Document 4aDy47Y3DLE8kVZEg8DZGxEL1

CG ' Of CODE YE-721-D iff s T/^L ("d a t e "") ("l o t "') 4448* LBS. ( EST WT ) /tO/J PROCESSES C^J ( ) YE-721-D (M> APPROVED BY: FWP 11/08/82 COMTYP JOB NAME: 01YE721DMM pmmsst- OBTAIN FOR S"12 TAIN FOR S-34 OBTAIN FOR S-38 BTAIN FOR S-40 I V^USB STTMAIN FOR S-44 ! 6-T 0OBBTTAA1IN FOR S-47 WEIGH IN: OPTR | 68 | 600 | 120 | 195 | 350 I 61 , MK &[, T-V?, ?<#_%! OPTR_____, MK T-_____ _ _____% N-CQDE 108-A 4-A 3-A 32-D 3-A 711-BD 10-D ACCT LBS 68 600 12G 195 350 61 1509 WEIGH IN: OPTR *J,,, MK VL-* T-3&, OPTR MK , T- ,,, _____% 423--D 243 0" (500 G) WATER INTO V-358 -359 INTO V-351 & PUMP IN V-351 TO 55* <2600 G) N N-108-A FROM SI.. 5 MIN & RECORD: PHJ/^^_(9.0"10.0) TO PH 9.8-9.9 & RECORD: PH.J&SL ^ASSUME 50% ASSUME 66% INTO V-351 FROM BADGER MEJDER^y OPTRJdM.--, MK_*3L, 33&ILJL FROM V-351 TO V-358 I FLUSH V-351 $i PUMPING LINES WITH 1000G WATER INTO V-358 } ADJ TO 74* (3530 G> AT 67-69*F V RECORD: V0LJ7i^' ^ -J&Lj** iyf I STIR 5 MIN 6 RECORD: PHj'JL<7.2-7. 4) & G/ML 1 * 055-1.058 ) | NOTE IF G/ML OUT OF LIMITS FILL OUT CHECK LIST & ATTACH. TAKE 1 QT SAMPLE. ---------- 1- sv RUN 20* (996 G) WATER INTO V5 RECORD N-41-D STORAGE TANK TO PUMPOM. L- CIRCLE ONE: 402 41 411 420 424*425? la-fT CHECK WITH CU SUPV: i | *STORAGE TANK MUST CONTAIN AT LEAST 1900 i | GAL: 402=39*, 410=20*, 411=38*, 420=20*, 1 | 424=20*, C425=25^ i ! ^STORAGE TAM MUST HAVE STIRRED AT LEAST | 1 20 MIN SINCE LAST ADDITION OR ADJUSTMENT ^STORAGE TANK MUST BE ISOLATED UNTIL ALL | PPUI MPING FOR THIS BATCH IS COMPLEJE^^ .sen s e t METER FOR 300 G 6 PUMP TO SV z: 7-D 3 3-D 2*::: 28-D w LOT: EQUIP MENT COMTYP JOB NAME: 01YE721DMM PAGE 02 DATE PRINTED:11/0S/82 USE N~ ACCT LBS CODE LBS W~ 5 CONT AT APPROX 100 G WHILE CONTINUING TO PUMP, CHECK PH & DENSITY. RECORD BELOW. IF NOT IN R&N.GEL STOP PUMPING & SEE SUPV. * PH^ptZ, <2.2-3.. 7) DENSITY: G/ML < 1.270-1 .328) IF S-23 OK A,WHEN S-22 COMPLETE, RECORD DENSITY /uZym G/ML ON TRAPPED SAMPLE I L^PROM END OF S-22 PUMPING. U#T USSING DENSITY FROM S-24, FIND METER SETTING FOR SECOND PUMPING IN TABLE BELOW. NOTE: TABLE ACCOUNTS FOR 300 G ALREADY PUMPED IN S-22. CIRCLE DENSITY t, SETTING IN TABLE BELOW. * TABLE *** 1 G/ML 1 1.270 1 1 .271 1 1.272 1 1 .273 I 1 .274 I 1 .275 1 1 .276 1 1.277 1 1 .273 1 1.279 1 1 .280 1 1.281 1 1.282 1 1.283 I 1.284 1 1 .285 1 1 .286 1 1 .287 1 1.288 1 1 .289 1 1.290 SETTING | G/ML SETTING | G/ML 1259 1 1.291 1146 | 1.312 1253 1248 1 1.292 1 1.293 1141 1136 | 1.313 | 1.314 1242 1 1.294 1131 " 1 1.315 1236 1231 1 1.295_ 1126 1 1.316 iq JJSL - 1120 | 1.317 1225 1 t T297 1116 [ 1.318 121 9 1 1.298 1112 | 1 .319 1214 1 1.299 1107 | 1.320 1208 1 1.300 __ 1103 | 1.321 1203 1 1.301 1098'-, 1 1 .322 1198 1 1.302 1094 >. 1.323 1193 1 1.303 1089 |\ 1.324 1187 | 1.304 1084 | 1 .325 1182 1 1.305 1080 |1j1.326 117? 1 1.306 1076 | '1.327 11 71 I 1.307 1070 | 1 .328 1166 | 1.308 1066 | 1 .329 1161 f 1.309 1061 1 1 .330 1155 I 1.310 1057 | 1 .331 1151 I 1.311 1053 | 1 .332 SETTING) 1049 | 1045 1 1040 | 1036 | 1032 | 102? | 1023 | 1019 | 1015 1 1010 1 1006 | 1003 | 999 | 995 | 991 | 987 | 983 ( 979 | 975 | 971 | 967 | f 1 ! 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 SET METER 6 PUMP (RECORD FROM TABLE) FLUSH LINE WITH WATER INTO SV FOR APPROXIMATELY 'SECONDS ADJ LEAD NITRATE TO 3244 G C68* 245 6 I I 41-D I gPI) AT 67-69*F II ^RECORD: & ICE CONSUMED <3304=/BLOCK) 1330X__ 1 57-A 2&\ STIB>5 MIN RECORD PH: (2.2-3.?) ! Js#m* USE TI TRIMETER TO A JUST N-41-D PH **** 2*f\ IF NECESSARY ADJ TO PH 3 0-3.1 ASSUME 66% .XJ 33-D RECORD PH: *3k3L ASSUME 50% 7-D E: DILUTEJ1-7-D 10:1 WITH WATER BEFORE ADDING RECORD: G/ML (1.128-1.129) IF OUT OF SPEC! FILL OUT CHECK LIST & ATTACH. STIR AT 6?-69#F FOR S-33. TAKE 1 QT SAMPLE. 4094 DUP050059717 Lof* _____ FQUIF: | MENT| | COMTYP JOB NAME: 01YE721DMM PAGE 03 BA TE PRI TED:11/08/82 USE N- | USE LBS CODE | LBS SV 132 I OBTAIN 1 QT SAMPLES OF S-19 & S-31 SOLUTIONS 5| <5, TITRATE TWICE CQNTI NOTIFY SUPV IF ML NH0-D IS NOT IN RANGE I 9.5-9.9 OR IF THE TWO TITRATIONS DIFFER BY MORE THAN 0.1O ML N-10-D (IF YES, FLUSH ALL EQUIPMENT & REPEAT TITRATIONS). DO NOT PROCEED IF N-IO-D TITRATION IS OUT OF RANGE ADJUST V-358 FOR A TITRATION PH OF ?n I FROM FINAL IN-LINE TITRAXION, RECORD LOWEST I PH & ML N-10-D /.7o-/.?0 33-D | 7-P | TITRATION~OK7~sfRIKE""v-38~fHRU""6t H~ UNDERSURFACE DISTRIBUTORS INTO SV IN 44-46 MIN I I RECORD: START TOTAL MIN____ &OL I I NOTE: STRIKE TIME UP WHEN i/2 VAT BOTTOM SHOWS ! & BUBBLES APPEAR IN SIGHT GLASSES A& I IMMEDIATELY DUMP IN N-4-A FROM S 2 & SET TIMER ' FOR 15 MINUTES TNG S 34, WASH IN V-358 TSTIR 2 MIN & RECORD PH___4J7_<1.7-1.8) BXS, _<MUST BE + ) 1 STIR TOTAL OF 15 MIN FROM S-34 & RECORD: TEMP_J/,,h F <67-73*F> JMP N-3-A FROM S-3 riR 3 MIN JR IN N-32-D FROM S-4 STIR 2 MIN RUN IN LIQUID ALUM USING BADGER METER STIR 3 MIN t, FLUSH ALUM LINE WITH WATER DUMP IN N-3 FROM S-5 1 STIR 4 MIN FOR S-49 115-DI 302 RUN IN HYDROCHLORIC ACID USING WEIGHT & FLOW. -CONTROL PANEL MK ___ , 0*9%--* MK, _______________ % O DURING S-45 SIFT N-7i1-B FROM S-6 INTO V-390 iJITH AGITATOR ON IN 1-2 MIN 1-2 MIN TO MILKY SOLUTION 28-D | 28-D |, I I 9 WHEN S-45 COMPLETE, IMMEDIATELY RUN IN N-711-B SOLUTION GRADUALLY OVER 5 MIN PERIOD INTO SV WATCH FOAM!!! IF FOAMING IS EXCESSIVE, STOP UNTIL FOAM SUBSIDES. JUMP IN BLANC FIXE N WHEN SCHEDULED, DUMP IN BLEND BACK LISTED ON TOP OF PAGE 1 , J-- RECORD: CODE____ r__, LOT, BKCp- STIR 20 MIN . ^ I^C^KRECORD: PH___ "t_L<5.8-6.0> V& | IF NECESSARY, ADJ TO PH 5.:8"6.0 ASSUME 50% | & RECORD: PH-____________ ASSUME 66% 1 FLOOD TO 153* (7298 G> & STOP AGITATOR i ^ * Siiht. 3FINISH OPTR .ML____ __ CM .jS&t 275 128-A| 275 I I I 7-D I. 33-DI. I * DUP050059718