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INTER-OFFIQE MEMO T E ?! M E C 0 CHEMICALS, IHC.
H.Bo Carr
at Burlington
date June 16, 1971
from p.w. Kanzler
at Burlington
subject Raw Material Handling and Testing
copy to H.R. Horton R. Roe
v/File
Reference: (l) Meeting 5/19/71 in Flemington
(2) Memo F.W. Kanzler to H.B. Carr dated 5/26/71
As -a follow-up to the revision submitted with the referenced memo, the ''Raw Material Sampling Procedures" and the ''Request for Raw Material Approval" have been prepared.
In addition, a revised version of the "Raw Material Receiving Form" is attached. Again your comments are requested. Please have suggestions and comments back to me no later than/5/21/71.
Also .attached are the self-sticking labels which will be used once the new "Raw Material Identification, Handling and Dispo sition" has been issued.
Attachments (6). FWK/jt
F.W. Kanzler
COLOR!TE 014114
TENNECO PLASTICS DIVISION TENNECO CHEMICALS, INC.
SECTION 5 RAW MATERIAL SAMPLING PROCEDURES
Raw Material Code Number Raw Material
90-012-05
Tributyl Phosphate
Sample Frequency 1/shipment
Sample Size 1 qt jar
Analysis Performed By QC Specific Gravity
Refractive Index
AC IR
85-015-05 80-018-06
Lauroyl Peroxide
*
Aqueous Ammonia (28#)
<
5 samples/ 1000 lbs/lot
1 12-02. cup/sample
QC Contamination
AC Assay A( 0)
1/truck
1 qt jar
QC Color Odor Specific Gravity
AC Assay
COLORITE 014115
80-021-06 90-025-06
DHW-80 (40#) Sodium Lauryl Sulfate
1/truck \
1/truck
1 qt jar
QC Total Solids PH
AC IR
1 qt jar
QC Total Solids pH Viscosity
AC Cloud Point fo EAS
Page 2
RAW MATERIAL SAMPLING PROCEDURES
Raw Material Code Number Raw Material
90-030-05
Colloids 58IB
Sample Frequency 1/shipment
Sample Size 1 qt jar
Analysis Performed By
QC Odor PH
90-032-04
Caustic Flakes
l/shipment
1 8-oz jar
QC Volatiles Contamination
AC Assay IR
90-033-01
Trisodium Phosphate
1/shipment
1 qt jar
QC Screen Analysis Contamination
AC IR
95-034-01
Sodium Carbonate (Soda Ash)
1/shipment
1 8-oz jar
QC Screen Analysis PH
AC IR
90-040-06
Lauryl Alcohol
1/truck \
1 qt jar
QC Color Odor Specific Gravity Refractive Index
AC G.C. IR
COLOR!TE 014116
90-041-05
Tween 20
1/shipment
1 qt jar
QC Specific Gravity Refractive Index
Page 5
Rav; Material Code Number 80-050-06
RAW MATERIAL SAMPLING PROCEDURES
Raw Material
Vinyl Chloride Monomer
Sample Frequency 1/tank car
Sample Size
1 gas sample container
1 Analysis Performed By
QC Odor G.C. Identification Residues
If needed: Moisture Acidity Iron
AC G.C. Light Ends on every 10th car
If needed: Acetylene Nitrogen Trace Oxygen
80-051-06
Vinyl Acetate Monomer
1/tank car or 1/truck
1 qt jar
QC Specific Gravity Refractive Index Color
AC IR G.C.
If needed: Acidity Hydroquinone
COLORITE 014117
8O-O56-O5
Triallyl Isocyanurate (T.A.I.C.)
1/shipment V\
1 qt jar
QC Refractive Index Viscosity
AC IR If needed: Gel Time Polymer Contamina tion
r
Page 4
Raw Material Code Number 95-001-01, -002-, -008-
RAW MATERIAL SAMPLING PROCEDURES
Raw. Material Methocel
Sample Frequency 1 sample/pallet
Sample Size 1 qt jar
Analysis Performed By
QC Moisture Screen Analysis Viscosity Contamination
90-010-05
Diallyl Maleate (E.I.)
l/shipment
QC Specific Gravity Refractive Index
AC Acidity
95-014-01
Sodium Bicarbonate
1/shipment
QC Screen Analysis pH Contamination
85-015-05
Ionol
1/shipment
1 8-oz jar QC Refractive Index
CHLORITE 014118
0-016-09, -10, -11, -12
t
90-100-05
t-Butyl Peroxypivalate (Lupersol 11)
Up to 20 cartons/ lot: Use the sq. root system for sampling,* if more than 20 cartons/
lot; 1 sample/5 cartons/lot
2-oz vial
Epoxol 9-5
\ 1/shipment
1 qt jar
AC Assay A(0)
AC Viscosity Specific Gravity
90-102-05
Foam-Trol 129B
1/shipment
1 qt jar
QC Viscosity Specific Gravity
Page 5
RAW MATERIAL SAMPLING PROCEDURES
Raw Material Code Number 90-101-05
Raw Material
Or gano-Silicone Fluid L-522
Sample Frequency 1/shipment
Sample Size 1 qt Jar
v
Analysis P>fformed By
AC Viscosity Specific Gravity
* go-042-06
Tridecanol
80-105-05
Octadecene-1
1/truck 1/shipment
1 qt jar 1 qt jar
QC Specific Gravity Refractive Index
AC IR G.C.
/
QC Specific Gravity Refractive Index
AC IR G.C.
COLORITE 0X 4119
95.000-01
1
\ 1
1 1 1
90-051-05 1 1 L
i
90-049-05
80-052-06
Polyvinyl Alcohol
Silicone Antifoam AF-60 Heptane Trichloroethylene
1/shipment
1/shipment s
l/shipment 1/truck
1 qt jar
QC pH Volatiles Contamination Screen Analysis
AC IR
1 qt jar
QC Total Solids Viscosity
1 qt Jar 1 qt jar
QC Specific Gravity Refractive Index
QC Specific Gravity Refractive Index
AC IR
Page 6
RAW MATERIAL SAMPLING PROCEDURES
Raw Material Code Number Raw Material
95-053-05
Styrene Monomer
Sample Frequency 1/shipment
Sample Size 1 qt jar
Analysis Performed By
QC Specific Gravity Refractive Index
95-004-04, -005-, -107- Gelatin
1/shipment
1 qt jar
0,0 Viscosity
pH Contamination Screen Analysis
- 80-029-05
Ninol 1281
1/shipment
1 qt jar
QC Refractive Index Specific Gravity
AC IR
80-114-12
Di(2-ethylhexyl) peroxydicarbonate 40^ (Lupersol 223M)
Up to 20 cartons/ lot: Use the sq. root system for sampling; if more than 20 cartons/
lot: 1 sample/5 cartons/lot
2-oz vial
AC Assay A(0)
COIiORXTE 0 1 4 X 2 0
85-115-16
80-071-15
Ammonium Persulfate Sulfuric Acid
1/shipment
\ 1/lot
8-oz jar 1 qt jar
QC Screen Analysis AC Assay
AC Specific Gravity QC Assay
80-120-07
Anhydrous Ammonia
TENNECO PLASTICS DIVISION
BURLINGTON PLANT
REQUEST FOR RAW MATERIAL APPROVAL \
Raw Material
Supplier__________________________________________________ _
Name
Address
Justification
Check One:
New Material
Alternate Supplier
Sample Forwarded with Request
Sample to be Forwarded
Technical Literature Being Forwarded
Technical Literature to be For warded
FDA Sanction Paragraphs
FDA Sanction Required and Being Requested By
FDA Sanction not Required for the Specific End Use, but Should be Ver ified for Possible Future Use.
FDA Sanction Cannot be Obtained and this Material Cannot be Used in the Manufacture of Products Requiring FDA Sanction.
Tests and Specifications Recommended for this Material:
Test
Specification
Name Date
COLORITE 014121
\
Material Supplier Lot/Car No. Sample Taken By
TENNECO PLASTICS DIVISION BURLINGTON PLANT
RAW MATERIAL RECEIVING FORM
Date Received
Order No.
Seal No.
Quantity
Submitted to QC: Date
Time
QUALITY CONTROL REPORT
Material and Lot Nos. Checked_____________________________________________ Is Shipment Properly Tagged Before and After Release?_____________ Is This a Pre-Shipment Sample^? Regular Shipment?____________________ Material is Approved - Rejected - Held for Recheck (Circle)
REASONS FOR REJECTION
Details of QC Analysis are Entered on Page of Quality Control Log book and Copy of This Form is Properly Filled.
Date________________________________ _________ Time Foreman Notified
Signed
QC Technician
L-103 Rev. No. 3 COLORITE 014122
6/71
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