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Nausea National Loss Control Service Corporation Long Grove, Illinois 60049-0075 (708) 540-2488 Fax (708) 540-4331 ENVIRONMENTAL SCIENCES LABORATORY, K-2 TO: HARK A. CHAMPAGNE OCCIDENTAL CHEMICAL CO. P.0. DRAUER CC INGLE5IDE TX 78362 LABORATORY ANALYSIS REPORT REPORT DATE OCT PA, 1992 SAMPLES REC'D OCT 20, 1992 REQUEST NUMBER 17842Q___ PAGE NUMBER 1 OF REQUEST. SAMPLE NUMBER ANALYSIS REQUESTED RESULTS 101492-1 BLANK. . . . BLANK.... ETHYLENE DICitORIDE VINYL CHLORIDE NOME DETECTED NOtC DETECTED Milligrams Front Back Front 101492-2 ETHYLENE DICH.ORIDE 0.023 <0.0045 0.50 VINYL CHLORIDE Micrograms Front Back Cl.5 <1.5 Front <0.05 Milligrams Front Back Front 101492-3 ETHYLENE BICHLORIDE 0.025 <0.0045 0.53 VINYL CHLORIDE Micrograms Front Back 1.9 <1.5 Front 0.06 Milligrams Front Back Front 101492-4 ETHYLEFE DICHLORIDE 0.19 <0.0045 4.2 VINYL CHLORIDE Micrograms Front Back 38 2.5 Freni 1.4 101492-5 ETHYLENE DICHLORIDE Milligrams Front Back <0.0045 <0.0045 Front <0.10 PPM Back <0.10 PPM Back <0.05 PPM Back <0.09 PPM Back <0.05 PPM Back <0.10 PPM Back 0.09 PPM Back <0.10 COMMENTS: ALL SAMPLES HAVE PREFIX "MAC". ( f)ANS LESS THAN THE RESULTS WERE CORRECTED FOR THE FOLLOWING DESORPTION EFFICIENCY: 93X - ETHYLENE DICHLORIDE. Flespectfully submitted, V " A- Yno Joan A. Wronski, CIH| Manager Environmental Sciences Laboratory ACCREDITED BY THE AMERICAN INDUSTRIAL HYGIENE ASSOCIATION NC 448-2 SOM 1-92 OCC 8655 PRINTED IN U.S.A. 4L N3TL5CD National Loss Control Service Corporation Long Grove, Illinois 60049-0075 y (708) 540-2488 Fax (708) 540-4331 ENVIRONMENTAL SCIENCES LABORATORY, K-2 TO: HARK A. CHAMPAGNE OCCIDENTAL CHEMICAL CO. P.0. DRAUER CC INGLESIDE TX 78362 LABORATORY ANALYSIS REPORT REPORT DATE OCT. 26. 1992 SAMPLES REC'D OCT. 20, 1992 REQUEST NUMBER 178420 PAGE NUMBER OF REQUEST. SAMPLE NUfffiER ANALYSIS REQUESTED 101492-5 VINYL CHLORIDE 101492-6 ETHYLENE DICHLORIDE VINYL CHLORIDE 101492-7 ETHYLEIC DICHLDRIDE VINYL CHLORIC? 101492-8 ETHYLEIC DICHLORIDE VINYL chlqr: ___________ .___RESULTS ________ Microqrams Front Back Front PPM Back Cl.5 Cl.5 CO. 05 CO. 05 Milligrams Front Back Front PPM Back 0.0082 CO.0045 0.19 CO. 10 Mierograms Front Back Cl.5 Cl.5 Front CO.05 PPM Back CO. 05 Milligrams Front Back Front PPM Back 0.026 CO.0045 0.64 CO. 11 Micrograms Front Back 1.5 Cl.5 Front 0.06 PPM Back CO. 06 Milligrams Front Back Front PPM Back CO.0045 CO.0045 CO. 12 CO. 12 Micrograms Front a.5 Back Cl.5 Front CO. 06 PPM Back CO. 06 COMMENTS: ALL SAMPLES HAVE PREFIX "MAC C MEANS LESS THAN THE RESULTS UERE CORRECTED FOR TIC FCSLLOUING DESORPTION EFFICIENCY: ?5% - ETHYLENE DICHLDRIDE. Respectfully submitted, \ V%. ... Joan A\ WronsKi, CIH, Manager Environmental Sciences Laboratory ACCREDITED BY THE AMERICAN INDUSTRIAL HYGIENE ASSOCIATION CC 8656 PRINTED IN U,$.A. n N3TL5C0 " National Loss Control Service Corporation Long Grove, Illinois 60049-0075 (708) 540-2488 Fax (708) 540-4331 ENVIRONMENTAL SCIENCES LABORATORY, K-2 TO: HARK A. CHAMPAGNE OCCIDENTAL CHEMICAL CO. P.0. DRAWER CC INGLESIDE TX 78362 LABORATORY ANALYSIS REPORT REPORT DATE OCT. 26, 1992 SAMPLES REC'D OCT. 20, 1992 REQUEST NUMBER 178420 PAGE NUMBER 3 OF REQUEST. SAMPLE NUMBER ANALYSIS REQUESTED 101492-9 ETHYLENE DICtCORIDE VINYL CHLORIDE 101492-10 ETHYLENE DICHLORIDE VINYL M.0RI0E 101492-11 ETHYLENE DICHLORIDE VINYL CHLORIDE 101492-12 ETHYLENE DICHLORIDE RESULTS Milligrams Front Back Front <0.0045 <0.0045 <0.11 Micrograms Front Back Cl.5 <1.5 Front <0.06 Milligrams Front Back Front <0.0045 <0.0045 <0.14 Micrograms Front Back <1.5 Cl.5 Front <0.07 Milligrams Front Back Front 0.012 <0.0045 0.33 Micrograms Front Back <1.5 <1.5 Front <0.06 Milligrams Front Back Front 0.19 <0.0045 5.3 PPM Back <0.11 PPM Back <0.06 PPM Back <0.14 PPM Back <0.07 PPM Back CO. 12 PPM Back <0.06 PPM Back <0.13 COMMENTS: ALL SAMPLES HAVE PREFIX "MAC". C MEANS LESS THAN THE RESULTS WERE CORRECTED FOR THE FOLLOWING DESORPTION EFFICIENCY: 93X - ETHYLENE DICHLORIDE. Respectfully submitted. Joan A.TA/roftski, QlH, Manager Environmental Sciences Laboratory ACCREDITED BY THE AMERICAN INDUSTRIAL HYGIENE ASSOCIATION NC 448-2 30M 1-92 OCC 8657 PRINTED IN U.S.A N3TL5CD National Loss Control Service Corporation Long Grove, Illinois 60049-0075 (708) 540-2488 Fax (708) 540-4331 ENVIRONMENTAL SCIENCES LABORATORY, K-2 TO: MARK A. CHAMPAGNE OCCIDENTAL CHEMICAL CO. P.0. DRAWER CC INGLESIDE TX 78362 LABORATORY ANALYSIS REPORT REPORT DATE _ . OCT. 96, 1992 SAMPLES REC'D f|f;T pft. 199P REQUEST NUMBER 17A49A _ _ PAGE NUMBER 4 OF REQUEST. SAMPLE NUMBER ANALYSIS REQUESTED 101492-12 VINYL CHLORIDE 101492-13 ETHYLENE DICHLORIDE VINYL CHLORIDE -RESULTS. Micrograas Front Back Front Cl.5 Cl.5 CO. 06 Milligrams Front Back Front 0.014 CO.0045 0.40 Hicrograms Front Back Cl.5 <1.5 Front CO. 07 PPM Back CO. 06 PPM Back CO. 13 PPM Back CO. 07 COMMENTS: ALL SAMPLES HAVE PREFIX "MAC" C MEANS LESS THAN THE RESULTS WERE CORRECTED FOR THE FOLLOWING DESORPTION EFFICIENCY: 95% - ETHYLENE D1CHLORIDE. Respectfully submitted, \\ x iv V' P Joan A. Wronski, CIH,` Manager Environmental Sciences Laboratory ACCREDITED BY THE AMERICAN INDUSTRIAL HYGIENE ASSOCIATION OCC 8658 PRINTED INU.S.A. n% N3TL5CD National Loss Control Service Corporation Long Grove, Illinois 60049-0075 (708) 540-2488 Fax (708) 540-4331 ENVIRONMENTAL SCIENCES LABORATORY, K-2 TO: HARK A. CHAMPAGNE OCCIDENTAL CHEMICAL CO. P.0 DRAWER CC INGLESIDE TX 78362 LABORATORY ANALYSIS REPORT REPORT DATE OCT. 26^ 1992 SAMPLES REC'D . _ OCT._2(L_ 1522 REQUEST NUMBER .122419_____ ___ PAGE NUMBER i OF REQUEST. SAMPLE NUMBER ANALYSIS REGUESTED 101292-1 101292-2 101292-3 ETHYLEIC DICHLORIDE ETHYLENE DICHLORIDE BLANK.... BLANK RESULTS Milligrams Front Back Front 0.040 CO.0045 11 0.038 CO.0045 11 NONE DETECTED PPM Back Cl.2 Cl.3 C MEANS LESS THAN THE RESULTS UERE CORRECTED FOR THE FOLLOWING DESORPTION EFFICIENCY: ?3X - ETHYLENE DICHLORIDE. Respectfully submitted, Joan A. Wronski, CIH, Manager Environmental Sciences Laboratory ACCREDITED BY THE AMERICAN INDUSTRIAL HYGIENE ASSOCIATION NC 448-2 30M 1-92 OCC 8659 PRINTED IN ILS.A. n NEITL5CD National Loss Control Service Corporation Long Grove, Illinois 60049-0075 (708) 540-2488 Fax (708) 540-4331 ENVIRONMENTAL SCIENCES LABORATORY, K-2 TO: HARK A. CHAMPAGNE OCCIDENTAL CHEHICAL CO. P.0. DRAUER CC INGLESIDE TX 78362 LABORATORY ANALYSIS REPORT REPORT DATE OCT. 26^_ 1992 SAMPLES REC'D OCT 20,. 1992 REQUEST NUMBER 128420____ ___ PAGE NUMBER OF REQUEST. ANALYSIS REQUESTED ETHYLENE DICHLORIDE VINYL CHLORIDE _______________________ BETBQDQLQGY___________________________ OSHA METHOD 07 EQUIVALENT QSHA METHOD 04 Respectfully submitted, Joan A. WronsKi, Vk Manager Environmental Sciences Laboratory ACCREDITED BY THE AMERICAN INDUSTRIAL HYGIENE ASSOCIATION NC 448-2 SOM 1-92 OCC 8660 PRINTED IN US.A. ^MflSCD National Loss Control Service Corporation ENVIRONMENTAL SCIENCES LABORATORY, K-2 O? .v ^ ,, - One Kemper Drive Long Grove, IL 60049-0075 708/540-2488 /TlotZName 0 CL Title , $&Clk / Firm At-- XJAx2>A <, Address /?/). IJ f C-7 ____________ ,7-Xfrh tdr J /ek as ~7zXS6~l Bus. Tel. No. f5/3) 9 7A' A O.BI A__________ ANALYSIS REQUEST No.178420 FIELD NUMBER SAMPLING VOLUME ANALYZE FOR- LABORATORY NO. RESULTS bC.; 1 A/an JL 088946 rr}ML/oim~2 h.^l jzhr c^CM 088947 MJT.IOMteS /l.fL /^r>r i/Cm. , 088948 rt.4c - B Arhc M_ichu /UJL -- / l/0 -------------- 088949 n. *jl t/C/K. 088950 /D, L7 7)c . /C/A. 088951 /nAumfaX iV.oL B A C l/tVX 088952 rffc/eflW-?' ML nxi L/r/n m.hzmwX 9'?^ ^AC i/O^z/o unc, lOHTl-lC %.0L 0(,0 Lyrskc l6MfX-f( 088953 088954 ______________II___________________________________________________________ II 088955 , 088956 9/7 L /-/) | 088957 nJK./ertU-tf ?,5L /?AC t/C./rX. 088958 DATE SAMPLES TAKEN DATE RECEIVED BY LABORATORY COMMENTS: l/C/n r iQL/o/L/cIz' P<& v-l fj> zX PP/X /// dSZ ^ DATE COMPLETED CO- 2.3 -ffz- ANALYTICAL METHOD: Ct(L NC 82-9 ISM 3-92 ^4-10H- OCC 8661 PRINTED IN U.S.A. .MjLsm_______________________ National Loss Control Service Corporation Name /rfafik U- Cl Title jhjj/fAlC Firm CJ'iCu kLl^Ctn _______ Address /?Q- J)aujr.j C,C^ 7C^&it:s/rIa r y^a s___ Bus. Tel. No. ENVIRONMENTAL SCIENCES LABORATORY, K-2 One Kemper Drive Long Grove, IL 60049-0075 708/540-2488 ANALYSIS REQUEST No.178419 NC 82-9 ISM 3-92 OCC 8662 PRINTED IN U.S.A.