Document 50JB1ONXN1dnqBaR8Oy6Ob9wD
".v : (LOT NUMBER) T, /V ''
ES7. WT. 2608* LBS.
/PREPARAT ION NOTES :
PROCESSES C >RT-695-D <G>
COMT-YP JOB NAME TYPED BY; KLW STANDARD HRS- ________
fiPPKOVESfJ&t
JJG -3/18/91
EWK 12/7/81
36RT695DM0 -
TIKE *7 f?.V>
.
5 .j/,.07i ATT-t
NON-BLEEDING
EQUIP ! KENT 1
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--- NAME: *BGN* RED DARK
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I USE | N-CDDE } ACCT
| LBS |
| LBS
PREP } <T IP NECESSARY, CLEAN,. DRESS SPARKLER 6 PRE- i
!..
j
1- } i^tOAT WITH 159 DICALITE FILTER AID-
l ..
777-A |
l>3r i OBTAIN FOR S 6 .2-CHL0R0-4-AMIN0 TOLUENE-5 I
] 740-C |
t . L^tfCFONIC ACID
I I.
|
i OBTAIN FOR Ss 42 3-HYDRGXY-2-NAPHTH0IC ACID| ^ ^ ) 82-C 1
vJLjyff-.
RUN 23* (7320 WATER INTO V-317
|i
1
WEIGH & POUR IN SODIUM HYDROXIDE n
I,
1
|
| RH ON AGITATOR & STEAK & DUMP IN FROM S 21
! 7-D . I 215 j .j
^
2-CHLORO-4-AiNO-TOLUENE-5-SULFONlC ACID 1
1 740-C Si
y/pi
PestJ^-P j7 j
---------
UMP IN ACTIVATED CARBON
MP IN DICALITE, FILTER -AID
AT TO 214-216 DEG. F
WATCH FOAM
RECORD: BY__ afe!(+)> IF NECESSARY ADJUST
+ BY SODIUM HYDROXIDE
ASSUME 50%
STIR 30 MIN. AT 212-214 DEG. F, THEN SHUT
OFF STEAM
WATCH FOAM
_,)
NOTE RECORD: SPARKLER PRESSURE 0_,,FS.I
IF NOT ZERO, NOTIFY SUPERVISOR
'CIRCULATE 15 MIN OR LONGER THRU SPARKLER
I UNTIL SOLUTION MS CLEAR
..
| MAINTAIN AT 190^5 DEG. F FOR S O/*
| RECORD: -HT/^i DEp-F 6 RECORj^EBlcS-DEG.F I
1 RECORD: STARt JKIt OTAL MINil_CLARITY|
HPT 1!Q 1Q&
uu 1
w*M
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50 10
100 ~s
IVy^LH^JN 91 (99G) WATER INTO V-100 j \5rX WHEN S-13 COMPLETE, PUMP v`317 THRU | ! SPARKLER. MAINTAIN V-317 AT 190-195 DEG.F
! RECORD; - START^^SiJTOTAL MIN^;?L I 1 SAMPLE FROM HOSE. SHOW -TO SUPV'R FOR OK
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I PAGE 02.OF 04 CG 36 CODE RT-695-D (0) i LBS i
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317 mEH S 13 COMPLETE, CLOSE V-31 7 OUTLET 6
r I - V-STOP PUMP
I \?c.\ RUN IN 7* (21 dG) WATER 6 HEAT TO 190-195
I i DEG F
_^ .
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317 I IO^CIRCULATE THRU SPARKLER UNTIL SOLUTION IS |
CONT'D! 4 ly I I
1
1 CLEAR l MAINTAIN
-I RECORD: V RECORD:
' -7 AT 190-195 DEG.' F FOR Sj 9 6
1. ]
HT_/f_JLj>G. F 6 RECORDER- .
l *,I
START^^.TOTAL MIH^SI_CLARITY_a&4-' '
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100 !1? I WHEN S 10 IS COMPLETE, PUMP V-317 THRU 5" 1 ^Ks PARKLER INTO V-100 120-1 R}JK[H 5* <90G) WATER & HEAT TO 190-195 I j ^Ue g . f 13*1 CIRCULATE 15 MIN THRU SPARKLER, PUMP V-317 I J^flRU SPARKLER INTO V-100. iOffVWHEN MT,' BLOW OUT SPARKLER INTO V-100 I23H HEAT TO 165-170 DEGL F (TAKE 1 QT. SAMPLE)
I i (WITH AGITATION ON) I i TEST FOR CLARITY OF SOLUTION. SHOW 1 ST. 1 i SAMPLE TO SHIFT SUPERVISOR FOR APPROVAL
1 ' I" (EJCAMPLE OF'ACCEPTABLE CLARIFICATION OF 1 ` 1/N-740-C IS AVAILABLE IN OFFICE TO COMPARE' l. A WITH) 13* I/IF $ 23 IS OK,- CONTINUE-WITH S 25. IF S 23 [ A IS NOT ACCEPTABLE, RECLARIFY THRU SPARKLER \2Wt. IF S- 23 IS OK, REHEAT V-100 TO 165-170
DEGI 7F FOR -S 26
.iL::
100 T2 TO 16* C1590G)
6 \*r IbEAT V-100 TO 165-170 DEG. F
\2^Thm IN V-324 HYDROCHLORIC ACID THRU DIRECT |
i ^Kl in e an d r in s e -in .
/^r
119J^JrTIR 15 MIN AT 165-170 DEG. F
'I
l-SOn ADJ TO 50* (4970G) AT 34-38 DEG. F
|
1 RECORD: TEMP 3j3^rLDEG. F AND IF NECESSARY150X330
ADJ TO 34-38 DEG. Fi
]
RECORD: TEMP___ ______.DEG. F
V\ 1___ _
*" I
IN 45* (4320G) WATER INTO V-i07
ON AGITATOR AND- STEAM- AND DUMP IN
JGANESE SULPHATE
'
IN BARIUM SULPHATE j .
-
IT TO 150-160 DEC*- F AND'-STIR .
iORD,.: PH LZi.JL_--X5.0-5 .5)
IF PH ABOVE 5.5, ADJ TO PH 5.5 OR LOWER
fULFURIC ACID- . - r . ' ` 'ASSUME 78%
-RECORD.: PH
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-
190" | NOTE: IF PH BELOW. 5.0, DO NOT ADJ UPWARD
HOLD FOR S 58
-
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.
n 400 l-` 250
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{--
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2S-D .443
57-A ! imp
57-A j,, 1
--_r.
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336-B I -14.00^
65-a I :u1&Q!k
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CG 36
ntiis j.i'fij xix>i i nuw i x uni . j d h i un uixx i
CODE RJ-695-D (0)
USE 1 N-CODE ! ACCT
UBS 1
. | LBS
N IN 47" (16100 WATER INTO. V-322
}
an d po u r in s o d iu m h y d r o x id e
I
M t tSO'f & j f.37
DUMP IN FROM S 3 3-HYDR0XY-2-NAPHTH0IC"a Ci'd |
; /tOT
-47 ^39
. WEIGH 1 -H^'DROXY-2-NAPHTHOIC AC3
L ^-fGSLANCE AND ADD LOT Zd> /O A
! TO 70-90 DEG * F
flFT IN BLANCOL N IN ONE TO 'TWO MI?RJTES
DUMP IN TETRASODIUM PYROPHOSPHATE 6 STIR 5 |
I MOTOR LONGER TO DISSOLVE
|
//s ? 1i 80-C / 3"*
567-B j 27
479-D i
0
l.
I. WEIGH SODIUM NITRITE 6 POUR INTO V- _____
! FOR S 5
. M__I
U>a 4-
725-A t ~365
1 !
A DU V-322 TO 65* (2240G) AT 77-8 DEG. F RECORD: TEMP_,,^DEG* F
SLURRY TRISULPHOIC SOAP D WITH 3 GALS WATER IN DRUM* POUR IN AND STIR 5 MIN*
160
39-A | 16
1 0 11
RUN IN N-725-A. FROM S 47 AFAP. INTO V-10
STJGR 3 MIN AT 36-38 DEG* F MAINTAINING
n, +KI
*..
RECORD: TIME START,CR_fc__K I
1 EMP_,g2.________DEG * F
I_______ I - 57-A ! _____
R--, KI- ADD 2t *AS IS* INCREMENTS]
RIC ACID .
ASSUME 32X1
RECORD: CR j.___ (+>, KI
<+) |
<r> IF CR+, KI- ADD 24 'AS.IS* INCREMENTS!
"ODIUM NITRITE /
ASSUME 333;
RECORD: CR ___ (+)', KJ _____ < + )
TEMP__*______DEG * F
COUPLE V-322 THRU UNDERSURFACE DISTRIBUTOR
I | INTO V--i IN 90-11 MIN (USE 9/16*OR-i-PICE)
I L-RECORD : STARTj2^ih~3t-T0T AL MIN_XQiL_
!5<T-WHEN S 53 COMPLETE STIR 15 MIN >
ISS't RECORDED I AZO_r-Gl^<-> i> BASE,,Jz _( + > i I PH jJL( 7*0-8*) TEMP^^pDEG* F (60-65 F) I
i I NOTE:
IF-PH IS.5.0-7*, WEIGH AND DUMP IN
304 * AS IS* N-7-D DILUTED TO 3 GAL
SODIUM HYDROXIDE
ASSUME 5X
:FOR PH ADJUSTMENTS USE ONLY DILUTED
N--.28--D AND N-7-D>
ADJ TO PH 9 *-9 *5 (SEE ATTACHED PH ADJ AID)
HYDROCHLORIC ACID
ASSUME 32X
(1) IF PH IS- 6.5-7*, WEIGH 404 AS IS
. N-7-D POUR INTO 5 GAL WATER (1/2
FULL) IN PT 6 RUN INTO CV 10 IN 15
MIN 6 RINSE IN PT. STIR 5 MIN S
RECORD: PH___ _______ ,(9.-9.5>
28-a 725-A
).
! I 1______
7-D \______ 28-D l___ _
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| PAGE 04 OF 04 CG 36 CODE RT-695-D (Q) I LBS !
ACCT LBS
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2) IF PH IS 7,0-7*5, WEIGH 35* AS IS N-7-D I
POUR INTO 50 GAL WATER (1/2 FULL) IN PT & I
RUN INTO CV 100 IN 15 MIN. & RINSE IN PT. I
STIR 5 MIN & RECORD: PH__________(9.0-9.5) 1
3)' IF PH IS 7.5-8.0, WEIGH 30* AS IS N-7-D I
POUR' INTO 30 GAL WATER (1/2 FULL) IN PT & 1
RUN INTO CV i00 IN 15 MIN. RINSE IN PT.
I
STIR 5 MIN & RECORD: PH:____________ (9.0-9.5) ]
4) IF PH' IS 8.0-8.5, WEIGH 10* AS. IS N-7-D |
POUR INTO 50 GAL WATER (1/2 FULL) IN PT & |
RUN INTO CV 100 IN 15 MIN. & RINSE IN PT. |
STIR 5 MIN & RECORD: PH___________ (9.0-9.5) I
5) IF PH IS 8.3-8.9, WEIGH 5*'AS IS N-7-D |
POUR INTO 50 GAL WATER (1/2 FULL) IN PT & |
RUN IhJTO CV 100 IN 15 MIN. i, RINSE IN PT. 1
SJR"5 MIN & RECORD: PH________(9.0-9.5)
i
%) IF PH IS ABOVE 9.5, DO NOT ADJUST
|
RECORD: PH________SODIUM HYDROXIDE ASSUME 50%1
NOTE: ADD N-28-D IN 5* *AS IS* INCREMENTS |
TO APPROACH PH 9.0-9.5 THEN USE
1
LESS N-28-D HYDROXHLORIC ACID
I
(CONCENTRATED N-28-D i N-7-D'AND TOO LOW l
CGUFUBNlTTEMPERATURE CAUSES MASSTONE TO
J
' TOO LIGHT)
*|
SHUT OFF AGITATOR
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DURING S 53 HEAT V-107 TO 210-212 DEG. F
& SHUT OFF STEAM
1
NOTE:__ IF NECESSARY REHEAT V-107 TO 210- i
g F f pr io r t o s t ar t o f s t r ik e
i
PUMP V-i 00 INTO V-1 07 IN 70-75 -MIN.
i
LET V-107 TEMP DROP TO 200-205 DEG. F
[
DURING STRIKE THEN MAINTAIN AT 203-205 DEG.I
F FOR^&ALANCE OF STRIKE WITH--AGITATOR SHUT }
V-100
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ECORD: TrART_L!<0 TOTALMIN_^L?
I
WHEN STRIKE COMPLETE, HEAT TO 210-212 DEG.Fi
15 MIN AT 210-212 DEG. F
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1 FLOOD TO 180-L90S (18240G).
I
t RECORD : '
__(6.5-7.2) AND STOP
1
I AGITATOR
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