Document 5LJoNgdGXBamJ5JZ6qZzakwoD
- f- -if-, w.'*.
0CI2 6.1982
< DATE )
CODE RT-6i0--D PKG ...
_.JJZH55 . _
(LOT NUMBER)
ES7- WT. 2470* LBS. STD/ HRS. __ TIME
PREPARATION NOTES
'tern?:
PROCESSES < >RT-618~D <T>
APPROVED BY EWK 12/8/81
^BT; KLW ME: 32RT618DMT
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---
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EB'UIP 1 MEN! i
NAME: WATCHUNG RED Y
I USE LBS
PREP 1
j I 1 I RECORD:_________BATCHES SINCE SPARKLER LAST
I CLEANED. AFTER 4 BATCHES, CLEAN, DRESS
I SPARKLER & PRE-COAT WITH 15* DICALITE
JEILT.ER AID ^TOBTAIN FOR S11 2-CHL0RD-4-AH INOTOJ... UENE-- 5-
ACID
FOR S24 3--H YDROX Y-2-NAPHTHD1C ACID
j INSTALL DV L CV RECORDER t, CONTROLLER CHART I NOTE: NOTIFY PRESS ROOM AND ROPE OFF AREA
i UNDER V-922
NDN-BLEEDiNO 1 N-CODE I AC.C7 | j LBS -
777-A 740--C 253-C
921. 931
2
JN 10- (1000) WATER INTO V-JZStZ & ADJ TO I Jss80-100 DEG F \0tf*LAm IN 1-2 MIN.. DRESINATEX i Q*TIR 2 MIN & RECORD; PH,,_/^J9.5-10..5) '
STIR 20 MIN OR LONGER FOR S27
50
530-A
50
"
t \j&rTr \\
/^TT!
30* (620G) WATER INTO V-922
HEt'CHUEM V-926 SODIUM HYDROXIDE G RUN IN.
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Ti UURnficxl UOfN HAuGr~ITJAmTiO.u Rj \ c&* iS> T* EeA.nMn f&t iD/uUMrjPr jI.Nf rFrR\uOMn mS42 ;
.Iaw n o t o l u en e
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t
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it
ACTIVATED CARBON
__ ____I 40 i
;AL.ITE FILTER AID
'
10 l
0 2.12-21 A DEG F, RECORD Wt AKL_# F,
DEG F WATCH FOAM
RECORD BY /"Tt ), IF NECESSARY ADJ TO +BY
SODIUM HYDROXIDE
ASSUME 50% .
R 3G MIN AT 212-214 DEG F, THEN SHUT
OFF STEAM
WATCH FOAM
-y
NOTE; RECORD: SPARKLER PRESSURE ,,_.iZ.,,PSI
IF NOX ZERO, NOTIFY SUPERVISOR
CIRCULATE 15 MIN OR LONGER THRU SPARKLER
UNTIL SOL1N IS CLEAR. MAINTAIN At 190-195 F
FOR Si9 & RECORD^T__/9!L$L_DEG F AND
RECORDER /.M-S... v&j
#
RECORD; START ^aJ^^A^QTAL MIN,./.*?_____ ,
CLARITY,. Ckkl-.. .NOTE: SAMPLE FROM HOSE -
SHOW TO SUPERVISOR FOR O.K
7-D I 178 740-C I 920
I 113-B 1
777-A 1
40 16
7-D i
H I SC
CV
P
MAKING INSTRUCTIONS:BATCH UNIT
OF 3 CG 32 CODE RT~618~B (T)
USE I N-CQBE j LBS
ACCT LBS
*UN 1" <50G> WATER INTO V-904
|
WHEN SI 7 COMPLETE, PUMP IN V-922 THRU
]
SPARKLER, MAINTAIN JA-922 AT 190-195 DEG F |
RECORD :: START_/*v~zz, TOTAL HIN_JL0____ ' !
WEIGH IN FT FOR S35 SODIUM NITRITE
M_,,_P_...... ,
MEASURE y__._.,,.UNITS IN V-92S FOR S33
' HYDROCHLORIC ACID
_____,
JMt [
725-A ] 2,8-D I
295 Si
14" (i330G) WATER IN V-926 SODIUM
DUMP IN FROM S3 . 3-HYDR0XY-2-
INTO VHYDROXIDE \
m_/Jl __
_ LOL-
RUN
IN
7~C | 450 253-C
r i I'Hiii'iiojjTt i i .lawww^.e
0--90 jyci i. STIR~TO DISSOLVE 'EAH EJECT V-921/931 INTO CV
; 99 SI 9 COMPLETE, SHUT OFF PUMP 6 INSERT I
j ^rV~922 FOOT PLUG
I
>P^Ai RUN IN 10" *207G) WATER & HEAT TO 190-195 Fi
; j cjf&BWtr?Tr i Ih iim t h r u s p a r k l e r .
i
J^SiT;PUKPJ^922 THm SPARKLER INTO V-904
j
RUN JtN 5* (183G> WATER INTO V-922 6 HEAT TO I : F * CIRCULATE 15 MIN THRU SPARKLER !
d^SSjaS^^V-922 THRU SPARKLER INTO V-904
I
-WHEN MTY BLOW OUT SPARKLER INTO V-904
j
HEAT TO 165-170 F (SHPL TO SUPVR FOR O.KJ i j RUN IN N-2S-D FROM S?i IN 12-15 MIN & STIR i
5 MIN AT 1,65-170 DEG F
ABJ TO 129"< 3409GU AT 23-30 DEG F AND
RECORD: TEMP
*F, _/.JLSt-" ICE
i
! V7 I
14#X330I
RUN IN N-725-A FROM S20 AFAR (5-10 MIN) & RINSE IN FT
STIR 30 MIN AT 28-35 DEG F MAINTAINING
I +CR, +KI FOR S41/ AND RECORD: j TIME STmTlQL2&f CR.jfe.-< + >, KIJL___ < +>
i NOTE (1) IF CR-, KI-> ADD 201) AS IS IN
CREMENTS
HYDROCHLORIC ACID ASSUME 32%
j RECORD : CR.,,,,___ < + > . KI_________ < + >
j <2) IF CR+, KI-, ADD 20# AS IS INCREMENTS
i SODIUM NITRITE.
ASSUME 33%
,|
RECORD: OR;______ <>, KI________ ._< + >
i
5 7-A il?jLiO
28-A 1 723-A
\,
*
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MAKING INSTRUCTIONS .`BATCH UNIT
PAGE 3 OF 3 CG 32 CODE RT-618-D (T)
1 USE | N-CODE 1 ACCT
1 LBS |
1 LBS
CV INTO CV BARIUM SULFATE
1 i W j ADJ TO 33* (3030 AT 23-Z2*F
ICE
V RECORD: TEMP,.*!#'____ .DDEEGG FF && VVOLUME Zh
J??L3r .WEIGH IN FROM DRUM AMMONIUM CHLORIDE
^
STIR 2-3 MIN
IMMEDIATELY COUPLE DV THRU UNDERSURFACE
! DISTRIBUTOR INTO CV IN 45-60 MIN* MA~ ~
iI CV AT 28.-32 DEG !* RECORD: START/Ai^
3&~~150 f 65-A 1 150
133X330| 57--A ! &&
Ii
1 212 1 ' 165-A i 212
IJ
1I
1i
A
J -- !. 57-A I
1 TOTAL MIN
yi STIR. 30 MIN b RECORD: BASE
___ (+ .) ,
I DIAZO --*PHJE2_____<9,--?8>
1 FINAL TEMP
...... ,,DEG F
43 i IF ifo'SARY, ABJ TO PH 9 * 0-9 *8 AND .RECORD j
I
____ SODIUM HYDROXIDE
ASSUME 50% |
7-D i
`i
^^HYDROCHLORIC ACID
ASSUME 32% ].
28-D
I HEAT TO
DEG F IN 63-70 MIN AND
1
#!
! RECORD: HTDEG F b RECORDER ...... DEG F i NOTE: AT 174-176 F, OPEN WATER SPRAY
1 i/4 TURNS
902 RUN 24" i618G>WATER INTO V902
i!
12 TURN ON AGITATOR b STEAM b DUMP IN BARIUM i 1440 I 16-B I 1440
^ CHLORIDE
_
iI
I
U*--T HEAT TO
b STIR TO DISSOLVE
Ii
I
KCV WHEN S44 COMPLETE, IMMEDIATELY STRIKE V?02 |
13 THRU UNDERSURFACE DISTRIBUTOR INTO CV IN 1
i i 7-10 MIN * MAINTAIN CV AT
DEG F.
I
| J^ftECORD: S TARTTOTAL MIN_7jS_____ \MT\ HEAT CV TO 198-202 DEG F IN i,e~j2 M>N
I |
so _______ ________
.. _ _ ... ...- . 1
%. ;
.
D TO 1 30;-1 SfiA--1 8 , 6Q0G ) & *r^Leu*+>\
32 'f RECORD: PH
<9 *0-9*4) b $TCP AGITATOR
j SHUT OFF WATER SPRAYS
I
FIN *9 ' vjft&j
OPTR _ ........?-
1 WHEN INSTRUCTED BY PROCESSING AREA HALF WAY!
f THRU PRESSING, BUMS-' IN, STIR 3 MaLN b STOP I
i AGITATOR* RESUME PRESSING* I-O.CTANOL
!
1 10|
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10
DUP050060814
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