Document 5Lo0xzJ6JaDGEK2jpYN3a8zd8

A CG'* Oi c DAJTE ) CODE YE-69, * (- __L2H09 < LOT ) t (D 5527* LBS, < EST WT ) # PROCESSES < ) YE-69B-D <T) APPROVE! FWP 10/15/82 C0MTYF' JOB NAME: 01YE698DMT BLENDED BACK: C SOI, P s<CODE) 4WWWSX-. EQUIP | MENT i ------------- 1 I NAME; MOLYBDATE ORANGE PREP 1 'I . OBTAIN SODIUM SULFATE FDR S-13 I 2^'CALCULATE 6 SET ON BADGER METER FOR S-16 Jr (NITRIC ACID WEAK) OBTAIN SODIUM CHLORIDE FOR S-33 Y\- OBTAIN. SODA ASH FOR S-37 OBTAIN SODIUM SILICATE FOR S-39 V> OBTAIN SODA ASH FOR S-43 I OBTAIN ANTIMONY TRIOXIDE FOR S-46 351 1 .E^WEIGH SODIUM CHROMATE INTO V-35! . v n i i' o p t r _____ , mk **_*z , IclZv. I| OPTR_____ , MK _________% USE | LBS } N-CODE 84 1 108-A 734 146 237 350 70 33-D I 4-A | 3-A | 32-D i 3-A 1 711-B mt 1 0--D \ 1 ACCT ) LBS j 1 84 I 1 60 i 734 1 146 1 237 I 350 I 70 l~--*-- 1 1885 1 1 359 3 i TX WEIGH IN SODIUM MOLYBDATE SOLUTION iI OPTR ______, MK T~1X OPTR __ MK T-^,___ . ___% 423-D 1 303 358 4 sv 5 1 Sr 1 ur" RUN 10" (SO G) WATER INTO V-358 RUN V-359 INTO V-351 & PUMP IN V-351 ADJ TO 55* <260 G) SIFT IN N-108-A FROM Ji - STIR 5 Ml'N 6 RECORD: PHfcgL'JL<9*^-1 0.0) ADJ TO PH 9.8-9*9 & RECORD: PHJ <CAUSTIC SODA SOLUTION) ASSUME SOX ASSUME 66% ADD N-33-D FROM S 2 USING BADGER METER ADJ TO 66" <3*31 G) AT 67-69*F RECORD: VOL _.*?_* & __Az *F STIR 5 MIN i, RECORD: PHj2isn.4-7.6) 6 G/ML j.KjJr\ * SO-1.083) NOTE IF G/ML OUT OF LIMITS FILL OUT CHECK LIST 6 ATTACH. TAKE 1 QT SAMPLE 1>T~RUN 20' <996 G) WATER INTO I RECORD N-41-D STORAGE TANK TO PUMP FROM. CIRCLE ONE: 402 410 411 420 424 425 CHECK WITH CU SUPV ^STORAGE TANK MUST CONTAIN AT LEAST 2376 GAL: 402=49", 410=25", 411=48", 420=25', 424=25*. 425=31" *STORAGE TANK MUST HAVE STIRRED AT LEAST 20 MIN SINCE LAST ADDITION OR ADJUSTMENT ^STORAGE TANK MUST BE ISOLATED UNTIL ALL PUMPING FOR THIS BATCH IS COMPLETE SET METER FOR 300 G 6 PUMP TO SV 7-D 33-D J |. |. H0V1 1982 I ii II 1 ' Cr\ LOT* EQUIP MENT I sv~~ | 5j CONT J 231 -- COMTYP JOB NAME: 01YE698DMT PAGE 02 ' DATE PR IN TED : 1 0/1 S/8.2 USE N- I ACCT LBS CQDE LBS AT APPROX 100 G WHILE CONTINUING TO PUMP, CHECK PH 6 DENSITY. RECORD BELOW. IF NOT IN RANGE, STOP PUMPING 6 SEE SUPV. * PH:_____ (2.2-3.7) * DENSITY: __________G/ML (1 .270-1.328) IF S-22 OK & WHEN S-21 COMPLETE, RECORD DENSITY ________ G/ML ON TRAPPED SAMPLE FROM END OF S-21 PUMPING. USING DENSITY FROM S-23, FIND METER SETTING FOR SECOND PUMPING IN TABLE BELOW. NOTE: TABLE ACCOUNTS FOR 3O0 G ALREADY PUMPED IN S~21 . CIRCLE DENSITY 6 SETTING IN TABLE BELOW. **:* TABLE *** 1 G/ML SETTING | G/ML SETTING 1 G/ML 1 1.270 1678 | 1 .291 1534 I 1.312 1 1.271 1670 | 1 .292 1527 1 1.313 1 1.272 1663 | 1 .293 1521 1 1.314 i 1.273 1656 | 1 .294 1515 1 1.315 1 1.274 1649 | 1 .295 1509 1 1.316 1 1.275 1641 | 1.296 1503 \ 1.31? 1 1.276 1634 | 1 .297 1497 1 1.318 1 1.277 1627 I 1 .298 1490 1 1.319 J 1.278 1620 | 1 .299 . 1484 1 1.320 1 1.279 1614 | 1 .300 1478 1 1.321 1 1.280 1607 | 1 .301 1473 1 1.322 1 1.281 1600 1 1 .302 1467 1 1.323 1 1.282 1593 | 1 .303 1461 1 1.324 1 1.283 1586 | 1 .304 1 455 1 1.325 J 1.284 1580 I 1 .305 1449 1 1.326 1 1.285 1573 | 1 .306 1444 1 1.327 1 1 .286 1566 i 1 .307 1438 1 1.328 1 1.286 1566 1 1 .307 1 438 1 1.328 1 1.287 1559 | 1 .308 1432 1 1.329 1 1.288 1553 | 1 .309 1427 1 1.330 1 1.289 1546 | 1 .310 1 421 1 1.331 1 1.290 1540 i.___ ._____ | 1 .311 1415 1 1.332 SETTING 1410 1404 1399 1394 1 388 1383 1378 1372 1367 1 362 1357 1351 1346 1341 1336 1331 1326 1326 1543 1537 1532 1526 1 SET METER 6 PUMP .G (RECORD FROM TABLE) ] FLUSH LINE WITH WATER INTO SV FOR APPROXIMATELY I 30 SECONDS 261 ADJ LEAD NITRATE TO 76' <3625 G) AT 67-69*F. I RECORD: ___________ *F 27| STIR 5 MIN 6 RECORD PH: _______ <2.2-3.7) 281 IF NECESSARY ADJ TO PH 3.0-3.1 ASSUME 66% I f. RECORD PH: _____ ASSUME 50% I NOTE: DILUTE N-7-D 10:1 WITH WATER BEFORE ADDING 291 RECORD: ________ G/ML (1.143-1.144) IF OUT OF SPEC I FILL OUT CHECK LIST & ATTACH. .. 30| STIR AT 67-69*F FOR S-31 . TAKE 1 QT SAMPLE. 41-D 57-A 5ft0 v DUP050059478 LOT:_______ EQUIP I MENU I COMTYP JOB NAME: 01YE69SDMT PAGE 02 D IJSar^T APPROX 100. G WHILE CONTINUING TO PUMP, 5I V-CONTi . v, f I CHECK PH 6 DENSITY. RECORD BELOW. If NOT IN RANGE, STOP PUMPING & SEE SUPV* PH:IlJ__ 42*2r3*7) * DENSITY: L<Uj L- G/ML (1 *270-1*328) IF S-22 OK & WHEN S-21 COMPLETE, RECORD LAJJLDENSITY C/ML ON TRAPPED SAMPLE "FROM END OF S-21 PUMPING* USING DENSITY FROM S-23, FIND METER SETTING FOR SECOND PUMPING IN TABLE BELOW* NOTE: TABLE ACCOUNTS FOR 30 G ALREADY PUMPED IN S-21* CIRCLE DENSITY & SETTING IN TABLE BELOW* *** TABLE ##.*# LBS CODE G/ML 1 * 270 1 *271 i -272 1 * 273 1 .274 1 * 275 1 *276 1 -277 1 .278 1 *279 1 *280 1*281 1 * 282 1 *283 1 * 284 1 * 285 1 * 286 1 .28? 1 .288 1 .289 1 .290 SETTING 1644 1637 1630 1623 1616 1609 1602 1395 1588 1582 1575 1568 1562 1555 1549 1542 1535 1528 1522 1515 1510 1 - G/ML 1 1*291 1 1*292 1 1*293 1 1.294 I 1*295 1 1.296 1 1.297 1 1*298 I 1*299 1 1-300 I 1*301 I 1.302 I 1*303 1 1*304 I 1*305 1 1*306 1 1.307 1 1 * 308 i 1*309 1 1.310 i d:*3i 1 SETTING i fr/ML 1504 I 1*312 i 487 i 1*313 1491 | 1 .314 1485 | 1 *315 1479 i 1.316 1473 1 1 *31? 1467 | 1 -318 1461 | 1 *319 1455 1 1 * 320 1443 | 1 -321 1444 | 1 .322 1438 i 1 *323 1432 | 1.324 1426 | 1*325 1420 I 1 * 326 1416 | 1-* 327 141 I 1*328 1404 | 1 * 329 1399 i 1 * 330 1393 t 1*331 138^ I 1.332 SETT11 1382 1376 1371 136? 1361 1356 1351 1345 1340 1335 1330 1324 1319 1315 131 1305 1300 1295 1290 1285 1280 SET METER & PUMP Z4_C?_G (RECORD. FROM TABLE) FLUSH LINE WITH WATER INTO SY FOR APPROXIMATELY 30 SECONDS ADJ LEAD NITRATE TO 3625 G <76"-242/245 & 74*5" 247) AT 67--69K-F ' RECORD: ____F 6 ICE CONSUMED <33*/BLOCK) STIR 5 MIN & RECORD PH: 3~.J~L <2-2-3-7) 'w*K USE TITRIMETER TO ADJUST N-41-D PH #**# l \i II I ! 330X_,,. | jj IF NECESSARY ADJ Dp PH 3*0-3*1 ASSUME 66%|j 6 RECORD F'H: -L'Z_._ ASSUME 50% | _| TE: DILUTE N~7~D 10:1 WITH WATER BEFORE ADDINGi i RECORD : G/ML (1*143-1.144) IF OUT OF SPEC| FILL OUT CHECK LIST & ATTACH. STIR AT -69-KF FOR S-31 * TAKE 1 QT SAMPLE. 41-D 57-A 33-D 7-D LBS 5110 DUP050059479 . LOT-.: -____ EQUIP' "'HENfi COMTYP JOB NAME; 01YE698DMT PAGE 03 BATE PRINTED; i 0/J5/82 USE N- |A OCT LBS CODE I LBS Stf | *5 -1 CONT | OBTAIN 1 ST SAMPLES OF S-18 A S-30 SOLUTIONS I KA TITRATE TWICE I NOTIFY SUPV IF ML N -10-D IS NOT IN RANGE i 7,1-7.4 OR IF THE TWO TITRATIONS DIFFER BY I MORE THAN 0.1O ML N-10-D (IF YES, FLUSH ALL I EQUIPMENT & REPEAT TITRATIONS). DO NOT I PROCEED IF N-10-D TITRATION IS OUT OF RANGE 1 ADJUST V-358 FOR A TITRATION PH OF fr *8 2t 0 I FROM, FINAL IN-LINE TITRAIO|^RECORD LOWEST I PH j UXJL A ML N-10 33-D 7-D WHEN S-31 TITRATION OK , STRIKE V-358 THRU BOTH UNDERSURFACE DISTRIBUTORS INTO SV IN 16-18 MIN ^ ^ g/ RECORD; START TOTAL MIN.._r,,^.. NOTE; STRIKE TIME UP WHEN 1/2 VAT BOTTOM SHOWS A BUBBLES APPEAR IN SIGHT GLASSES IMMEDIATELY DUMP IN N-4-A FROM S 3 & SET TIMER FOR 15 MINUTES DURING S 33, WASH IN V-358 . ' STIR 2 MIN A RECORD PH__4_lZ,,(1 .8-2.5) FBXS /__!ir__ (MUST . BE + ) TIR TOTAL OF 15 MIN FROM S-33 & RECORD; TEMP.^Jb^F <67-73*F) DUMP N-3-A FROM S-4 STIR 3 MIN POUR IN N-32-D FROM S-5 STIR 2 MIN RUN IN LIQUID ALUM USING BADGER METER STIR 3 MIN A FLUSH ALUM LINE WITH WATER JfcLWP IN N-3 FROM S-6 STIR 4 MIN FOR S-48 i | | j j | | I 734 1 1 5-D 367 \/T \ RUN IN HYDROCHLORIC ACID CONTROL PANEL DjJRING S-44 SIFT N-711-B USING WEIGHT MK_______ , MK _____ _ FROM S-7 INTO LOW V -39 . X WITH AGITATOR ON IN 1-2 MlN IAJr\ STIR 1-2 MIN TO MILKY SOLUTION SV |4^WHEN S--44 COMPLETE, IMMEDIATELY RUN IN N-711-B 8 i 1 SOLUTION GRADUALLY OVER 5.MIN PERIOD INTO SV WATCH FOAM!?! IF FOAMING IS EXCESSIVE, STOP UNTIL FOAM SUBSIDES. DUMP IN BLANC FIXE N WHEN SCHEDULED, DUMP IN BLEND BACK LISTED ON TOP' OF PAGE 1 L RECORD; CODE LOT___________________ 5<J STIR 20 MIN v.- 52LL RECORD: PH. ;Ll JQ.<5.8-6.0) 5<! IF NECESSARY, ADJ TO PM 5.8-6. ASSUME 50% I A RECORD: PH-____ASSUME 66% 5<*T1 FLOOD TO 153" (7298 G) A STOP AGITATOR 28-D 28-D 15 33rv/rT2S-A 330 ,,,,l 7-D ) 33-D "?2! Z, DUP050059480