Document 5xvkZzDdaXX5e2D6Y4nDGnnz
C.V. 105, (106)
D`V^Zd2^ 31?- 322' 323
llildsjL.CG 46
'
CODE YC-11-A
PKG
_ L2K80 _
C DATE )
(LOT NUMBER)
EST. WT. 2126* LBS.
PREPARATION NOTES:
S'
PROCESSES
APPROVED BY
(C)YC-i1-A < ) JJG 6/10/81
' EWK 10/21/81
TYPED BY; JMH STANDARD HRS.___ ___ ___
' rf TIME *_/^M
-------
-------- ---- ------BLEEDING
EQUIP* T I
-v
MENT I I . NAME; DALAMAR YELLOW
PREP 1
I1
I? .1 3 I
I
OBTAIN 5-NITRO--2-AMlNQANISQLE FOR S6.
OBTAIN ACETO ACET ORTHO ANISIDIDE FOR S22
CLEAN, DRESS, CLOSE 24* CLARIF PRESS
15 FRAMES
'.
1 USE I LBS
I
1 N'-CODE | ACCT | J LBS
1----------- JI 557-C | I 46-C 1
II II
DV TT RUN 17* (595 G) WATER INTO V________
2 I 5 WEIGH IN HYDROCHLORIC ACID FROM V-324
I M--- ------;__,_________ % i 6 DUMP & RINSE IN .5-NITR0-2-AMINQ ANISOLE
I
DRUMS FROM SI
.
i.
LOT * 107.
7.
i
i
i
1 ... .. , , .... .... I
1 I 1 ____ ,,1
_______ 1 ___ ____ I ____ __1
l 28-D 1 458
i
557-C 1 974
I
i 1
-
II1
_______ i
1
_______ i > ___ ____i
I 1
1
iI 1
1 i1
Ii
____ i
1
II
I 7 I STIR 10 MIN OR LONGER TO WET
i
i 8 I ADJ TO 33* (1155 G) AT 28-32 DEG F. (ICE) 10X330|
1 1 57-A l_____
I 9 I SIPHON IN SODIUM NITRITE IN 12-15 MIN
II
M____ ____ ___________ 7.
!'10 I STIR 30 MIN AT 28-32 DEG F MAINTAINING
+ CR, + KI FOR S 12
1f 725-A I 405
|1 I11
RECORD: TIME START____ CR____________ (+),
1i
1I
Kl____ _(+>
1l
NOTE;(1) IF CR-, KI-, ADD 20* *AS'IS*
I1
INCREMENTS- HYDROCHLORIC ACID
11
ASSUME 32% _______ 1 28-D l_____
RECORD: CR__,___ ,,( + >, KI______(+) (2) IF CR+,KI--, ADD 20* *AS IS* INCREMENTS
. 111
SODIUM NITRITE
ASSUME 33% _______ I
111 725-A l_
RECORD: CR___ :____ ( + ), KI______ (+>
i1AK.IK.ti, INSTRUCTIONS: BATCH UNIT
/ .
^
ECU IP ,| I
HENT
PAGE 2 OF 3 CG 46
CODE
CV ||>in RUN 10` (970 G) WATER INTO V_7JLfe. T 1 INSTALL TEMP CHART
OUR IN 'SODIUM HYDROXIDE M_i^3___ ,i. TO 40* <3904 G) AT 66-70 DEG' F'
OSE STACK DAMPER i STIR FOR S 17. . F
DATE PRINTED: H11/DD/YY
I USE ~7~ N-'cGDE I ACCT
< > ! CBS i
i LBS
I------- |---------- -
i-
I 'V "&sLZ\j2.6jgL\ 7-D
466
.4,3X3301 57~A
,r- 'I
I
I I
. I . ,'i
:.
DV 6
.I
I WHEN S 9 STIR COMPLETE,. TEST DV 6 RECORD
i I-
I . CR_rL_ < +> * KlLdt-- < + >' TEMP:
< 23-32 F > I
j
I
1NOTE: ti). IF CR-, KI-., ADD 20*-.`AS IS* | I
I
I INCREMENTS'HYDROCHLORIC ACID
! f,
f
I
'
ASSUME 327. 1___ ;____| 2B-D
! RECORD: ' CR______< + >, Kl_____ r< + ) 1 f \
| <2) IF CRT,KI-, ADD .20* `AS.IS* INCREMENTS!
I , I
I SODIUM NITRITE - ASSUME 337. ! ________{ 725-A
RECORD : CR,,_____<+> V KI______< + ) I I - . .
ADJUST TO 60 ` (2054G) WITH WATER AND ICE !
57-A JZ.
1 TO 2B-32F.
,r
I\
i
DUMP INTO m FROM S2 ACETO ACET ORTHO
ANISIDIDE. -
COT ' ZJMZ*: 7**7
OTE:
_2^43 _
J24$l <
BREAK UP
_&_
_e
LUMPS
_&?_ ____ S3-v- JJTu :_jp-
jf&PZ
R 10 MIN TO DISSOLVE
EN STACK DAMPER'
N UNDERSURFACE IN 20-25 MIN. ACETIC
ACID.
/J23S-
STIR 5 MIN & RECORD: PH_..'4e^(5.S-6.3)
IF NECESSARY, ADJ TO PH 5.8-:6.3
SODIUM HYDROXIDE
ASSUME 50% ______ i
ACETIC ACID
ASSUME 70%
RECORD: PH' (5.8-6.3.)
46-C ' f s 1265 I ! !- . j j
. -! .1.. .
30-D 1 71.3 I !
7-D 30-D I______
I
STIR 5 MIN & RECORD: TEMP_SO.,,<28-32 DEG F) 6 IF NECESSARY, ADJ TO 28-32 DEG F RECORD; ___ ,,__DEG F
T;EiYttWigr5Bi,DT"
. .IR 5 MIN & RECORD: Kl___ ______
IF NECESSARY, ADJ TO-fta & RECORD:
S^l^UM M tTfriTC
RECORD: DV, 5ESW&
KI_____ 32-%
57--A !___ _
'lie*
?
somun h y d r Gx id e 'in br u ms f o r ^35
i l ' m_J___.JS&JT&.J:
f29 1 DISSOLVE IGEPAL 00630 IN 2 GAL WATER IN
I i DRUMS FOR S3#
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j 1~D i 296
979-0 j 62
DUP050061254
S.V. CG
' ,C.V. 105,106 D, V. 306, 315, 317, 322, 323 DATE PRINTED: 1/67/02
48 CODE YT-868-D PKG
"'
'
PROCESSES
APPROVED BY
< ) YT-8G8-B < >
<"d a t e "T"~ "JCq t "n u mb er TM
TYPED BY: JHH
EST* WT. 2238* LBS.
. STANDARD HRS.
TIME______M
PREPARATION NOTES: X00-44 '
'
xizsvzzzxzz
sas-aBjcrJcssass;
NAME: DALAMAR YELL&3
TAIN 5--NITR0-2-AMIN0ANIS0LE FOR S5 OBTAIN ACETO ACET ORTHO ANISIDIDE FOR Si-7
. BLEEDING
USE I N-CODE { ACCT
LBS |
* I^ LBS
-------- - I ------ ------- 1-----I 557-C I
I- 46-C |
I . I
VJN 10* <323` G) WATER INTO V_J&ISL
WEjQOH IN HYDROCHLORIC ACID FROM V-324 M__s3_,_ Jbl'Mtyi.-Z
DUMP & RINSE IN 5-NITR0-2-AMINO ANISOLE
1 DRUMS FROM SI
LOT
* 166%
X
I I
.I
_"Jt/iJt&lL ____ WJb~ ______ __________
'
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J I2S-D | 450
557-C
974
V-
TIR 16 MIN OR LONGER TO WET
l*,r
DJ TO 33* <1155 G> AT 28-32 DEG F. (ICE) HX336
SIHON IN SODIUM NITRITE IN ISMS MIN
L-
M,, , XA*C3_-.%
I
STIR 66'MIN AT 2.8-32 DEG F MAINTAINING
+ CR, f KI FOR S 15
RECORD; TIME STARTjfl- < + > ,
KI,,-fc;:_< + )
,i
NOTE: (T) IF CR~, KI-, ADD 264- "AS IS"
)
INCREMENTS HYDROCHLORIC ACID .
]
ASSUMfe 32% i.
RECOR'D: CR,,______ < + ), KI______ < + >
[
(2) IF' CR+, K J>, ADD 26$' "AS IS* INCREMENTS!
SODIUM NITRITE "
ASSUME 33% I.
RECORD: CR________ < + >, KI______ <*>
I
i
57-A 725-A
28--D 725-A
l^SSp.
I 465 I
! I. . }____ ; 1 l !_
I
DUP050061255
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^ ^ HAK INIV INSTRUCTIONS: BATCH U|JIT
f PAGE 3 OF 3- CG 46 .CODE YjT-S
I USE ! N-CODE | ACCT
< ) ! LBS I
M LBS ...
WHES 27 COMPLETE. ADJ CV TO 48* (4685 G)
"88-84 DEG F
-
|
I
CHECK ACCURACY: HT_jgK.__DEG F &
[
RECORDER__^S-?,,. DEG F
1
WITH DV AGITATOR OFF/. IMMEDIATELY COUPLE DV|
THRU UNDERSURFACE DISTRIBUTOR IN 6~65 MIN,.|
MAINTAIN CVyAT^80~84*F. RECORD:
TOTAL
T'lilTl-----fli) liUHTTilT- Till ID" 1
...............................................
f
WHEN COUPLING COMPLETE, DISCONNECT TRANSFERJ
LINE AT DV OUTLET AND RINSE IN LINE INTO
CV, THEN DISCONNECT TRANSFER LINE AT CV
WHEN S33 COMPLETE, STIR 1 MIN.
.I
I
T
RECORD: DIAZO^JT--BASE__tr_.,,'< + >, PH <4,3-4.7)1
I I NOTE:
''
I I- <1) IF DIAZO +, BASE ~, AND PH BELOW 4.3:
I I <A) ADJ TO PH 4.3-4,7 SODIUM HYDROXIDE
1,1 I 1 .1 <B> RECORD: PH_____.
ASSUME 50%
7-B
I | <2> IF DIAZO +, BASE
& PH 4.3 OR ABOVE:
1 I < A i ADD 84 100% N-7-D SODIUM HYDROXIDE JO
I I
A 550 DRUM
i J .<B) ADJ WITH WATER TO 25G
_Jrt 7-
I f- <C) ADD- 20.4 160% N-46-C ACETO ACET ORTHO
II I. I
ANlSIDIDE (D) STIR TO DISSOLVE
' ___ i
46-
I i <E> POUR INTO CV
I / CF) STIR 10 MIN
(3) REPEAT (1) & (2) ABOVE AS NECESSARY "
' TO - DIAZO, * BASE
POUR IN N-7-D SODIUM. HYDROXIDE FROM S28 k
TIR- 5. MIN.
RECORD; PHjeigL(B.0-8.5) 6 IF NECESSARY ADJ
I i KL PH 8.0-8.5. SODIUM HYDROXIDE. ASSUME'50%
- 7- D
I J^RECORD PH_*?. HYDROCHLORIC ACID.ASSUME 32% PJtl 28- D
I DUMP IN N-979-D IGEPAL CO-630 FROM S29
135-T HEAT TO
F IN 58-62 MIN.
I 40-'T'STI-R @<Q KIN AT
F/
I L-RECORD: TIME START...
|>TJ FLOOD TO 94" (9174 G) & STOP AGITATOR .
iI
ii
START
FINISH .....jjpMfhl
PPTR
i
JUSL
i-
DUP050061256
MAKING INSTRUCTIONS:BATCH UNIT
..MEN? \
DV 8
II
* USE I
| | PAGE 3 OF 3 CG 46 CODE YC-II-A- tC) 1 LBS 1
J -- I----------------
128 J WHEN S 21 CLARIF COMPLETE, WASH DV <S 4> .1
1
I I LINES, PUMP & PRESS FOR 20 MIN OR TO A -CR 1
1
I I TEST ON A SAMPLE TO TOTAL PRESS EFFLUENT,* 1
1
I I WHICHEVER COMES FIRST . . COLLECT WASHINGS 1 .
1
i i IN DV (S21B).
iJ
i i RECORD: TIME START_^ir_U_CRi_____<- DR +) i
1
129 I STIR 5 MIN & RECORD:- TEMP____ _<28-32 DEG i_____ ._i
1 I F) & IF NECESSARY, ADJ TO 28-32 DEG F
i
i
1 I RECORD: _______ DEG F?;Cbf' .
> i
i
130 1 WEIGH IN. RUBBER BUCKET V WASH INTO DV
1 i
I 1 SULFAMIC ACID/
'
. -i
.i
131 1 STIR 5 MIN & RECORD: ~ KI_________C->
ii
132 I IF NECESSARY, ADJ TO -Kl $c RECORD: KI^.____ i.----ir.-. . Ml
I I SULFAMIC ACID.
i1
133 RECORD: DV_______* . :
*
i1
I i1
N-CODE
-
57-A 395-D * 395-D
| lACCT* 1 LBS
1 i 1 *'* ' J .. i .s 1
1 10
j ___; j
MISC
.9 `
134 i WEIGH SODIUM HYDROXIDE IN DRUMS FOR S41 . , 7
"T
I i
; M________ _________% r .-i----- |. -.J u 11
135 I DISSOLVE IGEPAL CQ630-IN 2 GAL WATER IN . i '62 i
I DRUMS FOR S43
ii
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r- :
ii
111 """ 7" "
7-D 1 296
979-D r 62 1 1
cv
-- 136 I WHEN S 33 COMPLETE, ADJ CV TO 48* <4685 G)
10 I I AT 80-84 DEG F
-V
13? 1 CHECK ACCURACY: HT_____ __DEG F &
I . RECORDER_________ DEG F
1I 38 | IMMEDIATELY RUN IN DV THRU UNDERSURFACE
1 DISTRIBUTOR IN 60-65 MIN. MAINTAIN CV .
I AT 80-84 DEG F
-
1 I RECORDTIME START_>^__, TOTAL MIN___^___
139 | WHEN S 38 COMPLETE, STIR 10 MIN
I I NOTE: IMMEDIATELY AFTER COUPLING DISCONNECT
1I
TRANSFER LINE AT CV
.
140 | RECORD: DIAZO___i_< - >, BASE_____ L_< + >,
1 PH <4.3-4.7)
NOTE:
<1> IF DIAZO
BASE
AND PH BELOW 4.3:
(A) ADJ TO PH 4.3-4.? SODIUM HYDROXIDE
||
.
l'| <B) RECORD: PH_,,>*._.f `
ASSUME 50%
_______ 1 7-D
| 1 <2> IF DIAZO + , BASE r, 6 PH 4.3 OR ABOVE
1 | (A) ADD 8* 100% N-7-0 SODIUM HYDROXIDE TO
I|
A 55G DRUM
7-D
| | <B> ADJ WITH WATER TO 25G
I.'. I <C) ADD 20* 100% N-46-C ACETO ACET ORTHO
I|
ANISIDIDE
L
46-C
1 . | <D) STIR TO DISSOLVE
l | <E> POUR INTO CV
| J <F) STIR 10 MIN
-'
.1
f 1 (3) REPEAT <1) & <21 ABOVE AS NECESSARY
I1
TO - DIAZO, + BASE
141 I JPOUR IN N-7-D SODIUM HYDROXIDE FROM S34 6
| | STIR 5 MIN. 142 1 RECORD: PH._____<8.0-8.5) & IF NECESSARY ADJ
| I TO PH 8.0-8.5. SODIUM HYDROXIDE. ASSUME 50% | 1 RECORD PH..,,. HYDROCHLORIC ACID.ASSUME 32%l
7-D 28-D
DUP050061257
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DUP050061258
DUP050061259