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GAS CHROMATOGRAPHY ABSTRACTING SERVICE
ANALYSIS OF POLYPHENYLS BY GAS-SOLID CHROMATOGRAPHY ON INORGANIC SALT COLUMNS.
Paul W. Solomon (Phillips Petroleum Co., Bartlesville, Okla.).
3-21-64 (40)
Anal. Chem. 36, No. 3t 476-480 (March 1964)
Column packings of LiCl-, CsCl-, and CaCl2-impregnated Chromosorb were suitable
for the gas-solid chromatographic sepn. of polyphenyIs in the temp, range of
/
200 to S00C.
f
Instrument: F & M Model 500
Detector: Thermal conductivity
Col. L/d: 5-ft. by 1/4-in.
Stat. ph./concn.: Non acid-washed Chromosorb P;, 60-80 mesh, and other packings.
Support/meSh size: 20% LiCl
Carrier gas/flow rate: helium; 60 ml./min.
Oper. Temp.: 200C
Programmed: No
Retention Data: Chromatograms p. 477-478 Remarks: Various packings and liquid phases were used
Compds. Sepd.i All the possible terphenyl (three) and quaterphenyl (nine) Isomers. UiyO Voah'a.Mt ofiKSoJj -4ZV-*-1 91-89-85-54
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