Document 609vmjrZmEapxeRV2ONGp12d
To: R. T. Ferrell
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Interoffice Communication
From: Date:
Subject:
J W. Were March 17, 1987
ABERDEEN MONTHLY PROGRESS REPORT FEBRUARY, 1987
There were no injuries recorded during the month of February. of February 28, 1987, the plant had operated 2,793 days 3,588,055 manhours without a lost time injury.
As or
PVC resin production for February was 33.7MM pounds. Mechanical downtime in the reactor areas was due primarily to agitator seal repairs on 400, safety disc replacement on 745 and miscellaneous reactor valve repairs. Resin production year-to-date totaled 177.8MM pounds. The VCM efficiency for February was 1.01638 pounds of VCM per pound of PVC produced versus a 1.00208 standard. Year-to-date VCM efficiency is 1.01065.
Compound production for February was 6.8MM pounds. Line I and Line III operated twenty-eight days and Line V operated fourteen days during the month. Production was limited primarily by product changes, Banbury . maintenance and Line III mill maintenance. Year-to-date compound production was 35.4MM pounds. Quality performance for flexible compounds was 1.5% off-grade of which 100% was due to mill scrap. "BC" production was 1.2%.
Dry blend production was 3.9MM pounds for February and 22.6MM pounds fiscal year-to-date. Production was limited primarily by product changes and quality control problems. Quality performance for the month was 99.8% customer grade.
The plasticizer unit operated twenty-eight days in February to produce 1.6MM pounds. Year-to-date plasticizer production is 9.4MM pounds.
Two of four active involvement teams have completed their projects. The vinyl team presented the results of their work to management and a miscellaneous capital project was approved to institute their proposal. Department steering teams have been formed and began regular meetings in February.
Total energy consumption for February was 112.690 MMM BTUs. The energy consumption per pound of product was 2444 BTUs, resulting in an adjusted CMA reduction of 52.3%. The adjusted CMA reduction for fiscal 1987 year-to-date is 54.2%.
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R. T. Ferrell 03/17/87 Aberdeen Monthly Progress Report
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The total plant variable cost variance for February was $277.4M unfavorable, resulting from an overall unfavorable price variance of $283.8M and a net favorable efficiency variance of $6.4M. The total fixed cost variance for February was $56.9M favorable.
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DISTRIBUTION HOUSTON
PONCA CITY
OKLAHOMA CITY LAKE CHARLES VCM PLANT LAKE CHARLES CHEMICAL PLANT BALTIMORE HAMMOND ABERDEEN
- J. D. BURNS
- R. E. LEHMKUHL
- R. T. FERRELL
- R. D. GAMBLIN
- J. J. LANGFORD
- R. E. SWANTKOWSKI
- D. F. HARMAN
- H. R. FLAMMER
- E. L. KIESCHNICK
- S. K. SABORSKY
- K. J. EGGERS
- D. H. SANDERS
- S. E. MCGUIRE
R. L. POE
- H. J. HALL
- C. M. STARKS
- HARRY GARRISON
- DICK CONRAD
- J. A. DEBERNARDI (COVER LETTER ONLY)
- T. H. HUFFMAN
(COVER LETTER AND SAFETY PORTION)
- R. W. SEYMOUR
(COVER LETTER AND SAFETY PORTION)
- J. B. MAHER
(SAFETY PORTION ONLY)
JF, JWW, DWH, PJK, TFL, RAF, JVU, RAM, VEM, HGC, CWT, REP, VLT, PJR, JGC, RBN
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SAFETY - J. V. UPTAIN
Occupational Injuries
Feb
Fiscal Y.T.D. 1987
Fiscal Y.T.D 1986
First Aid OSHA Recordable
Total Injuries Number of Restricted Workday Cases
(RWC Rate) Number of Lost Workday Cases
(LWC Rate)
0 0 0 0 (0.0) 0 (0.0)
4 1 5 0 (0.0) 0 (0.0)
12 2
14 1
(1.01) 0
(0.0)
Injuries by Department
Vinyl Operations Compound Operations Maintenance Laboratory Receiving/Warehouse Office
Totals
3 3 5 0 0 _3 14
Injuries by Type
Cuts and Abrasions Eye Injuries Burns Bruises Strains/Sprains Stings Other
Totals
0 0 0 0 0 0 0 0
Non-Occupational Injuries
Lost Workday Cases Days Lost
02 0 11
3 35
Safety Record
Last lost time injury
7/5/79
Days since -
2,793
Manhours since -
3,588,055
Training
Topics for the plant safety meetings during the month included: Housekeeping, Personal Responsibility to Act, Finding Cures for Accidents, The Team Approach to Safety, Review of 1986 Safety Performance, and Maintenance Weekly Safety and Job Review.
One R&D employee and six contract personnel received plant safety orientation.
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Health
Activity for the month included routine dosimetry (shown below) and the start of annual* medical health screening (van).
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Chemical
Number
PEL Percent
Number
PEL Percent
VCM Lead Total Particulates
77 16
7
100.0 88.9
100.0
0 0.0 2 11.1 0 0.8
The two lead overexposures occurred with respiratory protection.
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QUALITY IMPROVEMENT PROCESS - R. B. Newton
A one-day training course for involvement teams and problem solving techniques was prepared. It is scheduled to be given to the Vinyl Department the first two weeks of March.
Two of the four active teams completed their projects. The team of operators presented their solution to the problem of cross-contamination to management. A miscellaneous AFE request is approved to implement their recommendations.
vinyl resin being
The maintenance team that was preparing the Preventative Maintenance Program for the new plant crane completed its work. A presentation to management scheduled for early March.
An additional involvement team was formed in the Maintenance Department to address the problem of valve actuator mounting brackets.
Each department in the plant has formed a steering team to keep the quality improvement effort moving forward. These teams began meeting regularly during February.
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VINYL - D. W. Hollis, J. M. Edwards
Safety The Vinyl and Yard Departments operated without an injury in February.
Shift safety meeting topic for the month was Accident Prevention and a review of the plant s first aid and medical cases which resulted from accidents in recent years.
Production
February
Y.T.D.(Fiscal 87)
1. Production, MM Lbs. 2. Daily Production Rate, M Lbs./C.D. 3. Total Charges 4. Charges, Reactor Batches/C.D. 5. Reactor Stream Factor 6. Dryer Rate, Average Lbs./Hr. 7. Dryer Stream Factor 8. Accounting Days
33.7 1202
854 30.5 94.8 10616 59.0
28
177.8 1190 4431 29.3 90.6
10407 59.2 151
Vinyl Department production for February was 33.7MM pounds.
Reactors
The reactor stream factor for February was 94.8%. reactor area occurred as follows:
Downtime in the
1) Operational Downtime: Accounted for 71.3% of the total downtime and was due to reactor recovery scheduling conflicts, downtime due to rinsing the chem wash tank, waiting on particle size information before charging, reactor manway O-ring failures and downtime associated with test runs.
2) Maintenance Service Downtime: Accounted for no downtime because the cleaning of the reactor AMS injection ports and inert vent lines was accomplished while the reactors were normally down for other reasons.
3) Maintenance Repair/Revision Downtime: Accounted for 28.7% of the total downtime and was due to changing the agitator seal on D-400, changing D-300 and 745 primary VCM valves, changing various chem wash and rinse valves on D-500, D-700 and 745, changing the safety discs on 745 and changing the inboard seal on B-compressor.
Dryers
The dryer stream factor for February was 59.0%. Downtime in the dryer area occurred as follows:
1) Reactor Limited Production: Accounted for 92.8% of the total down time. Dryers were shut down when possible for energy conservation.
2) Operational Downtime: Accounted for 3.8% of the total downtime and was due to centrifuge plugging, burner flameouts, dryer cleaning and transfer activator problems, and the fluid bed scrubber plugging.
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VINYL - Continued
Dryers - Continued
3) Maintenance Repair/Revision Downtime: Accounted for 3.4% of the total downtime and was due to changing out #7 centrifuge, changing out the fluid bed exhauster sheave, #5 activator problems, #6 star valve problems and the #8 tumbler seals.
Product Quality Summary
Resin Type
Prime
% of Total "B" "H" Production
5265 5305 5385 5415 5425 5465 Debox Off-Grade Sifter Overflow Pond Resin
Total
1,483,273 2,899,270 17,691,415 7,270,740 1,828,830 1,388,600
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55,703
-
55,703
4.4 8.6 52.6 21.6 5.4 4.1 3.1 0.0 0.2 0.0 100.0
Quality performance for February was 99.8% customer grade with 0.2% "H" grade production.
A total of six railcars were shipped as "B" grade during the month which represented 5.6% of the 108 total resin hopper cars; shipped.
Load Date Ship Date Car No.
Customer
Product
Reason
01/21/87 02/02/87 RTMX 580054 Cont. Plast. Co.
Debox
Derailed
12/14/86 02/03/87 VIPX 45811 Wexford, CA
Pond
Quality
01/27/87 02/09/87 PLCX 43730 Wexford, WI
Debox
Quality
02/04/87 02/23/87 VIPX 45871 Wexford, CA
Debox
Quality
01/28/87 02/25/87 VIPX 45793 Wexford, WI
5385
Contamination
02/20/87 02/27/87 VIPX 45713 Griffco. MS
Debox
Quality
The Vinyl area received fifty-nine short lead time emergency type orders comprising 22% of the 269 Aberdeen resin shipments in February.
Monthly Variable Cost Performance
Variable costs for the month were unfavorable at $269.3M resulting from an overall unfavorable price variance of $247.8M and an unfavorable efficiency variance of $48.5M. Resin variable cost for the month was 18.996 cents/lb. versus the budgeted 18.086 cents/lb.
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VINYL - Continued
Monthly Variable Cost Performance - (Continued) The $247.8M unfavorable price variance was primarily attributed to higher than budgeted pricing for VCM, $342.1M.
The $48.5M unfavorable efficiency variance can be attributed mainly to the unfavorable efficiency variance of VCM, $72.7M. This was partially offset by a favorable efficiency variance in Polyvic, $10.3M.
VCM efficiency for the month was 1.01638 lbs. VCM/lb. PVC versus the budgeted 1.00208 lbs. VCM/lb. PVC.
YTD variable cost efficiency variances in the Vinyl Department totaled $223.6M unfavorable.
Energy Performance/Progress
1. Plant energy performance for February was 2444 BTU/lb.
Resin raw material in the 0744 account totaled $209.7M.
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COMPOUND - P. J. Kober, J. E. Nickerson
Compound Production
Operating Days
Month
Production (M Pounds)
Average
Operating Day
Fiscal
Rate
Y.T.D.
Line I Line V Line III Total
28 2142
77
14 827 59
28 3860 138
6829
11904 4268
19219 35391
Line I operated twenty-eight days during February at an average rate of 77M pounds per day. Major items affecting production efficiency were: product changes* 73 hours; Banbury maintenance and seal changes, 41 hours; ribbon blender maintenance, 11 hours; housekeeping, 11 hours; quality problems and Q.C., 14 hours; dicer problems and maintenance, 6 hours; and Modicon reprogramming, 6 hours.
Line V operated fourteen days during February at an average rate of 59M pounds per day. Major items affecting production efficiency were: product changes and startup, 33 hours; quality problems, 4 hours; and plasticizer system problems and maintenance, 3 hours.
Line III operated twenty-eight days during February at an average rate of 138M pounds per day. Major items affecting production were: product changes, 40 hours; mill drive shaft gear replacement, 16 hours; dicing system problems and maintenance, 6 hours; hydrotherm system maintenance, 5 hours; and transfer system problems and maintenance, 5 hours. A test run to investigate rigid PVC production on Line III lasted approximately 11 hours.
Quality performance for flexible compounds was 1.5% off-grade of which 100% was due to mill scrap. "BC" production was 1.2%.
The raw material requirement for flexible compounds was .99658 pounds of raw material per pound of compound versus a 1.00993 standard (YTD is 1.00462).
The variable cost variance for compound was $46.4M unfavorable with $59.5M unfavorable due to price and $13.1M favorable due to efficiency. The efficiency variance due to product mix was $8.4M unfavorable. There were no major compound raw material efficiency variances.
Total compound inventory fell .4MM pounds in February to 7.8MM pounds.
Dry Blend
Month
Average Operating-Day
Rate
Fiscal Y.T.D.
Production, M Pounds Operating Days
3926 28
140
22561 151
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COMPOUND - Continued
Dry Blend - continued
Dry blend operated twenty-eight days during February at an average rate of 140M pounds per day. Production included 80172C, 80273G, 90172D, RP-200T, RP-421, 186-74, 186-139, 223-36, 196-198, 223-57, 245-53, 269-12, 269-67, 269-66, 269-63 and 269-43.
Dry Blend production was hindered by: product changes, 53 hours; delays associated with quality and lab problems and normal Q.C., 38 hours; transfer system problems and maintenance, 15 hours; filler system problems and maintenance, 8 hours; Welex diverter valve maintenance, 8 hours; screener maintenance, 8 hours; and Welex maintenance, 5 hours. Quality performance for the month of February was 98.4% customer grade.
The raw material requirement for dry blend was 1.00744 pounds of raw material per pound of dry blend versus a standard of 1.00489 (YTD is 1.01018).
The variable cost variance for dry blend was $51.2M favorable with $14.9M favorable due to price and $36.3M favorable due to efficiency. The efficiency variance due to product mix was $38.3M favorable.
Plasticizer
Month
Average Operating-Day
Rate
Fiscal Y.T.D.
Production, M Pounds Operating Days
1624 28
58 -
9372 151
Plasticizer operated twenty-eight days during February at an average rate of 58M pounds per day. Production included 61OP and 108P.
VRP production totaled 142M pounds (9,6%).
The raw material requirement for plasticizer was 1.11239 pounds of raw materials per pound of plasticizer versus a 1.09848 standard (Y.T.D. is 1.11520).
The variable cost variance for plasticizer was $14.1M favorable with $8.6M favorable due to price and $5.5M favorable due to efficiency. There were no major plasticizer raw material variances.
The efficiency variance due to product mix was $1.7M favorable.
Quality Improvement
Charting of process variables is being practiced on all lines. The continuing monitoring of plasticizer reaction rate has demonstrated a statistical increase in rate and reduction of reaction time since the charting began. A quality information bulletin board was started in the production area. Customer problems and positive responses are posted on the board to help the operators grow more familiar with the customer and his concerns and to provide feedback for our quality effort.
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COMPOUND Continued
Enersy
Compound Dry Blend Plasticizer
________ Usage (BTU/Lb.)___________
Actual
Standard
1716.5 720.1
1792.0
1783.0 730.0
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MECHANICAL DEPARTMENT - T. F. Lyon
MAINTENANCE - G. A. Morgan, D. A. Miller
There were no injuries to Maintenance Department personnel during the month. Vinyl
The D-400 reactor agitator seal was repaired during the month. Four agitator seals have been replaced through the first five months of fiscal 1987. Ten reactor valves were replaced. The following work was accomplished on pumps and compressors: - The seal was replaced in the old module east VCM charge pump. - The seal was replaced in the old module north chem wash pump. - The south VCM sphere pump was replaced with a spare. - The impeller was replaced on the fluid bed dryer scrubber pump. - The seal was replaced in the old module high pressure service water
pump. - The outboard seal was replaced in the 706 emission recovery
compressor. All mercury manometers on the reactors were replaced with vacuum
The annual replacement of the D-745 reactor rupture discs were completed. The #6 dryer exhauster was replaced with a spare due to high vibration. The #7 dryer Bird centrifuge was replaced with a spare due to high vibration. Twenty-three steam leaks were repaired. The control room batteries and inverter system was PMTd. The new unit seal water separator temperature controller was replaced.
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MECHANICAL DEPARTMENT - Continued
Compound, Dry Blend, Plasticizer
The Line I Banbury seals were replaced and two seal yoke cylinders were replaced.
The Line I B-blender gearbox was replaced.
The Line I A-blender ribbon shaft was repaired in the outboard bearing area. New chain guards were installed on both blenders.
The Zone I Line III hydrotherm system pump was replaced.
The dry blend unit #1 Welex mixer drive motor was replaced with a
A rebuilt gearbox was Installed on the north gump screener.
The Line I Banbury inlet chute and Ram housing was modified to eliminate excessive dusting and a potential lead exposure hazard.
The Line V single screw hot oil system was overhauled.
The Line I pro-batcher weigh controller was repaired. Utilities
Dredging on pond #3 was completed and a subsurface aerator was installed.
A new sulphuric acid day tank was installed at pond #3.
The hydrazine based oxygen scavenger for the boilers was replaced with a hydroquinone based product to eliminate potential employee exposure hazards.
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MECHANICAL ENGINEERING - Continued
Contracts A total of twenty-five register tickets and one construction contract were issued during the month of February.
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PROCESS ENGINEERING - V. E. Messick
Resin Quality Improvement Project
A. Flexible Resin Technology - Three experimental designs were run during normal production this month to determine causes of 5415 particle size variability. In the first experimental design, the volume of recovered VCM, the on-charge temperature, the VCM density, and the time in the cycle that the steam was started to the jacket were varied to determine which were significant. Only the recovered VCM volume was determined to be a significant cause of particle size variability. A second experimental design showed a significant difference in recovered VCM in the new module depending on whether 5305 or 5265 was being produced in 745 reactor. The third experimental design was run to determine the batch-to-batch 5415 particle size variation when 5305 was being produced in 745 reactor. The test was also designed to determine the colloid amount necessary to counteract this particle size shift.
B. Rigid Resin Permanent Facilities - A piping review meeting of the D-700 pump system was held at the plant with GED and PED people in attendance. The kick-off meeting between Vista and Litwin for Phases III and IV was held with work starting on the building layout. Review of "For Construction" packages of piping and I&E continues as they are issued. A sample of Methocel was sent to Westphalia for centrifuge testing and evaluation. Operating procedures and training were provided on the use of the Compound P system. Initial testing shows favorable results from injecting the Compound P into the
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Compound Lines I and V Magnets
The final issue of the class "A" design was issued to install magnets on Compound Lines I and V. Miscellaneous capital was requested to fund this project.
Residual VCM Reduction Team Activities
The residual VCM reduction methods already in place for 5265 resin implemented on 5305 resin. These include twelve-hour blend tank aeration, twenty-four hour silo aeration and charting residual VCM data on the blend tanks and dryer outlet. Steam injection to the blend tanks was tested to determine the effect on residual VCM removal. On 5265 resin, an additional 30% removal was obtained over normal aeration. On 5305, no additional removal was seen.
Interpersonal Skills Management School
F. G. Jeanson attended Interpersonal Management Skills on February 19 and 20 in Houston.
5305 Particle Size Variability
The plant along with R&D tested separate Compound P makeup to determine the effect on particle size. Separate Compound P makeup gave more consistent particle size control. Compound P is now made up separately from the F-50/GH-20 solution for all 5305 production.
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A
Influence Management School
J. G. Cole attended Influence Management School on February 16, 17, and 18 in Houston.
Reactor Data Acquisition System
Vendor quotes were received for the hardware, software and configuration for this project. An estimate is now being completed.
Additional Pond Aeration
Dredging of pond #3 was completed during the month and the aerator was installed and put into operation on 2/11.
Subpart V Compliance Project
The final issue of the class "A" design was issued after incorporating comments from the review meeting. An AFE request has been written and is being reviewed.
RQIP Environmental Team Activity
An organic loading estimate was prepared during the month based on projected recipe formulations. The peak loading estimate will be used in a simulation program to determine the capability of the plant's wastewater system under increased organic loading.
Southwire Customer Trial
Samples of 35852 were produced on Lines I and III for customer trials at the Osceola, Arkansas plant, Results of the trials indicated that the material produced at higher stock temperatures ran better. A possible lead dispersion problem was discovered during analysis of samples by R&D.
PVC In-Depth Seminar
Brett Bass attended the PVC In-Depth Seminar in Ponca City during the month.
Dry Calcium Stearate Addition System
Resin static control testing at the plant has been completed. R&D is analyzing samples of different resin types for effects on downstream processing. The review issue of the class ''A" design has been completed and is being reviewed.
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PERSONNEL - R. A. Miller
EMPLOYMENT None
PROMOTIONS/TRANSFERS R. C. Towery from Lead Operator to Vinyl Chief Operator Jeffery C. Shields from "A" Operator to Vinyl Lead Operator
RETIREMENTS None
TERMINATIONS Sammie L. Stokes, employee resigned
TO/FROM LEAVE OF ABSENCE None
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Salaried Employees Hourly Employees Total Employees Employees (Hourly)
New Employees Terminations
72* 169
241_
0 0
DEPARTMENTS Warehouse
PAR
mm
14
# EMPLOYEES
16
MIN. ElfP.
7
Minority Employees #
Salaried Hour1y
7 65
10%
38%
Total
72 30%
Hourly Min Hired % Min. Hired
Hourly Min Term. % Min. Term.
a 0 a a
% MIN. NEW HIRES YTD TERM. YTD TURNOVER
44 0 0 0 0 0
YTD
0
Gen. Plant
14
15
6
40 0 7 0 0 0 0
Maintenance
39
38
8
0
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22
24
5
21 0
Qn 0
0 __ . *
0
_ 0__ 0
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33 40
m 0 0 0 0 Q ...
Vinyl 32 31 9 21 0 0 0
0n
Plasticizer
4
5
2
40 0 0 0 0 0 0
Number of Applicants:
Month
5 Year to Date
APPLICANT BREAKDOWN:
# Minority
1 % Minority
* Female
% Female
5
20
20.
Hires (Hourly) :
Month
0
Year to Date
7
Terminations (Hourly) :
Month
1
Year to Date
Overall Turnover
.6%
1
Projected Annual Turnover
3.6%
* Includes 1 temporary employee and one Co-op Engineer
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ENERGY CONSERVATION - F. G. Jeanson
I. Plant Operations
Total energy consumption for February was 112.690 MMM BTUs. Energy consumption decreased to 2444 BTU/lb. from 2495 BTU/lb. in January. An adjusted CMA reduction of 52.3% was obtained for the month. The adjusted CMA reduction for fiscal 1987 is 54.2%.
II. Plant Energy Conservation Program
A. Maintenance
There were twenty-two energy related items completed in February. Twenty of these items were steam leak repairs. The remaining two were steam trap repairs.
B. Steam Trap Survey
III.
The survey for the vinyl and plasticizer areas identified three steam trap items for repair.
i
Boiler Operation
Boilers
Combustion Efficiency %
February, 1987
February, 1986
No. 1 No. 2 No. 3
84.2 83.5 83.2
(l)
83.7
83.6
Note: (1) Boiler number one was not used during the month. (2) Boiler number one was operated three days during the month.
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ENERGY CONSERVATION DATA 1987
February
Production, MM Lbs,
Resin Dry Blend Compound Plasticizer
TOTAL
33.7 3.9 6.8 1.7
46.1
Natural Gas
Consumption, MSCF Conversion, BTU/SCF Energy Consumption, Energy Consumption,
MMM BTU BTU/lb.
58137 1020
59.300 1286
Electricity
Consumption, MM KWH Conversion, BTU/KWH Energy Consumption, Energy Consumption,
MMM BTU BTU/lb.
4
5.3390 10000
53.390 1158
Propane
Consumption, M Gal. Conversion, BTU/Gal. Energy Consumption, Energy Consumption,
MMM BTU BTU/lb.
0 92000
0 0
Total
Energy Consumption, BTU/lb.
2444
Energy Consumption, MMM BTU Actual Unadjusted Actual Adjusted 1972 Base Period
112.690 93.673
196.290
CMA Reduction (%)
Adjusted Unadjusted Fiscal 1987 Year-to-Date
Performance
54.2% Adjusted 44.5% Unadjusted
52.3 42.6
1986 February
35.2 4.7 5.5 1.3
46.7
58758
1020
59.933 1283
5.2236
10000
52.236 1119
0 92000
0 0
2402
112.169 85.882
197.026
56.4 43.1
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Water
One minor wastewater bypass occurred on February 12 as a result of a process sewer backing up during a deluge test and overflowing to a storm sewer. The State was notified of the bypass.
All other wastewater discharge para eters were within NPDES permit limits during February.
Waste Management
Two truckloads of waste oil were shipped to Stauffer Chemical Company in Baton Rouge, Louisiana.
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TABLE I WATER COMPLIANCE WITH NPDES PEFMIT PARAMETERS
Oct. - Ave. Max.
Nov. - Ave. Max.
Dec. - Ave. Max.
Jan. - Ave. Max.
Feb. - Ave. Max.
Mar. - Ave. Max.
Apr. - Ave. Max.
May - Ave. Max.
June - Ave. Max.
July - Ave. Max.
Aug. - Ave. Max.
Sept. - Ave. Max.
Flow GEM
1010 1207
1031 1075
987 1350
1062 1300
858 900
BOD FFM LB./DY.
6 77 10 120
15 183 17 213
23 268 46 373
15 194 20 310
14 142 26 266
a PEM lb./dy.
26 311 33 404
33 406 42 527
71 846 110 1284
53 662 57 775
42 431 75 766
Sus. Solids PEM LB./DY.
14 165 23 281
23 281 37 464
13 179 24 302
18 231 28 434
10 99 13 140
Diss. oz
7.4 8.0
8.2 9.1
7.6 8.6
9.6 10.3
10.0 10.6
ML LB./DY.
2.7 7.3
0.1 0.1
2.0 4.7
2.1 4.6
4.9 9.3
PH
7.6 8.0
7.6 7.8
7.3 7.8
7.7 7.8
7.7 8.0
NPDES Permit limits -
ril 30
Ave. Max.
32 431 43 800
- 1462 - 2713
NTOES Permit Limits - May 1 througjh Novenber 30
Ave. Max.
- 26 357 - 40 744
- 1212 - 2523
674 13%
? 6.0
13 6.0 - 9.0 28
674 13%
,> 6.0
13 6.0 - 9.0 28
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LABORATORY - H. G. Coleman/J. R. Williams
Safety
A. Safety
There were no recordable first aid or medical cases for the month. As of February 21, the lab completed two years without any such incidents.
B. Customer Relations
Customer Contacts
Southwire - Samples were exchanged for a correlation study of test methods (contamination and moisture) in an effort to reach an agreement on a 5415 resin specification for this customer. All testing is complete and the results are being analyzed. Southwire representatives visited the plant and received a lab tour on 2/26. Future reporting of SPC charts for compound was discussed.
General Cable - In response to several recent complaints, B. J. Harrison visited this customer along with C. E. Hoover and Ken Walker. Brian will give extra plant attention to compound made for General Cable to prevent recurrence of past problems.
Requests for Corrective Action
Date 2/06
Customer Chicago Magnet Wire
Product 35851 NAT
Reason
i
The customer experienced burning during wire extrusion. Adhesion also fluctuated widely.
2/18
General Binding Corp.
5385-3S
Customer experienced surging in the extruder and a grainy surface on the final product (notebook binders). Particle size was the suspected cause.
Customer Problem Reports
Date
Customer
Product
Reason
2/03
General Cable
46001 NAT
Spark failures
2/05
Southwire - Osceola, ARK.
35852 NAT
Excessive streamers
2/06
Southwire - Osceola, ARK.
35852 NAT
Spark failures; "oily appearance"
2/11
Times Fiber
38601 BLK
Blistering; rough extrusion
2/13
Southwire - Carrollton, GA. 35852 NAT
Spark failures
2/17
Harvey Hubble
38901 GRY
Contamination - aluminum chips
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LABORATORY - Continued
C. Quality Control Testing
Resin
Regular Samples Total Batches Bag Blends Bulk Shipments
398 850
17 260
(Railcars - 117;
Trucks - 143)
Dry Blend
Blenders Tested -
Blenders Adjusted -
Bulk Shipments
-
608
0%
26
(Railcars - 17;
Trucks - 9)
Compound
Blenders Produced - 1090
Blenders Adjusted - 3.1%
Bulk Shipments
28 (Railcars - 20;
Trucks
Waivers Issued Customer
Product
b
Reason
No.
Uniroyal
5305
Static Flow
1 HT
Uniroyal
5415
Static Flow
1 HT
D. Development Lab Summary
RVCM of In-Process Samples
The following is a summary of residual VCM results on in-process samples. None of the reactor daily averages exceeded 400 ppm during the month of February, 1987.
Reactor Slurries
5265
Drier
5305
Number of Samples 851 34
Average ppm, VCM 190 1.1
52 0.3
RVCM of Shipment Samples
The following is a summary of the residual VCM analysis of shipment samples for the month of February, 1987.
Product
5265 5305 5385 5415 Debox 5425 5465 Dry Blend
No. of Sanples
26 66 50 26 27
RVCM, ppm 1.2 0.2 0.6 0.1 0.6
12
0.3
8
0.1
15 0.9
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D. Development Lab Testing - Continued
Other
The Development Lab ran 138 non-routine COD tests on plant wastewater in February.
Resin Process Capabilities (CPK) - Regular (Dryer) Samples
Bulk Density
5265 0.91
5305
* 0.03
5385 2.00
5415 1.56
5465 2.48
Inherent Viscosity 1.29
1.19
0.70
0.81
0.67
"L" Color Value
1.43
3.93
4.22
3.08
4.44
"A" Color Value
1.33
8.67
3.00
--
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"B" Color Value
1.56
0.89
3.89
1.83
4.33
% on Pan (vs. 2% max.)
0.94
2.80
2.31
4.56
6.67
(1.83) (1.67)
% thru 140m
0.88
1.02
0.67
2.14
7.19
Dry time
--
--
--
0.67
1.17
Mets IR (vs. 95% of control)
--
------ ---
0.86
1.19
Hard Particles
(% > 10)
2.2 9.3 17.9
* 5305 bulk density CPK is unusually low due to elimination of antistat from dryer outlet (to satisfy Hoechst Celanese).
F. Compound Quality Summary - M Lbs.
Adjustments (%)
Rejections (%)
Hardness
15.0 (0.22)
1.5 (0.02)
Color/Clarity
196.1 (2.86)
39.5 (0.58)
Hard Particles Dispersion Dicing
Total
0.0 ( - ) 0.0 ( - ) 0.0 ( - ) 211.1 (3.08)
31.4 36.8 11.3 120.5
(0.46) (0.54) (0.16) (1.76)
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Summary
Rejections
%
Long Heat Stability
27.3
(0.7)
Color
23.4
(0.6)
Contamination
4.9 (0.1)
Total
55.6
(1.4)
H. Miscellaneous
1. B. J. Harrison received six days of training in Ponca City on rigid compound testing.
2. H. G. Coleman and B. J. Harrison participated in week-long PVC In-Depth Training program in Ponca City.
Precision testing on the RVCM headspace analyzer (HS-100) at sub-ppm levels was completed and a report was issued by D. S. Cox. Summarizing the data:
Sample
Avg. RVCM (PPB)
3 Sigma Limits
Relative Error (%)
Resin, 5385
682
70 10.3
Resin, 5425
220
48 21.8
Resin, 5305
85
35 41.2
Resin, 5415
26
6 23.1
Std Gas/lg Water
65
20 30.8
Std Gas/4g Water
16
3 18.8
The old Spectra Physics 4000 integrator used in the development lab for all chromatograph integrations died and could not be resurrected. A new SP4290 was ordered as a replacement.
5. It was decided that some TCLP testing will be done in Aberdeen. An AFE was submitted for the necessary equipment. Even though the Federal Register specifies a "purge and trap" analysis for VCM in the leachate, it was felt that our headspace analysis was sufficient for generating internal data.
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SHIPMENTS BY PRODUCT - M LBS.
Resin Plasticizer Dryb1end Compound
TOTAL
NUMBER OF SHIPMENTS BY MODE:
OT R/C BULK
OT VAN
FEB. 1987
26,922 803
3,780 7,363
TOFC
CC
A
FISCAL YEAR-TO DATE
135,167 3,419
22,435 35,045
195,066#
CPU AIR
TOTAL
NUMBER OF SHIPMENTS BY MONTH-YEAR-TO
R/C
Bulk
Van
October November December January February March April May June July August September
116 146 133 193
154
41 51 64 39 46 29
68 44
50 45
TOFC
2 2
1 3 3
CC CPU AIR
52 160
64 135
48 133
89 147
55 143
1
TOTAL
422 450 390 544 451
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ABERDEEN PLANT QUALITY PERFORMANCE
10/01/86 - 09/30/87
OFF-GRADE
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1.020 1.015 1.010 1.005
1.000
0.995
ABERDEEN PLANT EFFICIENCY
10/07/86 - Q9/30/87 POUNDS OF RAW MATERIAL/POUND OF PRODUCT
*
"
1.200
1.150
1.100
1.050
r=
i
Mar. Apr. May
19 86/87
i*
1
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1 1 :July
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ABERDEEN PLANT INVENTORIES
10/01/86 - 09/30/87
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MM POUNDS
ABERDEEN PLANT PRODUCTION
10/01/86 - 09/30/87
0
A
MM PO
2
1
0
Oct, Nov. | Dec. iJan. ! Feb. Mar. April
June
Sept.iOct.
---------------- Budget - - - - Actual
Cumulative
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