Document 65RdwMbyrMRJ8jL5KBOYo86j6
January 27, 1972
NEW FORMULA AX-501 Continued
Brabender Viscosity 480 - IQ. Viscosity can be adjusted by addition of water, reduction of mix water, or by addition of ASE-60 in small amounts. It is best to hold back a small amount of water to be added if the viscosity is too high. ASE-60 may be added to chicken the mix should too much water have been added. Should it be necessary to ado ASE-60, the pH oust again be checked since ASE-60 is acidic and its addition will lower pH. Remember, changes In the water concent affect flow properties as well as the wet density.,
WORKING CHARACTERISTICS: Shall extrude easily from tube and form a uniform bead that does not sag or run.
a
OPEN TIMS
- Refer to Plant Testing Procedure No. 114
WETTING CHARACTERISTICS; Refer to Plant Testing Procedure Ho. 115
TENSILE STRENGTH - Refer to Plant Testing Procedure No. 116
ALKALINITY
- Refer to Plant Testing Procedure No. 34, Adjust with small quantities of AMP
Specifications: Maximum
Minimum''
'Average
8.0 DENSITY
Specifications: - 10.75 Ibs/gal
7.7 10.65 lbs/gal
7.9 10.7 lbs/gal
Case weight should be 35 lbs. i 1 lb.
J-
EDOielz*
Lehnert 10.3.01-82
PLAINTIFF'S EXHIBIT GP-2284
SGP 0016181
February 11, 1572
Supersedes AK-501 Dated 1/27/72
AKRON, NEW YORK, PLANT FORMULA DRYWALL ADHESIVE AK-501
DESCRIPTION:
- Drywall stud adhesive. Provisional formula for salvaging formula AK-955.
FORMULA;
Raw Material
Function
HM Spec. Percent Lbs./Batch
Akron Stud Adhesive
AK-955
.
Water Advawet 33
Solvent
.
Wetting agent
Water
Solvent
Clay
Filler
Asbestos SG 210
Filler
Resin E3-12
Adhesive
Emulsion RA-315
Adhesive
217 .
Propasol
Filming Agent
Dibucyl Phthalata Plasticizer
Water
Solvent
Acrysol ASS-60
Thickening agent
AMP 95
pH Buffer
22S
54.9 1.6 1.0 6.0 9.0 0.8 8.2 5.2
X.l 0.8 7.3 3.5 0.6
(102 cases of small tubas 2818.0or 78i cases large tubes)
82.0 (9.8 gals.) 51.0 (6.1 gals.) 308.0 <37 gals.) 462.0 41.0 421.0 (56 gals.) 267.0 (30 gals.) 56.0 (7.8 gals.) 41.0 (4.7 gals.) 415.0 (50 gals.) 180.0 (21 gals.) 31.0 (395 gals.)
100.0
5133.0
YIELD
- One batch yield 480 gals.
5* MIXING PROCEDURE - Extract AK-955 directly into mixer and proceed in the ' following.order:
1) Add water followed by the Advawet 33.
2) Mix for five minutes.
,
3) Add the water ^2n<J addition) followfid by thfi filfly Slid SSbfiCtOSt
4) Kix for a further 30 minutes. 5) Add the following ingredients allowing each ingredient to be thoroughly
blended before addition of the next ingredient.
Resin S3-12 Emulsion RA-315 Propasol Dibutyl phthalate
<.
6) Add water and Acrysol ASE-60 (may be added simultaneously) AMP 55
VISCOSITY
- Refer to Plant Testing Procedure No. 109.
Specifications:120 to 300 Brabender unit
LeUnert 10-3 .01-83
SGP 0016182
k --$u
February 11, 1972 Supersede* AK-SOl (Coat.)
Dated 1/27/72
3rcber.der Viscosity
Viscosity-can be adjusted by addition
of water, reduction or mix water, or by addition of AS5-60 in small
amounts. It is bast to hold back a small amount of water to be added > if the viscosity is too high. ASE-60 may be added to thicken the mix
should too such water have been added. Should it be necessary to add
AS2-60, the pH must again be checked since ASE-60 is acidic and its
addition will lower pH. Remember, changes in the water content affect
flow properties as wall as the wet density.
TORKISu CHARACTERISTICS; Shall extrude eaai ly srom tube and fora a
uniform bead that does not sag or run.
OPEN TIK2
' - Refer to Plant Testing Procedure No. 114
NETTING CHARACTERISTICS? Refer to Plant Testing Procedure No. 115
TENSILE STRENGTH - Refer to Plant Testing Procedure No. 116
ALKALINITY
- Refer to Plant Testing Procedure No. 34. Adjust with small quantities of AMP
Specifications: Maximum
Minimum
Average
9.0
DENSITY Specifications: -11.20 lbs/gal
7.7 10.60 -Ibs/gal
6.3 10.9 lbs/gal
Case weight should be 35 lbs. - 1 lb.
D0:elz
Lehnert 10.3.01-84
SGP 001.6183 pi--Scl
February 18, 1972 r" Supersedes AK-501
Dated 2/11/72
AKRON, J3W YORK, PLANT FOESOJLA DRTOALL ADXZS5V5 AK-501
."ZSCr.IPTION:
- Dryvs.ll stud adhesive. Provisional formula for salvaging formula AX-955.
-QXWLA:
Raw Material
Function
R>t Spec. Percent Lbs./Patch
Akron Stud Adhesive AS-955
t'
Water
Solvent
Advawet 33
Wetting agent
Water
Solvent
Clay
Filler
Asbestos SG 210
Filler
Resin E3-12
Adhesive
Emulsion RA-315
Adhesive
217
?rop2sol
Filming Agent
Dibutyl Phthalate Plasticizer
Water
Solvent
Acrysol ASS-60
Thickening agent
AX? 55
'pH Buffer
225
54.9 1.6 1.0 6.0 9.0 0.8 8.2 5.2 1.1 0.8 7.3 3.5 0.6
100.0
(102 cases of snail tubas 2818.0or* 78$; cases
82.0 (9.8 gals.) 51.0 (6.1 gals.) 308.0 (37 gals.) 462.0 41.0 421.0 (56 gals.) 267.0 (30 gals.) 56.0 (7.8 gals.) 41.0 (4.7 gals.) 415.0 (50 gals.) 180.0 (21 gals.) 31.0 (395 gals.)
5173.00
VIZ13
- One batch yield 430 gals.
MIXING PROCEDURE - Extract AK-955 directly into mixer and proceed in^caa
i* -/%
following order: Add watar followed by tha Acvawet 33.
2) Kix for five minutes.
3> Adi the water (2nd addition) followed by the clay and asbestos.
4) Kix for a further 30 minutes.
5) Acd the following ingredients allowing each ingredient to be thoroughly
blended before addition of the next ingredient.
Resin E3-12 Emulsion RA-315 Propasol Dibutyl phthalate
-
6) Aid water and Acrysol ASS-60 (nay be aided simultaneously) an? 95
VISCOSITY
- Refer to Plant Tasting Procedure No. 109
S?acizications:120 to 300 Brabender unit
Lehnert 10.3.01-85
i
SGP 0016184
*3
/
/
February 18, 1972
Supersedes AK-501 (Cent.) Dated 2/U/72
/ ? '^
Brcboncar Viscosity
Viscosity can be adjusted by addition
of water, reduction of mix water, or by addition of ASS-60 in small
amounts. It is best to hold back a small amount of water to be added
if the viscosity is too high. ASS-60 may be added to thicken the mix
should too much water have been added. Should It be necessary to add
ASS-60, the pH must again be checked since ASS-60 is acidic and its
addition will lower pH. Remember, changes in the water content affect
flow properties as well as the vet density.
HORSING CHARACTERISTICSi Shall extrude easily from tube and form a uniform bead chat does not sag or run.
OPEN TIKE
- Refer to Plant Testing Procedure Ho. HA
KSTTISG CHARACTERISTICS; Refer to Plant Testing Procedure So. 115
TENSILE STRBKGIS - Refer to Plant Testing Procedure So, 116
ALKALINITY
- Refer to Plant Testing Procedure No. 34. Adjust with small quantities of AS?
Specifications: Maximum
DENSITY Spaci' .cations:
9.0
11.20' Ibs/gal
Minimum' 7.7
10.60.Ibs/gal
'Average
8.3
10.9 lbs/gal
Casa weight should be 35 lbs. - 1 lb. i
SD0:elz
I
Lehnert 10.3.01-86 SGP 0016A85