Document 5DME9KQk543LZ1JZdmExrg4X8
J. L. Ledbetter - B-2-N L. F. Steinbech - G-4-E
R. J. Stratmeyer - B-2-N N. L. Sample - B-2-N A. H. Sohwab - JFQ H. A. Partlow - JFQ R. D. McIntosh - JFQ
f bhH
J. R. Kellogg - JFQ H. L. Minckler - B-2-S T. M. Patrick - Res. 1 R. E. Keller - Res. 1 D. C. Reed - Res. 1 0. J. Marchand - Res, 1
MONSANTO COMPANY Organic Chemicals Division
Vo li-C-s-v^A 2/2
^// Z.
C trstt /<
To the Qeneral Manager Organic Chemicals Division
Estimate No. 1908 Dept. No. 76001*0000922 Plant - RSD Laboratories
pV
t -Ol-iJ
IrJjJZJL ^4.
J*
Pvft SLA*'
. t.'-'x.
**pp*.jtnniL
.-0v.
\ <C. <*^>3 c-A < 1 <c.
6^/ <*,( l> ( AT., ^ C' ^T/' ^ dy tCjf,
<Uc 0
T &/C3 V.O ''f
F F fi'
,
PURCHASE BIOMEDICAL SAS CHROMATOGRAPH
Capital Addition
$7,000
DESCRIPTION
Purchase biomedical gas chromatograph with all-glass system and multiple flame ionization and eleotron oapture deteotors for the analysis of thermally sensitive and polar materials.
APPROVAL General Manager
h.ii.fimcKier
Date
EXHIBIT WBP M-27
HONS 034702
LEXOLDMONOOO119 WATER PCB-00035586
Estimate No. 1908 Page 2
NEED FOR THE PROJECT
Late in 1966 Swedish researchers reported the presence of poly chlorinated biphenyls in a variety of biological samples. Since that time the Organic Chemicals Division has received a number of requests for Aroclor samples from active pesticide research groups. We also know that the U. S. Public Health authorities have initiated studies to evaluate the significance of this environmental contamination. To assess the validity of these findings, the impact they may have on our Aroclor business, and to avoid restrictive legislation, the functional Fluids Business Group has begun its own study. The Applied Sciences Section has been requested to develop the necessary analytical methodology for this project. To do this and to do it correctly, we need to purchase a biomedical gas chromato graph. This instrument is designed specifically for this type of analysis and is used by most pesticide researchers, including the Publio Health authorities. Any analytical information we generate will be judged in terms of the techniques and equipment used. By using ths tools most familiar to these people, we feel any information we provide will be more effective. The biomedioal-type chromatograph provides an all-glass system with direct injection into a U-shaped glass column which is attached directly to the base of the flame ionization or elaotron capture detector. This allows high efficiency analyses to be made on pesti cides, steroids, organo metallic* and polyfunctional organic chemioals which are thermally or catalytically unstable or have polar functional groups that, in the environment of the ordinary gas chromatograph, cause them to decompose or become irreversibly adsorbed. The R(D Labe do not at present have such instrumentation. Therefore, we recommend purchase of such a ohromatograph for initial use on the environmental Aroclor project and to broaden tha capability of the Applied Sciences Section in the gas chromatographic analysis of unstabls organic systems.
HONS 034703
LEXOLDMON000120 WATER PCB-00035587
1'
Estimate No. 1908 Page 3
STATUS OF THE PROJECT
No commitments will be made until this project is approved. RECOMMENDATION
It is recommended that this project be approved.
Submitted by
E, M. Emery Group Leader
R. E. Keller Research Section Manager
f." Hi Patrick ? Manager
RftD Laboratories
mw 8/28/88
HONS 03A7OA
LEXOLDMON000121 WATER PCB-00035588
A20C-C
Monsanto Company
PROJECT AUTHORITY FOR EXPENDITURE
and/or RETIREMENT
(THIS FORM TO BE USED FOR AUTHORITIES REQUIRING GENERAL MANAGER AND LOWER LEVEL OF APPROVAL)
PLANT
BUDGET ITEM NO.
DEPT. NO.
DATE
ENG. JOB NO.
Org. RSD Laboratories
76001-0000922
DESCRIPTION. REASON AND JUSTIFICATION FOR WORK:
8/28/68
PAGE 1 OF...
AUTHORITY NO.
1908
Purchase Biomedical Chromatograph
PREPARED BY
Marchand
ITEM
REVIEWED BY
GENERAL HGR.
DESCRIPTION
DATS
1. 29-4976, Chromatograph
29-4977, Recorder
29-4978, Integrator
*
PRODi HGR.
APPROVALS
DATE
PLANT MGR. .
.'
DATE
|
OTHER
DATE
EQUIPMENT
TRANS.
NEW
CONTR. WORK
MAT. ft STORES DIRECT SUPP. O'HEAD LABOR
SHOP
O'HEAD
TOTAL
7000
7000
1-1908-29/76001-0000922 Life - 5 years (U Bldg.)
EXHIBIT WBP M-27.1
INFORMATION FOR RETIREMENTS
SUMMARY OF ITEMS TO BE RETIRED I. INSTALLED COST
2. VALUE NOT RETIRED
INFORMATION FOR EXPENDITURES
CLASSIFICATION OP AMOUNT AUTHORIZED
PROJECT SUMMARY
CAPITAL EXPENDITURE 9. REPAIR OR OTHER EXPENSE
7000
Ut PROJECT TOTAL (ORIG OR REV.)
........ ' 1--.--------
IS. LESS PREVIOUSLY AUTH;
S. VALUE TO BE RETIRED 0-2)
10. LEASEHOLD IMPROVEMENTS
4. ACCRUED DEPRECIATION ON VALUE TO BE RETIRED
XU TRANSFERRED EQUIPMENT
|. DEPRECIATED VALUE f (3*4)
S. AMTi EXPECTED FROM SALE. TRADE-IN; ETC.
12. DISMANTLING EXPENSE [
: 13. TOTAL AMT. AUTHORIZED
7000
>. nnmi Mi.NT loss <a*s>
a {
! w* -\ u 4 ip.'--
p ${*
8 j... UVH I Oft LAPIiAI. APPWOVA1
UF- FORM A--823--1 TO DETAIL RETIREMENTS
| IS, PROJECT TOTAL ^ THIS REQ.
(U.15)
17. LESS TRANSFERRED EQUIPi
IS. NET CASH REQUIRED <16-17)1
1ft. AMOUNT AUTHORIZED = (16)
MON-MT-008602
7000 7000
7000 7000
LEXOLDMON000122 WATER PCB-00035589
RSD Laboratories - South Second Street
September 13, 1908 Hewlett-Packard Company
r Eraery VS. Tucker
Purcnaso Order AT-9M30
Vernon Fox Stores - J.F.Q. Plant
Sometime ago an instrument containing a radioactive source material was lost before reaching the Research Department, At that time we instigated tne following procedure for subsequent orders of like material or equipment:
"This order requires SPECIAL handling. Upon receipt of this equipment; ih the JFQ Storeroom, please inform:
Dr, Scott Tucker Station 3*139
Please deliver this equipment DIRECTLY to:
Dr, Scott Tucker . Lab 213, U Building
DO NOT LEAVE EQUIPMENT AT ANY DELIVERY STATIONS."
Attached is a Xerox copy of the Purchase Order, Since there is not space on the order to type this statement, will you please take action to insure that the procedure is carried out.
0, J. .Marc hand raw
MON-MT-008603
LEXOLDMON000123 WATER PCB-00035590
UcQUiSiViOil TO PURCHASING DEPARTMENT
INSTRUCTIONS TO REQUISITE |R
1. TIKS FORM MUST BE TYPEWk.lTEN
2. PO NOT fill IN SHADED AREAS
3. REMOVE^ 1ST. COPY FOR YOUR FILES
ESI. COS!
INQUIRY NO.
1/13/C8 2 wks. $678$
ill knowni Hewlett-Packard ~ 812" STTTrentwood "BXvdT
St. Louis, Mo. 63144 ' Attn: 'Hr. Lou Anderson
REMARKS
ol~ PURCHASE ^ n i. A
DATE
IOC.
NUM'JES
REQUISITION NUMBER
AT-
r.oa.POiNi
FREIGHT TtRMS
ROU1E EMERY AIR FREIGHT
TERMS
2011 Kosciusko St. Louis, Mo. 63177
.j___
P.C.ImCORHCM NO.I QUAN1IIY
1. 1
2. 1
3. 1
UNIT
DESCRIPMON
NE1 UNIT PRICE
ea. Model 402 Basic Dual Flame
$4000
Ionization Detector Gas Chromatogra] >h
ea. Model 71-27A Moseley single-channel
recorder
'
$1100
ea. Option 03 Electron Capture Detector)
with high temperature WT63 foil
(installed)
ea. iRecorder Option 07 - Disc Integrato^
(installed)
'
$1000 $ 685
AMOUNT
(a.E.C. License No. 24-01.113-14-Amen$ment 07
NOTE:
CONFIRMING ORDER
EMI BIT
^ "
This order was verbally plaied by our Dr. E. Emery to Mr, i. Anderson to reeefjye an instrument; however, no
Purchase Order was issued.
; WBPfyI-27.3| U ?h
SAl$ IAX
use tAx
OftMREO
Marchand
i^APKAEI-Jl APPfiOvjl ' VlSU-^XiuJl.
MAIERIAI 10
S. Tucker, Lab 213 SIANOAROS APRROVAI
OEPI.
176001-0000922 DATA REQUIRED
NIARGi: NUMBER' Div Pti. MAIN sun Cl ASS
VENDOR NO.
13 14 IS 16 17-19 30-31 ?3-34
"2 02 264 :oo
|
--
... -
t 'r
2S-4 9;^_- _Chromatogjparin 2q-4 977. - Recorcfir
~2S-4 9|8~j Integrate]
......
i . ..... f-- . .... --- ------------- ....
fttCClVING REPOftl PURCHASING APPROVAL
JOB NUMBER
1-1908-29
Jjl" IT _
--.
CH0O P< 7/61
MON-MT-008604
flFOiJismoMFR'<; mpv
LEXOLDMONOOOI24 WATER PCB-00035591