Document 4mQmNd8xwM87zGKpz04ozO8N
<*.?> '01 CODE YE-698-I)
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//#&/ -L2H13,
( DATE )
( LOT ) f
BLENDED BACK: CG
5527* LBS. ( EST WT 4.
PROCESSES ( ) YE-698-D (T)
APPROVED BY':* FWP 10/15/82*
COHTYP JOB NAME: 1YE698DMT
EQUIP MENT
NAME: MOLYBDATE ORANGE
USE I
} ACCT
LBS 1 N-CODE 1 LBS
PREP 1
'\yT I OBTAIN SODIUM SULFATE FOR S-13
i 2 ! CALCULATE 6 SET ON BADGER METER FOR S-16
I j (NITRIC ACID WEAK)
. lp4>4Qv.
\Jk^ OBTAIN SODIUM CHLORIDE FOR S-33
\\y\ OBTAIN. SODA ASH FOR S-37
OBTAIN SODIUM SILICATE FOR S-39 '
I'yO,-OBTAIN SODA ASH FOR S-43
OBTAIN ANTIMONY TRIOXIDE FOR S-46
84 I 1 0.8--A 1 84
S.3.-- 1
1
33-D 1
60
754 | 4-A 1 734
146 1 3-A 1 146
237 1 32-D i 237
350 1 3-A 1 350
70 | 711-8 I 70
42s&\
WEIGH SODIUM CHROMATE INTO V-351.
OPTR WL~, MK }2Qta &*Z&7.
i
10-D
I 1885 1
OPTR
MK___ _ ______ X
1
WEIGH IN SODIUM MOLYBDATE SOLUTION
WK\'
-1------- --
423-D 1 302'
OPTR, _V2_, MK ;___ , T-gfaO,
L'Sflt
^ ,; OPTR Jujlt, MK T~______ ______7.
10" (500 G) WATER INTO V-358
-359 INTO V-351 & PUMP IN V-351
TO 55 (260 G)
T IN N-108-A FROM S 1
. R 5 MIN 6 RECORD: PH.'0-10*0)
I ADO TO PH 9.8-9.9 6 RECORD:
{ (CAUSTIC SODA SOLUTION)
ASSUME 50%
ASSUME 667.
N-33-D FROM S 2 USING BADGER METER
I ADJ TO 66" (312) G) AT 67-69*F
^RECORD: VOL6__GQ*J
STIR 5 MIN 6 RECORD: PH_TL^T(7-.4-7.6> 6
I G/ML Zi.6S2.il .080-1 .083)
| NOTE IF G/ML. OUT OF LIMITS FILL OUT CHECK
J LIST & ATTACH. TAKE 1 QT SAMPLE
___i.
7-D 33rD
N 20" (996 G) WATER INTO ECORD N--41"D STORAGE TANK TO PUMP FROM.
CIRCLE ONE: 402 410 411 42 424 425 i CHECK WITH CU SUPV: | ^STORAGE TANK MUST CONTAIN AT LEAST 2376 | GAL: 402-49", 410=25", 411=48", 420=25",
| 424=25", 425=31* I *STtf$AGE TANK MUST HAVE STIRRED AT LEAST I 2 MIN SINCE' LAST ADDITION OR ADJUSTMENT i ^STORAGE TANK MUST BE ISOLATED UNTIL ALL
PUMPING FOR THIS BATCH IS COMF'LET,! SET METER FOR 300 G 6 PUMP TO SV
NOV 12 1982
.LOT EQUII MENT
sv~~
5 CONT
231
24
COMTYP JOB NAME: 01 YE698BMT
PAGE 02 '
DATE PRINTED: 10/fS/,82 USE i N~ |ACCT *
LBS | CODE | LBS
AT APPROX 100 G WHILE CONTINUING TO PUMP, CHECK PH & DENSITY. RECORD BELOW. IF NOT IN RANGE, STOP PUMPING 8 SEE SUPV.
* PH:_____ (2.2-3.7)
* DENSITY: _________ G/ML <1.270-1.323) IF S-22 OK & WHEN S-2l COMPLETE, RECORD
DENSITY _______ G/ML ON TRAPPED SAMPLE FROM END OF S-21 PUMPING.
USING DENSITY FROM S-23, FIND METER SETTING FOR
SECOND PUMPING IN TABLE BELOW. NOTE: TABLE ACCOUNTS FOR 300 G ALREADY PUMPED IN S-21 . CIRCLE DENSITY 6 SETTING IN TABLE BELOW.
##** TABLE *-*
I
G/ML SETTING I G/ML SETTING |1 G/ML SETTING 1
1.270 1673 I 1.291 1534 1 1.312 1410
1 .271 [ 1.272
1 .273 1 .274 1 1.275
1670 1663
1656 1649 1641
1 1.292 1 1.293
1 1.294 [ 1.295 I 1.296
1527 1521
1515 1509 1503
|i 1.313 | 1 .314
11 1.315 |I 1.316 |1 1.317
1404 1399
1394 1388 1383
1 1
1.276 1 .277 1.278
1 634 1627 1620
1 1.297 1497 1 1.298 1490 1 1.299 . 1484
| 1 .318 |I 1.319 | 1 .320
1378 1372 1367
1 1
1 .279 1.280
1614 1607
i 1.300 1 1.301
1478 1473
|[ 1.321 1 1.322
1362 1 1357
1.281 1 .282 1 .283 1.284
1600 1593 1586 1580
1 1.302 I 1.303 1 1.304 1 1.305
1467 1461 1455 1449
|1 1.323 |1 1 .324 |1 1.325 |1 1.326
1351 1346 1341 1338
1
I 1
f
1.285 1573 1 1.306 1444 |1 1.327 1 331
1.286 1 .286
1566 1566
1 1.307 1 1.307
1438 1438
|1 1.328 |I 1.328
T 326 1 326 |
1.287 1559 1 1.308 1432 11 1.329 1543
1.288 1553 I 1.309 1427 |I 1.330 1537 1
1 .289 1546 1 1.310 1421 |f 1.331 1 532 1
1.290 1540 f 1.311 1415 |1 1.332 1526
-- . _....---------------
------- ----- - -----------
1
25 SET METER 8 PUMP_______G (RECORD FROM TABLE)
FLUSH LINE WITH WATER INTO SV FOR APPROXIMATELY
30 SECONDS
26 ADJ LEAD NITRATE TO 76' <3625 G) AT 67-69*F.
RECORD: ____ _____ F
2? STIR 3 MIN & RECORD PH:
<2.2-3.7)
23 IF NECESSARY ADJ TO PH 3.0-3.1
ASSUME 667.
& RECORD PH:______
ASSUME 50Z
NOTE: DILUTE N-7-D 1:1 WITH WATER BEFORE ADDING
29 RECORD:____ _ G/ML <1.143-1.144) IF OUT OF SPEC
FILL OUT CHECK LIST & ATTACH.
30 STIR AT 67-69*F FOR S-31. TAKE 1 QT SAMPLE.
i 1 I 1
1 1 1 1 1 1 I 1 l 1 ! i
1 1 I 1
.1 1
1 1
I 41-D I 57-A
.1 3 3-D .( 7-D
51 iV mm;-
W.
DUP050059947
itii
Euip""T"
COMTYP JOB NAME: 01YE698DMT PAGE 02 T 6sFfEBiief8&!5
MENTI 1
LBS i CODE I LBS
-l__jL^l-------------------- \2&rAT APPROX 100- G WW1 HILE CONTINUING TO PUMP,
1 | CHECK PH & DENSITY. RECORD BELOW. IF NOT
` CONT1
IN RANGE, STOP PUMPING 6 SEE SUPV.
i i w iPM JL* / to o-~* ~7\
I :DENSIt y T JL%Q\_- G/ML <1.270-1.328)
lasn iIFf ,S-22 OK & WHEN S-21 COMPLETE, RECORD
DENSITY J$$L~ G/ML ON TRAPPED SAMPLE
FR^UEND OF S-21 PUMPING.
NG DENSITY FROM S-23, FIND METER SETTING FOR
SECOND PUMPING IN TABLE BELOW. NOTE: TABLE
ACCOUNTS FOR 300 G ALREADY PUMPED IN S-21.
CIRCLE DENSITY & SETTING IN TABLE BELOW.
\ -'-#f ## TABLE 1I I G/ML SETTING 1 G/ML SETTING i G'/ML SETTINGi
1 1 1.270 1644 1 1 1 .271 1637
1 1,291 I 1,292
1504 1487
1 1 .31 2 1 1 .313
1382 1 376
1 I 1 .272 1630 | 1,293 1491 I 1 .31 4 1371
I 1 1 .273 1 1 1,274
1623 1616
1 1.294 I 1.295
1485 1479
1 1 .315 i 1 .316
1 367 1361
1 1 1,275 i i 1.276 1 ! 1.277
1609 1602 15 95
| 1.296 I 1.297 1 1.298
1473 1467 1461
! 1 .317 1 1 .318 1 1 .319
1 356 i 351 1 345
I I 1.278 1588 i | 1.279 1582
i i 1.280 1575 I I 1.281 1-568 I 1 1.282 ' 1562
I 1.299 1 1,..300_ i 0/301 i ititr
1 1.303
1 455
144?) ills 1432
i 1 .320 i 1 .321 1 1 .322 l 1 .323
I 1.324
1340 1335 1330 1324
1319
1 1 1..2S* 1555 I 1.304 1426 1 1 .325 1315
1 I 1.284 1549 | 1.305 1420 I 1 .326 1310
A 1 1.285 1 542 I 1,306 1416 1 1-327 1305
1 ! 1,286 1535 1 1.307 1410 1 1 .328 1 300
1 I 1.287
i1f
I 1.288 I 1.289
1528 1522 1515
t 1.308 I 1,309 I 1.310
1404 1399 1393
I 1 .329 1 1 .330 1 1 .331
1295 1290 1 285
1 I 1-20 1510 I 1.311 1 387 i 1 .332 1280
SET METER & PUMP JX'iJ-S* (RECORD. FROM TABLE)
FUtfW LINE WITH WATER INTO SV FOR APPROXIMATELY
SECONDS ADJ LEAD NITRATE
TO
3625
G
<76'-242/245
&
~&S'
1
"247) AT 6?=69*F
I
ECORD: _Ji?L4 _*F 6 ICE CONSUMED (33OS/BL0CK) 330X___ I
STIR 5 MIN 6 RECORD PH: _2JjL <2.2-3.7.)
1
<### USE TITRIMETER TO ADJUST N-41-D PH ***
i
IF NECESSARY ADJ Tp PH 3.0-3.1
ASSUME 66% ...______ I
6 RECORD pH: _3i&
ASSUME 50% -Sfe-I
|OTE: DILUTE N/-7-D 10:1 WITH WATER BEFORE ADDING
'RECORD: LyLyjf G/ML (1.143-1.144), IF OUT OF SPEC
FILL OUT CHECK LIST 6 ATTACH.
STIR AT 67-6W FOR S-31. TAKE 1 QT SAMPLE.
41-D ! 5110
I
57-A |_______
i
I
33-D 7-D
|1______j_L___
DUP050059948
LOT'. WENT
COMTYP JOB NAME: 1YE698DMT PAGE 03 Mi- *
DATE PRINTED: 10/J 5/82 USE | N- IACCT LBS | CODE I LBS
SV . tONT
3^ I I 1 1 I I
I I I
OBTAIN 1 QT SAMPLES OF S-18 & S*:3 SOLUTIONS
& TITRATE TWICE NOTIFY SUPV IF ML N-10-D IS NOT IN RANGE
I
7-1-7.4 OR IF THE TWO TITRATIONS DIFFERJ&--
MORE THAN 0.1 ML N-10-D (IF YES, F>*SHALL
EQUIPMENT & REPEAT TITRATIONS). DO(NOT '
PROCEED IF N-10-D TITRATION IS OUTW RANGE
ADJUST V-358 FOR A TITRATION PH OF E.HTTO 1JZWTZ.-- _l
FROM FINAL IN-LINE TITRATION, RECORD. LOWEST - | Jiff |
PH sdQI- & ML N-10-D J7
-I I
33-D | 7-D |
'S'
|33^T WHEN S--31 TITRATION OK , STRIKE V-358 THRU
SV |
| BOTH UNDERMSuUnRrFuAuCcE DuISTRIBiUTOuRr\Sii Ij.Nf'TiiwO Sa Vv IiNr
6| I
I I
16-18 RECORD:
SMTINARRTT
TOTAL MIN__ ir___
v | | mm; STRIKE TIME UP WHEN 1/2 VAT BOTTOM SHOWS
| BUBBLES APPEAR IN SIGHT GLASSES
I38T I IMMEDIATELY DUMP IN N-4-A FROM S 3 & SET TIMER
UR 15 MINUTES ||3^XJWj&wRiSINi G S 33, WASH IN V-358 .
J35n STIR 2 MIN & RECORD PH^lSLtC~< 1.8-2.5)
<S,__^r,,,<MUST BE + )
SaTiiIKR T1O1 TAL OF 15 MIN FROM S-33 6
-RECORD: TEMP_^f__F <67-?3#F)
N--3-A FROM S-4
MIN |39. R IN N-32-D FROM S-5
14 STIR 2 MIN
14 gjk^IN LIQUID ALUM USING BADGER METER 142MMTINi & FLUSH ALUM LINE WITH WATER
\A-3TUimf IN N-3 FROM S-6
144 *'7 STIR 4 MIN FOR S-48
390 i
I4ST RUN IN HYDROCHLORIC ACID USING WEIGHT & FLOW
I I CONTROL PANEL
MK SLd^iSA
i 1^"
mk ______ ______ __%
146^1 DURING S-44 SIFT N-711-B FROM S-7 INTO V-390
| l^'WITH AGITATOR ON IN 1-2 MIN
|4>"T STIR. 1-2 MIN- TO MILKY SOLUTION
"X' + h. I 734 | 115-DI 367
II
II II ----- "I-----------)
II i 28-D I 105 .1 28-D I.
I) I1
SV WHEN S-44 COMPLETE, IMMEDIATELY RUN IN N-711-B
8 SOLUTION GRADUALLY OVER 5. MIN PERIOD INTO SV
WATCH FOAM!!! IF FOAMING IS EXCESSIVE, STOP
-UNTIL FOAM SUBSIDES.
S' T U Ft I AMT Ft YE W
330v^Kl i28-A! 330
{HEN SCHEDULED, DUMP IN^BLEND BACK LISTED ON
[!)/ 0F''FAGE'1\ > /' \
*51 )RD : 'CODE
[R 20 MIN
__
i52*f>eCSRD;
<5.8-6.0)
I
I52TT I EC-NECESSARY, ADJ TO PH 5.8-6.0
ASSUME 50%
7-D 1_____
6 RECORD: PH-_______ ASSUME 66%
33-D|_____
FLOOD TO 153* <7298 G) & STOP AGITATOR
I
I
FINISH
OPTR
I
zzmw>P '/IT-
DUP050059949