatse,rsvmiesderoregfafneikstkees fsloumoclkejveamrifkoerlsitsyrz,relssoenr,fiVnenketste&p, EShuaeknleosplcreeinttdi,eeksabepirsneyrfeioceo,fmenshnleeomsvahtkeoerlrogsfiar.natsDkeesftpfoefnxoetrreeirlnisgsgoeo:vpesvifniogcerkneorrksjaennnetuizesokleogi, vfeliuloerdknjienmgi.kalies ndr de brukes som forutsatt og i hemhold eil Svelging kan fore wil: sivuircikneaningogavryagygszmeenr:ters.ymptoner kan vare redusect urinsengde, blod AKsopuimzearsjnoendsp|retcumaognetn.e.(LZunngaelbmeicmennenleilsserssoanksktyilldecsilasttanfdreensmeexdlegenes 0025:  wsaeorng.dno.: rage 21031 FC-602 LIGHT WATER BRAND ATC PLUS i onpegsktaess0.9)9:blsoydnsotgomelsunkgaeabesveanzneelhsoestisnogm, kapnustveazveassLkievrs,irugeinsdpei.ng, Informasjon om allerg:, ovezfolsomhet: - kretsizeskallende egenskepes: Asvessoteskadelige egenskaes Repzoduksjonsakadelie egenskepes: AndeDseksesedevpircokdnuiknigee:s,inhneeihsoel:de: en eller flare ogeaiske { fluorkjesikelies, son muligens kan sosorbezes og lagres i kroppen | ocveedrhzylzenginegsstisco,ffeenrte(nnesseobmoluietgcaensg)s,moloegiyklaencakeliluemrulesraems ved gZjoernmtaetnzneeskeekrspoznaerienkgsepro.nerDiensg foovreerlifgogresorgienngiesnkekjefnltueorkhjeelmsiekeaflfeiketres aks de brukes som forutsatt og i hemtold til velledning. | gFeorzeeckeolnlsezebnefavolokrngienngiesnkeogfulnudoerrkpjoepmuilkeasliioerneri bsolmodeatrbetiidlerdee,n har || evasres apzusbeliidseerrss vsiisdeesn i1n9g70endzsekneed.eliJgse eefpfiedkeemeiro.logiske studies av | foresporsel. {|| c 12 orruvvsummczaroneuiLsvereazz.esnet memv rnt rmeS em-- 5 PecsisDteecntes/apirooldougkitseks niendnberhyoslhdaesrheesn: eller flere orgeniske faillujoecektjen(ipkeaslsiiesscenstoen).muligens ikke er nedbryihece og forblir i GkocaEstix3o4loiglijsok-eprdoadsua:kedatabled er tilgjencelig od foresporsel. AndzeNesdkbardyetvbiazrkhneitn:ges, milje: CBO0D0 5(Cdhaegmeircsal (O3xiyogcehnemDiecmaalndO)x:yge0n,55D2ema3/n3d;): 0,254 9/9; B2000da20gesdsageBros/:co0D,:4220,g7/6.g; Akvasisk gifighess 96 timers LCS0 for tisk (Fathead minaou (Pimeshales promelss)): > 0026! Labrefro: Page 28/31 593131 FC-602 LIGHT ATER BRAND ATC PLUS i18000timmge/r1s;ECS0 for daphnia (daphais magna): 1000 mg/l; 5(tmiicnzuostioxessSysotgem1)5: mhiennuntotelsdssviZsC502,10Pbhgo/tloboagct2e2z0imuS/p1h.osstoreus Sos for avfallshdndtering in:. gjeldende forskrifter. 1 13 FITWING AV KIENERALTZAVAALL- NetodeSsoesfioartafvjeearlnli.ngLaevverkjaevmfiaklallieialviaelnl:offentlis gockjeat iansaales, Sottaks- eller behendlingsanlesg for.spesieisviall. aHrObVeIsDeKlAsTeIGaOvRia0l7l:sgArVupFpAeLrL: FRA ORGANISKE PROSSSSER. sUeNnDsEjRoKcAiTaSgGsOnRiEdi0e7s,06:desAivnaflelksjfornasmPi3dDlBeravogfektotsssteotfifkeer., size, oZ5akm-okcoedreLu0c7. 05 03: Zalogenerte organiske losemidler, veskevaskes Avtallsiofiummes: 7151 Organisk aviall med halogen. Spestetle komponenter: Srylenglykol, fluosfosbindelser. 14 oPTLYSNINGER ON TAANSTONT. A0n-kiasse: - sitter - bokszav: . mazgnummes: - caricokore: - ON-nummer: - IcA0-Klasse: - I0G-Klasse: IH0G-side: - Eus-az.: - Hens: - || 00261 LFaabrretfsro. Page 290f31 - FC-602 LIGHT WATER BRAND ATC PLUS Ianeholder: 1 2-(3utoksyetoksy)-etanol 10-15 % - Et sntning av damp/sprarsasiie. Urs kansas ned synene 05 | ee roan Sh7ih seters $oundis ned. iors iogzin3se: || vann. Ved svelging, kontakt lege omglende og vis denne beholderen etye sppF iguine e ges untSeeeeisnsgoPehhatiHdrleingaevsare.sHeactkkeifnogresnkeivficles og vil Consoles: 1,2-asendiol, 2-(1-bussksyatoksy)-scanol Tve eentile erte steeedenerreo. mnUoannengahinTogrinvananensitdisnSsdainnneKgdovinvesaeavi.koedroaegmsposvda/ensneppp.urdtoevyHsnth,evtaDdnFxkshkeee.0n3sUavnneFnioqgtnodtosat.ktser e oe T ts enersyatfosr Tboernne. oii Lege wmiadaimate: 0026 CL Labrefro: page 200/31 FC-602 LIGHT WATER BRAND ATC PLUS re r ------ ee | ! ssesietie lover og bestemserses: SI.ikFkoercshkezsisfasasoamvtuiaasfsoeridfealrsieizeogkjdeimsitkrailbiuosrj:on av Helse, Miljo- og |! : 2. Forsxzifs on kisssifizaring og marking av farlise kjesikelies. | 3k.anFomresdkfroirfecmoimljekflaarses.ifisezing, merking m.v. av S:off som | | | 45o.. fFeoorrsskkrriifsc oomm sspteosfifaktaarvtioatielk.. | ; 16 ANON: ORRLSNINGER AV SETUONTNG FOR sRURGAIES STRRGRET 00 Bais. | AavendFeillsnedsaonmnseinddeer:siumkonsentrat for slukking av brann i hydsokarbones 0g polaze leseaidier eller vasker. |I{ VikzigDsetceablkeidldef(ar) 3v4eGdenuetraarlbeOifdfeilcseesn, avSt.EMSP-adula,tabMliandneets:ota, USA. !i RessWoeliet ocpaprdsabtlaarcieasgsar reviders. Tilpesses nye merke- og |i | #us-dazeblaciorskrifeer, fasssace & Januar 1998. Suc. | 257 oppiysninger: i c=IpnpfelovrtannaeisnjgopenrseonduokogtdebradsestaetnedoeprEpMiSna-odiranmtiaalnbeglasfdnoegrshhoelnedcr.eiETaihhxevineihryoldbberuutkkiloavgvhrphernodndsiuevkratirenergnedsneom i pIrkkoedukesxes 1seKmsovmebrinamseiconcasmteed AanNdSr-edeparboicaduerte,s eelllleerr esnohmvemredfaonrneern bruk av proses | | ec brekesens sasvaz. | i . I| ke  Lsawbrierflro. Page 31 of31 FG-602 LIGHT WATER BRAND ATC PLUS F0L0E0% SRODUKTER DEKKES AV DEFTE AWS-OKEALADET: | 3M Io-az. + X3M-0A0F0E8/-A0T2C21-75C-602 Brannsluknin i i| ssskun Produksjon i 3 10-nz. + X3-0L0i0g8h-t01W0a0t-e1r/GWASTE/ATC Fire i: Fighting Foam, FC-502,1000 L | 3 To-nr. + XF-0008-0073-5 F3i4ghLtiignhgt WFoaatme,rd/F6CN-A50F2T,E/AT2C0 Fire L 3 Tons. + X3M-0L0i0g8h-t00W7a7t-e1r3/6VATFZ/ATC F-irs |i Fighting Foam, FC-602, 200 L i |i | i | | -